JPS63191899A - トリグリセリド油の脱ガム化方法 - Google Patents

トリグリセリド油の脱ガム化方法

Info

Publication number: JPS63191899A
Authority: JP; Japan
Prior art keywords: oil; acid; citric acid; triglyceride; phosphorus
Prior art date: 1986-11-13
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Pending

Application number

JP28760487A

Other languages

English (en)

Japanese (ja)

Inventor

タカシ　カジ

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

KIYAMUBURIAN ENG GURUUPU Ltd

KIYAMUBURIAN ENG GURUUPU Ltd T

Original Assignee

KIYAMUBURIAN ENG GURUUPU Ltd

KIYAMUBURIAN ENG GURUUPU Ltd T

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1986-11-13

Filing date

1987-11-13

Publication date

1988-08-09

Family has litigation

First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=25458645&utm_source=***_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=JPS63191899(A) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.

1987-11-13 Application filed by KIYAMUBURIAN ENG GURUUPU Ltd, KIYAMUBURIAN ENG GURUUPU Ltd T filed Critical KIYAMUBURIAN ENG GURUUPU Ltd

1988-08-09 Publication of JPS63191899A publication Critical patent/JPS63191899A/ja

Status Pending legal-status Critical Current

Links

UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 title claims description 24
239000003921 oil Substances 0.000 claims description 163
KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid group Chemical group C(CC(O)(C(=O)O)CC(=O)O)(=O)O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 99
238000000034 method Methods 0.000 claims description 83
OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 41
229910052698 phosphorus Inorganic materials 0.000 claims description 41
239000011574 phosphorus Substances 0.000 claims description 41
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 26
238000004061 bleaching Methods 0.000 claims description 24
239000002253 acid Substances 0.000 claims description 23
239000000203 mixture Substances 0.000 claims description 21
239000007864 aqueous solution Substances 0.000 claims description 17
239000010802 sludge Substances 0.000 claims description 16
239000004927 clay Substances 0.000 claims description 15
238000003756 stirring Methods 0.000 claims description 14
239000001993 wax Substances 0.000 claims description 14
150000001875 compounds Chemical class 0.000 claims description 10
150000008065 acid anhydrides Chemical class 0.000 claims description 9
238000005119 centrifugation Methods 0.000 claims description 9
239000007788 liquid Substances 0.000 claims description 9
150000007524 organic acids Chemical class 0.000 claims description 9
FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 claims description 4
239000002994 raw material Substances 0.000 claims description 4
238000000926 separation method Methods 0.000 claims description 4
235000013311 vegetables Nutrition 0.000 claims description 4
239000007844 bleaching agent Substances 0.000 claims description 3
235000013305 food Nutrition 0.000 claims description 2
239000002199 base oil Substances 0.000 claims 2
239000006193 liquid solution Substances 0.000 claims 1
235000019198 oils Nutrition 0.000 description 123
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 14
239000000047 product Substances 0.000 description 14
235000021588 free fatty acids Nutrition 0.000 description 13
150000003904 phospholipids Chemical class 0.000 description 12
239000000344 soap Substances 0.000 description 9
229910000147 aluminium phosphate Inorganic materials 0.000 description 7
238000012545 processing Methods 0.000 description 7
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
150000003626 triacylglycerols Chemical class 0.000 description 6
238000004332 deodorization Methods 0.000 description 5
238000006386 neutralization reaction Methods 0.000 description 5
238000004042 decolorization Methods 0.000 description 4
238000000605 extraction Methods 0.000 description 4
238000001914 filtration Methods 0.000 description 4
239000003549 soybean oil Substances 0.000 description 4
235000012424 soybean oil Nutrition 0.000 description 4
239000007921 spray Substances 0.000 description 4
WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 3
LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 3
QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 3
WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 description 3
ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 3
239000005642 Oleic acid Substances 0.000 description 3
MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
235000019484 Rapeseed oil Nutrition 0.000 description 3
238000007796 conventional method Methods 0.000 description 3
230000001877 deodorizing effect Effects 0.000 description 3
QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 3
238000004519 manufacturing process Methods 0.000 description 3
ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 3
