JP5876172B1 - 酸化物焼結体、酸化物スパッタリングターゲット及び導電性酸化物薄膜並びに酸化物焼結体の製造方法 - Google Patents
酸化物焼結体、酸化物スパッタリングターゲット及び導電性酸化物薄膜並びに酸化物焼結体の製造方法 Download PDFInfo
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- JP5876172B1 JP5876172B1 JP2015012019A JP2015012019A JP5876172B1 JP 5876172 B1 JP5876172 B1 JP 5876172B1 JP 2015012019 A JP2015012019 A JP 2015012019A JP 2015012019 A JP2015012019 A JP 2015012019A JP 5876172 B1 JP5876172 B1 JP 5876172B1
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- oxide
- sintered body
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- sputtering
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- 238000004519 manufacturing process Methods 0.000 title claims description 6
- 239000010409 thin film Substances 0.000 title abstract description 33
- 238000005477 sputtering target Methods 0.000 title abstract description 16
- 239000010936 titanium Substances 0.000 claims abstract description 56
- 239000011701 zinc Substances 0.000 claims abstract description 40
- 229910052718 tin Inorganic materials 0.000 claims abstract description 22
- 229910052738 indium Inorganic materials 0.000 claims abstract description 17
- 229910052719 titanium Inorganic materials 0.000 claims abstract description 17
- 230000008033 biological extinction Effects 0.000 claims abstract description 15
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000001301 oxygen Substances 0.000 claims abstract description 11
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 11
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 10
- 229910052725 zinc Inorganic materials 0.000 claims abstract description 10
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims abstract description 8
- APFVFJFRJDLVQX-UHFFFAOYSA-N indium atom Chemical compound [In] APFVFJFRJDLVQX-UHFFFAOYSA-N 0.000 claims abstract description 8
- JBQYATWDVHIOAR-UHFFFAOYSA-N tellanylidenegermanium Chemical compound [Te]=[Ge] JBQYATWDVHIOAR-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000000843 powder Substances 0.000 claims description 67
- 230000003287 optical effect Effects 0.000 claims description 36
- 239000012298 atmosphere Substances 0.000 claims description 12
- 239000002994 raw material Substances 0.000 claims description 10
- 238000005245 sintering Methods 0.000 claims description 10
- 239000011261 inert gas Substances 0.000 claims description 6
- 239000012528 membrane Substances 0.000 claims description 3
- 238000000465 moulding Methods 0.000 claims description 2
- 239000010408 film Substances 0.000 abstract description 73
- 238000004544 sputter deposition Methods 0.000 abstract description 41
- 238000002834 transmittance Methods 0.000 abstract description 21
- XLOMVQKBTHCTTD-UHFFFAOYSA-N zinc oxide Inorganic materials [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 31
- 239000011787 zinc oxide Substances 0.000 description 16
- 239000000203 mixture Substances 0.000 description 14
- 229910010413 TiO 2 Inorganic materials 0.000 description 13
- 229910006404 SnO 2 Inorganic materials 0.000 description 12
- 239000000463 material Substances 0.000 description 12
- 230000015572 biosynthetic process Effects 0.000 description 11
- 239000011812 mixed powder Substances 0.000 description 11
- 239000012300 argon atmosphere Substances 0.000 description 10
- 238000002156 mixing Methods 0.000 description 10
- 239000002245 particle Substances 0.000 description 9
- 230000000052 comparative effect Effects 0.000 description 8
- 238000011156 evaluation Methods 0.000 description 8
- 238000000034 method Methods 0.000 description 7
- 238000010298 pulverizing process Methods 0.000 description 7
- 238000002425 crystallisation Methods 0.000 description 6
- 230000008025 crystallization Effects 0.000 description 6
- 230000031700 light absorption Effects 0.000 description 6
- 229910052751 metal Inorganic materials 0.000 description 6
