WO2018167268A1 - Pigments à effets - Google Patents

Pigments à effets Download PDF

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Publication number
WO2018167268A1
WO2018167268A1 PCT/EP2018/056662 EP2018056662W WO2018167268A1 WO 2018167268 A1 WO2018167268 A1 WO 2018167268A1 EP 2018056662 W EP2018056662 W EP 2018056662W WO 2018167268 A1 WO2018167268 A1 WO 2018167268A1
Authority
WO
WIPO (PCT)
Prior art keywords
tio
effect pigment
platelets
pigments
effect
Prior art date
Application number
PCT/EP2018/056662
Other languages
German (de)
English (en)
Inventor
Nicole Nelischer
Lukas Hamm
Original Assignee
Merck Patent Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Merck Patent Gmbh filed Critical Merck Patent Gmbh
Priority to JP2019551387A priority Critical patent/JP2020514511A/ja
Priority to EP18712176.9A priority patent/EP3596170A1/fr
Priority to CN201880017446.1A priority patent/CN110402273A/zh
Publication of WO2018167268A1 publication Critical patent/WO2018167268A1/fr

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/0015—Pigments exhibiting interference colours, e.g. transparent platelets of appropriate thinness or flaky substrates, e.g. mica, bearing appropriate thin transparent coatings
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/0015—Pigments exhibiting interference colours, e.g. transparent platelets of appropriate thinness or flaky substrates, e.g. mica, bearing appropriate thin transparent coatings
    • C09C1/0024—Pigments exhibiting interference colours, e.g. transparent platelets of appropriate thinness or flaky substrates, e.g. mica, bearing appropriate thin transparent coatings comprising a stack of coating layers with alternating high and low refractive indices, wherein the first coating layer on the core surface has the high refractive index
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/02—Printing inks
    • C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
    • C09D11/037—Printing inks characterised by features other than the chemical nature of the binder characterised by the pigment
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K9/00—Use of pretreated ingredients
    • C08K9/02—Ingredients treated with inorganic substances
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2200/00—Compositional and structural details of pigments exhibiting interference colours
    • C09C2200/10—Interference pigments characterized by the core material
    • C09C2200/1004—Interference pigments characterized by the core material the core comprising at least one inorganic oxide, e.g. Al2O3, TiO2 or SiO2
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2200/00—Compositional and structural details of pigments exhibiting interference colours
    • C09C2200/10—Interference pigments characterized by the core material
    • C09C2200/102—Interference pigments characterized by the core material the core consisting of glass or silicate material like mica or clays, e.g. kaolin
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2200/00—Compositional and structural details of pigments exhibiting interference colours
    • C09C2200/30—Interference pigments characterised by the thickness of the core or layers thereon or by the total thickness of the final pigment particle
    • C09C2200/307—Thickness of an outermost protective layer
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2200/00—Compositional and structural details of pigments exhibiting interference colours
    • C09C2200/30—Interference pigments characterised by the thickness of the core or layers thereon or by the total thickness of the final pigment particle
    • C09C2200/308—Total thickness of the pigment particle
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2200/00—Compositional and structural details of pigments exhibiting interference colours
    • C09C2200/40—Interference pigments comprising an outermost surface coating
    • C09C2200/401—Inorganic protective coating
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2220/00—Methods of preparing the interference pigments
    • C09C2220/10—Wet methods, e.g. co-precipitation
    • C09C2220/106—Wet methods, e.g. co-precipitation comprising only a drying or calcination step of the finally coated pigment

