RU2009136172A - Полиуретановый состав и его применение для получения голографических сред - Google Patents

Полиуретановый состав и его применение для получения голографических сред Download PDF

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RU2009136172A
RU2009136172A RU2009136172/28A RU2009136172A RU2009136172A RU 2009136172 A RU2009136172 A RU 2009136172A RU 2009136172/28 A RU2009136172/28 A RU 2009136172/28A RU 2009136172 A RU2009136172 A RU 2009136172A RU 2009136172 A RU2009136172 A RU 2009136172A
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polyurethane composition
composition according
groups
polyisocyanates
formula
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RU2009136172/28A
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RU2518125C2 (ru
RU2518125C9 (ru
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Марк-Штефан ВАЙЗЕР (DE)
Марк-Штефан ВАЙЗЕР
Томас РЕЛЛЕ (DE)
Томас РЕЛЛЕ
Фридрих-Карл БРУДЕР (DE)
Фридрих-Карл БРУДЕР
Томас ФЭККЕ (DE)
Томас ФЭККЕ
Деннис ХЕНЕЛЬ (DE)
Деннис ХЕНЕЛЬ
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Байер МатириальСайенс АГ (DE)
Байер Матириальсайенс Аг
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    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L75/00—Compositions of polyureas or polyurethanes; Compositions of derivatives of such polymers
    • C08L75/04—Polyurethanes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/42—Polycondensates having carboxylic or carbonic ester groups in the main chain
    • C08G18/4266—Polycondensates having carboxylic or carbonic ester groups in the main chain prepared from hydroxycarboxylic acids and/or lactones
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    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
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    • C08G18/40—High-molecular-weight compounds
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    • C08G18/4833—Polyethers containing oxyethylene units
    • C08G18/4837—Polyethers containing oxyethylene units and other oxyalkylene units
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    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/67—Unsaturated compounds having active hydrogen
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    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/77—Polyisocyanates or polyisothiocyanates having heteroatoms in addition to the isocyanate or isothiocyanate nitrogen and oxygen or sulfur
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    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/77—Polyisocyanates or polyisothiocyanates having heteroatoms in addition to the isocyanate or isothiocyanate nitrogen and oxygen or sulfur
    • C08G18/78—Nitrogen
    • C08G18/7806—Nitrogen containing -N-C=0 groups
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    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/77—Polyisocyanates or polyisothiocyanates having heteroatoms in addition to the isocyanate or isothiocyanate nitrogen and oxygen or sulfur
    • C08G18/78—Nitrogen
    • C08G18/7875—Nitrogen containing heterocyclic rings having at least one nitrogen atom in the ring
    • C08G18/7887—Nitrogen containing heterocyclic rings having at least one nitrogen atom in the ring having two nitrogen atoms in the ring
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    • C08K5/00—Use of organic ingredients
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    • C08K5/005—Stabilisers against oxidation, heat, light, ozone
    • G—PHYSICS
    • G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
    • G03F—PHOTOMECHANICAL PRODUCTION OF TEXTURED OR PATTERNED SURFACES, e.g. FOR PRINTING, FOR PROCESSING OF SEMICONDUCTOR DEVICES; MATERIALS THEREFOR; ORIGINALS THEREFOR; APPARATUS SPECIALLY ADAPTED THEREFOR
    • G03F7/00—Photomechanical, e.g. photolithographic, production of textured or patterned surfaces, e.g. printing surfaces; Materials therefor, e.g. comprising photoresists; Apparatus specially adapted therefor
    • G03F7/0005—Production of optical devices or components in so far as characterised by the lithographic processes or materials used therefor
    • G03F7/001—Phase modulating patterns, e.g. refractive index patterns
    • G—PHYSICS
    • G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
    • G03F—PHOTOMECHANICAL PRODUCTION OF TEXTURED OR PATTERNED SURFACES, e.g. FOR PRINTING, FOR PROCESSING OF SEMICONDUCTOR DEVICES; MATERIALS THEREFOR; ORIGINALS THEREFOR; APPARATUS SPECIALLY ADAPTED THEREFOR
    • G03F7/00—Photomechanical, e.g. photolithographic, production of textured or patterned surfaces, e.g. printing surfaces; Materials therefor, e.g. comprising photoresists; Apparatus specially adapted therefor
    • G03F7/004—Photosensitive materials
    • G03F7/027—Non-macromolecular photopolymerisable compounds having carbon-to-carbon double bonds, e.g. ethylenic compounds
    • G—PHYSICS
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    • G03F7/004—Photosensitive materials
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    • G03H1/00—Holographic processes or apparatus using light, infrared or ultraviolet waves for obtaining holograms or for obtaining an image from them; Details peculiar thereto
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    • G—PHYSICS
    • G11—INFORMATION STORAGE
    • G11B—INFORMATION STORAGE BASED ON RELATIVE MOVEMENT BETWEEN RECORD CARRIER AND TRANSDUCER
    • G11B7/00—Recording or reproducing by optical means, e.g. recording using a thermal beam of optical radiation by modifying optical properties or the physical structure, reproducing using an optical beam at lower power by sensing optical properties; Record carriers therefor
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Abstract

