CO6251313A2 - Proceso para la preparacion de pirazoles - Google Patents
Proceso para la preparacion de pirazolesInfo
- Publication number
- CO6251313A2 CO6251313A2 CO09142558A CO09142558A CO6251313A2 CO 6251313 A2 CO6251313 A2 CO 6251313A2 CO 09142558 A CO09142558 A CO 09142558A CO 09142558 A CO09142558 A CO 09142558A CO 6251313 A2 CO6251313 A2 CO 6251313A2
- Authority
- CO
- Colombia
- Prior art keywords
- hal
- formula
- compound
- preparation
- pirazoles
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 3
- 150000001875 compounds Chemical class 0.000 abstract 5
- WTKZEGDFNFYCGP-UHFFFAOYSA-N Pyrazole Chemical compound C=1C=NNC=1 WTKZEGDFNFYCGP-UHFFFAOYSA-N 0.000 abstract 1
- 150000002084 enol ethers Chemical class 0.000 abstract 1
- 230000026030 halogenation Effects 0.000 abstract 1
- 238000005658 halogenation reaction Methods 0.000 abstract 1
- HDZGCSFEDULWCS-UHFFFAOYSA-N monomethylhydrazine Chemical compound CNN HDZGCSFEDULWCS-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D231/16—Halogen atoms or nitro radicals
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C251/00—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C251/72—Hydrazones
- C07C251/74—Hydrazones having doubly-bound carbon atoms of hydrazone groups bound to hydrogen atoms or to acyclic carbon atoms
- C07C251/76—Hydrazones having doubly-bound carbon atoms of hydrazone groups bound to hydrogen atoms or to acyclic carbon atoms to carbon atoms of a saturated carbon skeleton
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/12—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with only hydrogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to ring carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Plural Heterocyclic Compounds (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP07012546A EP2008996A1 (en) | 2007-06-27 | 2007-06-27 | Process for the production of pyrazoles |
Publications (1)
Publication Number | Publication Date |
---|---|
CO6251313A2 true CO6251313A2 (es) | 2011-02-21 |
Family
ID=38812166
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CO09142558A CO6251313A2 (es) | 2007-06-27 | 2009-12-14 | Proceso para la preparacion de pirazoles |
CO09142556A CO6251314A2 (es) | 2007-06-27 | 2009-12-14 | Procesos para la preparacion de pirazoles |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CO09142556A CO6251314A2 (es) | 2007-06-27 | 2009-12-14 | Procesos para la preparacion de pirazoles |
Country Status (18)
Country | Link |
---|---|
US (3) | US8269020B2 (pt) |
EP (3) | EP2008996A1 (pt) |
JP (2) | JP5563449B2 (pt) |
KR (2) | KR20100025533A (pt) |
CN (3) | CN102516175A (pt) |
AR (2) | AR067356A1 (pt) |
AU (2) | AU2008267472A1 (pt) |
BR (2) | BRPI0813903A2 (pt) |
CA (2) | CA2689218A1 (pt) |
CL (2) | CL2008001896A1 (pt) |
CO (2) | CO6251313A2 (pt) |
CR (2) | CR11162A (pt) |
EC (2) | ECSP099817A (pt) |
IL (2) | IL202419A0 (pt) |
MX (2) | MX2009013591A (pt) |
RU (2) | RU2010102137A (pt) |
TW (2) | TW200914428A (pt) |
WO (2) | WO2009000441A1 (pt) |
Families Citing this family (27)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2008996A1 (en) * | 2007-06-27 | 2008-12-31 | Syngeta Participations AG | Process for the production of pyrazoles |
EP2133341A1 (de) * | 2008-02-25 | 2009-12-16 | Bayer CropScience AG | Verfahren zur regioselektiven Synthese von 1-Alkyl-3-haloalkyl-pyrazol-4-carbonsäure-Derivaten |
JP6180705B2 (ja) * | 2008-09-30 | 2017-08-16 | ソルヴェイ(ソシエテ アノニム) | ハロゲン化環式化合物の合成方法 |
GB0908435D0 (en) | 2009-05-15 | 2009-06-24 | Syngenta Ltd | Processes |
WO2012025469A1 (en) * | 2010-08-24 | 2012-03-01 | Solvay Sa | Improved process for the preparation of esters of 1-h-pyrazole-4-carboxylic acids |
