CN105125421A - UV solidified water-based strippable polish gum and preparation method thereof - Google Patents
UV solidified water-based strippable polish gum and preparation method thereof Download PDFInfo
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- CN105125421A CN105125421A CN201510631023.7A CN201510631023A CN105125421A CN 105125421 A CN105125421 A CN 105125421A CN 201510631023 A CN201510631023 A CN 201510631023A CN 105125421 A CN105125421 A CN 105125421A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/87—Polyurethanes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q3/00—Manicure or pedicure preparations
- A61Q3/02—Nail coatings
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/54—Polymers characterized by specific structures/properties
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Abstract
The invention provides UV solidified water-based strippable polish gum. The UV solidified water-based strippable polish gum is prepared from, by weight, 50-80 parts of UV solidified waterborne polyurethane acrylate, 0.05-0.1 part of flatting agent, 1-10 parts of wetting agents, 1-3 parts of thickening agents, 0.2-1 part of defoaming agent, 2-5 parts of coalescing agents, 1-10 parts of water-based color paste, 1-10 parts of water-based strippable agents and 3-5 parts of water-soluble photoinitiator. The invention further provides a preparation method of the strippable polish gum. The preparation method includes the steps of adding the wetting agents, the flatting agent, the deforming agent and the water-based color paste into a high-speed dispersion machine, conducting stirring and dispersing, lowering the stirring speed, adding the UV solidified waterborne polyurethane acrylate, the thickening agents, the coalescing agents, the water-based strippable agents and the water-soluble photoinitiator, continuing to conduct dispersion, conducting even mixing, and obtaining the UV solidified water-based strippable polish gum. High film hardness and high gloss are achieved after the UV solidified water-based strippable polish gum is painted to form a film.
Description
Technical field
The invention belongs to polymeric material field, relate to peelable nail polish glue of a kind of UV curable water-borne and preparation method thereof.
Background technology
Strippable property nail polish glue is one ornamental nail-care products in short-term that in recent years occur, that deeply like by numerous female friends, have painting unload convenient, change feature easily, manicure style everyday different, difference constantly can be accomplished.In recent years, along with the cry of environmental protection is more and more higher, and it is more and more stricter to the discharge restriction of air to VOC, solvent-borne type strippable property nail polish glue develops to environment-friendly water-based strippable property nail polish glue, it is little that it has pollution, raw material availability is high, but current environment-friendly water-based strippable property nail polish adhesive curing film formation time is longer, the decorate properties of cured film is poor, glossiness is lower, greatly reduce the using character of nail polish glue, make numerous friend Mies still be deeply in love the high solvent-borne type nail polish glue product not environmentally of glossiness, hinder the update of environment-friendly products of new generation; Have current aqueous strippable property nail polish glue serviceability also poor again, wearability and hardness and solvent type product also have gap, are difficult to meet the needs of social development to high-performance strippable property nail polish glue, limit it and apply.
Summary of the invention
For above-mentioned technical problem of the prior art, the invention provides peelable nail polish glue of a kind of UV curable water-borne and preparation method thereof, it is longer that described this UV curable water-borne peelable nail polish glue and preparation method thereof solves aqueous strippable property nail polish adhesive curing film formation time of the prior art, the decorate properties of cured film is poor, the technical problem that glossiness is lower.
The invention provides the peelable nail polish glue of a kind of UV curable water-borne, calculate by weight, its raw material composition and content as follows:
UV solidfication water polyurethane acrylate 50-80 part,
Levelling agent 0.05-0.1 part,
Wetting agent 1-10 part,
Thickening agent 1-3 part,
Defoamer 0.2-1 part,
Coalescents 2-5 part,
Aqueous color paste 1-10 part,
Aqueous peelable dose of 1-10 part,
Water-soluble photoinitiator 3-5 part,
Wherein, described UV solidfication water polyurethane acrylate is quick-setting aqueous polyurethane acrylate under a kind of UV light irradiation;
Described levelling agent is selected from polydimethylsiloxane compounds or polyethers or acrylate modified polydimethylsiloxane;
Described wetting agent is polyether-modified polysiloxane type compounds;
Described thickening agent is aqueous nonionic association type rheology modifier;
Described defoamer is the mixture of polysiloxanes;
Described coalescents is one or both mixture in dipropylene, alcohol ester 12;
Described aqueous remover is one or both mixture in organic silicon emulsion or wax emulsion;
Described water-soluble photoinitiator is the mixture of any one or the two or more arbitrary proportion composition in Irgacure2959, IRGACURE500, IRGACURE819 or IRGACURE819DW.
