CN105596232A - Peelable nail polish and preparation method thereof - Google Patents
Peelable nail polish and preparation method thereof Download PDFInfo
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- CN105596232A CN105596232A CN201610038642.XA CN201610038642A CN105596232A CN 105596232 A CN105596232 A CN 105596232A CN 201610038642 A CN201610038642 A CN 201610038642A CN 105596232 A CN105596232 A CN 105596232A
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- nail polish
- byk
- peelable
- polish glue
- peelable nail
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q3/00—Manicure or pedicure preparations
- A61Q3/02—Nail coatings
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F283/00—Macromolecular compounds obtained by polymerising monomers on to polymers provided for in subclass C08G
- C08F283/12—Macromolecular compounds obtained by polymerising monomers on to polymers provided for in subclass C08G on to polysiloxanes
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
- A61K2800/432—Direct dyes
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- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Veterinary Medicine (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
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- Chemical Kinetics & Catalysis (AREA)
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Abstract
The invention discloses a peelable nail polish and a preparation method thereof. The peelable nail polish comprises, by weight, 50-80 parts of UV cured resin A, 50-80 parts of UV curing compound, 0.05-0.1 part of flatting agent, 1-10 parts of wetting agent, 0.2-1 part of defoamer, 1-10 parts of color paste special for UV nail polish, 3-5 parts of photoinitiator A and 3-5 parts of photoinitiator B. The peelable nail polish is capable of being cured rapidly after being irradiated by a 365nm UV-LED light and capable of being applied to fields of nail manicure for different groups of people widely.
Description
Technical field
The invention belongs to technical field of polymer materials, be specifically related to a kind of peelable nail polish glue and preparation method thereof, this is peelableBeing specially adapted to 365nmUV-LED light source from nail polish glue irradiates curing.
Background technology
Ms to manicure like come from one and have deep love for. When using, nail polish glue is applied to nail with instrument, through common UV light source lightAfter the treatment with irradiation of source, there is cross-linking polymerization, nail polish adhesive curing thing full, the change nothing beautiful in colour, glittering and translucent of generationThoroughly, be ladies' favorite. Compared with common UV light source curing mode, UV-LED light source has that luminous efficiency is high, the life-spanThe plurality of advantages such as length, reaction speed is fast, heat release is few, energy-saving and environmental protection, substitute common UV light source gradually. Along with city is rawThe quickening of the abundant and rhythm of life conversion of living, ladies have liked the nail of allegro conversion oneself. Peelable nail polish glueEasy to use, need to take off time, peel off with regard to whole of energy without cleaner, easily, be particularly suitable for child and use. But currentPeelable nail polish glue is generally water-based, needs collocation transparent water or sealing water to use; In persistence, be not so good as oiliness nail polish glue,Dry slower, and peelable nail polish glue generally added peelable component in the formula of nail polish glue, gives the production of nail polish glue and makesWith making troubles.
Based on above background, need to develop one can rapid curing, have decorative effect, have from peeling off component, stripping simultaneouslyFrom effective peelable nail polish glue and preparation method thereof.
Summary of the invention
One of the object of the invention is to provide one can rapid curing, have decorative effect, have from peeling off component, peeling off simultaneouslyEffective peelable nail polish glue.
Two of the object of the invention is to provide the preparation method of above-mentioned a kind of peelable nail polish glue.
Technical scheme of the present invention is specifically described as follows.
The invention provides a kind of peelable nail polish glue, calculate by weight, its raw material composition and content are as follows:
The chemical structural formula of wherein said UV cured resin A is as follows:
Wherein: m is the integer within the scope of 1-30; N is the integer within the scope of 1-30.
