RU2016142191A - Промежуточная пленка для многослойных стекол, способ получения промежуточной пленки для многослойных стекол и многослойное стекло - Google Patents
Промежуточная пленка для многослойных стекол, способ получения промежуточной пленки для многослойных стекол и многослойное стекло Download PDFInfo
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- RU2016142191A RU2016142191A RU2016142191A RU2016142191A RU2016142191A RU 2016142191 A RU2016142191 A RU 2016142191A RU 2016142191 A RU2016142191 A RU 2016142191A RU 2016142191 A RU2016142191 A RU 2016142191A RU 2016142191 A RU2016142191 A RU 2016142191A
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- Prior art keywords
- ethylene oxide
- hexamine
- epoxy
- poly
- functional groups
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- 239000011521 glass Substances 0.000 title 3
- 238000004519 manufacturing process Methods 0.000 title 1
- 239000003054 catalyst Substances 0.000 claims 7
- 239000000178 monomer Substances 0.000 claims 6
- 239000004593 Epoxy Substances 0.000 claims 5
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims 5
- GYZLOYUZLJXAJU-UHFFFAOYSA-N diglycidyl ether Chemical group C1OC1COCC1CO1 GYZLOYUZLJXAJU-UHFFFAOYSA-N 0.000 claims 5
- 235000010299 hexamethylene tetramine Nutrition 0.000 claims 5
- 239000004312 hexamethylene tetramine Substances 0.000 claims 5
- VKYKSIONXSXAKP-UHFFFAOYSA-N hexamethylenetetramine Chemical compound C1N(C2)CN3CN1CN2C3 VKYKSIONXSXAKP-UHFFFAOYSA-N 0.000 claims 5
- 230000002209 hydrophobic effect Effects 0.000 claims 5
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims 4
- 150000001342 alkaline earth metals Chemical class 0.000 claims 4
- 239000007900 aqueous suspension Substances 0.000 claims 4
- 238000000034 method Methods 0.000 claims 4
- 239000002699 waste material Substances 0.000 claims 3
- 239000011701 zinc Substances 0.000 claims 3
- 229910052725 zinc Inorganic materials 0.000 claims 3
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 claims 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims 2
- 125000003118 aryl group Chemical group 0.000 claims 2
- 229910052500 inorganic mineral Inorganic materials 0.000 claims 2
- 239000000463 material Substances 0.000 claims 2
- 239000011707 mineral Substances 0.000 claims 2
- 239000002245 particle Substances 0.000 claims 2
- 239000011236 particulate material Substances 0.000 claims 2
- 239000002954 polymerization reaction product Substances 0.000 claims 2
- 238000006467 substitution reaction Methods 0.000 claims 2
- 239000000725 suspension Substances 0.000 claims 2
- -1 zinc alkoxide Chemical class 0.000 claims 2
- RAGOGQITHBODEI-UHFFFAOYSA-N 1,1,2,2,3,3,4,4-octafluoro-5-(2,2,3,3,4,4,5,5-octafluoropentoxy)pentane Chemical compound FC(F)C(F)(F)C(F)(F)C(F)(F)COCC(F)(F)C(F)(F)C(F)(F)C(F)F RAGOGQITHBODEI-UHFFFAOYSA-N 0.000 claims 1
- BBBUAWSVILPJLL-UHFFFAOYSA-N 2-(2-ethylhexoxymethyl)oxirane Chemical compound CCCCC(CC)COCC1CO1 BBBUAWSVILPJLL-UHFFFAOYSA-N 0.000 claims 1
- QNYBOILAKBSWFG-UHFFFAOYSA-N 2-(phenylmethoxymethyl)oxirane Chemical compound C1OC1COCC1=CC=CC=C1 QNYBOILAKBSWFG-UHFFFAOYSA-N 0.000 claims 1
- AVKQYWUBGXNBCW-UHFFFAOYSA-N 2-[(4-nonylphenoxy)methyl]oxirane Chemical compound C1=CC(CCCCCCCCC)=CC=C1OCC1OC1 AVKQYWUBGXNBCW-UHFFFAOYSA-N 0.000 claims 1
- IOHJQSFEAYDZGF-UHFFFAOYSA-N 2-dodecyloxirane Chemical compound CCCCCCCCCCCCC1CO1 IOHJQSFEAYDZGF-UHFFFAOYSA-N 0.000 claims 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical group [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims 1
- 229910019142 PO4 Inorganic materials 0.000 claims 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims 1
- 229910052770 Uranium Inorganic materials 0.000 claims 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims 1
- 150000001669 calcium Chemical class 0.000 claims 1
- 239000003245 coal Substances 0.000 claims 1
- 229910052802 copper Inorganic materials 0.000 claims 1
- 239000010949 copper Substances 0.000 claims 1
- 230000018044 dehydration Effects 0.000 claims 1
- 238000006297 dehydration reaction Methods 0.000 claims 1
- 239000010432 diamond Substances 0.000 claims 1
- 230000016615 flocculation Effects 0.000 claims 1
- 238000005189 flocculation Methods 0.000 claims 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 claims 1
- 239000010931 gold Substances 0.000 claims 1
- 229910052737 gold Inorganic materials 0.000 claims 1
- 229910052742 iron Inorganic materials 0.000 claims 1
- 239000011133 lead Substances 0.000 claims 1
- 239000002480 mineral oil Substances 0.000 claims 1
- 235000010446 mineral oil Nutrition 0.000 claims 1
- 229910052759 nickel Inorganic materials 0.000 claims 1
- 239000003921 oil Substances 0.000 claims 1
- 235000021317 phosphate Nutrition 0.000 claims 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 claims 1
- 229910052709 silver Inorganic materials 0.000 claims 1
- 239000004332 silver Substances 0.000 claims 1
- JFALSRSLKYAFGM-UHFFFAOYSA-N uranium(0) Chemical compound [U] JFALSRSLKYAFGM-UHFFFAOYSA-N 0.000 claims 1
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- B32B17/10761—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the resin layer, i.e. interlayer containing vinyl acetal
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- B32B27/306—Layered products comprising a layer of synthetic resin comprising vinyl (co)polymers; comprising acrylic (co)polymers comprising vinyl acetate or vinyl alcohol (co)polymers
