HRP20000749B1 - Purification of carboxaldehyde - Google Patents

Purification of carboxaldehyde

Info

Publication number: HRP20000749B1
Authority: HR; Croatia
Prior art keywords: carboxaldehyde; purification; biphenylcarboxaldehyde; chloro; bisulfite adduct
Prior art date: 1998-05-05

Application number

HR20000749A

Other languages

English (en)

Croatian (hr)

Inventor

Alan Berglund Richard

Original Assignee

Eli Lilly And Company

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1998-05-05

Filing date

2000-11-03

Publication date

2007-02-28

2000-11-03 Application filed by Eli Lilly And Company filed Critical Eli Lilly And Company

2001-10-31 Publication of HRP20000749A2 publication Critical patent/HRP20000749A2/hr

2007-02-28 Publication of HRP20000749B1 publication Critical patent/HRP20000749B1/xx

Links

MBVFRSJFKMJRHA-UHFFFAOYSA-N 4-fluoro-1-benzofuran-7-carbaldehyde Chemical compound FC1=CC=C(C=O)C2=C1C=CO2 MBVFRSJFKMJRHA-UHFFFAOYSA-N 0.000 title 1
238000000746 purification Methods 0.000 title 1
WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 abstract 6
LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 abstract 2
UXCMNUUPBMYDLJ-UHFFFAOYSA-N 4-(4-chlorophenyl)benzaldehyde Chemical compound C1=CC(Cl)=CC=C1C1=CC=C(C=O)C=C1 UXCMNUUPBMYDLJ-UHFFFAOYSA-N 0.000 abstract 1
GCWSKJAUAKBMFR-UHFFFAOYSA-N S(O)(O)=O.ClC1=CC=C(C=C1)C1=CC=C(C=C1)C=O Chemical compound S(O)(O)=O.ClC1=CC=C(C=C1)C1=CC=C(C=C1)C=O GCWSKJAUAKBMFR-UHFFFAOYSA-N 0.000 abstract 1
DWAQJAXMDSEUJJ-UHFFFAOYSA-M Sodium bisulfite Chemical compound [Na+].OS([O-])=O DWAQJAXMDSEUJJ-UHFFFAOYSA-M 0.000 abstract 1
239000007864 aqueous solution Substances 0.000 abstract 1
238000000034 method Methods 0.000 abstract 1
235000010267 sodium hydrogen sulphite Nutrition 0.000 abstract 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
- C07F5/02—Boron compounds
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C309/00—Sulfonic acids; Halides, esters, or anhydrides thereof
- C07C309/01—Sulfonic acids
- C07C309/02—Sulfonic acids having sulfo groups bound to acyclic carbon atoms
- C07C309/24—Sulfonic acids having sulfo groups bound to acyclic carbon atoms of a carbon skeleton containing six-membered aromatic rings
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/78—Separation; Purification; Stabilisation; Use of additives
- C07C45/85—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to a chemical modification

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
General Chemical & Material Sciences (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Removal Of Specific Substances (AREA)
Detergent Compositions (AREA)
Nitrogen Condensed Heterocyclic Rings (AREA)
Pyrrole Compounds (AREA)

HR20000749A 1998-05-05 2000-11-03 Purification of carboxaldehyde HRP20000749B1 (en)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
US8429998P	1998-05-05	1998-05-05
PCT/US1999/005666 WO1999057123A1 (en)	1998-05-05	1999-03-15	Purification of carboxaldehyde

Publications (2)

Publication Number	Publication Date
HRP20000749A2 HRP20000749A2 (en)	2001-10-31
HRP20000749B1 true HRP20000749B1 (en)	2007-02-28

Family

ID=22184070

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
HR20000749A HRP20000749B1 (en)	1998-05-05	2000-11-03	Purification of carboxaldehyde

Country Status (26)