In the present invention, UV curing compound is selected from double pentaerythritol methacrylate, diethylene glycol diacrylate, tetrahydrochyseneFuranacrylate, tetramethylol methane tetraacrylate, ethoxyquin bisphenol a dimethacrylate, two-trimethylolpropaneTetraacrylate, three (2-ethoxy) isocyanuric acid triacrylate, pentaerythritol triacrylate, ethoxyquin three hydroxyl firstBase propane triacrylate, the third oxidation trimethylolpropane triacrylate, ethoxyquin tetramethylol methane tetraacrylate, propyleneAcid isobornyl thiocyanoacetate, tristane dimethanol diacrylate, the third oxidation neopentylglycol diacrylate, ethoxyquin trihydroxy methylPropane triacrylate, hyperbranched polyester acrylic ester, alkoxy acrylic ester, carbonic acid mono acrylic ester, imidazole radicals list thirdIn olefin(e) acid ester, cyclic carbonate ester mono acrylic ester, epoxy silicone monomer, silicone acrylate and vinyl ethers monomerOne or more.
In the present invention, described UV nail polish special-used colour starch for comprise green-yellow light, blue green glow, redness, white, green,Orange, purple, yellow, orange, pink, pink, light green, fluorescein, fluorescence green, fluorescein, fluorescent blue are interiorVersicolor UV nail polish special-used colour starch.
In the present invention, described levelling agent be selected from the high TegoGlide410 of enlightening, German BYK Bi Ke BYK-UV3510,One or more in BYK-341, BYK-344, BYK-345, BYK-346, BYK-347 or BYK-348; DescribedUV wetting agent be selected from one or both in NP-100 or the German BYK333 levelling agent of LG-DOW company; InstituteThe defoamer of stating be selected from German BYK Bi Ke BYK-024, BYK-025, BYK-035, BYK-037, BYK-038,One or more in BYK-044 or BYK-038; Described light trigger A be selected from BASF Irgacure1173,Irgacure184D、IrgacureTPO、Irgacure369、Irgacure651、Irgacure379、Irgacure819、Irgacure907 or macromolecular photoinitiator EsacureKIP150 in one or more; Described photoinitiator b is selected from BASF barIn this husband's light trigger Irgacure2959, IRGACURE500 or IRGACURE819DW one or more.
In the present invention, described UV cured resin A calculates by weight, and its composition and content are as follows:
Described UV cured resin A is prepared as follows:
Methyl Hydrogen Polysiloxane Fluid and ethoxylated trimethylolpropane triacrylate are joined in reaction vessel in proportion, then addEnter polymerization inhibitor, pass into protective gas, stir and heat, be warming up to 60～80 DEG C, add catalyst, stir lower constant temperature 3～5H, stops heating, treats that temperature drops to room temperature, obtains UV cured resin A.
The present invention also provides a kind of preparation method of peelable nail polish glue, and concrete steps are as follows:
According to formula, in the high speed dispersor of controlling rotating speed 300-400r/min, add UV wetting agent, levelling agent, froth breakingAgent and UV nail polish special-used colour starch are down to 300r/min by rotating speed after disperseing 15-20min under 600-800r/min rotating speed,Add UV cured resin A, UV curing compound and light trigger A, photoinitiator b, continue to disperse 5-10min,Mix, obtain peelable nail polish glue.
Useful achievement of the present invention is as follows:
The peelable nail polish glue of one of the present invention, due to after the peelable nail polish glue of one of the present invention curing of coating, contain numerous canCrosslinked acrylate structural can be realized rapid curing under the UV-LED of 365nm light source irradiates.
Further, after the peelable nail polish glue film of gained of the present invention through the peelable nail polish glue of 365nmUV-LED light irradiation precoatingThe surface of slide, according to fingers-touch method, (surface of the peelable nail polish glue of the pressing solidly that press...with one's finger a period of time, with notSticky hand is as completely crued standard, and while solidifying completely with peelable nail polish glue, the shortest time used characterizes), after testing,Be 10-50s the hardening time of the peelable nail polish glue of quick-drying of the present invention.