Further, calculate by weight, its raw material composition and content as follows:
UV solidfication water polyurethane acrylate 50 parts,
Levelling agent 0.05 part,
Wetting agent 1 part,
Thickening agent 1 part,
Defoamer 0.2 part,
Coalescents 2 parts,
Aqueous color paste 1 part,
Aqueous peelable dose 1 part,
Water-soluble photoinitiator 3 parts,
Wherein said UV solidfication water polyurethane acrylate is the JAZO of Nanjing Jia Zhong Chemical Industry Science Co., Ltd;
Described levelling agent is enlightening height TegoGlide410;
Described wetting agent is the NP-100 of LG-DOW company;
Described thickening agent is the RM825 of ROHM AND HAAS company limited;
Described defoamer is the mixture of German BYK-035, BYK-037 1:1 in mass ratio;
Described coalescents is U.S. Yi Shiman TEXANOL coalescents alcohol ester 12;
Described aqueous remover is organic silicon emulsion;
Described water-soluble photoinitiator be BASF BASF light trigger Irgacure2959, IRGACURE500, IRGACURE819 in mass ratio 1:1:1 composition mixture.
Further, calculate by weight, its raw material composition and content as follows:
UV solidfication water polyurethane acrylate 80 parts,
Levelling agent 0.1 part,
Wetting agent 10 parts,
Thickening agent 3 parts,
Defoamer 1 part,
Coalescents 5 parts,
Aqueous color paste 10 parts,
Aqueous peelable dose 10 parts,
Water-soluble photoinitiator 5 parts,
Wherein said UV solidfication water polyurethane acrylate is the JAZO of Nanjing Jia Zhong Chemical Industry Science Co., Ltd;
Described levelling agent be German BYK-345, BYK-346 in mass ratio 1:1 composition mixture;
Described wetting agent is Si Luoke-aqueous wetting dispersing agent Silok-7117W;
The RM-8W aqueous nonionic association type rheology modifier that described thickening agent provides for Guangzhou Heng Yu Chemical Co., Ltd.;
Described defoamer is German BYK Bi Ke BYK-024, BYK-025, BYK-035 is the mixture of 1:1:1 composition in mass ratio;
Described coalescents is the dipropylene of Dow Chemical company;
Described aqueous remover is the mixture of organic silicon emulsion and wax emulsion 2:1 composition in mass ratio;
Described water-soluble photoinitiator be BASF BASF light trigger Irgacure2959, IRGACURE500, IRGACURE819DW in mass ratio 2:1:1 composition mixture.
The present invention is owing to adopting UV curing formula, therefore, containing numerous cross-linked structure after a kind of UV curable water-borne of the present invention peelable nail polish glue curing of coating, on the one hand achieve fast setting, make on the one hand this film close to or reach the high rigidity of solvent-borne type peelable nail polish glue, high glaze and excellent resistance to water.The present invention adds due to the aqueous remover in raw material, and its molecular structure is organosilicon, has lower surface energy, can migrate to the interface between fingernail and nail polish glue in the curing process, reduces the tack of nail polish glue, makes it have good strippable property.
Through the surface of the microscope slide of UV nail polish light irradiation precoating nail polish glue after the UV curable water-borne peelable nail polish glue film of gained of the present invention, according to the fingers-touch method (surface of the nail polish glue of the cured a period of time that press...withes one's finger, using tack-free as completely crued standard, shortest time used when solidifying completely with nail polish glue characterizes), after testing, the hardening time of quick-drying nail polish glue of the present invention is 35-45s.
