SE451718B - Sett att omkristallisera sprengemnena oktogen och hexogen - Google Patents

Sett att omkristallisera sprengemnena oktogen och hexogen

Info

Publication number
SE451718B
SE451718B SE8401857A SE8401857A SE451718B SE 451718 B SE451718 B SE 451718B SE 8401857 A SE8401857 A SE 8401857A SE 8401857 A SE8401857 A SE 8401857A SE 451718 B SE451718 B SE 451718B
Authority
SE
Sweden
Prior art keywords
octogen
hexogen
explosive
lactone
water
Prior art date
Application number
SE8401857A
Other languages
English (en)
Swedish (sv)
Other versions
SE8401857L (sv
SE8401857D0 (sv
Inventor
L Svensson
J-O Nyqvist
L Westling
Original Assignee
Nobel Kemi Ab
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nobel Kemi Ab filed Critical Nobel Kemi Ab
Priority to SE8401857A priority Critical patent/SE451718B/sv
Publication of SE8401857D0 publication Critical patent/SE8401857D0/xx
Priority to GB08506432A priority patent/GB2156805B/en
Priority to IN216/DEL/85A priority patent/IN163711B/en
Priority to YU423/85A priority patent/YU45244B/xx
Priority to DE3510761A priority patent/DE3510761C2/de
Priority to US06/716,066 priority patent/US4638065A/en
Priority to NO851270A priority patent/NO160775B/no
Priority to AR299928A priority patent/AR240789A1/es
Priority to IT47908/85A priority patent/IT1181872B/it
Priority to RO118238A priority patent/RO93878B/ro
Priority to ES541846A priority patent/ES8608325A1/es
Priority to CA000478130A priority patent/CA1243672A/fr
Priority to JP60069862A priority patent/JPS60226500A/ja
Priority to BR8501575A priority patent/BR8501575A/pt
Priority to AU40806/85A priority patent/AU567609B2/en
Priority to FR8505087A priority patent/FR2562538B1/fr
Publication of SE8401857L publication Critical patent/SE8401857L/xx
Publication of SE451718B publication Critical patent/SE451718B/sv

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D257/00—Heterocyclic compounds containing rings having four nitrogen atoms as the only ring hetero atoms
    • C07D257/02—Heterocyclic compounds containing rings having four nitrogen atoms as the only ring hetero atoms not condensed with other rings
    • C—CHEMISTRY; METALLURGY
    • C06—EXPLOSIVES; MATCHES
    • C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
    • C06B25/00—Compositions containing a nitrated organic compound
    • C06B25/34—Compositions containing a nitrated organic compound the compound being a nitrated acyclic, alicyclic or heterocyclic amine
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
    • C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
    • C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
    • C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
    • C07D251/40—Nitrogen atoms
    • C07D251/54—Three nitrogen atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
  • Saccharide Compounds (AREA)
  • Liquid Crystal Substances (AREA)
  • Peptides Or Proteins (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
SE8401857A 1984-04-04 1984-04-04 Sett att omkristallisera sprengemnena oktogen och hexogen SE451718B (sv)

Priority Applications (16)