239000002244 precipitate Substances 0.000 description 3
238000000638 solvent extraction Methods 0.000 description 3
235000014698 Brassica juncea var multisecta Nutrition 0.000 description 2
235000006008 Brassica napus var napus Nutrition 0.000 description 2
235000006618 Brassica rapa subsp oleifera Nutrition 0.000 description 2
244000188595 Brassica sinapistrum Species 0.000 description 2
235000004977 Brassica sinapistrum Nutrition 0.000 description 2
235000019486 Sunflower oil Nutrition 0.000 description 2
235000013252 Viburnum trilobum Nutrition 0.000 description 2
244000306586 Viburnum trilobum Species 0.000 description 2
238000001816 cooling Methods 0.000 description 2
235000014113 dietary fatty acids Nutrition 0.000 description 2
239000008157 edible vegetable oil Substances 0.000 description 2
230000000694 effects Effects 0.000 description 2
238000002474 experimental method Methods 0.000 description 2
229930195729 fatty acid Natural products 0.000 description 2
239000000194 fatty acid Substances 0.000 description 2
150000004665 fatty acids Chemical class 0.000 description 2
230000000977 initiatory effect Effects 0.000 description 2
JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 2
235000019645 odor Nutrition 0.000 description 2
150000003018 phosphorus compounds Chemical class 0.000 description 2
238000000746 purification Methods 0.000 description 2
235000011121 sodium hydroxide Nutrition 0.000 description 2
239000000126 substance Substances 0.000 description 2
239000002600 sunflower oil Substances 0.000 description 2
POXUQBFHDHCZAD-MHTLYPKNSA-N (2r)-2-[(4s)-2,2-dimethyl-1,3-dioxolan-4-yl]-3,4-dihydroxy-2h-furan-5-one Chemical compound O1C(C)(C)OC[C@H]1[C@@H]1C(O)=C(O)C(=O)O1 POXUQBFHDHCZAD-MHTLYPKNSA-N 0.000 description 1
241000196324 Embryophyta Species 0.000 description 1
241001465754 Metazoa Species 0.000 description 1
OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 1
150000007513 acids Chemical class 0.000 description 1
230000002411 adverse Effects 0.000 description 1
238000013459 approach Methods 0.000 description 1
235000019568 aromas Nutrition 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
238000006243 chemical reaction Methods 0.000 description 1
238000005352 clarification Methods 0.000 description 1
230000000052 comparative effect Effects 0.000 description 1
230000003750 conditioning effect Effects 0.000 description 1
239000000356 contaminant Substances 0.000 description 1
239000002285 corn oil Substances 0.000 description 1
235000005687 corn oil Nutrition 0.000 description 1
238000002425 crystallisation Methods 0.000 description 1
230000008025 crystallization Effects 0.000 description 1
230000007423 decrease Effects 0.000 description 1
239000000706 filtrate Substances 0.000 description 1
239000012467 final product Substances 0.000 description 1
238000009775 high-speed stirring Methods 0.000 description 1
238000005984 hydrogenation reaction Methods 0.000 description 1
239000012535 impurity Substances 0.000 description 1
238000009434 installation Methods 0.000 description 1
NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 1
239000004310 lactic acid Substances 0.000 description 1
235000014655 lactic acid Nutrition 0.000 description 1
VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 1
239000011976 maleic acid Substances 0.000 description 1
238000002156 mixing Methods 0.000 description 1
235000006408 oxalic acid Nutrition 0.000 description 1
125000002743 phosphorus functional group Chemical group 0.000 description 1
230000000704 physical effect Effects 0.000 description 1
238000003825 pressing Methods 0.000 description 1
238000007670 refining Methods 0.000 description 1
235000014102 seafood Nutrition 0.000 description 1
239000002002 slurry Substances 0.000 description 1
239000000243 solution Substances 0.000 description 1
239000002904 solvent Substances 0.000 description 1
241000894007 species Species 0.000 description 1
229910001220 stainless steel Inorganic materials 0.000 description 1
239000010935 stainless steel Substances 0.000 description 1
238000001256 steam distillation Methods 0.000 description 1
238000012360 testing method Methods 0.000 description 1
VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
238000003828 vacuum filtration Methods 0.000 description 1
230000000007 visual effect Effects 0.000 description 1
238000005406 washing Methods 0.000 description 1
239000002699 waste material Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/02—Refining fats or fatty oils by chemical reaction
- C11B3/04—Refining fats or fatty oils by chemical reaction with acids

Landscapes

Chemical & Material Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
Microbiology (AREA)
Engineering & Computer Science (AREA)
Oil, Petroleum & Natural Gas (AREA)
Wood Science & Technology (AREA)
Organic Chemistry (AREA)
General Chemical & Material Sciences (AREA)
Fats And Perfumes (AREA)