By the gloss after HG/T3828-2006 standard testing a kind of UV curable water-borne of the present invention peelable nail polish glue film, it is 92-95 that result shows 60 ° of mirror lusters, according to the hardness of film after GB/T1730-1993 standard testing a kind of UV curable water-borne of the present invention peelable nail polish glue film, after testing, the hardness of film of the peelable nail polish glue of UV curable water-borne of the present invention is 2H.The CMT5104 electronic tension tester that peel strength adopts Shenzhen newly to think carefully company at room temperature carries out the stripping test of 180 ° by GB/T2790-1995 standard " adhesive 180 ° of peeling strength test methods ", draw speed 50mm/min; Recording peel strength is 0.23-0.25kN/m.
The present invention compares with prior art, and its technological progress is significant.The peelable nail polish glue of a kind of UV curable water-borne of the present invention, has higher hardness of film, gloss, wearability is good, strippable property is good, and hardening time is short after film.And its preparation method due to technique simple, easy to control, therefore possess skills maturation, the feature such as quick, efficient, and be suitable for suitability for industrialized production, can be applicable to as automobile, woodenware, industrial maintenance, plastics and wind electricity blade, the contour performance technical field of solaode.
Detailed description of the invention
Below by embodiment, the present invention is described in further detail, but do not limit the present invention.
In the raw material that various embodiments of the present invention are used except the special producer that shows and specification, other raw materials are commercially available, and specification is chemical pure.
The model of the various equipment that the present invention is used and the information of manufacturer as follows:
GFJ-0.4 type high speed dispersor, Shanghai Xin Nuo instrument and equipment company limited produces;
The hard instrument QHQ of film Pencil scratch, Tianjin Material Testing Machine factory produces;
The portable mirror luster meter of WGG-60, Shanghai is praised mapping test instrument company limited and is produced.
embodiment 1
The peelable nail polish glue of a kind of UV curable water-borne, calculates by weight, its raw material composition and content as follows:
UV solidfication water polyurethane acrylate 50 parts
Levelling agent 0.05 part
Wetting agent 1 part
Thickening agent 1 part
Defoamer 0.2 part
Coalescents 2 parts
Aqueous color paste 1 part
Aqueous peelable dose 1 part
Water-soluble photoinitiator 3 parts
Wherein said UV solidfication water polyurethane acrylate is the JAZO of Nanjing Jia Zhong Chemical Industry Science Co., Ltd;
Described levelling agent is enlightening height TegoGlide410;
Described wetting agent is the NP-100 of LG-DOW company;
Described thickening agent is the RM825 of ROHM AND HAAS company limited;
Described defoamer is the mixture of German BYK-035, BYK-037 1:1 in mass ratio;
Described coalescents is U.S. Yi Shiman TEXANOL coalescents alcohol ester 12;
Described aqueous remover is organic silicon emulsion;
Described water-soluble photoinitiator be BASF BASF light trigger Irgacure2959, IRGACURE500, IRGACURE819 in mass ratio 1:1:1 composition mixture;
The preparation method of the above-mentioned peelable nail polish glue of a kind of UV curable water-borne, specifically comprises the steps:
(1), the preparation of the peelable nail polish glue of UV curable water-borne
According to formula, 1 part of wetting agent, 0.05 part of levelling agent, 0.2 part of defoamer and 1 part of aqueous color paste is added in the GFJ-0.4 type high speed dispersor (Shanghai Xin Nuo instrument and equipment company limited) controlling rotating speed 300r/min, after disperseing 15min under 600r/min rotating speed, rotating speed is down to 300r/min, add 50 parts of UV solidfication water polyurethane acrylates, 1 part of thickening agent, 2 parts of coalescents, 1 part of aqueous peelable dose and 3 parts water-soluble photoinitiators, continue dispersion 5min, mix homogeneously, namely obtains the peelable nail polish glue of UV curable water-borne.
