NO326665B1 - Fremgangsmate for fremstilling av vannholdige hydroksylaminopplosninger som er i det vesentlige frie for metallioner - Google Patents

Fremgangsmate for fremstilling av vannholdige hydroksylaminopplosninger som er i det vesentlige frie for metallioner Download PDF

Info

Publication number: NO326665B1
Authority: NO; Norway
Prior art keywords: hydroxylamine solution; metal ions; treatment; cation exchanger; hydroxylamine
Prior art date: 1998-02-17

Application number

NO20004076A

Other languages

English (en)

Norwegian (no)

Other versions

NO20004076D0 (no

NO20004076L (no

Inventor

Hans-Michael Schneider

Otto Watzenberger

Original Assignee

Basf Ag

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1998-02-17

Filing date

2000-08-15

Publication date

2009-01-26

2000-08-15 Application filed by Basf Ag filed Critical Basf Ag

2000-08-15 Publication of NO20004076D0 publication Critical patent/NO20004076D0/no

2000-08-15 Publication of NO20004076L publication Critical patent/NO20004076L/no

2009-01-26 Publication of NO326665B1 publication Critical patent/NO326665B1/no

Links

AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical compound ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 title claims abstract description 61
229910021645 metal ion Inorganic materials 0.000 title claims abstract description 24
238000000034 method Methods 0.000 title claims abstract description 16
238000002360 preparation method Methods 0.000 title abstract description 6
150000001768 cations Chemical class 0.000 claims abstract description 40
230000002378 acidificating effect Effects 0.000 claims abstract description 11
239000000243 solution Substances 0.000 claims description 62
150000001450 anions Chemical class 0.000 claims description 18
239000002253 acid Substances 0.000 claims description 13
239000003381 stabilizer Substances 0.000 claims description 12
125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 8
239000007864 aqueous solution Substances 0.000 claims description 5
150000002500 ions Chemical class 0.000 description 12
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 6
238000004821 distillation Methods 0.000 description 5
239000011734 sodium Substances 0.000 description 5
229910001413 alkali metal ion Inorganic materials 0.000 description 4
-1 ammonium ions Chemical class 0.000 description 4
229920001429 chelating resin Polymers 0.000 description 4
238000000354 decomposition reaction Methods 0.000 description 4
238000004519 manufacturing process Methods 0.000 description 4
229920001467 poly(styrenesulfonates) Polymers 0.000 description 4
238000000746 purification Methods 0.000 description 4
229910001415 sodium ion Inorganic materials 0.000 description 4
239000000126 substance Substances 0.000 description 4
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 3
KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
229920002125 Sokalan® Polymers 0.000 description 3
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 3
239000008139 complexing agent Substances 0.000 description 3
239000003456 ion exchange resin Substances 0.000 description 3
229920003303 ion-exchange polymer Polymers 0.000 description 3
NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 2
238000005349 anion exchange Methods 0.000 description 2
125000000129 anionic group Chemical group 0.000 description 2
239000002585 base Substances 0.000 description 2
238000005341 cation exchange Methods 0.000 description 2
