KR20210012999A - 신규 산화 티탄 분체 및 이것을 배합하는 화장료 - Google Patents

신규 산화 티탄 분체 및 이것을 배합하는 화장료 Download PDF

Info

Publication number: KR20210012999A
Authority: KR; South Korea
Prior art keywords: titanium oxide; oxide powder; coated titanium; powder; skin
Prior art date: 2018-05-23

Application number

KR1020207021634A

Other languages

English (en)

Korean (ko)

Inventor

유리코 토미타

유지 마스부치

미키 이데

료 사사키

료스케 칸난

Original Assignee

가부시키가이샤 코세

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2018-05-23

Filing date

2019-05-17

Publication date

2021-02-03

2019-05-17 Application filed by 가부시키가이샤 코세 filed Critical 가부시키가이샤 코세

2021-02-03 Publication of KR20210012999A publication Critical patent/KR20210012999A/ko

Links

GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 title claims abstract description 260
239000000843 powder Substances 0.000 title claims abstract description 235
OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 title claims abstract description 227
239000002537 cosmetic Substances 0.000 title claims description 45
238000002834 transmittance Methods 0.000 claims abstract description 86
239000002245 particle Substances 0.000 claims abstract description 84
230000000694 effects Effects 0.000 claims abstract description 70
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract description 48
XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims abstract description 33
230000005540 biological transmission Effects 0.000 claims abstract description 32
229910052710 silicon Inorganic materials 0.000 claims abstract description 27
239000010703 silicon Substances 0.000 claims abstract description 27
238000000034 method Methods 0.000 claims abstract description 26
229910052782 aluminium Inorganic materials 0.000 claims abstract description 24
229910052742 iron Inorganic materials 0.000 claims abstract description 24
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims abstract description 23
230000003595 spectral effect Effects 0.000 claims abstract description 12
238000001000 micrograph Methods 0.000 claims abstract description 11
238000000576 coating method Methods 0.000 claims description 59
239000011248 coating agent Substances 0.000 claims description 57
239000004205 dimethyl polysiloxane Substances 0.000 claims description 33
235000013870 dimethyl polysiloxane Nutrition 0.000 claims description 33
229920000435 poly(dimethylsiloxane) Polymers 0.000 claims description 33
239000011247 coating layer Substances 0.000 claims description 27
XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 26
238000004381 surface treatment Methods 0.000 claims description 24
229940008099 dimethicone Drugs 0.000 claims description 21
239000010410 layer Substances 0.000 claims description 18
238000000790 scattering method Methods 0.000 claims description 12
239000006185 dispersion Substances 0.000 claims description 11
238000003703 image analysis method Methods 0.000 claims description 9
238000002360 preparation method Methods 0.000 claims description 9
239000011521 glass Substances 0.000 claims description 8
238000001228 spectrum Methods 0.000 claims description 8
229920001577 copolymer Polymers 0.000 claims description 7
239000002904 solvent Substances 0.000 claims description 7
238000000411 transmission spectrum Methods 0.000 claims description 7
NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 6
230000001678 irradiating effect Effects 0.000 claims description 5
238000010191 image analysis Methods 0.000 abstract description 5
238000011156 evaluation Methods 0.000 description 72
239000000047 product Substances 0.000 description 49
239000010408 film Substances 0.000 description 46
230000003287 optical effect Effects 0.000 description 34
UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 33
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 32
-1 aluminum compound Chemical class 0.000 description 28
239000004615 ingredient Substances 0.000 description 20
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 20
238000004519 manufacturing process Methods 0.000 description 18
239000007787 solid Substances 0.000 description 17
XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 16
229920001296 polysiloxane Polymers 0.000 description 16
239000000377 silicon dioxide Substances 0.000 description 15
239000000454 talc Substances 0.000 description 15
229910052623 talc Inorganic materials 0.000 description 15
239000000203 mixture Substances 0.000 description 14
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 13
230000000052 comparative effect Effects 0.000 description 13
238000009826 distribution Methods 0.000 description 12
229910000358 iron sulfate Inorganic materials 0.000 description 12
BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 description 12
239000003921 oil Substances 0.000 description 11
229910052751 metal Inorganic materials 0.000 description 10
239000002184 metal Substances 0.000 description 10
WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 9
229920006037 cross link polymer Polymers 0.000 description 9
238000010586 diagram Methods 0.000 description 9
PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 9
239000010931 gold Substances 0.000 description 9
229910052737 gold Inorganic materials 0.000 description 9
238000000691 measurement method Methods 0.000 description 9
239000012188 paraffin wax Substances 0.000 description 9
IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical class CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 description 8
XMSXQFUHVRWGNA-UHFFFAOYSA-N Decamethylcyclopentasiloxane Chemical compound C[Si]1(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O1 XMSXQFUHVRWGNA-UHFFFAOYSA-N 0.000 description 8
239000004698 Polyethylene Substances 0.000 description 8
239000002253 acid Substances 0.000 description 8
239000010445 mica Substances 0.000 description 8
229910052618 mica group Inorganic materials 0.000 description 8
229920000573 polyethylene Polymers 0.000 description 8
239000011787 zinc oxide Substances 0.000 description 8
MSRJTTSHWYDFIU-UHFFFAOYSA-N octyltriethoxysilane Chemical compound CCCCCCCC[Si](OCC)(OCC)OCC MSRJTTSHWYDFIU-UHFFFAOYSA-N 0.000 description 7
239000000049 pigment Substances 0.000 description 7
PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 6
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 6
239000007864 aqueous solution Substances 0.000 description 6
239000003205 fragrance Substances 0.000 description 6
WTFXARWRTYJXII-UHFFFAOYSA-N iron(2+);iron(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[O-2].[Fe+2].[Fe+3].[Fe+3] WTFXARWRTYJXII-UHFFFAOYSA-N 0.000 description 6
SZVJSHCCFOBDDC-UHFFFAOYSA-N iron(II,III) oxide Inorganic materials O=[Fe]O[Fe]O[Fe]=O SZVJSHCCFOBDDC-UHFFFAOYSA-N 0.000 description 6
239000007788 liquid Substances 0.000 description 6
229960003493 octyltriethoxysilane Drugs 0.000 description 6
239000008213 purified water Substances 0.000 description 6
239000004375 Dextrin Substances 0.000 description 5
229920001353 Dextrin Polymers 0.000 description 5
RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 5
235000019425 dextrin Nutrition 0.000 description 5
238000001035 drying Methods 0.000 description 5
238000010304 firing Methods 0.000 description 5
239000003755 preservative agent Substances 0.000 description 5
239000002994 raw material Substances 0.000 description 5
229960004029 silicic acid Drugs 0.000 description 5
239000004408 titanium dioxide Substances 0.000 description 5
239000001993 wax Substances 0.000 description 5
PDQICKRFOKDJCH-INIZCTEOSA-N (2s)-6-amino-2-(dodecanoylamino)hexanoic acid Chemical compound CCCCCCCCCCCC(=O)N[C@H](C(O)=O)CCCCN PDQICKRFOKDJCH-INIZCTEOSA-N 0.000 description 4
PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 4
235000021355 Stearic acid Nutrition 0.000 description 4
238000004458 analytical method Methods 0.000 description 4
235000014113 dietary fatty acids Nutrition 0.000 description 4
239000000194 fatty acid Substances 0.000 description 4
229930195729 fatty acid Natural products 0.000 description 4
IPCSVZSSVZVIGE-UHFFFAOYSA-M hexadecanoate Chemical compound CCCCCCCCCCCCCCCC([O-])=O IPCSVZSSVZVIGE-UHFFFAOYSA-M 0.000 description 4
238000009616 inductively coupled plasma Methods 0.000 description 4
238000002156 mixing Methods 0.000 description 4
QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 4
OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 4
230000009467 reduction Effects 0.000 description 4
239000002002 slurry Substances 0.000 description 4
239000011734 sodium Substances 0.000 description 4
235000013599 spices Nutrition 0.000 description 4
239000008117 stearic acid Substances 0.000 description 4
239000000126 substance Substances 0.000 description 4
125000003944 tolyl group Chemical group 0.000 description 4
230000000007 visual effect Effects 0.000 description 4
229940058015 1,3-butylene glycol Drugs 0.000 description 3
QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 description 3
229910052582 BN Inorganic materials 0.000 description 3
PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 description 3
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
YBGZDTIWKVFICR-JLHYYAGUSA-N Octyl 4-methoxycinnamic acid Chemical compound CCCCC(CC)COC(=O)\C=C\C1=CC=C(OC)C=C1 YBGZDTIWKVFICR-JLHYYAGUSA-N 0.000 description 3
DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
235000019437 butane-1,3-diol Nutrition 0.000 description 3
