KR870010105A - 경화 실리콘 고무분말의 제조방법 - Google Patents

경화 실리콘 고무분말의 제조방법 Download PDF

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KR870010105A
KR870010105A KR870003648A KR870003648A KR870010105A KR 870010105 A KR870010105 A KR 870010105A KR 870003648 A KR870003648 A KR 870003648A KR 870003648 A KR870003648 A KR 870003648A KR 870010105 A KR870010105 A KR 870010105A
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water
silicone rubber
temperature
per molecule
surfactant
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KR870003648A
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KR940008995B1 (ko
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고지 시미즈
미쯔오 하마다
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존 윌리암 처치필드
도레이 실리콘 캄파니, 리미티드
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/12—Powdering or granulating
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/12—Powdering or granulating
    • C08J3/16—Powdering or granulating by coagulating dispersions
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/24—Crosslinking, e.g. vulcanising, of macromolecules
    • C08J3/26—Crosslinking, e.g. vulcanising, of macromolecules of latex
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2383/00—Characterised by the use of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen, or carbon only; Derivatives of such polymers
    • C08J2383/04—Polysiloxanes

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

내용 없음

Description

경화 실리콘 고무분말의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (5)

1) 물과 계면활성제를 포함하는 혼합물 중에 경화성 액상 실리콘 고무 조성물을 유화시키고, 이때 상기 혼합물은 0 내지 25℃의 온도로 유지시키며, 2) 형성된 에멀젼을 25℃ 이상의 온도로 유지시킨 물 중에 분산시켜 액상 실리콘 고무 조성들을 분말 형태로 경화시키고, 3) 형성된 경화 분말을 분리시킴을 포함하는 극미소입자 형태인 경화 실리콘 고무 분말을 제조하는 방법.
제 1항에 있어서, 상기 조성물을 (1) 분자당 2개 이상의 저급 알케닐 라디칼을 함유하는 오가노폴리실옥산과 분자당 2개 이상의 실리콘-결합 수소원자를 함유하는 오가노하이드로겐 폴리실옥산과의 백금-촉매화 부가반응, 또는 (2) 유기 퍼옥사이드의 존재하에 수행하는 분자당 2개 이상의 비닐라디칼을 함유하는 오가노폴리실옥산의 유리라디칼-개시 중합반응에 의해 경화시키는 방법.
제 2항에 있어서, 상기 조성물을 상기 백금-촉매화부가 반응에 의해 경화시키고, 상기 오가노하이드로겐 폴리실옥산 분자당 실리콘-결합 수소원자 수와 상기 오가노플리실옥산 분자당 실리콘-결합 저급 알케닐 라디칼 수와의 합이 5 이상이며, 상기 오가노폴리실옥산이 디메틸비닐실옥시-말단디메틸폴리실옥산이고 상기 오가노하이드로겐폴리실옥산이 메틸하이드로겐폴리실옥산인 방법.
제 1항에 있어서, 경화성 액상 실리콘 고무 조성물을 물과 계면활성제 이 혼합물에 첨가하기전에 -30내지 0℃의 온도로 유지시키고 물과 계면활성제의 혼합물의 온도가 5 내지 10℃인 방법.
제 1항에 있어서, 상기 계면활성제가 비이온 형태이고, 에멀젼이 분산되는 물의 용적이 상기 에멀젼의 용적의 2배 이상이며, 에멀젼이 분산되는 물의 온도가 40 내지 80℃인 방법.
※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019870003648A 1986-04-17 1987-04-16 경화 실리콘 고무 분말의 제조방법 KR940008995B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP86-89063 1986-04-17
JP61089063A JPS62243621A (ja) 1986-04-17 1986-04-17 シリコ−ンゴム粒状物の製造方法
JP89063 1986-04-17

Publications (2)

Publication Number Publication Date
KR870010105A true KR870010105A (ko) 1987-11-30
KR940008995B1 KR940008995B1 (ko) 1994-09-28

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KR1019870003648A KR940008995B1 (ko) 1986-04-17 1987-04-16 경화 실리콘 고무 분말의 제조방법

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Country Link
US (1) US4742142A (ko)
EP (1) EP0242219B1 (ko)
JP (1) JPS62243621A (ko)
KR (1) KR940008995B1 (ko)
AU (1) AU588995B2 (ko)
BR (1) BR8701861A (ko)
CA (1) CA1282529C (ko)
DE (1) DE3782266T2 (ko)
ES (1) ES2003260A6 (ko)

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BR8701861A (pt) 1988-01-26
ES2003260A6 (es) 1988-10-16
EP0242219B1 (en) 1992-10-21
EP0242219A3 (en) 1988-09-07
DE3782266D1 (de) 1992-11-26
JPS62243621A (ja) 1987-10-24
CA1282529C (en) 1991-04-02
KR940008995B1 (ko) 1994-09-28
DE3782266T2 (de) 1993-05-06
US4742142B1 (ko) 1991-02-26
US4742142A (en) 1988-05-03
EP0242219A2 (en) 1987-10-21
JPH0455611B2 (ko) 1992-09-03
AU7174187A (en) 1987-10-22

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