238000004140 cleaning Methods 0.000 description 2
NBZBKCUXIYYUSX-UHFFFAOYSA-N iminodiacetic acid Chemical group OC(=O)CNCC(O)=O NBZBKCUXIYYUSX-UHFFFAOYSA-N 0.000 description 2
239000012535 impurity Substances 0.000 description 2
238000005342 ion exchange Methods 0.000 description 2
PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
229920005989 resin Polymers 0.000 description 2
239000011347 resin Substances 0.000 description 2
229910021653 sulphate ion Inorganic materials 0.000 description 2
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 1
OKIZCWYLBDKLSU-UHFFFAOYSA-M N,N,N-Trimethylmethanaminium chloride Chemical compound [Cl-].C[N+](C)(C)C OKIZCWYLBDKLSU-UHFFFAOYSA-M 0.000 description 1
VEQPNABPJHWNSG-UHFFFAOYSA-N Nickel(2+) Chemical compound [Ni+2] VEQPNABPJHWNSG-UHFFFAOYSA-N 0.000 description 1
PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
150000007513 acids Chemical class 0.000 description 1
229910052783 alkali metal Inorganic materials 0.000 description 1
BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 1
229910052921 ammonium sulfate Inorganic materials 0.000 description 1
239000001166 ammonium sulphate Substances 0.000 description 1
235000011130 ammonium sulphate Nutrition 0.000 description 1
239000011575 calcium Substances 0.000 description 1
229910001424 calcium ion Inorganic materials 0.000 description 1
239000003054 catalyst Substances 0.000 description 1
238000003889 chemical engineering Methods 0.000 description 1
238000006243 chemical reaction Methods 0.000 description 1
239000003795 chemical substances by application Substances 0.000 description 1
230000000052 comparative effect Effects 0.000 description 1
230000000536 complexating effect Effects 0.000 description 1
239000000356 contaminant Substances 0.000 description 1
238000011437 continuous method Methods 0.000 description 1
230000007423 decrease Effects 0.000 description 1
230000006735 deficit Effects 0.000 description 1
238000001514 detection method Methods 0.000 description 1
230000000694 effects Effects 0.000 description 1
239000004744 fabric Substances 0.000 description 1
229910001385 heavy metal Inorganic materials 0.000 description 1
150000002443 hydroxylamines Chemical group 0.000 description 1
238000002955 isolation Methods 0.000 description 1
239000007788 liquid Substances 0.000 description 1
229910052751 metal Inorganic materials 0.000 description 1
239000002184 metal Substances 0.000 description 1
150000002736 metal compounds Chemical class 0.000 description 1
238000002156 mixing Methods 0.000 description 1
238000012544 monitoring process Methods 0.000 description 1
229910001453 nickel ion Inorganic materials 0.000 description 1
230000000452 restraining effect Effects 0.000 description 1
238000000926 separation method Methods 0.000 description 1
229910052938 sodium sulfate Inorganic materials 0.000 description 1
235000011152 sodium sulphate Nutrition 0.000 description 1
238000003756 stirring Methods 0.000 description 1
239000012498 ultrapure water Substances 0.000 description 1
238000010626 work up procedure Methods 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
- C01B21/1481—Purification
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J45/00—Ion-exchange in which a complex or a chelate is formed; Use of material as complex or chelate forming ion-exchangers; Treatment of material for improving the complex or chelate forming ion-exchange properties