1. Полиуретановый состав, включающий ! A) полиизоцианатный компонент, ! B) изоцианат-реакционноспособный компонент, включающий, меньшей мере, до 50 вес.%, в расчете на общую смесь B), полиэфирполиолов В1) со среднечисленными молекулярными весами больше 1000 г/моль, которые содержат одно или несколько оксиалкильных звеньев формул (I)-(III) ! -СН2-СН2-О- формула (I) -CH2-CH(R)-O- формула (II) -СН2-СН2-СН2О- формула (III) ! при этом R является алкильным или арильным остатком, который может быть замещен или прерван гетероатомами, ! C) соединения, которые содержат группы, реагирующие при действии актиничного излучения с этилен-ненасыщенными соединения с полимеризацией (отверждаемые излучением группы), и сами не содержат NCO-групп, ! D) стабилизаторы радикалов, ! E) фотоинициаторы, ! F) при необходимости, катализаторы, ! G) при необходимости, вспомогательные вещества и добавки. ! 2. Полиуретановый состав по п.1, отличающийся тем, что в A) используют полиизоцианаты и/или преполимеры, основанные на HDI, TMDI и/или TIN. ! 3. Полиуретановый состав по п.1, отличающийся тем, что в A) используют полиизоцианаты, основанные на HDI, со структурами изоцианурата и/или иминооксадиазиндиона или преполимеры с NCO-функциональностями от 2 до 5 и исключительно первичными NCO-группами. ! 4. Полиуретановый состав по п.1, отличающийся тем, что соединения, используемые в А) в качестве полиизоцианатов, имеют остаточные содержания свободного мономерного изоцианата меньше, чем 0,5 вес.%. ! 5. Полиуретановый состав по п.1, отличающийся тем, что полиэфирполиолы, используемые в B), имеют средние ОН-функциональности от 1,8 до 4,0 и среднечисленные молекулярные веса от 1000 до 8500 г/моль. ! 6. Полиуретанов�

Claims (13)

1. Полиуретановый состав, включающий
A) полиизоцианатный компонент,
B) изоцианат-реакционноспособный компонент, включающий, меньшей мере, до 50 вес.%, в расчете на общую смесь B), полиэфирполиолов В1) со среднечисленными молекулярными весами больше 1000 г/моль, которые содержат одно или несколько оксиалкильных звеньев формул (I)-(III)
-СН2-СН2-О- формула (I) -CH2-CH(R)-O- формула (II) -СН2-СН2-СН2О- формула (III)
при этом R является алкильным или арильным остатком, который может быть замещен или прерван гетероатомами,
C) соединения, которые содержат группы, реагирующие при действии актиничного излучения с этилен-ненасыщенными соединения с полимеризацией (отверждаемые излучением группы), и сами не содержат NCO-групп,
D) стабилизаторы радикалов,
E) фотоинициаторы,
F) при необходимости, катализаторы,
G) при необходимости, вспомогательные вещества и добавки.
2. Полиуретановый состав по п.1, отличающийся тем, что в A) используют полиизоцианаты и/или преполимеры, основанные на HDI, TMDI и/или TIN.
3. Полиуретановый состав по п.1, отличающийся тем, что в A) используют полиизоцианаты, основанные на HDI, со структурами изоцианурата и/или иминооксадиазиндиона или преполимеры с NCO-функциональностями от 2 до 5 и исключительно первичными NCO-группами.
4. Полиуретановый состав по п.1, отличающийся тем, что соединения, используемые в А) в качестве полиизоцианатов, имеют остаточные содержания свободного мономерного изоцианата меньше, чем 0,5 вес.%.
5. Полиуретановый состав по п.1, отличающийся тем, что полиэфирполиолы, используемые в B), имеют средние ОН-функциональности от 1,8 до 4,0 и среднечисленные молекулярные веса от 1000 до 8500 г/моль.
6. Полиуретановый состав по п.1, отличающийся тем, что в B1) используют полиэфирполиолы, основанные на пропиленоксиде, или статистические или блок-сополимеры, основанные на пропиленоксиде с другими 1-алкиленоксидами с долей 1-алкиленоксида не выше, чем 80 вес.%, и/или поли(триметиленоксиды).
7. Полиуретановый состав по п.1, отличающийся тем, что полиэфирполиолы, используемые в компоненте B), имеют показатель преломления nD 20<1,55.
8. Полиуретановый состав по п.1, отличающийся тем, что соединения, используемые в компоненте C), имеют показатель преломления nD 20<1,55.
9. Полиуретановый состав по одному из пп.1-8, отличающийся тем, что в компоненте C) используют уретанакрилаты и уретанметакрилаты на основе ароматических изоцианатов и 2-гидроксиэтилакрилата, гидроксипропилакрилата, 4-гидрокси-бутил-акрилата, полиэтиленоксид-моно(мет)акрилата, полипропиленоксид-моно(мет)акрилата, полиалкиленоксид-моно(мет)акрилата и поли(ε-капролактон)-моно(мет)акрилатов.
10. Способ получения сред для записи визуальных голограмм, при котором полиуретановый состав по одному из пп.1-9 наносится на субстрат или в форму и отверждается.
11. Среда для записи визуальных голограмм, получаемых по способу по п.10.
12. Применение среды по п.11 в качестве оптических элементов изображений или для получения изображения или проекции.
13. Способ записи голограммы, при котором используют среду по п.12.
RU2009136172/04A 2008-10-01 2009-09-30 Полиуретановый состав и его применение для получения голографических сред RU2518125C9 (ru)

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CA2680969A1 (en) 2010-04-01
EP2172502A1 (de) 2010-04-07
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EP2172502B1 (de) 2016-04-20
US20100112459A1 (en) 2010-05-06
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TWI461454B (zh) 2014-11-21
BRPI0903949A2 (pt) 2010-07-20
CN101712745A (zh) 2010-05-26
IL200995A0 (en) 2010-06-30
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JP2010084147A (ja) 2010-04-15
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