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- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
- C08J5/04—Reinforcing macromolecular compounds with loose or coherent fibrous material
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- C08J5/08—Reinforcing macromolecular compounds with loose or coherent fibrous material using pretreated fibrous materials glass fibres
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- C08J5/18—Manufacture of films or sheets
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- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
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- C08K5/0008—Organic ingredients according to more than one of the "one dot" groups of C08K5/01 - C08K5/59
- C08K5/0016—Plasticisers
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- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
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- C08K5/09—Carboxylic acids; Metal salts thereof; Anhydrides thereof
- C08K5/098—Metal salts of carboxylic acids
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- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L29/00—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical; Compositions of hydrolysed polymers of esters of unsaturated alcohols with saturated carboxylic acids; Compositions of derivatives of such polymers
- C08L29/14—Homopolymers or copolymers of acetals or ketals obtained by polymerisation of unsaturated acetals or ketals or by after-treatment of polymers of unsaturated alcohols
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- C08J2329/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal, or ketal radical; Hydrolysed polymers of esters of unsaturated alcohols with saturated carboxylic acids; Derivatives of such polymer
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Claims (37)
1. Поли(этиленоксидный) сополимер, включающий продукт реакции полимеризации от 95 до 5 мас.% этиленоксида и от 5 до 95 мас.% одного или более гидрофобного мономера с эпоксидными или простыми глицидилэфирными функциональными группами в присутствии катализатора на основе алкоксида цинка или катализатора на основе модифицированного гексамина щелочноземельного металла, при этом гидрофобный мономер с эпоксидными или простыми глицидилэфирными функциональными группами описывается одной или несколькими из следующих структур:
где R1 представляет -(СН2)nCH3 и n=0-15;
где Х представляет СН2 или О,
R2 представляет Н, -(СН2)mCH3 и m равно числу от 0 до 10, или -(CF2)nCF3 и n=0-10,
и
R3 представляет Н или -(СН2)pCH3 и р равно числу от 0 до 5;
или
где Х представляет СН2 или О
и
R4 представляет -CH2(С6Н5) или -(С6Н4)-СН2-(СН2)q-CH3 и q равно числу от 0 до 10, замещение на арильном кольце может быть в мета-, орто- или параположениях.
2. Поли(этиленоксидный) сополимер по п.1, в котором катализатор на основе модифицированного гексамин щелочноземельного металла является катализатором на основе модифицированного гексаммина кальция.
3. Поли(этиленоксидный) сополимер по п.1, где гидрофобный мономер с эпоксидными или простыми глицидилэфирными функциональными группами представляет собой 1,2-эпокситетрадекан; 2-этилгексилглицидиловый простой эфир; 2,2,3,3,4,4,5,5-октафторпентиловый простой эфир; бензилглицидиловый простой эфир и 4-нонилфенилглицидиловый простой эфир.
4. Поли(этиленоксидный) сополимер по п.1, дополнительно включающий один или несколько дополнительных мономеров.
5. Способ обезвоживания водной суспензии материала в форме частиц, включающий следующие стадии:
добавление к водной суспензии материала в форме частиц поли(этиленоксидного) сополимера, который представляет собой продукт реакции полимеризации от 95 до 5 мас.% этиленоксида и от 5 до 95 мас.% гидрофобного мономера с эпоксидными или простыми глицидилэфирными функциональными группами в присутствии катализатора на основе алкоксида цинка или катализатора на основе модифицированного гексамина щелочноземельного металла, где гидрофобный мономер с эпоксидными или простыми глицидилэфирными функциональными группами описывается одной или несколькими из следующих структур:
где R1 представляет -(СН2)nCH3 и n=0-15;
где Х представляет СН2 или О,
R2 представляет Н, -(СН2)mCH3 и m равно числу от 0 до 10, или
-(CF2)nCF3 и n=0-10,
и
R3 представляет Н или -(СН2)pCH3 и р равно числу от 0 до 5;
или
где Х представляет СН2 или О
и
R4 представляет -CH2(С6Н5) или -(С6Н4)-СН2-(СН2)q-CH3 и q равно числу от 0 до 10, замещение на арильном кольце может быть в мета-, орто- или параположениях;
флокуляция суспензии;
и
обезвоживание суспензии.
6. Способ по п.5, где катализатор на основе модифицированного гексамина щелочноземельного металла представляет катализатор на основе модифицированного гексамина кальция.
7. Способ по п.5, где водная суспензия материала в форме частиц содержит отвалы и другие отходы переработки, получаемые в результате переработки минерального сырья фосфатов, алмазов, золота, минеральных песков, цинка, свинца, меди, серебра, урана, никеля, железной руды, угля, нефтеносных песков или красного шлама.
8. Способ по п.5, где водная суспензия материала в форме частиц, включающего отвалы и другие отходы переработки, получаемые в результате переработки минеральных пород нефтеносных песков.
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