Further, peelable nail polish glue of the present invention, as the UV cured resin A molecular structure of main film forming substance for havingMachine silicon structure, has very low surface energy, has reduced the interaction between film and base material, makes it to embody better from peeling offProperty, do not need to add again and peel off auxiliary agent. The CMT5104 electronic tension tester that company is newly thought carefully in peel strength employing Shenzhen is in chamberTemperature is lower carries out the test of peeling off of 180 ° by GB/T2790-1995 standard " 180 ° of peeling strength test methods of adhesive ", and speed stretchesDegree 50mm/min; Recording peel strength is 0.21～0.24kN/m;
Further, peelable nail polish glue prepared by the present invention has added UV nail polish special-used colour starch, makes it have light resistance, resistance toHou Xing, resistant to chemical media and heat resistance.
In sum, the peelable nail polish glue of one of the present invention has faster curing rate and has good after filmDecorative effect. And its preparation method is because technique is simple, easy to control, the maturation that therefore possesses skills, the feature such as quick, efficient,And be suitable for suitability for industrialized production.
Detailed description of the invention
Below by embodiment, the present invention is described in further detail, but do not limit the present invention.
In various embodiments of the present invention raw material used, except the special producer and specification showing, other raw materials are commercially available, specificationBe chemical pure.
The model of various device and the information of manufacturer that the present invention is used are as follows:
GFJ-0.4 type high speed dispersor, Shanghai Xin Nuo instrument and equipment Co., Ltd produces.
Embodiment 1
A kind of peelable nail polish glue, calculates by weight, and its raw material composition and content are as follows:
Wherein: described UV cured resin A calculates by weight, its raw material composition and content are as follows:
Described UV cured resin A is prepared as follows: by 10 parts of Methyl Hydrogen Polysiloxane Fluids and 10 parts of ethoxylations threeHydroxymethyl-propane triacrylate joins in the there-necked flask of 500ml, then adds the hydroquinone of polymerization retarder of 0.01 part, passes intoProtective gas, stirs and heats, and is warming up to 60 DEG C, adds the complex compound of 0.03 part of chloroplatinic acid, stirs lower constant temperature 3h, stopsHeating, treats that flask temperature drops to room temperature, obtains UV cured resin A.
UV curing compound be diethylene glycol diacrylate, oxolane acrylate, hyperbranched polyester acrylic ester byThe mixture of mass ratio 1:2:1 composition;
Described levelling agent is the high TegoGlide410 of enlightening;
Described wetting agent is the NP-100 of LG-DOW company;
The yellowish green MG-1 that described UV nail polish special-used colour starch provides for Dongguan City Chun Liang process materials Co., Ltd;
Described defoamer is German BYK-035, the BYK-037 mixture of 1:1 in mass ratio;
Described light trigger A is BASF Irgacure1173, Irgacure184D, IrgacureTPO 1:1:2 in mass ratioThe mixture of composition;
Described photoinitiator b be BASF BASF light trigger Irgacure2959, IRGACURE500 in mass ratioThe mixture of 1:1 composition;
In the present embodiment, a kind of preparation method of peelable nail polish glue, specifically comprises the steps:
Methyl Hydrogen Polysiloxane Fluid and ethoxylated trimethylolpropane triacrylate are joined to three of 500ml according to a certain percentageIn mouth flask, then add a certain amount of polymerization inhibitor, pass into protective gas, stir and heat, be warming up to 60～80 DEG C, addCatalyst, stirs lower constant temperature 3～5h, stops heating, treats that flask temperature drops to room temperature, obtains UV cured resin A.
According to formula, in GFJ-0.4 type high speed dispersor (the limited public affairs of the new promise instrument and equipment in Shanghai of controlling rotating speed 300r/minDepartment) add 1 part of wetting agent, 0.05 part of levelling agent, 0.2 part of defoamer and 1 part of UV nail polish special color in high speed dispersorSlurry, after disperseing 15min under 600r/min rotating speed, rotating speed is down to 300r/min, add 50 parts of UV cured resin A,50 parts of UV curing compounds and 3 parts of light trigger A, 3 parts of photoinitiator bs, continue to disperse 5min, mixes,Obtain peelable nail polish glue.