Definitions

  • the disadvantage here is that the use is limited exclusively to special gold-colored pearlescent pigments based on mica, wherein the layer structure of the gold-colored pearlescent pigments is not disclosed.
  • the number and color selection of the pigments which can be used is thus very limited in CN 101462895A.
  • Suitable effect pigments are in particular pearlescent pigments,
  • Effect pigments with one or more transparent, semi-transparent and / or opaque layers containing metal oxides, metal oxide hydrates, metal suboxides, metals, metal fluorides, metal nitrides, metal oxynitrides or mixtures of these materials may be coated.
  • the metal oxide, metal oxide hydrates, metal suboxides, metals, metal fluorides, metal nitrides, metal oxynitrides or mixtures of these materials may be coated.
  • Paint binders such as e.g. Polyurethane-acrylate resins, acrylate-melamine resins, alkyd resins, polyester resins, polyurethanes, nitrocellulose, ketone resins, aldehyde resins and polyvinyl butyral, acrylic resins or epoxy resins and mixtures thereof are used as binders.
  • the slip slip may contain up to 15% by weight, preferably 0.1 to 5% by weight, of one or more viscosity modifiers.
  • Such modifiers are also known in the art and examples thereof include ethylcellulose, nitrocellulose, hydroxypropylcellulose, hydroxypropylmethylcellulose, acrylic resins, poly (vinyl) butyral resins, carboxymethylcellulose, and ethylhydroxyethylcellulose.
  • the effect pigment from Example 6 is stable at temperatures> 1000 ° C.
  • the printed and dried tile is now fired in the kiln by means of a temperature profile.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Pigments, Carbon Blacks, Or Wood Stains (AREA)
  • Paints Or Removers (AREA)
  • Cosmetics (AREA)
  • Inks, Pencil-Leads, Or Crayons (AREA)

Abstract

La présente invention concerne des pigments à effet stables à la glaçure et à l'émaillage, dotés d'une couche de recouvrement en oxyde d'antimoine ou mélange d'oxyde d'antimoine, les pigments à effet présentant une stabilité améliorée, notamment à des températures supérieures à 1000 °C dans des glaçures, des émaux ou des matériaux céramiques ou vitreux.
PCT/EP2018/056662 2017-03-17 2018-03-16 Pigments à effets WO2018167268A1 (fr)

Priority Applications (3)

Application Number Priority Date Filing Date Title
JP2019551387A JP2020514511A (ja) 2017-03-17 2018-03-16 エフェクト顔料
EP18712176.9A EP3596170A1 (fr) 2017-03-17 2018-03-16 Pigments à effets
CN201880017446.1A CN110402273A (zh) 2017-03-17 2018-03-16 效应颜料

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102017002554.1 2017-03-17
DE102017002554.1A DE102017002554A1 (de) 2017-03-17 2017-03-17 Effektpigmente

Publications (1)

Publication Number Publication Date
WO2018167268A1 true WO2018167268A1 (fr) 2018-09-20

Family

ID=61691991

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2018/056662 WO2018167268A1 (fr) 2017-03-17 2018-03-16 Pigments à effets

Country Status (6)

Country Link
EP (1) EP3596170A1 (fr)
JP (1) JP2020514511A (fr)
CN (1) CN110402273A (fr)
DE (1) DE102017002554A1 (fr)
TW (1) TW201902847A (fr)
WO (1) WO2018167268A1 (fr)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110724396A (zh) * 2019-09-24 2020-01-24 河北欧克新型材料股份有限公司 耐温黑色珠光颜料及其制备方法
WO2021013513A1 (fr) * 2019-07-19 2021-01-28 Henkel Ag & Co. Kgaa Pigments à effet colorés et leur fabrication
CN115304275A (zh) * 2022-05-09 2022-11-08 承德石油高等专科学校 一种适于超临界水中应用的复合绝缘釉及其加工方法

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113717549A (zh) * 2021-09-30 2021-11-30 福建坤彩材料科技股份有限公司 绿色珠光颜料及其制备方法与应用
WO2024017885A1 (fr) 2022-07-19 2024-01-25 Sun Chemical Corporation Pigments à effets avec brillance