Through the surface of the microscope slide of UV nail polish light irradiation precoating nail polish glue after the UV curable water-borne peelable nail polish glue film of gained of the present invention, according to the fingers-touch method (surface of the nail polish glue of the cured a period of time that press...withes one's finger, using tack-free as completely crued standard, shortest time used when solidifying completely with nail polish glue characterizes), after testing, the hardening time of quick-drying nail polish glue of the present invention is 45s.
According to HG/T3828-2006 standard, utilize Shanghai to praise the peelable nail polish glue of the UV curable water-borne of mapping test instrument company limited WGG-60 portable mirror luster meter to above-mentioned gained and test the glossiness after its film, result shows that film 60 ° of mirror lusters are 92.
According to GB/T1730-1993 standard, QHQ film Pencil scratch hard instrument (the Tianjin Material Testing Machine factory) hardness of film to the peelable nail polish glue of the UV curable water-borne of above-mentioned gained is adopted to test, result shows, the hardness of film of the peelable nail polish glue of UV curable water-borne of gained is 2H.
The CMT5104 electronic tension tester that peel strength adopts Shenzhen newly to think carefully company at room temperature carries out the stripping test of 180 ° by GB/T2790-1995 standard " adhesive 180 ° of peeling strength test methods ", draw speed 50mm/min; Recording peel strength is 0.23kN/m;
After the UV curable water-borne peelable nail polish glue film of gained of the present invention in sum, there is higher hardness of film, gloss and shorter hardening time, hardness, gloss reach the hardness of film after solvent-borne type nail polish glue film, and hardening time shortened greatly compared with the hardening time of tens minutes of the peelable nail polish glue of aqueous.
embodiment 2
The peelable nail polish glue of a kind of UV curable water-borne, calculates by weight, its raw material composition and content as follows:
UV solidfication water polyurethane acrylate 80 parts
Levelling agent 0.1 part
Wetting agent 10 parts
Thickening agent 3 parts
Defoamer 1 part
Coalescents 5 parts
Aqueous color paste 10 parts
Aqueous peelable dose 10 parts
Water-soluble photoinitiator 5 parts
Wherein said UV solidfication water polyurethane acrylate is the JAZO of Nanjing Jia Zhong Chemical Industry Science Co., Ltd;
Described levelling agent be German BYK-345, BYK-346 in mass ratio 1:1 composition mixture;
Described wetting agent is Si Luoke-aqueous wetting dispersing agent Silok-7117W;
The RM-8W aqueous nonionic association type rheology modifier that described thickening agent provides for Guangzhou Heng Yu Chemical Co., Ltd.;
Described defoamer is German BYK Bi Ke BYK-024, BYK-025, BYK-035 is the mixture of 1:1:1 composition in mass ratio;
Described coalescents is the dipropylene of Dow Chemical company;
Described aqueous remover is the mixture of organic silicon emulsion and wax emulsion 2:1 composition in mass ratio;
Described water-soluble photoinitiator be BASF BASF light trigger Irgacure2959, IRGACURE500, IRGACURE819DW in mass ratio 2:1:1 composition mixture;
The preparation method of the above-mentioned peelable nail polish glue of a kind of UV curable water-borne, specifically comprises the steps:
According to formula, 10 parts of wetting agent, 0.1 part of levelling agent, 1 part of defoamer and 10 parts of aqueous color pastes are added in the GFJ-0.4 type high speed dispersor (Shanghai Xin Nuo instrument and equipment company limited) controlling rotating speed 400r/min, after disperseing 20min under 800r/min rotating speed, rotating speed is down to 300r/min, add 80 parts of UV solidfication water polyurethane acrylates, 3 parts of thickening agents, 5 parts of coalescents, 10 parts of aqueouss peelable dose and 5 parts water-soluble photoinitiators, continue dispersion 10min, mix homogeneously, namely obtains the peelable nail polish glue of UV curable water-borne.