Country	Link
US (1)	US6355843B1 (xx)
EP (1)	EP1075480B1 (xx)
JP (1)	JP2002513794A (xx)
KR (1)	KR100624585B1 (xx)
CN (1)	CN1168694C (xx)
AT (1)	ATE267209T1 (xx)
AU (1)	AU748094B2 (xx)
BR (1)	BR9911006A (xx)
CA (1)	CA2330621A1 (xx)
CZ (1)	CZ295089B6 (xx)
DE (1)	DE69917445T2 (xx)
DK (1)	DK1075480T3 (xx)
EA (1)	EA003558B1 (xx)
ES (1)	ES2220053T3 (xx)
HR (1)	HRP20000749B1 (xx)
HU (1)	HUP0101830A3 (xx)
ID (1)	ID26405A (xx)
IL (1)	IL138636A0 (xx)
NO (1)	NO20005529D0 (xx)
NZ (1)	NZ507054A (xx)
PL (1)	PL191095B1 (xx)
PT (1)	PT1075480E (xx)
SK (1)	SK285059B6 (xx)
TR (1)	TR200003203T2 (xx)
UA (1)	UA81595C2 (xx)
WO (1)	WO1999057123A1 (xx)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
GB2413795A (en)	2004-05-05	2005-11-09	Cipla Ltd	Process for the preparation of rosiglitazone
ES2374379T3 (es) *	2005-01-14	2012-02-16	Schering Corporation	Síntesis exo y diastereoselectiva de análogos de himbacina.
WO2009147068A1 (en)	2008-06-06	2009-12-10	F. Hoffmann-La Roche Ag	Process for the preparation of halogenated benzoic acid derivatives
CN103804445B (zh) *	2013-12-30	2016-01-13	广州自远生物科技有限公司	一种改进的乙酰异戊酰泰乐菌素的制备方法
JP6712991B2 (ja)	2014-07-17	2020-06-24	ザメディシンズカンパニー	高純度のオリタバンシン及びその製造方法
CN109897020B (zh) *	2017-12-07	2020-12-25	中国科学院宁波材料技术与工程研究所	一种粗品5-羟甲基-2-呋喃甲醛的精制方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS5325530A (en) *	1976-08-20	1978-03-09	Sumitomo Chem Co Ltd	Purification of aldehydes
US4075248A (en) *	1976-09-07	1978-02-21	Domtar Limited	Production of syringealdehyde from hardwood waste pulping liquors
US4065505A (en) *	1976-11-05	1977-12-27	Shell Oil Company	Oxidation process
US5840684A (en) *	1994-01-28	1998-11-24	Eli Lilly And Company	Glycopeptide antibiotic derivatives

1999
- 1999-03-15 PL PL343758A patent/PL191095B1/pl unknown
- 1999-03-15 HU HU0101830A patent/HUP0101830A3/hu unknown
- 1999-03-15 PT PT99911411T patent/PT1075480E/pt unknown
- 1999-03-15 WO PCT/US1999/005666 patent/WO1999057123A1/en active IP Right Grant
- 1999-03-15 CN CNB99805710XA patent/CN1168694C/zh not_active Expired - Fee Related
- 1999-03-15 CA CA002330621A patent/CA2330621A1/en not_active Abandoned
- 1999-03-15 JP JP2000547092A patent/JP2002513794A/ja not_active Withdrawn
- 1999-03-15 EA EA200001153A patent/EA003558B1/ru not_active IP Right Cessation
- 1999-03-15 AT AT99911411T patent/ATE267209T1/de not_active IP Right Cessation
- 1999-03-15 ID IDW20002247A patent/ID26405A/id unknown
- 1999-03-15 BR BR9911006-7A patent/BR9911006A/pt not_active Application Discontinuation
- 1999-03-15 TR TR2000/03203T patent/TR200003203T2/xx unknown
- 1999-03-15 CZ CZ20004082A patent/CZ295089B6/cs not_active IP Right Cessation
- 1999-03-15 UA UA2000116251A patent/UA81595C2/ru unknown
- 1999-03-15 US US09/673,347 patent/US6355843B1/en not_active Expired - Fee Related
- 1999-03-15 AU AU30057/99A patent/AU748094B2/en not_active Ceased
- 1999-03-15 KR KR1020007012278A patent/KR100624585B1/ko not_active IP Right Cessation
- 1999-03-15 DE DE69917445T patent/DE69917445T2/de not_active Expired - Fee Related
- 1999-03-15 NZ NZ507054A patent/NZ507054A/xx unknown
- 1999-03-15 ES ES99911411T patent/ES2220053T3/es not_active Expired - Lifetime
- 1999-03-15 IL IL13863699A patent/IL138636A0/xx not_active IP Right Cessation
- 1999-03-15 DK DK99911411T patent/DK1075480T3/da active
- 1999-03-15 SK SK1632-2000A patent/SK285059B6/sk unknown
- 1999-03-15 EP EP99911411A patent/EP1075480B1/en not_active Expired - Lifetime
2000
- 2000-11-02 NO NO20005529A patent/NO20005529D0/no not_active Application Discontinuation
- 2000-11-03 HR HR20000749A patent/HRP20000749B1/xx not_active IP Right Cessation