- 239000002184 metal Substances 0.000 description 6
- 239000011324 bead Substances 0.000 description 5
- 238000005530 etching Methods 0.000 description 5
- 239000000758 substrate Substances 0.000 description 5
- 230000006872 improvement Effects 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 238000001552 radio frequency sputter deposition Methods 0.000 description 3
- 238000002441 X-ray diffraction Methods 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 230000033228 biological regulation Effects 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 239000000523 sample Substances 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- GYHNNYVSQQEPJS-UHFFFAOYSA-N Gallium Chemical compound [Ga] GYHNNYVSQQEPJS-UHFFFAOYSA-N 0.000 description 1
- 241001089723 Metaphycus omega Species 0.000 description 1
- 229910007541 Zn O Inorganic materials 0.000 description 1
- JODIJOMWCAXJJX-UHFFFAOYSA-N [O-2].[Al+3].[O-2].[Zn+2] Chemical compound [O-2].[Al+3].[O-2].[Zn+2] JODIJOMWCAXJJX-UHFFFAOYSA-N 0.000 description 1
- AZWHFTKIBIQKCA-UHFFFAOYSA-N [Sn+2]=O.[O-2].[In+3] Chemical compound [Sn+2]=O.[O-2].[In+3] AZWHFTKIBIQKCA-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000000280 densification Methods 0.000 description 1
- 238000001739 density measurement Methods 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 229910052733 gallium Inorganic materials 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000009616 inductively coupled plasma Methods 0.000 description 1
- 238000002354 inductively-coupled plasma atomic emission spectroscopy Methods 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000012788 optical film Substances 0.000 description 1
- 150000002926 oxygen Chemical class 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000001028 reflection method Methods 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 230000009291 secondary effect Effects 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 239000012780 transparent material Substances 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- OYQCBJZGELKKPM-UHFFFAOYSA-N zinc indium(3+) oxygen(2-) Chemical compound [O-2].[Zn+2].[O-2].[In+3] OYQCBJZGELKKPM-UHFFFAOYSA-N 0.000 description 1
- UMIKMTIOESTGKJ-UHFFFAOYSA-N zinc indium(3+) oxygen(2-) titanium(4+) Chemical compound [O-2].[Ti+4].[O-2].[In+3].[O-2].[Zn+2] UMIKMTIOESTGKJ-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/62218—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining ceramic films, e.g. by using temporary supports
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/64—Burning or sintering processes
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/64—Burning or sintering processes
- C04B35/645—Pressure sintering
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/06—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the coating material
- C23C14/08—Oxides
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/34—Sputtering
- C23C14/3407—Cathode assembly for sputtering apparatus, e.g. Target
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/34—Sputtering
- C23C14/3407—Cathode assembly for sputtering apparatus, e.g. Target
- C23C14/3414—Metallurgical or chemical aspects of target preparation, e.g. casting, powder metallurgy
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
- C04B2235/9646—Optical properties
- C04B2235/9653—Translucent or transparent ceramics other than alumina
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Physical Vapour Deposition (AREA)
- Compositions Of Oxide Ceramics (AREA)
Priority Applications (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2015012019A JP5876172B1 (ja) | 2014-10-06 | 2015-01-26 | 酸化物焼結体、酸化物スパッタリングターゲット及び導電性酸化物薄膜並びに酸化物焼結体の製造方法 |