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Inorganic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

NO20004076A 1998-02-17 2000-08-15 Fremgangsmate for fremstilling av vannholdige hydroksylaminopplosninger som er i det vesentlige frie for metallioner NO326665B1 (no)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
DE19806578A DE19806578A1 (de)	1998-02-17	1998-02-17	Verfahren zur Herstellung wäßriger, im wesentlichen metallionenfreier Hydroxylaminlösungen
PCT/EP1999/000993 WO1999042434A2 (fr)	1998-02-17	1999-02-16	Procede pour produire des solutions aqueuses d'hydroxylamine, pratiquement exemptes d'ion metallique

Publications (3)

Publication Number	Publication Date
NO20004076D0 NO20004076D0 (no)	2000-08-15
NO20004076L NO20004076L (no)	2000-08-15
NO326665B1 true NO326665B1 (no)	2009-01-26

Family

ID=7858040

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NO20004076A NO326665B1 (no)	1998-02-17	2000-08-15	Fremgangsmate for fremstilling av vannholdige hydroksylaminopplosninger som er i det vesentlige frie for metallioner

Country Status (16)

Country	Link
US (1)	US6524545B1 (fr)
EP (1)	EP1056713B1 (fr)
JP (1)	JP4285904B2 (fr)
KR (1)	KR100564191B1 (fr)
CN (1)	CN1269727C (fr)
AT (1)	ATE243674T1 (fr)
AU (1)	AU756907B2 (fr)
CA (1)	CA2321032C (fr)
DE (2)	DE19806578A1 (fr)
ES (1)	ES2203081T3 (fr)
IL (1)	IL137647A (fr)
MY (1)	MY120796A (fr)
NO (1)	NO326665B1 (fr)
TR (1)	TR200002384T2 (fr)
TW (1)	TW460407B (fr)
WO (1)	WO1999042434A2 (fr)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE19936594A1 (de)	1999-08-04	2001-02-08	Basf Ag	Verfahren zur Herstellung von hochreinen stabilisierten Hydroxylaminlösungen
JP4582602B2 (ja) *	2000-03-24	2010-11-17	ビーエーエスエフソシエタス・ヨーロピア	ヒドロキシルアミン水溶液およびその製造方法
US6432752B1 (en) *	2000-08-17	2002-08-13	Micron Technology, Inc.	Stereolithographic methods for fabricating hermetic semiconductor device packages and semiconductor devices including stereolithographically fabricated hermetic packages
WO2005016817A2 (fr)	2003-08-13	2005-02-24	Showa Denko K. K.	Procede de production d'hydroxylamine
JP4578885B2 (ja) *	2003-08-13	2010-11-10	昭和電工株式会社	ヒドロキシルアミンの製造方法
US7396519B2 (en) *	2004-01-26	2008-07-08	San Fu Chemical Company, Ltd.	Preparation of a high purity and high concentration hydroxylamine free base
JP4578999B2 (ja) *	2005-02-10	2010-11-10	昭和電工株式会社	ヒドロキシルアミンの製造方法
JP4578998B2 (ja) *	2005-02-10	2010-11-10	昭和電工株式会社	ヒドロキシルアミンの製造方法
JP2023528572A (ja) *	2020-04-08	2023-07-05	ダウグローバルテクノロジーズエルエルシー	有機アミン精製方法

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
NL6914306A (fr) *	1969-09-20	1971-03-23
JPS4914640B1 (fr) *	1970-08-25	1974-04-09
JPS5534764B2 (fr)	1972-06-02	1980-09-09
FR2243904B1 (fr) *	1973-09-14	1976-06-18	Commissariat Energie Atomique
US4147623A (en) *	1977-10-28	1979-04-03	Allied Chemical Corporation	Hydroxylamine purification via ion exclusion
US4202765A (en) *	1977-10-28	1980-05-13	Allied Chemical Corporation	Hydroxylamine purification via cation exchange
DE3607998A1 (de) *	1986-03-11	1987-09-17	Basf Ag	Verfahren zur aufarbeitung von hydroxylamin oder dessen salze enthaltenden abwaessern
DE3608495A1 (de)	1986-03-14	1987-09-17	Basf Ag	Verfahren zur herstellung von waessrigen loesungen von hydroxylamin
US5266290A (en) *	1992-07-10	1993-11-30	Thiokol Corporation	Process for making high purity hydroxylammonium nitrate
HRP960601B1 (en) *	1995-12-20	2001-12-31	Basf Ag	Process for separating medium boiling substances from a mixture of low, medium and high boiling substances
US5788946A (en)	1997-07-16	1998-08-04	Ashland Inc.	Purification of hydroxylamine
US5872295A (en) *	1998-02-13	1999-02-16	Concept Sciences, Inc.	Purification of hydroxylamine

