JPS59195523A - ゼオライトの製造方法 - Google Patents

ゼオライトの製造方法

Info

Publication number: JPS59195523A
Authority: JP; Japan
Prior art keywords: silica; zeolite; product; sodium hydroxide; water
Prior art date: 1983-04-20
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Granted

Application number

JP6934883A

Other languages

English (en)

Japanese (ja)

Other versions

JPH0581525B2 (de

Inventor

Masahiro Numata

沼田　全弘

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Taiheiyo Cement Corp

Onoda Chemical Industry Co Ltd

Original Assignee

Onoda Cement Co Ltd

Onoda Chemical Industry Co Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1983-04-20

Filing date

1983-04-20

Publication date

1984-11-06

1983-04-20 Application filed by Onoda Cement Co Ltd, Onoda Chemical Industry Co Ltd filed Critical Onoda Cement Co Ltd

1983-04-20 Priority to JP6934883A priority Critical patent/JPS59195523A/ja

1984-11-06 Publication of JPS59195523A publication Critical patent/JPS59195523A/ja

1993-11-15 Publication of JPH0581525B2 publication Critical patent/JPH0581525B2/ja

Status Granted legal-status Critical Current

Links

239000010457 zeolite Substances 0.000 title claims abstract description 51
229910021536 Zeolite Inorganic materials 0.000 title claims abstract description 49
HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 title claims abstract description 49
238000004519 manufacturing process Methods 0.000 title abstract description 22
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 128
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 114
239000006227 byproduct Substances 0.000 claims abstract description 42
WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims abstract description 24
229910001868 water Inorganic materials 0.000 claims abstract description 24
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 20
238000006243 chemical reaction Methods 0.000 claims abstract description 14
KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims abstract description 11
PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims abstract description 8
IRPGOXJVTQTAAN-UHFFFAOYSA-N 2,2,3,3,3-pentafluoropropanal Chemical compound FC(F)(F)C(F)(F)C=O IRPGOXJVTQTAAN-UHFFFAOYSA-N 0.000 claims abstract description 5
KLZUFWVZNOTSEM-UHFFFAOYSA-K Aluminum fluoride Inorganic materials F[Al](F)F KLZUFWVZNOTSEM-UHFFFAOYSA-K 0.000 claims abstract description 5
229910001610 cryolite Inorganic materials 0.000 claims abstract description 5
239000000725 suspension Substances 0.000 claims abstract description 4
229910052593 corundum Inorganic materials 0.000 claims abstract 3
229910001845 yogo sapphire Inorganic materials 0.000 claims abstract 3
LRCFXGAMWKDGLA-UHFFFAOYSA-N dioxosilane;hydrate Chemical compound O.O=[Si]=O LRCFXGAMWKDGLA-UHFFFAOYSA-N 0.000 claims abstract 2
238000000034 method Methods 0.000 claims description 47
238000003756 stirring Methods 0.000 claims description 12
238000004090 dissolution Methods 0.000 claims description 11
239000000126 substance Substances 0.000 claims description 7
230000002194 synthesizing effect Effects 0.000 claims description 4
239000000470 constituent Substances 0.000 claims description 2
239000000377 silicon dioxide Substances 0.000 abstract description 57
230000015572 biosynthetic process Effects 0.000 abstract description 9
238000003786 synthesis reaction Methods 0.000 abstract description 8
239000000271 synthetic detergent Substances 0.000 abstract description 4
229910052681 coesite Inorganic materials 0.000 abstract description 3
229910052906 cristobalite Inorganic materials 0.000 abstract description 3
229910052682 stishovite Inorganic materials 0.000 abstract description 3
229910052905 tridymite Inorganic materials 0.000 abstract description 3
229910021502 aluminium hydroxide Inorganic materials 0.000 abstract 2
229910001679 gibbsite Inorganic materials 0.000 abstract 2
229960004029 silicic acid Drugs 0.000 abstract 1
235000012239 silicon dioxide Nutrition 0.000 abstract 1
239000002994 raw material Substances 0.000 description 23
239000000203 mixture Substances 0.000 description 17
238000002156 mixing Methods 0.000 description 13
239000000047 product Substances 0.000 description 12
239000000843 powder Substances 0.000 description 10
239000007787 solid Substances 0.000 description 8
SFKTYEXKZXBQRQ-UHFFFAOYSA-J thorium(4+);tetrahydroxide Chemical compound [OH-].[OH-].[OH-].[OH-].[Th+4] SFKTYEXKZXBQRQ-UHFFFAOYSA-J 0.000 description 8
239000013078 crystal Substances 0.000 description 7
238000002425 crystallisation Methods 0.000 description 7
230000008025 crystallization Effects 0.000 description 7
230000000694 effects Effects 0.000 description 7
230000000704 physical effect Effects 0.000 description 7
239000007788 liquid Substances 0.000 description 6
230000007423 decrease Effects 0.000 description 5
239000003599 detergent Substances 0.000 description 4
238000001035 drying Methods 0.000 description 4
239000000706 filtrate Substances 0.000 description 4
238000005342 ion exchange Methods 0.000 description 4
239000000463 material Substances 0.000 description 4
239000011164 primary particle Substances 0.000 description 4
239000011541 reaction mixture Substances 0.000 description 4
229910052665 sodalite Inorganic materials 0.000 description 4
WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 description 3
ANBBXQWFNXMHLD-UHFFFAOYSA-N aluminum;sodium;oxygen(2-) Chemical compound [O-2].[O-2].[Na+].[Al+3] ANBBXQWFNXMHLD-UHFFFAOYSA-N 0.000 description 3
238000010438 heat treatment Methods 0.000 description 3
239000002245 particle Substances 0.000 description 3
230000009257 reactivity Effects 0.000 description 3
229910001388 sodium aluminate Inorganic materials 0.000 description 3
NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical group [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 3
229910002012 Aerosil® Inorganic materials 0.000 description 2
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
239000004115 Sodium Silicate Substances 0.000 description 2
238000002441 X-ray diffraction Methods 0.000 description 2
239000004927 clay Substances 0.000 description 2
230000000052 comparative effect Effects 0.000 description 2
239000010419 fine particle Substances 0.000 description 2
239000012535 impurity Substances 0.000 description 2
229910052911 sodium silicate Inorganic materials 0.000 description 2
238000005406 washing Methods 0.000 description 2
BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical group [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 1
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
229910005260 GaCl2 Inorganic materials 0.000 description 1
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 1
BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
235000019892 Stellar Nutrition 0.000 description 1
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
238000010306 acid treatment Methods 0.000 description 1
230000032683 aging Effects 0.000 description 1
229910052782 aluminium Inorganic materials 0.000 description 1
239000004411 aluminium Substances 0.000 description 1
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
229910000147 aluminium phosphate Inorganic materials 0.000 description 1
VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminum chloride Substances Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 description 1
238000001479 atomic absorption spectroscopy Methods 0.000 description 1
230000005540 biological transmission Effects 0.000 description 1
238000001354 calcination Methods 0.000 description 1
229910001424 calcium ion Inorganic materials 0.000 description 1
239000003153 chemical reaction reagent Substances 0.000 description 1
239000003795 chemical substances by application Substances 0.000 description 1
239000002734 clay mineral Substances 0.000 description 1
239000003086 colorant Substances 0.000 description 1
238000004040 coloring Methods 0.000 description 1
238000001816 cooling Methods 0.000 description 1
235000013365 dairy product Nutrition 0.000 description 1
230000001934 delay Effects 0.000 description 1
JYIMWRSJCRRYNK-UHFFFAOYSA-N dialuminum;disodium;oxygen(2-);silicon(4+);hydrate Chemical compound O.[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Na+].[Na+].[Al+3].[Al+3].[Si+4] JYIMWRSJCRRYNK-UHFFFAOYSA-N 0.000 description 1
239000006185 dispersion Substances 0.000 description 1
238000009826 distribution Methods 0.000 description 1
239000000428 dust Substances 0.000 description 1
238000010410 dusting Methods 0.000 description 1
238000001914 filtration Methods 0.000 description 1
150000002222 fluorine compounds Chemical class 0.000 description 1
239000003292 glue Substances 0.000 description 1
238000001027 hydrothermal synthesis Methods 0.000 description 1
FAHBNUUHRFUEAI-UHFFFAOYSA-M hydroxidooxidoaluminium Chemical compound O[Al]=O FAHBNUUHRFUEAI-UHFFFAOYSA-M 0.000 description 1
229910052500 inorganic mineral Inorganic materials 0.000 description 1
229910052742 iron Inorganic materials 0.000 description 1
239000007791 liquid phase Substances 0.000 description 1
229910052744 lithium Inorganic materials 0.000 description 1
238000005259 measurement Methods 0.000 description 1
238000002844 melting Methods 0.000 description 1
230000008018 melting Effects 0.000 description 1
239000011707 mineral Substances 0.000 description 1
230000000877 morphologic effect Effects 0.000 description 1
239000012452 mother liquor Substances 0.000 description 1
239000011824 nuclear material Substances 0.000 description 1
238000003921 particle size analysis Methods 0.000 description 1
239000011574 phosphorus Substances 0.000 description 1
229910052698 phosphorus Inorganic materials 0.000 description 1
235000019353 potassium silicate Nutrition 0.000 description 1
239000002244 precipitate Substances 0.000 description 1
238000001556 precipitation Methods 0.000 description 1
238000010298 pulverizing process Methods 0.000 description 1
238000000746 purification Methods 0.000 description 1
238000004626 scanning electron microscopy Methods 0.000 description 1
125000005372 silanol group Chemical group 0.000 description 1
239000000741 silica gel Substances 0.000 description 1
229910002027 silica gel Inorganic materials 0.000 description 1
RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 1
239000002002 slurry Substances 0.000 description 1
239000011734 sodium Substances 0.000 description 1
229910052708 sodium Inorganic materials 0.000 description 1
238000000967 suction filtration Methods 0.000 description 1
239000011593 sulfur Substances 0.000 description 1
239000002023 wood Substances 0.000 description 1