Carrying through the peelable nail polish glue of 365nmUV-LED light irradiation precoating after the peelable nail polish glue film of the present embodiment gainedThe surface of slide, according to fingers-touch method, (surface of the peelable nail polish glue of the pressing solidly that press...with one's finger a period of time, with tack-freeAs completely crued standard, while solidifying completely with peelable nail polish glue, the shortest time used characterizes), after testing, thisBe 10s the hardening time of the peelable nail polish glue of quick-drying of invention.
Further, the peelable nail polish glue of the one of the present embodiment, as the UV cured resin A molecule knot of main film forming substanceStructure is organosilicon structure, has very low surface energy, has reduced the interaction between film and base material, makes it to embody betterRippability, peel strength adopt CMT5104 electronic tension tester that Shenzhen newly thinks carefully company at room temperature byGB/T2790-1995 standard " 180 ° of peeling strength test methods of adhesive " is carried out the test of peeling off of 180 °, draw speed50mm/min; Recording peel strength is 0.24kN/m;
Rapid curing performance after the peelable nail polish glue film of the present embodiment gained, has good fissility in sum.
Embodiment 2
A kind of peelable nail polish glue, calculates by weight, and its raw material composition and content are as follows:
Wherein said UV cured resin A calculates by weight, and its composition and content are as follows:
Described UV cured resin A is prepared as follows: by 20 parts of Methyl Hydrogen Polysiloxane Fluids and 20 parts of ethoxylations threeHydroxymethyl-propane triacrylate joins in the there-necked flask of 500ml, then adds the hydroquinone of polymerization retarder of 0.02 part, passes intoProtective gas, stirs and heats, and is warming up to 80 DEG C, adds the complex compound of 0.05 part of chloroplatinic acid, stirs lower constant temperature 5h, stopsHeating, treats that flask temperature drops to room temperature, obtains UV cured resin A.
UV curing compound is that diethylene glycol diacrylate, oxolane acrylate, alkoxy acrylic ester are by qualityThan the mixture of 1:2:1 composition;
Described levelling agent is German BYK-345, the BYK-346 mixture of 1:1 composition in mass ratio;
Described wetting agent is German BYK333;
To learn the sky blue UV nail polish that Materials Co., Ltd provides special for Foshan City hard iron light for described UV nail polish special-used colour starchMill base;
Described defoamer is that German BYK Bi Ke BYK-024, BYK-025, BYK-035 are 1:1:1 composition in mass ratioMixture;
Described light trigger A is BASF Irgacure184D, IrgacureTPO, Irgacure369, Irgacure819The mixture of 1:1:1:1 composition in mass ratio;
Described photoinitiator b be BASF BASF light trigger Irgacure2959, IRGACURE500 in mass ratioThe mixture of 1:2 composition;
In the present embodiment, a kind of preparation method of peelable nail polish glue, specifically comprises the steps:
According to formula, in GFJ-0.4 type high speed dispersor (the limited public affairs of the new promise instrument and equipment in Shanghai of controlling rotating speed 400r/minDepartment) in add 10 parts of wetting agents, 0.1 part of levelling agent, 1 part of defoamer and 10 parts of UV nail polish special-used colour starch, through 800r/minUnder rotating speed, disperse, after 20min, rotating speed is down to 300r/min, add 80 parts of UV cured resin A, 80 parts of curingization of UVCompound, 5 parts of light trigger A and 5 parts of photoinitiator bs, continue to disperse 10min, mixes, and obtains peelable firstFactice.