239000007822 coupling agent Substances 0.000 description 3
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239000013078 crystal Substances 0.000 description 3
239000000839 emulsion Substances 0.000 description 3
238000005516 engineering process Methods 0.000 description 3
UCNNJGDEJXIUCC-UHFFFAOYSA-L hydroxy(oxo)iron;iron Chemical compound [Fe].O[Fe]=O.O[Fe]=O UCNNJGDEJXIUCC-UHFFFAOYSA-L 0.000 description 3
150000002506 iron compounds Chemical class 0.000 description 3
235000014413 iron hydroxide Nutrition 0.000 description 3
RUTXIHLAWFEWGM-UHFFFAOYSA-H iron(3+) sulfate Chemical compound [Fe+3].[Fe+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O RUTXIHLAWFEWGM-UHFFFAOYSA-H 0.000 description 3
229910000360 iron(III) sulfate Inorganic materials 0.000 description 3
238000005259 measurement Methods 0.000 description 3
GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 description 3
229960001679 octinoxate Drugs 0.000 description 3
230000035699 permeability Effects 0.000 description 3
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BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 3
238000010298 pulverizing process Methods 0.000 description 3
235000012239 silicon dioxide Nutrition 0.000 description 3
239000000243 solution Substances 0.000 description 3
238000003756 stirring Methods 0.000 description 3
230000000475 sunscreen effect Effects 0.000 description 3
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125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 3
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238000005406 washing Methods 0.000 description 3
MXOAEAUPQDYUQM-QMMMGPOBSA-N (S)-chlorphenesin Chemical compound OC[C@H](O)COC1=CC=C(Cl)C=C1 MXOAEAUPQDYUQM-QMMMGPOBSA-N 0.000 description 2
VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 description 2
206010014970 Ephelides Diseases 0.000 description 2
241001553290 Euphorbia antisyphilitica Species 0.000 description 2
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208000003351 Melanosis Diseases 0.000 description 2
VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 description 2
RGMZNZABJYWAEC-UHFFFAOYSA-N Methyltris(trimethylsiloxy)silane Chemical compound C[Si](C)(C)O[Si](C)(O[Si](C)(C)C)O[Si](C)(C)C RGMZNZABJYWAEC-UHFFFAOYSA-N 0.000 description 2
TUNFSRHWOTWDNC-UHFFFAOYSA-N Myristic acid Natural products CCCCCCCCCCCCCC(O)=O TUNFSRHWOTWDNC-UHFFFAOYSA-N 0.000 description 2
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FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
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MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 2
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235000001014 amino acid Nutrition 0.000 description 2
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FDATWRLUYRHCJE-UHFFFAOYSA-N diethylamino hydroxybenzoyl hexyl benzoate Chemical compound CCCCCCOC(=O)C1=CC=CC=C1C(=O)C1=CC=C(N(CC)CC)C=C1O FDATWRLUYRHCJE-UHFFFAOYSA-N 0.000 description 2
229960001630 diethylamino hydroxybenzoyl hexyl benzoate Drugs 0.000 description 2
LRCFXGAMWKDGLA-UHFFFAOYSA-N dioxosilane;hydrate Chemical compound O.O=[Si]=O LRCFXGAMWKDGLA-UHFFFAOYSA-N 0.000 description 2
NOPFSRXAKWQILS-UHFFFAOYSA-N docosan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCCCCCO NOPFSRXAKWQILS-UHFFFAOYSA-N 0.000 description 2
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STVZJERGLQHEKB-UHFFFAOYSA-N ethylene glycol dimethacrylate Chemical compound CC(=C)C(=O)OCCOC(=O)C(C)=C STVZJERGLQHEKB-UHFFFAOYSA-N 0.000 description 2
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KWLMIXQRALPRBC-UHFFFAOYSA-L hectorite Chemical compound [Li+].[OH-].[OH-].[Na+].[Mg+2].O1[Si]2([O-])O[Si]1([O-])O[Si]([O-])(O1)O[Si]1([O-])O2 KWLMIXQRALPRBC-UHFFFAOYSA-L 0.000 description 2
229910000271 hectorite Inorganic materials 0.000 description 2
IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 2
NCNCGGDMXMBVIA-UHFFFAOYSA-L iron(ii) hydroxide Chemical compound [OH-].[OH-].[Fe+2] NCNCGGDMXMBVIA-UHFFFAOYSA-L 0.000 description 2
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PRAKJMSDJKAYCZ-UHFFFAOYSA-N squalane Chemical compound CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 description 2
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UUJLHYCIMQOUKC-UHFFFAOYSA-N trimethyl-[oxo(trimethylsilylperoxy)silyl]peroxysilane Chemical compound C[Si](C)(C)OO[Si](=O)OO[Si](C)(C)C UUJLHYCIMQOUKC-UHFFFAOYSA-N 0.000 description 2
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- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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KR1020207021634A 2018-05-23 2019-05-17 신규 산화 티탄 분체 및 이것을 배합하는 화장료 KR20210012999A (ko)