FR2975992B1 (fr) * | 2011-06-01 | 2013-11-08 | Rhodia Operations | Procede de preparation d'un compose fluoromethylpyrazole sous forme acide carboxylique ou derivee |
FR2975990B1 (fr) * | 2011-06-01 | 2013-05-24 | Rhodia Operations | Procede de preparation d'un compose organique fluore |
WO2013171134A1 (de) * | 2012-05-14 | 2013-11-21 | Bayer Cropscience Ag | Verfahren zum herstellen von 1-alkyl-3-fluoralkyl-1h-pyrazol-4-carbonsäurechloriden |
US8871947B2 (en) | 2013-02-04 | 2014-10-28 | KingChem LLC | Preparation of alkyl 3-difluoromethyl-1-methyl-1H-pyrazole-4-carboxylic acid ester |
WO2015059067A1 (de) | 2013-10-23 | 2015-04-30 | Bayer Cropscience Ag | Verfahren zur herstellung von halogenketonen |
CN103570623B (zh) * | 2013-11-12 | 2015-05-20 | 湖南化工研究院 | 一种3-(二氟甲基)-1-甲基-1h-吡唑-4-羧酸的制备方法 |
US9139507B2 (en) | 2013-12-09 | 2015-09-22 | KingChem LLC. | Process for the preparation of alkyl 3-difluoromethyl-1-methyl-1H-pyrazole-4-carboxylate and its analogs |
CN103787977B (zh) * | 2014-01-21 | 2016-05-25 | 南通雅本化学有限公司 | 一种空气氧化制备3-氟代烷基-1-取代吡唑-4-羧酸的方法 |
CN105541716B (zh) | 2015-03-26 | 2024-02-23 | Agc株式会社 | 吡唑衍生物的制造方法 |
WO2016202254A1 (zh) * | 2015-06-19 | 2016-12-22 | 浙江永太科技股份有限公司 | 一种用于制备吡唑甲酸衍生物的方法及其中间体 |
CN104945325B (zh) * | 2015-06-19 | 2017-04-05 | 浙江永太科技股份有限公司 | 一种吡唑甲酸衍生物的制备方法 |
CN106554311B (zh) * | 2015-09-28 | 2019-03-01 | 常州市卜弋科研化工有限公司 | 3-氟代烷基-1-甲基吡唑-4-羧酸的制备方法 |
WO2017054112A1 (zh) * | 2015-09-28 | 2017-04-06 | 常州市卜弋科研化工有限公司 | 3-氟代烷基-1-甲基吡唑-4-羧酸的制备方法 |
EP3797099B1 (en) | 2018-05-21 | 2023-11-01 | PI Industries Ltd. | Method for preparing substituted heterocyclic compounds |
CN109232425A (zh) * | 2018-10-16 | 2019-01-18 | 山东省农药科学研究院 | 一种苯丙烯氟菌唑中间体3-(二氟甲基)-1-甲基-1h-吡唑-4-羧酸的合成方法 |
CN110577503A (zh) | 2019-08-02 | 2019-12-17 | 宿迁市科莱博生物化学有限公司 | 一种卤素取代化合物及其制备方法和应用 |
CN111303035A (zh) * | 2020-03-18 | 2020-06-19 | 徐州圣元化工有限公司 | 一种3-(二氟甲基)-1-甲基-1h-吡唑-4-羧酸的制备方法 |
CN111233768B (zh) * | 2020-03-18 | 2021-08-03 | 徐州圣元化工有限公司 | 一种3-(二氟甲基)-1-甲基-1h-吡唑-4-羧酸乙酯的制备方法 |
WO2022233129A1 (en) | 2021-05-05 | 2022-11-10 | Fujian Yongjing Technology Co., Ltd | New process for the synthesis of 5-fluoro-3- (difuoromethyl) -5-fluoro-1-methyl-1h-pyrazole-4-carboxylic acid derivatives and the free acid thereof |
CN114195715B (zh) * | 2021-12-31 | 2024-05-10 | 福建永晶科技股份有限公司 | 1-甲基-3-二氟甲基-4-吡唑酸和1-甲基-3-三氟甲基-4-吡唑酸的制备方法 |
CN117384096A (zh) * | 2023-12-13 | 2024-01-12 | 山东国邦药业有限公司 | 一种二氟吡唑酸的制备方法 |
CN117447401B (zh) * | 2023-12-26 | 2024-04-19 | 山东国邦药业有限公司 | 一种二氟吡唑酸的合成方法 |
Family Cites Families (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0759558B2 (ja) * | 1987-12-25 | 1995-06-28 | 三井東圧化学株式会社 | 1,3−ジアルキルピラゾール−4−アルデヒド類の製造法 |
JPH0759557B2 (ja) * | 1987-12-25 | 1995-06-28 | 三井東圧化学株式会社 | 1,3−ジアルキルピラゾール−4−アルデヒド誘導体の製造方法 |
JPH089599B2 (ja) * | 1988-08-02 | 1996-01-31 | 三井東圧化学株式会社 | ピラゾールカルボン酸類の製造方法 |
AU2003295041A1 (en) * | 2002-11-20 | 2004-06-18 | L'oreal | Composition for hair care or eyelashes containing a pyrazol-carboxamide, its use for stimulating hair and eyelash growth and/or for preventing loss thereof |
DE10349500A1 (de) * | 2003-10-23 | 2005-06-02 | Bayer Cropscience Ag | Verfahren zum Herstellen von 2-Dihalogenacyl-3-amino-acrylsäureestern und 3-Dihalogenmethyl-pyrazol-4-carbonsäureestern |
WO2005092885A1 (en) * | 2004-02-27 | 2005-10-06 | Eli Lilly And Company | 4-amino-piperidine derivatives as monoamine uptake inhibitors |
BRPI0512118A (pt) * | 2004-06-18 | 2008-02-06 | Basf Ag | composto, processo para combater fungos nocivos, e, agente fungicida |
AU2005273619B2 (en) * | 2004-08-18 | 2009-05-28 | Pfizer Inc. | Inhibitors of hepatitis C virus RNA-dependent RNA polymerase, and compositions and treatments using the same |