Through the peelable nail polish glue of 365nmUV-LED light irradiation precoating after the peelable nail polish glue film of the present embodiment gainedThe surface of slide, according to fingers-touch method, (surface of the peelable nail polish glue of the pressing solidly that press...with one's finger a period of time, with tack-freeAs completely crued standard, while solidifying completely with peelable nail polish glue, the shortest time used characterizes), after testing, thisBe 50s the hardening time of the peelable nail polish glue of quick-drying of invention.
Further, the peelable nail polish glue of the one of the present embodiment, as the UV cured resin A molecule knot of main film forming substanceStructure is organosilicon structure, has very low surface energy, has reduced the interaction between film and base material, makes it to embody betterRippability, peel strength adopt CMT5104 electronic tension tester that Shenzhen newly thinks carefully company at room temperature byGB/T2790-1995 standard " 180 ° of peeling strength test methods of adhesive " is carried out the test of peeling off of 180 °, draw speed50mm/min; Recording peel strength is 0.21kN/m;
Rapid curing performance after the peelable nail polish glue film of the present embodiment gained, has good fissility in sum.
In sum, what the peelable nail polish glue of the present embodiment adopted is UV curing formula, and the high speed of UV is solidified and promoted itCuring rate, only has 10-50s. Easily peel off, peel strength is 0.21～0.24kN/m; Peelable nail polish glue has added UV to refer toNail polish special-used colour starch, makes it have light resistance, weatherability, resistant to chemical media and heat resistance.
Described content is only the basic explanation of the present invention under conceiving, and any equivalence of doing according to technical scheme of the present invention becomesChange, all should belong to protection scope of the present invention.
Claims (7)
1. a peelable nail polish glue, is characterized in that, calculates by weight, and its raw material composition and content are as follows:
The chemical structural formula of wherein said UV cured resin A is as follows:
Wherein: m is the integer within the scope of 1-30; N is the integer within the scope of 1-30.
2. peelable nail polish glue according to claim 1, is characterized in that, UV curing compound is selected from bipentaerythrite sixAcrylate, diethylene glycol diacrylate, oxolane acrylate, tetramethylol methane tetraacrylate, ethoxyquin bis-phenolA dimethylacrylate, two-trimethylolpropane tetra-acrylate, three (2-ethoxy) isocyanuric acid triacrylate,Pentaerythritol triacrylate, ethoxyquin trimethylolpropane triacrylate, the third oxidation trimethylolpropane triacrylate,Ethoxyquin tetramethylol methane tetraacrylate, isobornyl acrylate, tristane dimethanol diacrylate, the third oxidation new pentaOmega-diol diacrylate, ethoxyquin trimethylolpropane triacrylate, hyperbranched polyester acrylic ester, alkoxypropan olefin(e) acidEster, carbonic acid mono acrylic ester, imidazole radicals mono acrylic ester, cyclic carbonate ester mono acrylic ester, epoxy silicone monomer, siliconeOne or more in acrylate and vinyl ethers monomer.
3. peelable nail polish glue according to claim 1, is characterized in that, described UV nail polish special-used colour starch is for comprisingGreen-yellow light, blue green glow, redness, white, green, orange, purple, yellow, orange, pink, pink, light green, glimmeringLight Huang, fluorescence green, fluorescein, fluorescent blue are at interior versicolor UV nail polish special-used colour starch.
4. peelable nail polish glue according to claim 1, is characterized in that, described levelling agent is selected from the high TegoGlide of enlightening410, German BYK Bi Ke BYK-UV3510, BYK-341, BYK-344, BYK-345, BYK-346, BYK-347Or one or more in BYK-348; Described UV wetting agent is selected from NP-100 or the Germany of LG-DOW companyOne or both in BYK333 levelling agent; Described defoamer be selected from German BYK Bi Ke BYK-024, BYK-025,One or more in BYK-035, BYK-037, BYK-038, BYK-044 or BYK-038; Described is light-initiatedAgent A be selected from BASF Irgacure1173, Irgacure184D, IrgacureTPO, Irgacure369, Irgacure651,One in Irgacure379, Irgacure819, Irgacure907 or macromolecular photoinitiator EsacureKIP150 or severalKind; Described photoinitiator b be selected from BASF BASF light trigger Irgacure2959, IRGACURE500 orIn IRGACURE819DW one or more.