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JP2018099130		2018-05-23
JPJP-P-2018-099130		2018-05-23
PCT/JP2019/019621 WO2019225491A1 (ja)	2018-05-23	2019-05-17	新規酸化チタン粉体及びそれを配合する化粧料

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EP (1)	EP3798191B1 (zh)
JP (1)	JP7116790B2 (zh)
KR (1)	KR20210012999A (zh)
CN (1)	CN111683904B (zh)
TW (1)	TWI815892B (zh)
WO (1)	WO2019225491A1 (zh)

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KR102410953B1 (ko) *	2021-12-15	2022-06-22	한국콜마주식회사	다크닝 현상을 억제하고 우수한 지속력을 갖는 화장료 조성물

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WO2021200781A1 (ja) *	2020-03-30	2021-10-07	株式会社コーセー	粉末含有化粧料
CN113317997B (zh) *	2021-07-02	2023-04-11	广州集妍化妆品科技有限公司	一种抗黯沉组合物、抗黯沉化妆品及其制备方法
WO2024080367A1 (ja) *	2022-10-13	2024-04-18	住友大阪セメント株式会社	ポリシロキサン被覆金属酸化物粒子、分散液、組成物、化粧料、ポリシロキサン被覆金属酸化物粒子の製造方法
WO2024095598A1 (ja) *	2022-11-02	2024-05-10	日光ケミカルズ株式会社	油性分散体の製造方法およびこの油性分散体を配合した化粧料
CN115919664B (zh) *	2022-12-27	2023-11-28	广东普本纳米科技有限公司	超微二氧化钛及其制备方法

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- 2019-05-17 CN CN201980009731.3A patent/CN111683904B/zh active Active
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EP3798191A4 (en)	2022-05-04
TWI815892B (zh)	2023-09-21
EP3798191A1 (en)	2021-03-31
CN111683904B (zh)	2023-05-02
WO2019225491A1 (ja)	2019-11-28
JP7116790B2 (ja)	2022-08-10
CN111683904A (zh)	2020-09-18
TW202003389A (zh)	2020-01-16
EP3798191B1 (en)	2023-06-14
JPWO2019225491A1 (ja)	2021-05-13

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KR20210012999A - 신규 산화 티탄 분체 및 이것을 배합하는 화장료 - Google Patents

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