FR2965490B1 - Dispositif et procede pour la phosgenation en continu - Google Patents

Dispositif et procede pour la phosgenation en continu

Info

Publication number
FR2965490B1
FR2965490B1 FR1003879A FR1003879A FR2965490B1 FR 2965490 B1 FR2965490 B1 FR 2965490B1 FR 1003879 A FR1003879 A FR 1003879A FR 1003879 A FR1003879 A FR 1003879A FR 2965490 B1 FR2965490 B1 FR 2965490B1
Authority
FR
France
Prior art keywords
reactor
phosgene
continuous
continuous phosgenation
phosgenation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
FR1003879A
Other languages
English (en)
Other versions
FR2965490A1 (fr
Inventor
Raimondo Pilia
Alexandre Trani
Sabrina Marie
Panthou Fabrice De
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Yriel SAS
Original Assignee
AET Group
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by AET Group filed Critical AET Group
Priority to FR1003879A priority Critical patent/FR2965490B1/fr
Priority to JP2013530774A priority patent/JP2013541533A/ja
Priority to EP11771212.5A priority patent/EP2621627A1/fr
Priority to PCT/FR2011/000530 priority patent/WO2012042130A1/fr
Priority to US13/816,785 priority patent/US20130303783A1/en
Publication of FR2965490A1 publication Critical patent/FR2965490A1/fr
Application granted granted Critical
Publication of FR2965490B1 publication Critical patent/FR2965490B1/fr
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0046—Sequential or parallel reactions, e.g. for the synthesis of polypeptides or polynucleotides; Apparatus and devices for combinatorial chemistry or for making molecular arrays
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/20—Stationary reactors having moving elements inside in the form of helices, e.g. screw reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/20—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium
    • B01J8/22—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid
    • B01J8/222—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid in the presence of a rotating device only
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/80—Phosgene
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/02—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of compounds containing imino groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C68/00—Preparation of esters of carbonic or haloformic acids
    • C07C68/02—Preparation of esters of carbonic or haloformic acids from phosgene or haloformates
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
    • C07D233/54—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members
    • C07D233/56—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, attached to ring carbon atoms
    • C07D233/60—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, attached to ring carbon atoms with hydrocarbon radicals, substituted by oxygen or sulfur atoms, attached to ring nitrogen atoms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00027—Process aspects
    • B01J2219/0004—Processes in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00245—Avoiding undesirable reactions or side-effects
    • B01J2219/00256—Leakage
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/141—Feedstock

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
FR1003879A 2010-09-30 2010-09-30 Dispositif et procede pour la phosgenation en continu Expired - Fee Related FR2965490B1 (fr)

Priority Applications (5)

Application Number Priority Date Filing Date Title
FR1003879A FR2965490B1 (fr) 2010-09-30 2010-09-30 Dispositif et procede pour la phosgenation en continu
JP2013530774A JP2013541533A (ja) 2010-09-30 2011-09-28 連続ホスゲン化のための装置及び方法
EP11771212.5A EP2621627A1 (fr) 2010-09-30 2011-09-28 Dispositif et procédé pour la phosgénation en continu
PCT/FR2011/000530 WO2012042130A1 (fr) 2010-09-30 2011-09-28 Dispositif et procédé pour la phosgénation en continu
US13/816,785 US20130303783A1 (en) 2010-09-30 2011-09-28 Device and process for continuous phosgenation

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR1003879A FR2965490B1 (fr) 2010-09-30 2010-09-30 Dispositif et procede pour la phosgenation en continu

Publications (2)

Publication Number Publication Date
FR2965490A1 FR2965490A1 (fr) 2012-04-06
FR2965490B1 true FR2965490B1 (fr) 2013-01-11

Family

ID=44065608

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1003879A Expired - Fee Related FR2965490B1 (fr) 2010-09-30 2010-09-30 Dispositif et procede pour la phosgenation en continu

Country Status (5)