5. peelable nail polish glue according to claim 1, is characterized in that, described UV cured resin A by weightNumber calculates, and its composition and content are as follows:
Described UV cured resin A is prepared as follows:
Methyl Hydrogen Polysiloxane Fluid and ethoxylated trimethylolpropane triacrylate are joined in reaction vessel in proportion, then addEnter polymerization inhibitor, pass into protective gas, stir and heat, be warming up to 60～80 DEG C, add catalyst, stir lower constant temperature 3～5H, stops heating, treats that temperature drops to room temperature, obtains UV cured resin A.
6. peelable nail polish glue as claimed in claim 1, is characterized in that, be 10-50s hardening time, at draw speedThe peel strength recording when 50mm/min is 0.21～0.24kN/m.
7. a preparation method for peelable nail polish glue, is characterized in that, concrete steps are as follows:
According to formula, in the high speed dispersor of controlling rotating speed 300-400r/min, add UV wetting agent, levelling agent, froth breakingAgent and UV nail polish special-used colour starch are down to 300r/min by rotating speed after disperseing 15-20min under 600-800r/min rotating speed,Add UV cured resin A, UV curing compound and light trigger A, photoinitiator b, continue to disperse 5-10min,Mix, obtain peelable nail polish glue.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201610038642.XA CN105596232B (en) | 2016-01-20 | 2016-01-20 | Peelable nail polish glue and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610038642.XA CN105596232B (en) | 2016-01-20 | 2016-01-20 | Peelable nail polish glue and preparation method thereof |
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| CN105596232B CN105596232B (en) | 2019-01-04 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112480314A (en) * | 2020-12-04 | 2021-03-12 | 西安石油大学 | Film-forming substance for water-based strippable nail polish and preparation method thereof |
| CN112807246A (en) * | 2019-11-15 | 2021-05-18 | 万华化学集团股份有限公司 | Ultraviolet-curing optically variable nail polish and preparation method thereof |
| CN113576144A (en) * | 2021-08-03 | 2021-11-02 | 上海慧姿化妆品有限公司 | Composition for nail sticker and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006327941A (en) * | 2005-05-23 | 2006-12-07 | Daito Kasei Kogyo Kk | Aqueous nail polish |
| CN105125421A (en) * | 2015-09-29 | 2015-12-09 | 上海应用技术学院 | UV solidified water-based strippable polish gum and preparation method thereof |
-
2016
- 2016-01-20 CN CN201610038642.XA patent/CN105596232B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006327941A (en) * | 2005-05-23 | 2006-12-07 | Daito Kasei Kogyo Kk | Aqueous nail polish |
| CN105125421A (en) * | 2015-09-29 | 2015-12-09 | 上海应用技术学院 | UV solidified water-based strippable polish gum and preparation method thereof |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112807246A (en) * | 2019-11-15 | 2021-05-18 | 万华化学集团股份有限公司 | Ultraviolet-curing optically variable nail polish and preparation method thereof |
| CN112807246B (en) * | 2019-11-15 | 2023-01-13 | 万华化学集团股份有限公司 | Ultraviolet-curing optically variable nail polish and preparation method thereof |
| CN112480314A (en) * | 2020-12-04 | 2021-03-12 | 西安石油大学 | Film-forming substance for water-based strippable nail polish and preparation method thereof |
| CN113576144A (en) * | 2021-08-03 | 2021-11-02 | 上海慧姿化妆品有限公司 | Composition for nail sticker and preparation method thereof |
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| CN105596232B (en) | 2019-01-04 |
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