JP2006111856A - 粘着剤組成物、粘着シート類、および表面保護フィルム - Google Patents
粘着剤組成物、粘着シート類、および表面保護フィルム Download PDFInfo
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- JP2006111856A JP2006111856A JP2005148181A JP2005148181A JP2006111856A JP 2006111856 A JP2006111856 A JP 2006111856A JP 2005148181 A JP2005148181 A JP 2005148181A JP 2005148181 A JP2005148181 A JP 2005148181A JP 2006111856 A JP2006111856 A JP 2006111856A
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- Prior art keywords
- sensitive adhesive
- pressure
- weight
- meth
- adhesive composition
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- XJRBAMWJDBPFIM-UHFFFAOYSA-N methyl vinyl ether Chemical compound COC=C XJRBAMWJDBPFIM-UHFFFAOYSA-N 0.000 description 1
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- 229940088644 n,n-dimethylacrylamide Drugs 0.000 description 1
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- OMNKZBIFPJNNIO-UHFFFAOYSA-N n-(2-methyl-4-oxopentan-2-yl)prop-2-enamide Chemical compound CC(=O)CC(C)(C)NC(=O)C=C OMNKZBIFPJNNIO-UHFFFAOYSA-N 0.000 description 1
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- 125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 description 1
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- 239000012766 organic filler Substances 0.000 description 1
- 125000002524 organometallic group Chemical group 0.000 description 1
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- 239000002245 particle Substances 0.000 description 1
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 1
- 229940044654 phenolsulfonic acid Drugs 0.000 description 1
- 125000002467 phosphate group Chemical group [H]OP(=O)(O[H])O[*] 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 238000009832 plasma treatment Methods 0.000 description 1
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- 229920003207 poly(ethylene-2,6-naphthalate) Polymers 0.000 description 1
- 229920001200 poly(ethylene-vinyl acetate) Polymers 0.000 description 1
- 229920000767 polyaniline Polymers 0.000 description 1
- 229920002857 polybutadiene Polymers 0.000 description 1
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- 229920001225 polyester resin Polymers 0.000 description 1