Country Link
US (1) US20130303783A1 (fr)
EP (1) EP2621627A1 (fr)
JP (1) JP2013541533A (fr)
FR (1) FR2965490B1 (fr)
WO (1) WO2012042130A1 (fr)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104428247B (zh) 2012-07-11 2017-03-29 科思创德国股份有限公司 用于产生碳酰氯的设备和方法
FR3012145B1 (fr) * 2013-10-18 2015-12-18 Yriel Procede continu de preparation d'acides boroniques et de leurs derives
CN103570018A (zh) * 2013-10-29 2014-02-12 嘉兴学院 一种安全的光气制备方法与装置
ES2804677T3 (es) * 2014-06-11 2021-02-09 Haldor Topsoe As Un proceso para la producción segura de fosgeno
KR101842501B1 (ko) 2014-08-20 2018-03-27 바이엘 악티엔게젤샤프트 하이드록실, 티올, 아미노 및/또는 포름아미드기를 포함하는 화합물의 포스겐화 방법
WO2020050368A1 (fr) * 2018-09-06 2020-03-12 国立大学法人神戸大学 Procédé de préparation d'un réactif de vilsmeier
CN113651326A (zh) * 2021-08-31 2021-11-16 重庆长风化学工业有限公司 一种用于生成光气平台***