TW104127113A TWI537404B (zh) | 2014-10-06 | 2015-08-20 | Oxide sintered body, oxide sputtering target, and method for producing conductive oxide film and oxide sintered body |
KR1020150139701A KR101668963B1 (ko) | 2014-10-06 | 2015-10-05 | 산화물 소결체 및 그 제조 방법, 산화물 스퍼터링 타깃 그리고 도전성 산화물 박막 |
CN201510646309.2A CN105481352A (zh) | 2014-10-06 | 2015-10-08 | 氧化物烧结体、氧化物溅射靶和导电性氧化物薄膜以及氧化物烧结体的制造方法 |
CN201811061549.6A CN109437856A (zh) | 2014-10-06 | 2015-10-08 | 氧化物烧结体、氧化物溅射靶和导电性氧化物薄膜以及氧化物烧结体的制造方法 |
Applications Claiming Priority (3)
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JP2014205403 | 2014-10-06 | ||
JP2014205403 | 2014-10-06 | ||
JP2015012019A JP5876172B1 (ja) | 2014-10-06 | 2015-01-26 | 酸化物焼結体、酸化物スパッタリングターゲット及び導電性酸化物薄膜並びに酸化物焼結体の製造方法 |
Publications (2)
Publication Number | Publication Date |
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JP5876172B1 true JP5876172B1 (ja) | 2016-03-02 |
JP2016074579A JP2016074579A (ja) | 2016-05-12 |
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JP2015012019A Active JP5876172B1 (ja) | 2014-10-06 | 2015-01-26 | 酸化物焼結体、酸化物スパッタリングターゲット及び導電性酸化物薄膜並びに酸化物焼結体の製造方法 |
Country Status (4)
Country | Link |
---|---|
JP (1) | JP5876172B1 (ko) |
KR (1) | KR101668963B1 (ko) |
CN (2) | CN109437856A (ko) |
TW (1) | TWI537404B (ko) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
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JP7086080B2 (ja) * | 2017-08-08 | 2022-06-17 | 三井金属鉱業株式会社 | 酸化物焼結体およびスパッタリングターゲット |
JP2019131866A (ja) * | 2018-01-31 | 2019-08-08 | 住友金属鉱山株式会社 | 酸化物スパッタ膜、酸化物スパッタ膜の製造方法、酸化物焼結体及び透明樹脂基板 |
TWI819633B (zh) * | 2022-05-31 | 2023-10-21 | 光洋應用材料科技股份有限公司 | 氧化銦鈦鋅濺鍍靶材、其薄膜及其製法 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0971860A (ja) * | 1995-06-28 | 1997-03-18 | Idemitsu Kosan Co Ltd | ターゲットおよびその製造方法 |
WO2010058533A1 (ja) * | 2008-11-20 | 2010-05-27 | 出光興産株式会社 | ZnO-SnO2-In2O3系酸化物焼結体及び非晶質透明導電膜 |
WO2012153507A1 (ja) * | 2011-05-10 | 2012-11-15 | 出光興産株式会社 | In2O3-SnO2-ZnO系スパッタリングターゲット |
JP2014109071A (ja) * | 2012-12-03 | 2014-06-12 | Solar Applied Materials Technology Corp | スパッタリングターゲット |
JP2014111818A (ja) * | 2012-11-09 | 2014-06-19 | Idemitsu Kosan Co Ltd | スパッタリングターゲット、酸化物半導体薄膜及びそれらの製造方法 |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7141186B2 (en) * | 2002-10-29 | 2006-11-28 | Sumitomo Metal Mining Co., Ltd. | Oxide sintered body and sputtering target, and manufacturing method for transparent conductive oxide film as electrode |
JP4933756B2 (ja) * | 2005-09-01 | 2012-05-16 | 出光興産株式会社 | スパッタリングターゲット |
JP4994068B2 (ja) | 2006-08-09 | 2012-08-08 | 出光興産株式会社 | 酸化物導電性材料及びその製造方法 |
JP2013220805A (ja) | 2012-04-19 | 2013-10-28 | Toyota Boshoku Corp | 車室の吹出口構造 |
-
2015
- 2015-01-26 JP JP2015012019A patent/JP5876172B1/ja active Active
- 2015-08-20 TW TW104127113A patent/TWI537404B/zh active
- 2015-10-05 KR KR1020150139701A patent/KR101668963B1/ko active IP Right Grant
- 2015-10-08 CN CN201811061549.6A patent/CN109437856A/zh active Pending
- 2015-10-08 CN CN201510646309.2A patent/CN105481352A/zh active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0971860A (ja) * | 1995-06-28 | 1997-03-18 | Idemitsu Kosan Co Ltd | ターゲットおよびその製造方法 |
WO2010058533A1 (ja) * | 2008-11-20 | 2010-05-27 | 出光興産株式会社 | ZnO-SnO2-In2O3系酸化物焼結体及び非晶質透明導電膜 |
WO2012153507A1 (ja) * | 2011-05-10 | 2012-11-15 | 出光興産株式会社 | In2O3-SnO2-ZnO系スパッタリングターゲット |
JP2014111818A (ja) * | 2012-11-09 | 2014-06-19 | Idemitsu Kosan Co Ltd | スパッタリングターゲット、酸化物半導体薄膜及びそれらの製造方法 |
JP2014109071A (ja) * | 2012-12-03 | 2014-06-12 | Solar Applied Materials Technology Corp | スパッタリングターゲット |
Also Published As
Publication number | Publication date |
---|---|
TWI537404B (zh) | 2016-06-11 |
TW201614084A (en) | 2016-04-16 |
KR101668963B1 (ko) | 2016-10-24 |
KR20160041013A (ko) | 2016-04-15 |
CN109437856A (zh) | 2019-03-08 |
CN105481352A (zh) | 2016-04-13 |
JP2016074579A (ja) | 2016-05-12 |
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