- 239000004645 polyester resin Substances 0.000 description 1
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- 239000005056 polyisocyanate Substances 0.000 description 1
- 229920001228 polyisocyanate Polymers 0.000 description 1
- 229920006254 polymer film Polymers 0.000 description 1
- 239000003505 polymerization initiator Substances 0.000 description 1
- 229920000306 polymethylpentene Polymers 0.000 description 1
- 239000011116 polymethylpentene Substances 0.000 description 1
- 229920000098 polyolefin Polymers 0.000 description 1
- 229920005606 polypropylene copolymer Polymers 0.000 description 1
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- 239000005033 polyvinylidene chloride Substances 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- ADYYRXNLCZOUSU-UHFFFAOYSA-M potassium;propan-2-ol;hydroxide Chemical compound [OH-].[K+].CC(C)O ADYYRXNLCZOUSU-UHFFFAOYSA-M 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- KRIOVPPHQSLHCZ-UHFFFAOYSA-N propiophenone Chemical class CCC(=O)C1=CC=CC=C1 KRIOVPPHQSLHCZ-UHFFFAOYSA-N 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 125000000467 secondary amino group Chemical group [H]N([*:1])[*:2] 0.000 description 1
- 229920006012 semi-aromatic polyamide Polymers 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 238000005118 spray pyrolysis Methods 0.000 description 1
- 238000004544 sputter deposition Methods 0.000 description 1
- 150000003440 styrenes Chemical class 0.000 description 1
- 125000001424 substituent group Chemical group 0.000 description 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
- 150000003458 sulfonic acid derivatives Chemical class 0.000 description 1
- 125000000542 sulfonic acid group Chemical group 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 238000010557 suspension polymerization reaction Methods 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 125000001302 tertiary amino group Chemical group 0.000 description 1
- UWHCKJMYHZGTIT-UHFFFAOYSA-N tetraethylene glycol Chemical compound OCCOCCOCCOCCO UWHCKJMYHZGTIT-UHFFFAOYSA-N 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
- 239000011135 tin Substances 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 238000001771 vacuum deposition Methods 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