Family Cites Families (48)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR502672A (fr) 1915-12-21 1920-05-22 Air Liquide Procédé général de catalyse et son application à la fabrication synthétique de l'oxychlorure de carbone
FR502673A (fr) 1915-12-24 1920-05-22 Air Liquide Matière catalysante pour la fabrication par catalyse à basse température de l'oxychlorure de carbone
US1746506A (en) 1927-10-04 1930-02-11 Pont Ammonia Corp Du Process for the preparation of phosgene
US2457493A (en) 1947-09-03 1948-12-28 American Marietta Co Art of making phenol-aldehyde reaction products and the product thereof
US3226410A (en) 1962-07-20 1965-12-28 Fmc Corp Continuous method of preparing aromatic isocyanates
US3321283A (en) * 1963-12-23 1967-05-23 Mobay Chemical Corp Apparatus for conducting rapid chemical reactions
GB1324465A (en) 1970-07-08 1973-07-25 Hoechst Ag Process for the preparation of carbon tetrachloride and phosgene
FR2109186A5 (en) 1970-10-06 1972-05-26 France Etat Phosgene - prepd from chlorine and excess carbon monoxide, - partially condensing product and recycling part of gaseous residue
DE2058032A1 (de) * 1970-11-25 1972-05-31 Zimmer Ag Ind Anlagen Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Isocyanaten
US3996273A (en) 1971-07-05 1976-12-07 Rhone-Progil Manufacture of phosgene from chlorine obtained by oxidation of hydrochloric gas and fixed on reactional chlorine exchanger masses
FR2144960A5 (fr) 1971-07-05 1973-02-16 Saint Gobain
FR2297190A1 (fr) 1975-01-08 1976-08-06 Tolochimie Procede de fabrication de phosgene
FR2345394A2 (fr) 1975-01-08 1977-10-21 Tolochimie Procede de fabrication de phosgene
FR2297191A1 (fr) 1975-01-08 1976-08-06 Tolochimie Procede de fabrication de phosgene
JPS53131298A (en) 1977-03-18 1978-11-15 Ube Ind Ltd Production of phosgene
US4231959A (en) 1978-02-15 1980-11-04 Stauffer Chemical Company Phosgene manufacture
US4346047A (en) 1978-10-02 1982-08-24 The Lummus Company Production of phosgene
US4493818A (en) 1982-11-08 1985-01-15 The Dow Chemical Company Phosgene removal process
DE3327274A1 (de) 1983-07-28 1985-02-07 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von phosgen unter gleichzeitiger erzeugung von dampf
CN1099044A (zh) * 1993-04-16 1995-02-22 大世吕化学工业株式会社 (共)聚碳酸酯的制备方法
SK281459B6 (sk) 1994-11-17 2001-03-12 Bayer Aktiengesellschaft Spôsob jednostupňovej kontinuálnej prípravy izokyanatanov
JP3124455B2 (ja) 1994-12-01 2001-01-15 出光石油化学株式会社 ホスゲンの製造方法
AU7551296A (en) 1996-02-21 1997-09-10 E.I. Du Pont De Nemours And Company Phosgene manufacturing process
US5672747A (en) 1996-05-17 1997-09-30 Stauffer; John E. Phosgene process
DE69706862T2 (de) 1996-06-28 2002-04-11 Du Pont Verfahren zur herstellung von phosgen
DE19638567A1 (de) 1996-09-20 1998-03-26 Bayer Ag Mischer-Reaktor und Verfahren zur Durchführung von Reaktionen, insbesondere die Phosgenierung von primären Aminen
US5986037A (en) 1996-12-09 1999-11-16 Mitsubishi Chemical Corporation Polycarbonate resin with a reduced volatile chlorine content and process for producing the same
US6054612A (en) 1996-12-20 2000-04-25 E. I. Du Pont De Nemours And Company Phosgene manufacturing process
DE19740577A1 (de) 1997-09-15 1999-03-18 Eckert Gmbh Dr Verfahren und Vorrichtung zur Herstellung von Phosgen aus Diphosgen und/oder Triphosgen
DE19848668A1 (de) 1998-10-22 2000-04-27 Bayer Ag Tetrachlorkohlenstoffarmes Phosgen
DE19916856A1 (de) 1999-04-14 1999-09-23 Eckert Gmbh Dr Verfahren zur Herstellung von Carbonyldichlorid aus Chlor und Kohlenmonoxid
EP1112997B1 (fr) 1999-12-28 2009-05-13 Mitsubishi Chemical Corporation Procédé de préparation du carbonate de diaryle
DE10036602A1 (de) 2000-07-27 2002-02-14 Cpc Cellular Process Chemistry Mikroreaktor für Reaktionen zwischen Gasen und Flüssigkeiten
DE10158160A1 (de) 2001-11-28 2003-06-12 Basf Ag Herstellung von Isocyanaten in der Gasphase
CN1302842C (zh) 2002-02-27 2007-03-07 巴斯福股份公司 用于生产光气的反应器和方法
DE10260084A1 (de) 2002-12-19 2004-07-01 Basf Ag Auftrennung eines Stoffgemisches aus Clorwasserstoff und Phosgen
US7250530B2 (en) 2003-07-30 2007-07-31 General Electric Company Processes and systems for making phosgene
DE102004041777A1 (de) 2004-08-28 2006-03-02 Bayer Materialscience Ag Verfahren und Vorrichtung zur Herstellung von Phosgen
DE102005032663A1 (de) 2005-07-13 2007-01-18 Bayer Materialscience Ag Verfahren zur Herstellung von Isocyanaten
DE102006022761A1 (de) * 2006-05-16 2007-11-22 Bayer Materialscience Ag Verfahren zur Herstellung von Isocyanaten
DE102006024542A1 (de) 2006-05-23 2007-11-29 Bayer Materialscience Ag Verfahren zur Abtrennung von Kohlenmonoxid aus einem chlorwasserstoffhaltigen Gas
DE102006024549A1 (de) 2006-05-23 2007-11-29 Bayer Materialscience Ag Verfahren zur Herstellung von organischen Isocyanaten
US7547801B2 (en) 2006-06-26 2009-06-16 Bayer Materialscience Llc Process for the continuous preparation of isocyanates
EP2028178A1 (fr) 2007-08-22 2009-02-25 Bayer MaterialScience AG Fabrication d'isocyanates à teneur réduite en chlore
DE102007057462A1 (de) 2007-11-29 2009-06-10 Bayer Materialscience Ag Verfahren zur Herstellung von Phosgen mit reduzierter CO-Emission
DE102008009761A1 (de) 2008-02-19 2009-08-27 Bayer Materialscience Ag Verfahren zur Herstellung von Isocyanaten
DE102008025850A1 (de) 2008-05-29 2009-12-03 Bayer Technology Services Gmbh Verfahren zur Herstellung von Phosgen
FR2940283B1 (fr) 2008-12-18 2011-03-11 Perstorp Tolonates France Utilisation d'un reacteur de type piston pour la mise en oeuvre d'un procede de phosgenation.

Also Published As

Publication number Publication date
WO2012042130A1 (fr) 2012-04-05
JP2013541533A (ja) 2013-11-14
FR2965490A1 (fr) 2012-04-06
EP2621627A1 (fr) 2013-08-07
US20130303783A1 (en) 2013-11-14

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