JP28760487A 1986-11-13 1987-11-13 トリグリセリド油の脱ガム化方法 Pending JPS63191899A (ja)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
US92988986A	1986-11-13	1986-11-13
US929889		1992-08-11

Publications (1)

Publication Number	Publication Date
JPS63191899A true JPS63191899A (ja)	1988-08-09

Family

ID=25458645

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP28760487A Pending JPS63191899A (ja)	1986-11-13	1987-11-13	トリグリセリド油の脱ガム化方法

Country Status (4)

Country	Link
EP (1)	EP0269277B1 (fr)
JP (1)	JPS63191899A (fr)
DE (1)	DE3771670D1 (fr)
DK (1)	DK579887A (fr)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPH041296A (ja) *	1990-04-19	1992-01-06	Nisshin Oil Mills Ltd:The	植物油の脱ロウ法
JPH0551593A (ja) *	1991-08-26	1993-03-02	Nisshin Oil Mills Ltd:The	食用油の製造法
JP2009536970A (ja) *	2006-02-28	2009-10-22	グレース・ゲーエムベーハー・ウント・コムパニー・カーゲー	バイオディーゼル燃料を製造するための吸着剤粒子を用いる物理的精製方法
JP2022515784A (ja) *	2018-12-28	2022-02-22	ネステオサケユキチュアユルキネン	脂質材料を処理するための方法
WO2022270596A1 (fr) *	2021-06-24	2022-12-29	不二製油グループ本社株式会社	Procédé de production d'huile et de matière grasse alimentaire

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US5286886A (en) *	1988-06-21	1994-02-15	Van Den Bergh Foods Co., Division Of Conopco, Inc.	Method of refining glyceride oils
GB8814732D0 (en) *	1988-06-21	1988-07-27	Unilever Plc	Method of refining clyceride oils
DE69127127T2 (de) *	1990-05-04	1998-01-08	Unilever Nv	Verfahren zur Raffination eines Glyceridols
HU208037B (en) *	1990-08-23	1993-07-28	Noevenyolajipari Mososzergyart	Process for diminishing nonhydratable slime- and vax-content of plant-oils
AU672858B2 (en) *	1992-12-03	1996-10-17	Unilever Plc	Process for the refining of edible oils
DE102006061603A1 (de) *	2006-12-27	2008-07-03	Alois Dotzer	Kraftstoff
FR2935709B1 (fr) *	2008-09-05	2011-06-03	Veolia Proprete	Procede de traitement de dechets gras
DE102008048009A1 (de)	2008-09-19	2010-03-25	Rmenergy Umweltverfahrenstechnik Gmbh	Vorrichtung zur dezentralen Aufbereitung nativer Öle und Fette zur Nutzung als Kraftstoff oder als Rohstoff für die Biodieselherstellung
DE102009049950A1 (de)	2009-10-19	2011-04-21	Lurgi Gmbh	Verfahren zur Aufarbeitung von leicht verseifbarem Rohöl pflanzlicher oder tierischer Herkunft, für die Weiterverarbeitung zu Biodiesel
DE102010048367A1 (de)	2010-10-13	2012-04-19	Süd-Chemie AG	Verfahren zur Entfernung von Phosphor-haltigen Verbindungen aus Triglycerid-haltigen Zusammensetzungen
DE102010055969A1 (de)	2010-12-23	2012-06-28	Süd-Chemie AG	Verfahren zur Aufreinigung von organischen Flüssigkeiten
CN103635564B (zh)	2011-04-14	2015-07-01	魄勒欧米茄公司	一种分离磷脂的方法
CA3026848A1 (fr)	2016-06-10	2017-12-14	Drei Lilien Pvg Gmbh & Co. Kg	Procede d'extraction aqueuse pour obtenir des substances mucilagineuses et induire une separation d'emulsion
CN109259237B (zh) *	2018-10-22	2021-11-09	辽渔南极磷虾科技发展有限公司	一种高epa/dha型南极磷虾油磷脂丸及其制备方法
CN109439430B (zh) *	2018-10-22	2021-10-08	辽渔南极磷虾科技发展有限公司	一种南极磷虾油的精炼方法
CN109198042B (zh) *	2018-10-22	2021-10-08	辽渔南极磷虾科技发展有限公司	一种高epa/dha型南极磷虾油磷脂口服液及其制备方法