Application Number Priority Date Filing Date Title
SE8401857A SE451718B (sv) 1984-04-04 1984-04-04 Sett att omkristallisera sprengemnena oktogen och hexogen
GB08506432A GB2156805B (en) 1984-04-04 1985-03-13 Recrystallisation of the high explosives hmx and rdx
IN216/DEL/85A IN163711B (fr) 1984-04-04 1985-03-15
YU423/85A YU45244B (en) 1984-04-04 1985-03-18 Process for recrystallisation of octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine and hexahydro-1,3,5-trinitro-1,3,5-triazinedd
DE3510761A DE3510761C2 (de) 1984-04-04 1985-03-25 Verfahren zum Umkristallisieren von Octogen oder Hexogen
US06/716,066 US4638065A (en) 1984-04-04 1985-03-26 Crystallization method for HMX and RDX
NO851270A NO160775B (no) 1984-04-04 1985-03-28 Fremgangsm te ved omkrystallisering av hoeyenergisprfene octogen og hexogen.
AR299928A AR240789A1 (es) 1984-04-04 1985-03-29 Procedimiento para recristalizar los altos explosivos hmx y rdx.
JP60069862A JPS60226500A (ja) 1984-04-04 1985-04-02 結晶化法
IT47908/85A IT1181872B (it) 1984-04-04 1985-04-02 Procedimento di ricristallizzazione di esplosivi ad alto potenziale
RO118238A RO93878B (ro) 1984-04-04 1985-04-02 Procedeu de recristalizare
ES541846A ES8608325A1 (es) 1984-04-04 1985-04-02 Metodo de cristalizacion
CA000478130A CA1243672A (fr) 1984-04-04 1985-04-02 Methode de cristallisation
BR8501575A BR8501575A (pt) 1984-04-04 1985-04-03 Processo para recristalizacao dos auto-explosivos hmx e rdx
AU40806/85A AU567609B2 (en) 1984-04-04 1985-04-03 Recrystallizing explosive
FR8505087A FR2562538B1 (fr) 1984-04-04 1985-04-03 Procede de recristallisation d'explosifs brisants

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SE8401857A SE451718B (sv) 1984-04-04 1984-04-04 Sett att omkristallisera sprengemnena oktogen och hexogen

Publications (3)

Publication Number Publication Date
SE8401857D0 SE8401857D0 (sv) 1984-04-04
SE8401857L SE8401857L (sv) 1985-10-05
SE451718B true SE451718B (sv) 1987-10-26

Family

ID=20355439

Family Applications (1)

Application Number Title Priority Date Filing Date
SE8401857A SE451718B (sv) 1984-04-04 1984-04-04 Sett att omkristallisera sprengemnena oktogen och hexogen

Country Status (16)

Country Link
US (1) US4638065A (fr)
JP (1) JPS60226500A (fr)
AR (1) AR240789A1 (fr)
AU (1) AU567609B2 (fr)
BR (1) BR8501575A (fr)
CA (1) CA1243672A (fr)
DE (1) DE3510761C2 (fr)
ES (1) ES8608325A1 (fr)
FR (1) FR2562538B1 (fr)
GB (1) GB2156805B (fr)
IN (1) IN163711B (fr)
IT (1) IT1181872B (fr)
NO (1) NO160775B (fr)
RO (1) RO93878B (fr)
SE (1) SE451718B (fr)
YU (1) YU45244B (fr)