Landscapes

Silicates, Zeolites, And Molecular Sieves (AREA)

JP6934883A 1983-04-20 1983-04-20 ゼオライトの製造方法 Granted JPS59195523A (ja)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP6934883A JPS59195523A (ja)	1983-04-20	1983-04-20	ゼオライトの製造方法

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP6934883A JPS59195523A (ja)	1983-04-20	1983-04-20	ゼオライトの製造方法

Publications (2)

Publication Number	Publication Date
JPS59195523A true JPS59195523A (ja)	1984-11-06
JPH0581525B2 JPH0581525B2 (de)	1993-11-15

Family

ID=13399952

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP6934883A Granted JPS59195523A (ja)	1983-04-20	1983-04-20	ゼオライトの製造方法

Country Status (1)

Country	Link
JP (1)	JPS59195523A (de)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US7605099B2 (en)	2001-05-08	2009-10-20	Schott Ag	Optical glasses and their uses

Citations (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS4855899A (de) *	1971-11-18	1973-08-06
JPS56149313A (en) *	1980-04-22	1981-11-19	Denpatsu Furaiatsushiyu Kk	Manufacture of porous substance
JPS5734018A (en) *	1980-08-06	1982-02-24	Agency Of Ind Science & Technol	Production of boiling stone mainly consisting of coal ash rich in alumina

1983
- 1983-04-20 JP JP6934883A patent/JPS59195523A/ja active Granted

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS4855899A (de) *	1971-11-18	1973-08-06
JPS56149313A (en) *	1980-04-22	1981-11-19	Denpatsu Furaiatsushiyu Kk	Manufacture of porous substance
JPS5734018A (en) *	1980-08-06	1982-02-24	Agency Of Ind Science & Technol	Production of boiling stone mainly consisting of coal ash rich in alumina

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US7605099B2 (en)	2001-05-08	2009-10-20	Schott Ag	Optical glasses and their uses

Also Published As

Publication number	Publication date
JPH0581525B2 (de)	1993-11-15

Publication	Publication Date	Title
US4562055A (en)	1985-12-31	Process for preparation of zeolites
US4587115A (en)	1986-05-06	Process for preparation of high-silica faujasite type zeolite
US9272919B2 (en)	2016-03-01	Hydrothermal synthesis of zeolites or zeolite-like materials using modified mixed hydroxides
US20060147367A1 (en)	2006-07-06	Process for the produciton of synthetic magnesium silicate compositons
JPH0239446B2 (de)	1990-09-05
EP0109729B1 (de)	1988-03-09	Verfahren zur Herstellung eines Zeolithen vom Mordenit-Typ
US4891199A (en)	1990-01-02	Preparation of zeolites of type ZSM-5
CA1249989A (en)	1989-02-14	Process for preparation of faujasite type zeolite
US4226636A (en)	1980-10-07	Production of calcium silicate having high specific bulk volume and calcium silicate-gypsum composite
HU181898B (en)	1983-11-28	Semicontinuous industrial process for producing zeolite a
EP0614853B1 (de)	1999-04-21	Methode zur Herstellung von Beta-Zeolith
JPS59195523A (ja)	1984-11-06	ゼオライトの製造方法
EP0273403B1 (de)	1993-12-08	Verfahren zur Herstellung synthetischen Mazzits
JPH0339974B2 (de)	1991-06-17
AU2001237708B2 (en)	2004-10-14	A process for the manufacture of zeolite-A useful as a detergent builder
JPS5954620A (ja)	1984-03-29	ゼオライトを製造する方法
US5262143A (en)	1993-11-16	Production of finely divided particulate siliceous material by decomposition of alkali metal silicate with sulfitic species
JPS61155215A (ja)	1986-07-14	Ｌ型ゼオライトの撹拌合成法
JPH05339B2 (de)	1993-01-05
JPS62191417A (ja)	1987-08-21	アモルフアスアルミノシリケ−トの製造方法
JPH024528B2 (de)	1990-01-29
JPS62191419A (ja)	1987-08-21	アモルフアスアルミノシリケ−トの製造方法
JPS5969419A (ja)	1984-04-19	フエリエライト型ゼオライトの製造方法
JPH0525806B2 (de)	1993-04-14
JPS62132726A (ja)	1987-06-16	Ｌ型ゼオライトの製造法

JPS59195523A - ゼオライトの製造方法 - Google Patents

Info

Links

Landscapes

Priority Applications (1)

Applications Claiming Priority (1)

Publications (2)

Family

ID=13399952

Family Applications (1)

Country Status (1)

Cited By (1)

Citations (3)

Patent Citations (3)

Cited By (1)

Also Published As

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