Through the surface of the microscope slide of UV nail polish light irradiation precoating nail polish glue after the UV curable water-borne peelable nail polish glue film of gained of the present invention, according to the fingers-touch method (surface of the nail polish glue of the cured a period of time that press...withes one's finger, using tack-free as completely crued standard, shortest time used when solidifying completely with nail polish glue characterizes), after testing, the hardening time of quick-drying nail polish glue of the present invention is 35s.
According to HG/T3828-2006 standard, utilize Shanghai to praise the peelable nail polish glue of the UV curable water-borne of mapping test instrument company limited WGG-60 portable mirror luster meter to above-mentioned gained and test the glossiness after its film, result shows that film 60 ° of mirror lusters are 95.
According to GB/T1730-1993 standard, QHQ film Pencil scratch hard instrument (the Tianjin Material Testing Machine factory) hardness of film to the peelable nail polish glue of the UV curable water-borne of above-mentioned gained is adopted to test, result shows, the hardness of film of the peelable nail polish glue of UV curable water-borne of gained is 2H.
The CMT5104 electronic tension tester that peel strength adopts Shenzhen newly to think carefully company at room temperature carries out the stripping test of 180 ° by GB/T2790-1995 standard " adhesive 180 ° of peeling strength test methods ", draw speed 50mm/min; Recording peel strength is 0.25kN/m;
After the UV curable water-borne peelable nail polish glue film of gained of the present invention in sum, there is higher hardness of film, gloss and shorter hardening time, hardness, gloss reach the hardness of film after solvent-borne type nail polish glue film, and hardening time shortened greatly compared with the hardening time of tens minutes of the peelable nail polish glue of aqueous.
In sum, what the peelable nail polish glue of UV curable water-borne of the present invention adopted is UV curing formula, and the high speed curable of UV improves its curing rate, and the hardening time of nail polish glue more peelable than aqueous substantially reduces, and only has 35-45s; Due to adding of the aqueous remover in raw material, its molecular structure is organosilicon, has lower surface energy, the interface between fingernail and nail polish glue can be migrated in the curing process, reduce the tack of nail polish glue, make it have good strippable property, peel strength is 0.23-0.25kN/m; Containing numerous cross-linked structure after a kind of UV curable water-borne of the present invention peelable nail polish glue curing of coating, achieve fast setting on the one hand, make on the one hand this film close to or reach the high rigidity of solvent-borne type peelable nail polish glue, high glaze and excellent resistance to water.
Described content be only the present invention conceive under basic explanation, and according to any equivalent transformation that technical scheme of the present invention is done, all should protection scope of the present invention be belonged to.
Claims (4)
1. the peelable nail polish glue of UV curable water-borne, is characterized in that calculating by weight, its raw material composition and content as follows:
UV solidfication water polyurethane acrylate 50-80 part,
Levelling agent 0.05-0.1 part,
Wetting agent 1-10 part,
Thickening agent 1-3 part,
Defoamer 0.2-1 part,
Coalescents 2-5 part,
Aqueous color paste 1-10 part,
Aqueous peelable dose of 1-10 part,
Water-soluble photoinitiator 3-5 part,
Wherein, described UV solidfication water polyurethane acrylate is quick-setting aqueous polyurethane acrylate under a kind of UV light irradiation;
Described levelling agent is selected from polydimethylsiloxane compounds or polyethers or acrylate modified polydimethylsiloxane;
Described wetting agent is polyether-modified polysiloxane type compounds;
Described thickening agent is aqueous nonionic association type rheology modifier;
Described defoamer is the mixture of polysiloxanes;
Described coalescents is one or both mixture in dipropylene, alcohol ester 12;
Described aqueous remover is one or both mixture in organic silicon emulsion or wax emulsion;
Described water-soluble photoinitiator is the mixture of any one or the two or more arbitrary proportion composition in Irgacure2959, IRGACURE500, IRGACURE819 or IRGACURE819DW.