Families Citing this family (34)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3527200A1 (de) * 1985-07-30 1987-03-19 Horst Dipl Ing Hommel Verfahren zum herstellen von sphaerolitischem kristallisat hoher schuett- und packungsdichte, insbesondere von kugelig kristallisiertem nitroguanidin
DE3605634A1 (de) * 1986-02-21 1987-08-27 Messerschmitt Boelkow Blohm Verfahren zur behandlung kristalliner sprengstoffe fuer hochleistungssprengladungen
DE3617408C1 (de) * 1986-05-23 1987-06-11 Dynamit Nobel Ag Verfahren zur Herstellung von feinkoernigem beta-Oktogen
ES2053705T3 (es) * 1987-04-22 1994-08-01 Nobel Kemi Ab Metodo para la fabricacion de explosivos cristalinos.
DE4237580C1 (de) * 1992-11-06 1994-03-17 Wasagchemie Sythen Gmbh Aufbereitung wachshaltiger Explosivstoffe
SE504054C2 (sv) * 1995-01-27 1996-10-28 Bofors Explosives Ab Flödesschema över återvinning av sprängämne
IL130308A0 (en) * 1996-12-17 2000-06-01 Cordant Tech Inc Salting-out process of crystallizing 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazatetracyclo¬5.5.0.0.5,903,11¾-dodecane
US6214988B1 (en) 1999-01-03 2001-04-10 Schlumberger Technology Corporation Process for making an HMX product
US6194571B1 (en) 1999-05-26 2001-02-27 Schlumberger Technology Corporation HMX compositions and processes for their preparation
US6428724B1 (en) 1999-05-26 2002-08-06 Schlumberger Technology Corporation Granulation process
US6201117B1 (en) 1999-05-26 2001-03-13 Schlumberger Technology Corporation Process for making a 1,3,5,7-tetraalkanoyl-1,3,5,7-tetraazacyclooctane
US6265573B1 (en) 1999-05-26 2001-07-24 Schlumberger Technology Corporation Purification process
JP4530528B2 (ja) * 2000-12-11 2010-08-25 旭化成ケミカルズ株式会社 粉状火薬組成物の製法
NO318866B1 (no) * 2003-10-06 2005-05-18 Dyno Nobel Asa Pressbar plastisk bundet sprengstoffkomposisjon
FR2887544B1 (fr) * 2005-06-02 2008-07-18 Saint Louis Inst Particules d'explosif peu sensibles aux chocs et procede de traitement associe
GB2426755B (en) * 2005-06-02 2009-07-22 Saint Louis Inst Crystalline explosive form and preparation process thereof
FR2886641A1 (fr) * 2005-06-02 2006-12-08 Saint Louis Inst Particules d'explosif peu sensibles aux chocs et procede de traitement associe
US20060272756A1 (en) * 2005-06-06 2006-12-07 Schlumberger Technology Corporation RDX Composition and Process for Its Manufacture
JP2008189515A (ja) * 2007-02-05 2008-08-21 Nippon Koki Co Ltd 鈍感化爆薬組成物およびその製造方法
JP5253762B2 (ja) * 2007-06-07 2013-07-31 日本工機株式会社 Ｒｄｘの球状化方法
JP2009051692A (ja) * 2007-08-27 2009-03-12 Nippon Koki Co Ltd 多面体化したｒｄｘ、ｒｄｘの多面体化方法、球状化ｒｄｘの製造方法
US8002917B2 (en) 2009-02-09 2011-08-23 The United States Of America As Represented By The Secretary Of The Army Adjusting yield of a manufacturing process for energetic compounds through solubility modification
CN101955469A (zh) * 2010-09-17 2011-01-26 北京理工大学 一种奥克托今与黑索今混合物分离方法
CN101973947B (zh) * 2010-09-25 2015-12-09 北京理工大学 一种用结晶控制技术制备球形化黑索今的方法
JP5993241B2 (ja) * 2012-08-02 2016-09-14 中国化薬株式会社 Ｒｄｘの製造方法
CN102887870B (zh) * 2012-09-22 2015-07-15 山西北化关铝化工有限公司 导爆管用奥克托今
CN102887865A (zh) * 2012-09-22 2013-01-23 山西北化关铝化工有限公司 特质黑索今的制备方法
CN102887866B (zh) * 2012-09-22 2015-08-12 山西北化关铝化工有限公司 改性黑索今的生产方法
CN103044173B (zh) * 2012-12-06 2015-03-04 中国工程物理研究院化工材料研究所 一种有序多孔含能晶体材料的制备方法
CN103936534B (zh) * 2014-05-09 2016-07-06 北京理工大学 一种特质细化hmx晶体及制备方法
CN104294366B (zh) * 2014-10-11 2017-01-18 中北大学 一种厘米级奥克托今单晶的培养方法
RU2670231C1 (ru) * 2017-11-15 2018-10-19 Акционерное общество "Федеральный научно-производственный центр "Алтай" Способ перекристаллизации октогена
KR101999744B1 (ko) * 2017-12-29 2019-07-12 주식회사 한화 사이클로 트리메틸렌 트리나이트라민의 제조 방법
CN114230534B (zh) * 2021-11-23 2023-11-24 中北大学 一种声共振辅助溶剂侵蚀技术制备黑索今球晶方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2656355A (en) * 1953-10-20 Purification of cyclonite
CA816157A (en) * 1969-06-24 D. Evans Albert Crystallization of fine hmx
US2434230A (en) * 1948-01-06 Method of preparing i
DE681848C (de) * 1937-04-11 1939-09-15 Edmund Von Herz Verfahren zur Gewinnung von reinem Cyclotrimethylentrinitramin
US2959587A (en) * 1943-07-16 1960-11-08 John R Johnson Sensitivity control during purification of crude cyclonite
US3133054A (en) * 1962-03-07 1964-05-12 Eastman Kodak Co Processing of hmx
US3297681A (en) * 1964-02-26 1967-01-10 Eastman Kodak Co Crystallization of fine hmx
AU6718365A (en) * 1965-11-29 1967-06-01 Eastman Kodakcompany Crystallization of fine hmx
JPS4714112Y1 (fr) * 1969-07-08 1972-05-22
US4092383A (en) * 1977-08-15 1978-05-30 The United States Of America As Represented By The Secretary Of The Navy Modification of ballistic properties of HMX by spray drying