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US3590059A (en) *	1969-09-11	1971-06-29	Salador Huileries Antonin Roux	Process for the purification of edible oils
GB1541017A (en) *	1975-03-10	1979-02-21	Unilever Ltd	Degumming process for triglyceride oils
CA1157883A (fr) *	1981-01-26	1983-11-29	United Oilseed Products Ltd.	Demucilagination des huiles vegetales brutes par procede chimique

1987
- 1987-10-29 DE DE8787309597T patent/DE3771670D1/de not_active Expired - Lifetime
- 1987-10-29 EP EP19870309597 patent/EP0269277B1/fr not_active Revoked
- 1987-11-04 DK DK579887A patent/DK579887A/da not_active Application Discontinuation
- 1987-11-13 JP JP28760487A patent/JPS63191899A/ja active Pending

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPH041296A (ja) *	1990-04-19	1992-01-06	Nisshin Oil Mills Ltd:The	植物油の脱ロウ法
JPH0551593A (ja) *	1991-08-26	1993-03-02	Nisshin Oil Mills Ltd:The	食用油の製造法
JP2009536970A (ja) *	2006-02-28	2009-10-22	グレース・ゲーエムベーハー・ウント・コムパニー・カーゲー	バイオディーゼル燃料を製造するための吸着剤粒子を用いる物理的精製方法
JP2022515784A (ja) *	2018-12-28	2022-02-22	ネステオサケユキチュアユルキネン	脂質材料を処理するための方法
WO2022270596A1 (fr) *	2021-06-24	2022-12-29	不二製油グループ本社株式会社	Procédé de production d'huile et de matière grasse alimentaire
JPWO2022270596A1 (fr) *	2021-06-24	2022-12-29

Also Published As

Publication number	Publication date
EP0269277B1 (fr)	1991-07-24
DE3771670D1 (de)	1991-08-29
EP0269277A2 (fr)	1988-06-01
EP0269277A3 (en)	1988-07-06
DK579887A (da)	1988-05-14
DK579887D0 (da)	1987-11-04

Publication	Publication Date	Title
JPS63191899A (ja)	1988-08-09	トリグリセリド油の脱ガム化方法
US5239096A (en)	1993-08-24	Degumming process for plant oils
US5696278A (en)	1997-12-09	Degumming of crude glyceride oils not exposed to prior enzymatic activity
EP1201737B1 (fr)	2005-10-05	Procédé de purification d'huile végétale
EP0348004B1 (fr)	1993-06-09	Procédé pour raffiner les huiles glycéridiques
US4280962A (en)	1981-07-28	Methods for refining oils and fats
DK153228B (da)	1988-06-27	Fremgangsmaade til afgummiering af triglyceridolier
US4162260A (en)	1979-07-24	Oil purification by adding hydratable phosphatides
EP0737238B1 (fr)	2001-05-30	Procede d'elimination d'impuretes ayant la couleur de la chlorophylle presentes dans des huiles vegetales
JP2709736B2 (ja)	1998-02-04	油脂の精製方法
EP0122727B1 (fr)	1987-05-20	Procédé relatif aux huiles triglycéridiques
US3943155A (en)	1976-03-09	Simultaneous refining and dewaxing of crude vegetable oil
US6376689B1 (en)	2002-04-23	Removal of gum and chlorophyll-type compounds from vegetable oils
EP0389057B1 (fr)	1993-12-01	Procédé pour raffiner les huiles glycéridiques au moyen d'hydrogel de silice
KR890001463B1 (ko)	1989-05-04	유(油)의 정제방법
Forster et al.	1983	Physical refining
EP0170242B1 (fr)	1989-10-25	Elimination par étapes de cires d'huiles végétales comestibles
JPS6243476B2 (fr)	1987-09-14
US10329514B2 (en)	2019-06-25	Enzymatic degumming
JP2000119682A (ja)	2000-04-25	米ぬか油の製造方法
JPS62256894A (ja)	1987-11-09	油脂の精製法
JP3949901B2 (ja)	2007-07-25	リン含有分の低い米ぬか油の製造方法
GB2162530A (en)	1986-02-05	Bleaching and dewaxing vegetable oils
WO2023122596A1 (fr)	2023-06-29	Procédé d'élimination d'impuretés d'une huile végétale
JPS6314759B2 (fr)	1988-04-01