- 239000011787 zinc oxide Substances 0.000 description 1
Images
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J133/00—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Adhesives based on derivatives of such polymers
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- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
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- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J7/00—Adhesives in the form of films or foils
- C09J7/20—Adhesives in the form of films or foils characterised by their carriers
- C09J7/22—Plastics; Metallised plastics
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
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Landscapes
- Chemical & Material Sciences (AREA)
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Abstract
【解決手段】炭素数6〜14であるアルキル基を有する(メタ)アクリル系モノマーを主成分とする(メタ)アクリル系ポリマーを含む粘着剤組成物において、エチレンオキシド基含有化合物およびアルカリ金属塩を含有し、前記(メタ)アクリル系ポリマー100重量部に対し、前記アルカリ金属塩1重量部未満を含有してなることを特徴とする粘着剤組成物。
【選択図】なし
Description
酸価は、自動滴定装置(平沼産業株式会社製、COM−550)を用いて測定を行い、下記式より求めた。
A;酸価
Y;サンプル溶液の滴定量(ml)
X;混合溶媒50gのみの溶液の滴定量(ml)
f;滴定溶液のファクター
M;ポリマーサンプルの重量(g)
サンプル溶液:ポリマーサンプル約0.5gを混合溶媒(トルエン/2−プロパノール/蒸留水=50/49.5/0.5、重量比)50gに溶解してサンプル溶液とした。
滴定溶液:0.1N、2−プロパノール性水酸化カリウム溶液(和光純薬工業社製、石油製品中和価試験用)
電極:ガラス電極;GE−101、比較電極;RE−201
測定モード:石油製品中和価試験1
重量部平均分子量は、東ソー株式会社製GPC装置(HLC−8220GPC)を用いて測定を行った。測定条件は下記の通りである。
サンプル注入量:10μl
溶離液:THF
流速:0.6ml/min
測定温度:40℃
カラム:
サンプルカラム;
TSKguardcolumn SuperHZ−H(1本)+TSKgel SuperHZM−H(2本)
リファレンスカラム;
TSKgel SuperH−RC(1本)
検出器:示差屈折計(RI)
なお、重量部平均分子量はポリスチレン換算値にて求めた。
ガラス転移温度Tg(℃)は、各モノマーによるホモポリマーのガラス転移温度Tgn(℃)として下記の文献値を用い、下記の式により求めた。
〔式中、Tg(℃)は共重合体のガラス転移温度、Wn(−)は各モノマーの重量分率、Tgn(℃)は各モノマーによるホモポリマーのガラス転移温度、nは各モノマーの種類を表す。〕
文献値:
2−エチルヘキシルアクリレート:−70℃
2−ヒドロキシエチルアクリレート:−15℃
粘着シートを幅70mm、長さ130mmのサイズにカットし、セパレーターを剥離した後、あらかじめ除電しておいたアクリル板(厚み:1mm、幅:70mm、長さ:100mm)に貼り合わせた偏光板(日東電工社製、SEG1425EWVAGS2B、幅:70mm、長さ:100mm)表面に片方の端部が30mmはみ出すようにハンドローラーにて圧着した。
厚み90μmのトリアセチルセルロースフィルム(富士写真フィルム社製、フジタック)を幅70mm、長さ100mmにカットし、60℃の水酸化ナトリウム水溶液(10重量%)に1分間浸漬した後、蒸留水にて洗浄し被着体を作製した。
汚染が認められなかった場合:○
汚染が認められた場合:×
トリアセチルセルロースフィルム(富士フィルム社製、フジタック、厚み:90μm)を幅70mm、長さ100mmにカットし、60℃の水酸化ナトリウム水溶液(10重量%)に1分間浸漬した後、蒸留水にて洗浄し被着体を作製した。
〔アクリル系ポリマー(A)〕