1998
- 1998-02-17 DE DE19806578A patent/DE19806578A1/de not_active Withdrawn
1999
- 1999-02-12 TW TW088102275A patent/TW460407B/zh not_active IP Right Cessation
- 1999-02-13 MY MYPI99000533A patent/MY120796A/en unknown
- 1999-02-16 TR TR2000/02384T patent/TR200002384T2/xx unknown
- 1999-02-16 US US09/622,170 patent/US6524545B1/en not_active Expired - Lifetime
- 1999-02-16 KR KR1020007008924A patent/KR100564191B1/ko active IP Right Grant
- 1999-02-16 ES ES99908908T patent/ES2203081T3/es not_active Expired - Lifetime
- 1999-02-16 AU AU28343/99A patent/AU756907B2/en not_active Ceased
- 1999-02-16 WO PCT/EP1999/000993 patent/WO1999042434A2/fr active IP Right Grant
- 1999-02-16 CA CA002321032A patent/CA2321032C/fr not_active Expired - Fee Related
- 1999-02-16 EP EP99908908A patent/EP1056713B1/fr not_active Expired - Lifetime
- 1999-02-16 CN CNB998050792A patent/CN1269727C/zh not_active Expired - Lifetime
- 1999-02-16 AT AT99908908T patent/ATE243674T1/de active
- 1999-02-16 IL IL13764799A patent/IL137647A/en not_active IP Right Cessation
- 1999-02-16 JP JP2000532387A patent/JP4285904B2/ja not_active Expired - Lifetime
- 1999-02-16 DE DE59906097T patent/DE59906097D1/de not_active Expired - Lifetime
2000
- 2000-08-15 NO NO20004076A patent/NO326665B1/no not_active IP Right Cessation

Also Published As

Publication number	Publication date
CA2321032C (fr)	2008-05-06
WO1999042434A2 (fr)	1999-08-26
CN1269727C (zh)	2006-08-16
NO20004076D0 (no)	2000-08-15
MY120796A (en)	2005-11-30
JP4285904B2 (ja)	2009-06-24
WO1999042434A3 (fr)	1999-10-21
KR20010078694A (ko)	2001-08-21
JP2002503633A (ja)	2002-02-05
ES2203081T3 (es)	2004-04-01
KR100564191B1 (ko)	2006-03-27
CN1297422A (zh)	2001-05-30
TW460407B (en)	2001-10-21
DE19806578A1 (de)	1999-08-19
NO20004076L (no)	2000-08-15
ATE243674T1 (de)	2003-07-15
AU2834399A (en)	1999-09-06
EP1056713B1 (fr)	2003-06-25
TR200002384T2 (tr)	2000-12-21
US6524545B1 (en)	2003-02-25
CA2321032A1 (fr)	1999-08-26
IL137647A (en)	2004-08-31
DE59906097D1 (de)	2003-07-31
IL137647A0 (en)	2001-10-31
AU756907B2 (en)	2003-01-23
EP1056713A2 (fr)	2000-12-06

Legal Events

Date	Code	Title	Description
2017-09-25	MM1K	Lapsed by not paying the annual fees

Publication	Publication Date	Title
NO326665B1 (no)	2009-01-26	Fremgangsmate for fremstilling av vannholdige hydroksylaminopplosninger som er i det vesentlige frie for metallioner
JP4948727B2 (ja)	2012-06-06	高い安定状態のヒドロキシルアミン溶液の製造方法
US5788946A (en)	1998-08-04	Purification of hydroxylamine
US6001324A (en)	1999-12-14	Process for the preparation of an ultra pure hydrogen peroxide solution by ion exchange in the presence of acetate ions
US3297404A (en)	1967-01-10	Purification of hydrogen peroxide
US3067007A (en)	1962-12-04	Separation of strong polybasic acids from their salts
US5318762A (en)	1994-06-07	Process for treating aqueous solutions of hydroxylamine salts containing excess acid
US5872295A (en)	1999-02-16	Purification of hydroxylamine
MXPA00007956A (en)	2001-07-09	Method for producing aqueous hydroxylamine solutions which are substantially free of metal ions
JPS6137261B2 (fr)	1986-08-22
US7399885B2 (en)	2008-07-15	Method for preparing hydroxylamine
JP2002119872A (ja)	2002-04-23	陰イオン交換樹脂
US5976487A (en)	1999-11-02	Process for purifying an aqueous solution of hydrogen peroxide
US2792415A (en)	1957-05-14	Purification of acrylonitrile
EP0122249B1 (fr)	1986-05-21	Récupération du vanadium et du cuivre de la production de l'acide adipique
JPS62139890A (ja)	1987-06-23	高純度水酸化第四アンモニウム水溶液の製造方法