WO2006090778A1 (ja) * | 2005-02-25 | 2006-08-31 | Sagami Chemical Research Center | 1-置換-3-フルオロアルキルピラゾール-4-カルボン酸エステルの製造方法 |
EP2253622A1 (en) * | 2005-09-16 | 2010-11-24 | Syngenta Participations AG. | Process for the production of amides |
EP2164831B1 (de) * | 2007-06-01 | 2013-07-17 | Basf Se | Verfahren zur herstellung n-substituierter (3-dihalomethyl-1-methyl-pyrazol-4-yl)carboxamide |
EP2008996A1 (en) * | 2007-06-27 | 2008-12-31 | Syngeta Participations AG | Process for the production of pyrazoles |
-
2007
- 2007-06-27 EP EP07012546A patent/EP2008996A1/en not_active Ceased
-
2008
- 2008-06-16 US US12/666,179 patent/US8269020B2/en active Active
- 2008-06-16 BR BRPI0813903-2A2A patent/BRPI0813903A2/pt not_active Application Discontinuation
- 2008-06-16 KR KR1020097026870A patent/KR20100025533A/ko not_active Application Discontinuation
- 2008-06-16 WO PCT/EP2008/004829 patent/WO2009000441A1/en active Application Filing
- 2008-06-16 JP JP2010513717A patent/JP5563449B2/ja active Active
- 2008-06-16 CN CN2011103836384A patent/CN102516175A/zh active Pending
- 2008-06-16 AU AU2008267472A patent/AU2008267472A1/en not_active Abandoned
- 2008-06-16 MX MX2009013591A patent/MX2009013591A/es active IP Right Grant
- 2008-06-16 CA CA002689218A patent/CA2689218A1/en not_active Abandoned
- 2008-06-16 BR BRPI0813284-4A patent/BRPI0813284B1/pt active IP Right Grant
- 2008-06-16 CA CA2690246A patent/CA2690246A1/en not_active Abandoned
- 2008-06-16 WO PCT/EP2008/004830 patent/WO2009000442A2/en active Application Filing
- 2008-06-16 US US12/665,738 patent/US20100256390A1/en not_active Abandoned
- 2008-06-16 JP JP2010513718A patent/JP2010531315A/ja active Pending
- 2008-06-16 MX MX2009013592A patent/MX2009013592A/es not_active Application Discontinuation
- 2008-06-16 RU RU2010102137/04A patent/RU2010102137A/ru not_active Application Discontinuation
- 2008-06-16 KR KR1020097026780A patent/KR20100025531A/ko not_active Application Discontinuation
- 2008-06-16 EP EP08773461A patent/EP2167461B1/en active Active
- 2008-06-16 RU RU2010102135/04A patent/RU2010102135A/ru not_active Application Discontinuation
- 2008-06-16 CN CN200880021857A patent/CN101796021A/zh active Pending
- 2008-06-16 AU AU2008267473A patent/AU2008267473A1/en not_active Abandoned
- 2008-06-16 CN CN200880022057A patent/CN101687806A/zh active Pending
- 2008-06-16 EP EP08773462A patent/EP2170832A2/en not_active Withdrawn
- 2008-06-23 TW TW097123280A patent/TW200914428A/zh unknown
- 2008-06-23 TW TW097123281A patent/TW200916445A/zh unknown
- 2008-06-26 CL CL2008001896A patent/CL2008001896A1/es unknown
- 2008-06-26 CL CL2008001897A patent/CL2008001897A1/es unknown
- 2008-06-27 AR ARP080102805A patent/AR067356A1/es not_active Application Discontinuation
- 2008-06-27 AR ARP080102804A patent/AR067355A1/es not_active Application Discontinuation
-
2009
- 2009-11-30 IL IL202419A patent/IL202419A0/en unknown
- 2009-12-10 IL IL202664A patent/IL202664A/en active IP Right Grant
- 2009-12-14 CR CR11162A patent/CR11162A/es not_active Application Discontinuation
- 2009-12-14 CO CO09142558A patent/CO6251313A2/es not_active Application Discontinuation
- 2009-12-14 CR CR11161A patent/CR11161A/es not_active Application Discontinuation
- 2009-12-14 CO CO09142556A patent/CO6251314A2/es not_active Application Discontinuation
- 2009-12-18 EC EC2009009817A patent/ECSP099817A/es unknown
- 2009-12-18 EC EC2009009818A patent/ECSP099818A/es unknown
-
2012
- 2012-09-17 US US13/621,686 patent/US8785657B2/en active Active
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Legal Events
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FC | Application refused |