攪拌羽根、温度計、窒素ガス導入管、冷却器を備えた四つ口フラスコに2−エチルヘキシルアクリレート200重量部、2−ヒドロキシエチルアクリレート8重量部、重合開始剤として2,2’−アゾビスイソブチロニトリル0.4重量部、酢酸エチル312重量部を仕込み、緩やかに撹拌しながら窒素ガスを導入し、フラスコ内の液温を65℃付近に保って6時間重合反応を行い、アクリル系ポリマー(A)溶液(40重量%)を調製した。前記アクリル系ポリマー(A)の重量平均分子量は54万、ガラス転移温度(Tg)は−68℃、酸価は0.0であった。
〔帯電防止剤溶液(a)〕
攪拌羽根、温度計、冷却器を備えた四つ口フラスコにヨウ化リチウム0.5重量部、ポリプロピレングリコール−ポリエチレングリコール−ポリプロピレングリコール共重合体(数平均分子量2000、エチレンオキシド基含有率:50重量%)49.5重量部、酢酸エチル200重量部を仕込み、フラスコ内の液温を80℃付近に保って2時間混合撹拌を行い、帯電防止剤溶液(a)(20重量%)を調製した。
攪拌羽根、温度計、冷却器を備えた四つ口フラスコにLiN(C2F5SO2)21重量部、ポリプロピレングリコール−ポリエチレングリコール−ポリプロピレングリコール共重合体(数平均分子量2000、エチレンオキシド基含有率:50重量%)12.5重量部、酢酸エチル54重量部を仕込み、フラスコ内の液温を80℃付近に保って2時間混合撹拌を行い、帯電防止剤溶液(b)(20重量%)を調製した。
攪拌羽根、温度計、冷却器を備えた四つ口フラスコにヨウ化リチウム1重量部、ポリプロピレングリコール−ポリエチレングリコール−ポリプロピレングリコール共重合体(数平均分子量2700、エチレンオキシド基含有率:40重量%)49.5重量部、酢酸エチル202重量部を仕込み、フラスコ内の液温を80℃付近に保って2時間混合撹拌を行い、帯電防止剤溶液(c)(20重量%)を調製した。
攪拌羽根、温度計、冷却器を備えた四つ口フラスコにヨウ化リチウム1重量部、ポリプロピレングリコール−ポリエチレングリコール−ポリプロピレングリコール共重合体(数平均分子量3300、エチレンオキシド基含有率:10重量%)49重量部、酢酸エチル200重量部を仕込み、フラスコ内の液温を80℃付近に保って2時間混合撹拌を行い、帯電防止剤溶液(d)(20重量%)を調製した。
攪拌羽根、温度計、冷却器を備えた四つ口フラスコにヨウ化リチウム0.5重量部、ポリプロピレングリコール(ジオール型、数平均分子量2000、エチレンオキシド基含有率:0重量%)49.5重量部、酢酸エチル200重量部を仕込み、フラスコ内の液温を80℃付近に保って2時間混合撹拌を行い、帯電防止剤溶液(e)(20重量%)を調製した。
攪拌羽根、温度計、冷却器を備えた四つ口フラスコにヨウ化リチウム5重量部、ポリプロピレングリコール−ポリエチレングリコール−ポリプロピレングリコール共重合体(数平均分子量2000、エチレンオキシド基含有率:50重量%)45重量部、酢酸エチル200重量部を仕込み、フラスコ内の液温を80℃付近に保って2時間混合撹拌を行い、帯電防止剤溶液(f)(20重量%)を調製した。
攪拌羽根、温度計、冷却器を備えた四つ口フラスコにヨウ化リチウム1重量部、非イオン型反応性界面活性剤(旭電化工業社製、アデカリアソープER−10)49重量部、酢酸エチル200重量部を仕込み、フラスコ内の液温を80℃付近に保って2時間混合撹拌を行い、帯電防止剤溶液(g)(20重量%)を調製した。
帯電防止剤(ソルベックス社製、マイクロソルバーRMd−142、主成分:酸化スズおよびポリエステル樹脂)10重量部を、水30重量部とメタノール70重量部からなる混合溶媒で希釈することにより帯電防止剤溶液を調製した。
〔粘着剤溶液の調製〕
上記アクリル系ポリマー(A)溶液(40重量%)を酢酸エチルで20重量%に希釈し、この溶液100重量部に上記帯電防止剤溶液(a)(20重量%)10重量部、架橋剤としてヘキサメチレンジイソシアネートのイソシアヌレート体(日本ポリウレタン工業社製、コロネートHX、100重量%)0.4重量部、架橋触媒としてジラウリン酸ジブチルスズ(1重量%酢酸エチル溶液)0.4重量部を加えて混合撹拌を行い、アクリル系粘着剤溶液(1)を調製した。なお、アクリル系粘着剤溶液(1)においては、アクリル系ポリマー100重量部に対するアルカリ金属塩(リチウム塩)の配合量は0.1重量部であった。
上記アクリル系粘着剤溶液(1)を、上述のように作製した帯電防止処理ポリエチレンテレフタレートフィルムの帯電防止処理面とは反対の面に塗布し、110℃で3分間加熱して、厚さ20μmの粘着剤層を形成した。次いで、上記粘着剤層の表面に、片面にシリコーン処理を施したポリエチレンテレフタレートフィルム(厚さ25μm)のシリコーン処理面を貼り合わせ、粘着シートを作製した。
〔粘着剤溶液の調製〕
上記アクリル系ポリマー(A)溶液(40重量%)を酢酸エチルで20重量%に希釈し、この溶液100重量部に上記帯電防止剤溶液(b)(20重量%)2.7重量部、架橋剤としてヘキサメチレンジイソシアネートのイソシアヌレート体(日本ポリウレタン工業社製、コロネートHX、100重量%)0.5重量部、架橋触媒としてジラウリン酸ジブチルスズ(1重量%酢酸エチル溶液)0.4重量部を加えて混合撹拌を行い、アクリル系粘着剤溶液(2)を調製した。なお、アクリル系粘着剤溶液(2)においては、アクリル系ポリマー100重量部に対するアルカリ金属塩(リチウム塩)の配合量は0.2重量部であった。