Also Published As

Publication number Publication date
JPH0471039B2 (fr) 1992-11-12
GB8506432D0 (en) 1985-04-17
ES8608325A1 (es) 1986-07-16
NO851270L (no) 1985-10-07
IT8547908A0 (it) 1985-04-02
NO160775B (no) 1989-02-20
SE8401857L (sv) 1985-10-05
AR240789A1 (es) 1991-02-28
JPS60226500A (ja) 1985-11-11
FR2562538A1 (fr) 1985-10-11
US4638065A (en) 1987-01-20
YU42385A (en) 1988-10-31
AU567609B2 (en) 1987-11-26
IT1181872B (it) 1987-09-30
AR240789A2 (es) 1991-02-28
YU45244B (en) 1992-05-28
IN163711B (fr) 1988-10-29
FR2562538B1 (fr) 1987-04-30
CA1243672A (fr) 1988-10-25
AU4080685A (en) 1985-10-10
RO93878A (fr) 1988-02-29
DE3510761C2 (de) 1997-03-06
ES541846A0 (es) 1986-07-16
GB2156805A (en) 1985-10-16
BR8501575A (pt) 1985-12-03
GB2156805B (en) 1987-10-07
SE8401857D0 (sv) 1984-04-04
DE3510761A1 (de) 1985-10-17
RO93878B (ro) 1988-03-01

Similar Documents

Publication Publication Date Title
SE451718B (sv) Sett att omkristallisera sprengemnena oktogen och hexogen
US2391893A (en) Production of sugar cane wax
JP2802388B2 (ja) 微粒子化爆発性物質の製造方法及び装置
US3304300A (en) Method for isolation and purification of hmx
US3004959A (en) Polymers of substituted tetrazoles
US5393880A (en) Cyclodextrin refining process
JPH09504472A (ja) 過塩素酸塩の除去方法
US2656355A (en) Purification of cyclonite
US4900819A (en) Method in the production of crystalline explosives
US2847462A (en) Method of fractionating mixed isomers of trichlorobenzoic acid
US2974135A (en) Method of making plastic pellets
US2982643A (en) Nitrocellulose
US2585898A (en) Removal of troublesome fractions from benzene hexachloride
EP0246526B1 (fr) Procédé pour la production de bêta-octogène à grain fin
US3264262A (en) Polycarbonate recovery system
US3676425A (en) Process for the separation of hmx from mixtures comprising rdx and hmx
US2347660A (en) Manufacture of explosives
US4967000A (en) Spherical nitroguanidine process
US4767854A (en) Separation of RDX and HMX
US2771489A (en) Chemical process
US2964521A (en) Treatment of plastics
US2669576A (en) Method of improving the properties of certain explosives
US2525252A (en) Cyclo-trimethylenetrinitramine
US4260837A (en) Recrystallization of hexsanitrostilbene from nitric acid and water
US2394223A (en) Pentaerythritol tetranitrate recovery

Legal Events

Date Code Title Description
NAV Patent application has lapsed

Ref document number: 8401857-1