Also Published As

Publication number	Publication date
SK285059B6 (sk)	2006-05-04
EP1075480B1 (en)	2004-05-19
PL343758A1 (en)	2001-09-10
CN1299363A (zh)	2001-06-13
DE69917445T2 (de)	2005-05-25
KR100624585B1 (ko)	2006-09-18
NZ507054A (en)	2002-11-26
DE69917445D1 (de)	2004-06-24
AU748094B2 (en)	2002-05-30
BR9911006A (pt)	2001-02-13
CZ20004082A3 (cs)	2001-02-14
EP1075480A4 (en)	2002-01-23
EA003558B1 (ru)	2003-06-26
ATE267209T1 (de)	2004-06-15
IL138636A0 (en)	2001-10-31
NO20005529L (no)	2000-11-02
EA200001153A1 (ru)	2001-04-23
JP2002513794A (ja)	2002-05-14
US6355843B1 (en)	2002-03-12
PT1075480E (pt)	2004-08-31
HRP20000749A2 (en)	2001-10-31
HUP0101830A3 (en)	2002-10-28
ES2220053T3 (es)	2004-12-01
CZ295089B6 (cs)	2005-05-18
CN1168694C (zh)	2004-09-29
KR20010043313A (ko)	2001-05-25
PL191095B1 (pl)	2006-03-31
NO20005529D0 (no)	2000-11-02
DK1075480T3 (da)	2004-08-16
SK16322000A3 (sk)	2001-08-06
CA2330621A1 (en)	1999-11-11
UA81595C2 (xx)	2008-01-25
HUP0101830A2 (hu)	2001-09-28
TR200003203T2 (tr)	2001-03-21
WO1999057123A1 (en)	1999-11-11
ID26405A (id)	2000-12-21
AU3005799A (en)	1999-11-23
EP1075480A1 (en)	2001-02-14

Legal Events

Date	Code	Title	Description
2001-10-31	A1OB	Publication of a patent application
2002-04-19	AIPI	Request for the grant of a patent on the basis of a substantive examination of a patent application
2007-02-28	B1PR	Patent granted
2008-02-19	ODRP	Renewal fee for the maintenance of a patent	Payment date: 20080219 Year of fee payment: 10
2009-09-16	PBON	Lapse due to non-payment of renewal fee	Effective date: 20090316

Publication	Publication Date	Title
PT952148E (pt)	2004-09-30	Derivados de acido ciclobutil-ariloxiarilsulfonilamino-hidroxamico
ES2195510T3 (es)	2003-12-01	Derivados de imidazopiridina y procedimiento para prepararlos.
HRP20000749B1 (en)	2007-02-28	Purification of carboxaldehyde
BR9901378A (pt)	2000-04-11	Processo de purificação de uma solução aquosa em relação a compostos orgânicos..
IT1292130B1 (it)	1999-01-25	Processo per la preparazione dell'acido 1,4,7,10-tetraazaciclododecan -1,4,7-triacetico e suoi derivati
SG96791G (en)	1992-01-17	Process for preparing retinoyl chlorides
AR029885A1 (es)	2003-07-23	Procedimiento para preparar n-fosfono metilglicina (glifosato) o una sal de la misma
NO20010552L (no)	2001-02-01	FremgangsmÕte for fremstilling av zofenopril kalsiumsalt
ES2149354T3 (es)	2000-11-01	Solucion acuosa, estable de folinato.
UA8020A1 (uk)	1995-12-26	Спосіб отримання 2,4-діхлор-5-фторбензойної кислоти
MX9301042A (es)	1993-12-01	Nuevo derivado sulfatado de diosmina.
SE0101323D0 (sv)	2001-04-12	New process
FR2816954B1 (fr)	2003-01-03	Solution aqueuse boree, realiser a partir d'un compose d'acide borique et de carbonate de sodium
AR015878A1 (es)	2001-05-30	Proceso para la preparacion de 3-isocromanona
ES2194745T3 (es)	2003-12-01	Procedimiento para la obtencion de 4,6-dicloropirimidi-na.
BR0004879A (pt)	2001-10-02	Composições de borracha contendo um sal dissódico do ácido 3,3'-ditiodipropiÈnico
UA6239A1 (uk)	1994-12-29	Спосіб одержання 3,9-диєтил-3'-(3-сульфопропіл)-5-метокси-4',5'-бензотиакарбоціанинбетаіна
SU1790190A1 (ru)	1996-04-27	Цис-хлордиаммин-1,3-диметилксантинплатины (ii) хлорид дигидрат, проявляющий противоопухолевую активность
MX9606563A (es)	1997-09-30	Procedimiento para preaparar compuestos de hidrocarburo aromatico sustituidos con bromoalquilo.