上記アクリル系粘着剤溶液(1)に代えて、上記アクリル系粘着剤溶液(2)を用いた以外は、実施例1と同様の方法により粘着シートを作製した。
〔粘着剤溶液の調製〕
上記アクリル系ポリマー(A)溶液(40重量%)を酢酸エチルで20重量%に希釈し、この溶液100重量部に上記帯電防止剤溶液(c)(20重量%)3重量部、架橋剤としてヘキサメチレンジイソシアネートのイソシアヌレート体(日本ポリウレタン工業社製、コロネートHX、100重量%)0.6重量部、架橋触媒としてジラウリン酸ジブチルスズ(1重量%酢酸エチル溶液)0.4重量部を加えて混合撹拌を行い、アクリル系粘着剤溶液(3)を調製した。なお、アクリル系粘着剤溶液(3)においては、アクリル系ポリマー100重量部に対するアルカリ金属塩(リチウム塩)の配合量は0.06重量部であった。
上記アクリル系粘着剤溶液(1)に代えて、上記アクリル系粘着剤溶液(3)を用いた以外は、実施例1と同様の方法により粘着シートを作製した。
〔粘着剤溶液の調製〕
上記アクリル系ポリマー(A)溶液(40重量%)を酢酸エチルで20重量%に希釈し、この溶液100重量部に上記帯電防止剤溶液(d)(20重量%)5重量部、架橋剤としてトリメチロールプロパン/トリレンジイソシアネート3量体付加物(日本ポリウレタン工業社製、コロネートL、75重量%酢酸エチル溶液)0.5重量部、架橋触媒としてジラウリン酸ジブチルスズ(1重量%酢酸エチル溶液)0.6重量部を加えて混合撹拌を行い、アクリル系粘着剤溶液(4)を調製した。なお、アクリル系粘着剤溶液(4)においては、アクリル系ポリマー100重量部に対するアルカリ金属塩(リチウム塩)の配合量は0.1重量部であった。
上記アクリル系粘着剤溶液(1)に代えて、上記アクリル系粘着剤溶液(4)を用いた以外は、実施例1と同様の方法により粘着シートを作製した。
〔粘着剤溶液の調製〕
上記帯電防止剤溶液(a)を用いなかった以外は、実施例1と同様の方法によりアクリル系粘着剤溶液(5)を調製した。
上記アクリル系粘着剤溶液(1)に代えて、上記アクリル系粘着剤溶液(5)を用いた以外は、実施例1と同様の方法により粘着シートを作製した。
〔粘着剤溶液の調製〕
上記アクリル系ポリマー(A)溶液(40重量%)を酢酸エチルで20重量%に希釈し、この溶液100重量部に上記帯電防止剤溶液(e)(20重量%)10重量部、架橋剤としてトリメチロールプロパン/トリレンジイソシアネート3量体付加物(日本ポリウレタン工業社製、コロネートL、75重量%酢酸エチル溶液)0.5重量部、架橋触媒としてジラウリン酸ジブチルスズ(1重量%酢酸エチル溶液)0.6重量部を加えて混合撹拌を行い、アクリル系粘着剤溶液(6)を調製した。なお、アクリル系粘着剤溶液(6)においては、アクリル系ポリマー100重量部に対するアルカリ金属塩(リチウム塩)の配合量は0.1重量部であった。
上記アクリル系粘着剤溶液(1)に代えて、上記アクリル系粘着剤溶液(6)を用いた以外は、実施例1と同様の方法により粘着シートを作製した。
〔粘着剤溶液の調製〕
上記アクリル系ポリマー(A)溶液(40重量%)を酢酸エチルで20重量%に希釈し、この溶液100重量部にアニオン系界面活性剤であるジアルキルスルホコハク酸エステルナトリウム塩(第一工業製薬社製、ネオコールP)2.0重量部、架橋剤としてトリメチロールプロパン/トリレンジイソシアネート3量体付加物(日本ポリウレタン工業社製、コロネートL、75重量%酢酸エチル溶液)1重量部、架橋触媒としてジラウリン酸ジブチルスズ(1重量%酢酸エチル溶液)0.6重量部を加えて混合撹拌を行い、アクリル系粘着剤溶液(7)を調製した。
上記アクリル系粘着剤溶液(1)に代えて、前記アクリル系粘着剤溶液(7)を用いた以外は、実施例1と同様の方法により粘着シートを作製した。
〔粘着剤溶液の調製〕
上記アクリル系ポリマー(A)溶液(40重量%)を酢酸エチルで20重量%に希釈し、この溶液100重量部に上記帯電防止剤溶液(f)(20重量%)10重量部、架橋剤としてヘキサメチレンジイソシアネートのイソシアヌレート体(日本ポリウレタン工業社製、コロネートHX、100重量%)0.4重量部、架橋触媒としてジラウリン酸ジブチルスズ(1重量%酢酸エチル溶液)0.4重量部を加えて混合撹拌を行い、アクリル系粘着剤溶液(8)を調製した。なお、アクリル系粘着剤溶液(8)においては、アクリル系ポリマー100重量部に対するアルカリ金属塩(リチウム塩)の配合量は1重量部であった。
上記アクリル系粘着剤溶液(1)に代えて、上記アクリル系粘着剤溶液(8)を用いた以外は、実施例1と同様の方法により粘着シートを作製した。
〔粘着剤溶液の調製〕