2. the peelable nail polish glue of a kind of UV curable water-borne as claimed in claim 1, is characterized in that calculating by weight, its raw material composition and content as follows:
UV solidfication water polyurethane acrylate 50 parts,
Levelling agent 0.05 part,
Wetting agent 1 part,
Thickening agent 1 part,
Defoamer 0.2 part,
Coalescents 2 parts,
Aqueous color paste 1 part,
Aqueous peelable dose 1 part,
Water-soluble photoinitiator 3 parts,
Wherein said UV solidfication water polyurethane acrylate is selected from the JAZO of Nanjing Jia Zhong Chemical Industry Science Co., Ltd;
Described levelling agent is selected from enlightening height TegoGlide410;
Described wetting agent is selected from the NP-100 of LG-DOW company;
Described thickening agent is selected from the RM825 of ROHM AND HAAS company limited;
Described defoamer is the mixture of German BYK-035, BYK-037 1:1 in mass ratio;
Described coalescents is selected from U.S. Yi Shiman TEXANOL coalescents alcohol ester 12;
Described aqueous remover is organic silicon emulsion;
Described water-soluble photoinitiator be BASF BASF light trigger Irgacure2959, IRGACURE500, IRGACURE819 in mass ratio 1:1:1 composition mixture.
3. the peelable nail polish glue of a kind of UV curable water-borne as claimed in claim 1, is characterized in that calculating by weight, its raw material composition and content as follows:
UV solidfication water polyurethane acrylate 80 parts,
Levelling agent 0.1 part,
Wetting agent 10 parts,
Thickening agent 3 parts,
Defoamer 1 part,
Coalescents 5 parts,
Aqueous color paste 10 parts,
Aqueous peelable dose 10 parts,
Water-soluble photoinitiator 5 parts,
Wherein said UV solidfication water polyurethane acrylate is selected from the JAZO of Nanjing Jia Zhong Chemical Industry Science Co., Ltd;
Described levelling agent be German BYK-345, BYK-346 in mass ratio 1:1 composition mixture;
Described wetting agent is Si Luoke-aqueous wetting dispersing agent Silok-7117W;
The RM-8W aqueous nonionic association type rheology modifier that described thickening agent provides for Guangzhou Heng Yu Chemical Co., Ltd.;
Described defoamer is German BYK Bi Ke BYK-024, BYK-025, BYK-035 is the mixture of 1:1:1 composition in mass ratio;
Described coalescents is the dipropylene of Dow Chemical company;
Described aqueous remover is the mixture of organic silicon emulsion and wax emulsion 2:1 composition in mass ratio;
Described water-soluble photoinitiator be BASF BASF light trigger Irgacure2959, IRGACURE500, IRGACURE819DW in mass ratio 2:1:1 composition mixture.
4. claim 1, the preparation method of the peelable nail polish glue of a kind of UV curable water-borne described in 2 or 3, it is characterized in that: take each reacting substance according to parts by weight, wetting agent is added in the high speed dispersor controlling rotating speed 300-400r/min, levelling agent, defoamer and aqueous color paste, after disperseing 15-20min under 600-800r/min rotating speed, rotating speed is down to 300r/min, add UV solidfication water polyurethane acrylate, thickening agent, coalescents, peelable dose of aqueous and water-soluble photoinitiator, continue dispersion 5-10min, mix homogeneously, namely the peelable nail polish glue of UV curable water-borne is obtained.
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| CN201510631023.7A CN105125421B (en) | 2015-09-29 | 2015-09-29 | A kind of peelable nail polish glue of UV curable water-bornes and preparation method thereof |
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| CN114392208A (en) * | 2021-12-21 | 2022-04-26 | 上海魅奈儿科技有限公司 | Peelable nail polish gel for high-precision ink-jet nail printing and preparation method thereof |
| CN115569089A (en) * | 2022-11-09 | 2023-01-06 | 郑州圣莱特空心微珠新材料有限公司 | Matte nail polish gel and preparation method thereof |
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