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DE1959998A1 (de) 1969-11-29 1971-07-08 Merck Patent Gmbh Perlglanzpigmente und Verfahren zu ihrer Herstellung
DE1952538A1 (de) 1969-10-18 1971-07-08 Bayer Ag Verfahren zur Verbesserung der Licht- und Temperaturbestaendigkeit von bleichromathaltigen Pigmenten
DE2106613A1 (de) 1970-02-13 1971-08-19 E I du Pont de Nemours and Co , Wilmington, Del (V St A) Perlmutterartige Glimmerpigment massen
DE2009566B1 (de) 1970-02-28 1971-11-11 Merck Patent Gmbh Verfahren zur Herstellung von Titandioxid- bzw. Titandioxidaquatüberzügen
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Publication number Priority date Publication date Assignee Title
DE1467468A1 (de) 1961-06-28 1968-12-12 Du Pont Glimmerschuppenpigment
GB974874A (en) * 1961-06-28 1964-11-11 Du Pont New pigment compositions
DE1952538A1 (de) 1969-10-18 1971-07-08 Bayer Ag Verfahren zur Verbesserung der Licht- und Temperaturbestaendigkeit von bleichromathaltigen Pigmenten
DE1959998A1 (de) 1969-11-29 1971-07-08 Merck Patent Gmbh Perlglanzpigmente und Verfahren zu ihrer Herstellung
DE2106613A1 (de) 1970-02-13 1971-08-19 E I du Pont de Nemours and Co , Wilmington, Del (V St A) Perlmutterartige Glimmerpigment massen
DE2009566B1 (de) 1970-02-28 1971-11-11 Merck Patent Gmbh Verfahren zur Herstellung von Titandioxid- bzw. Titandioxidaquatüberzügen
DE2214545A1 (de) 1971-03-26 1972-10-05 E.I. Du Pont De Nemours And Co., Wilmington, Del. (V.St.A.) Perlmuttpigmente und deren Herstellung
DE2215191A1 (de) 1971-03-30 1972-10-12 E I du Pont de Nemours and Co , Wilmington, Del (V St A) Verbesserte Pigmente
US4038099A (en) 1971-08-30 1977-07-26 The Mearl Corporation Rutile-coated mica nacreous pigments and process for the preparation thereof
DE2244298A1 (de) 1972-09-09 1974-03-28 Merck Patent Gmbh Perlglanzpigmente und verfahren zu ihrer herstellung
DE2313331A1 (de) 1973-03-17 1974-09-19 Merck Patent Gmbh Eisenhaltige glimmerschuppenpigmente
DE2429762A1 (de) 1974-06-21 1976-01-15 Merck Patent Gmbh Farbstoffhaltige glanzpigmente
DE2522572A1 (de) 1975-05-22 1976-12-09 Merck Patent Gmbh Rutilhaltige perlglanzpigmente
DE2522572C2 (de) 1975-05-22 1982-06-03 Merck Patent Gmbh, 6100 Darmstadt Rutilhaltige Perlglanzpigmente
EP0045851A1 (fr) 1980-08-08 1982-02-17 BASF Aktiengesellschaft Procédé pour la fabrication de pigments micacés en forme d'écailles recouvertes d'oxydes métalliques et leur utilisation
GB2096592A (en) 1981-03-19 1982-10-20 Takahashi Yuichiro Ground strengthening composition
US4353991A (en) 1981-04-13 1982-10-12 Ferro Corporation Glass composition and method of manufacture and article produced therefrom
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* Cited by examiner, † Cited by third party
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WO2021013513A1 (fr) * 2019-07-19 2021-01-28 Henkel Ag & Co. Kgaa Pigments à effet colorés et leur fabrication
CN114207051A (zh) * 2019-07-19 2022-03-18 汉高股份有限及两合公司 有色效应颜料及其制备
CN110724396A (zh) * 2019-09-24 2020-01-24 河北欧克新型材料股份有限公司 耐温黑色珠光颜料及其制备方法
CN110724396B (zh) * 2019-09-24 2021-10-01 河北欧克新型材料股份有限公司 耐温黑色珠光颜料及其制备方法
CN115304275A (zh) * 2022-05-09 2022-11-08 承德石油高等专科学校 一种适于超临界水中应用的复合绝缘釉及其加工方法
CN115304275B (zh) * 2022-05-09 2023-11-17 承德石油高等专科学校 一种适于超临界水中应用的复合绝缘釉及其加工方法

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EP3596170A1 (fr) 2020-01-22
JP2020514511A (ja) 2020-05-21

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