上記アクリル系ポリマー(A)溶液(40重量%)を酢酸エチルで20重量%に希釈し、この溶液100重量部に上記帯電防止剤溶液(g)(20重量%)5.0重量部、架橋剤としてヘキサメチレンジイソシアネートのイソシアヌレート体(日本ポリウレタン工業社製、コロネートHX、100重量%)0.4重量部、架橋触媒としてジラウリン酸ジブチルスズ(1重量%酢酸エチル溶液)0.4重量部を加えて混合撹拌を行い、アクリル系粘着剤溶液(9)を調製した。なお、アクリル系粘着剤溶液(9)においては、アクリル系ポリマー100重量部に対するアルカリ金属塩(リチウム塩)の配合量は0.1重量部であった。
上記アクリル系粘着剤溶液(1)に代えて、上記アクリル系粘着剤溶液(9)を用いた以外は、実施例1と同様の方法により粘着シートを作製した。
Claims (7)
- 炭素数6〜14であるアルキル基を有する(メタ)アクリル系モノマーを主成分とする(メタ)アクリル系ポリマーを含む粘着剤組成物において、エチレンオキシド基含有化合物およびアルカリ金属塩を含有し、前記(メタ)アクリル系ポリマー100重量部に対し、前記アルカリ金属塩1重量部未満を含有してなることを特徴とする粘着剤組成物。
- 前記エチレンオキシド基含有化合物のエチレンオキシド基含有率が5〜85重量%である請求項1に記載の粘着剤組成物。
- 前記アルカリ金属塩がリチウム塩であることを特徴とする請求項1〜2のいずれかに記載の粘着剤組成物。
- 前記(メタ)アクリル系ポリマーが、ヒドロキシル基を有する(メタ)アクリル系モノマーをさらに構成成分として含むことを特徴とする請求項1〜3のいずれかに記載の粘着剤組成物。
- 請求項1〜4のいずれかに記載の粘着剤組成物を架橋してなる粘着剤層。
- 請求項1〜4のいずれかに記載の粘着剤組成物を架橋してなる粘着剤層を支持体の片面または両面に形成してなることを特徴とする粘着シート類。
- 請求項1〜4のいずれかに記載の粘着剤組成物を架橋してなる粘着剤層を、帯電防止処理されてなるプラスチック基材からなる支持体の片面または両面に形成してなることを特徴とする表面保護フィルム。
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TW094125822A TW200619341A (en) | 2004-09-16 | 2005-07-29 | Adhesive composition, adhesive sheets and surface protecting film |
EP10179205A EP2277966A1 (en) | 2004-09-16 | 2005-09-15 | Pressure-sensitive adhesive compositions, pressure-sensitive adhesive sheets and surface protecting films |
KR1020050086297A KR20060051342A (ko) | 2004-09-16 | 2005-09-15 | 점착제 조성물, 점착 시트류, 및 표면 보호 필름 |
AT05020138T ATE533822T1 (de) | 2004-09-16 | 2005-09-15 | Druckempfindliche klebstoffzusammensetzung, druckempfindliche klebefolien, und oberflächenschutzfilm |
US11/226,956 US8092907B2 (en) | 2004-09-16 | 2005-09-15 | Pressure-sensitive adhesive compositions, pressure-sensitive adhesive sheets and surface protecting films |
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CN1749345A (zh) | 2006-03-22 |
KR20100109882A (ko) | 2010-10-11 |
CN1749345B (zh) | 2010-05-05 |
TWI354007B (ja) | 2011-12-11 |
KR20060051342A (ko) | 2006-05-19 |
ATE533822T1 (de) | 2011-12-15 |
JP4531628B2 (ja) | 2010-08-25 |
TW200619341A (en) | 2006-06-16 |
US20060057371A1 (en) | 2006-03-16 |
EP1640427A1 (en) | 2006-03-29 |
KR20120085218A (ko) | 2012-07-31 |
KR101183728B1 (ko) | 2012-09-17 |
EP1640427B1 (en) | 2011-11-16 |
KR101185637B1 (ko) | 2012-09-24 |
EP2277966A1 (en) | 2011-01-26 |
US8092907B2 (en) | 2012-01-10 |
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