CN104556699B - A kind of red-purple crystal bead blank and preparation method thereof - Google Patents
A kind of red-purple crystal bead blank and preparation method thereof Download PDFInfo
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- CN104556699B CN104556699B CN201510003836.1A CN201510003836A CN104556699B CN 104556699 B CN104556699 B CN 104556699B CN 201510003836 A CN201510003836 A CN 201510003836A CN 104556699 B CN104556699 B CN 104556699B
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Abstract
The invention discloses a kind of red-purple crystal bead blank and preparation method thereof, this red-purple crystal bead blank is made up of following weight composition: quartz sand 80-160 part, zinc oxide 7-15.5 part, soda ash 27-51 part, salt of wormwood 16-30 part, boric acid 7-16 part, calcium carbonate 2.5-5.5 part, aluminium hydroxide 0.8-3.5 part, salt 1-2 part, antimonous oxide 1.5-3.5 part, saltpetre 12-27 part, gold trichloride 0.01-0.035 part, cerium oxide 1-5 part and potassium permanganate 0.001-0.002 part.Adopt potassium permanganate to adjust golden colored glass absorbing wavelength time prepared by red-purple crystal bead blank of the present invention, aobvious gorgeous red-purple, does golden painted protecting glue with zinc oxide, and cerium oxide adjustment redox condition, makes technique more stable; Adopt unleaded raw material, have glossiness good, bright-colored, neat, no color differnece, without decorative pattern, output is high, unleaded pollution-free, the advantage that productivity effect is good.
Description
Technical field
The present invention relates to a kind of red-purple crystal bead blank and preparation method thereof.
Background technology
Red-purple crystal bead blank is used to the work in-process preparing red-purple crystal product, existing red-purple crystal bead blank technique adopts crucible manufacture, there is aberration, color is uneven, have decorative pattern, unstable product quality, production efficiency is low, be not suitable for continuous production in enormous quantities, and cause environmental pollution by coal burning.And use raw material containing lead contaminate environment in existing technical recipe, white arsenic is poisonous, consumes more gold or gold trichloride to obtain darker violet tint, economic benefit and social benefit lower.
Summary of the invention
It is good that technical problem to be solved by this invention is to provide a kind of color reproduction, and solid colour no color differnece, without decorative pattern, constant product quality, production efficiency is high, and can be applicable to the production operation of continuous tank furnace, production cost is low, free of contamination red-purple crystal bead blank.
For solving the problem, the present invention is achieved through the following technical solutions: a kind of red-purple crystal bead blank, and this red-purple crystal bead blank is made up of following weight composition: quartz sand 80-160 part, zinc oxide 7-15.5 part, soda ash 27-51 part, salt of wormwood 16-30 part, boric acid 7-16 part, calcium carbonate 2.5-5.5 part, aluminium hydroxide 0.8-3.5 part, salt 1-2 part, antimonous oxide 1.5-3.5 part, saltpetre 12-27 part, gold trichloride 0.01-0.035 part, cerium oxide 1-5 part and potassium permanganate 0.001-0.002 part.
Another technical problem to be solved by this invention is to provide a kind of preparation method of red-purple crystal bead blank,
The present invention is achieved through the following technical solutions: the preparation process of described red-purple crystal bead blank is as follows:
1) extract quartz sand 80-160 part, zinc oxide 7-15.5 part, soda ash 27-51 part, salt of wormwood 16-30 part, boric acid 7-16 part, calcium carbonate 2.5-5.5 part, aluminium hydroxide 0.8-3.5 part, salt 1-2 part, antimonous oxide 1.5-3.5 part, saltpetre 12-27 part, gold trichloride 0.01-0.035 part, cerium oxide 1-5 part and potassium permanganate 0.001-0.002 part by weight ratio to mix;
2) the red-purple crystal bead blank raw material mixed is carried out granulation by tablets press;
3) granular red-purple crystal bead blank raw material will be made put into glass quartz tank furnace and found, when founding, keep strong oxidizing atmosphere and liquation liquid level stabilizing;
4) crystal liquation is molded into red-purple crystal bead blank after the homogenizing cooling of material road;
5) shaping pearl embryo is put into fire and throw stove polishing, integer, uniform coloring, shaping pearl embryo is allowed at the uniform velocity to enter stainless steel pipes, pipe temperature controls at 800 DEG C-900 DEG C, rotating speed 180 revolutions per seconds, in pipeline 5 minutes, pipeline was out just through integer, solid colour, no color differnece, red-purple crystal bead blank without decorative pattern.
Further, described in the preparation process 3 of red-purple crystal bead blank, when founding, temperature controls at 1380 DEG C-1450 DEG C.
Further, described in the preparation process 4 of red-purple crystal bead blank, cooling temperature controls at 800 DEG C-1000 DEG C.
The beneficial effect of red-purple crystal bead blank of the present invention is: adopt potassium permanganate to adjust golden colored glass absorbing wavelength time prepared by described red-purple crystal bead blank, aobvious gorgeous red-purple, do golden painted protecting glue with zinc oxide, cerium oxide adjustment redox condition, makes technique more stable; Adopt unleaded raw material, have glossiness good, bright-colored, neat, no color differnece, without decorative pattern, output is high, unleaded pollution-free, the advantage that productivity effect is good.
Embodiment
Following examples for illustration of the present invention, but are not used for limiting the scope of the invention.
Embodiment 1
A kind of red-purple crystal bead blank of the present invention, this red-purple crystal bead blank is made up of following weight composition: quartz sand 150 parts, 11 parts, zinc oxide, soda ash 38 parts, 29 parts, salt of wormwood, boric acid 11 parts, 3.5 parts, calcium carbonate, 2.2 parts, aluminium hydroxide, salt 1.6 parts, antimonous oxide 2.6 parts, 21 parts, saltpetre, gold trichloride 0.015 part, cerium oxide 1.9 parts and 0.0015 part, potassium permanganate.
The preparation process of described red-purple crystal bead blank is as follows:
1) extract quartz sand 150 parts, 11 parts, zinc oxide, soda ash 38 parts, 29 parts, salt of wormwood, boric acid 11 parts, 3.5 parts, calcium carbonate, 2.2 parts, aluminium hydroxide, salt 1.6 parts, antimonous oxide 2.6 parts, 21 parts, saltpetre, gold trichloride 0.015 part, cerium oxide 1.9 parts and 0.0015 part, potassium permanganate by weight ratio to mix;
2) the red-purple crystal bead blank raw material mixed is carried out granulation by tablets press;
3) will make granular red-purple crystal bead blank raw material to put into glass quartz tank furnace and found, keep strong oxidizing atmosphere and liquation liquid level stabilizing when founding, glass melting temperature controls at 1380 DEG C-1450 DEG C;
4) crystal liquation is molded into red-purple crystal bead blank after the homogenizing cooling of material road, cooling temperature controls at 800 DEG C-1000 DEG C;
5) shaping pearl embryo is put into fire and throw stove polishing, integer, uniform coloring, shaping pearl embryo is allowed at the uniform velocity to enter stainless steel pipes, pipe temperature controls at 800 DEG C-900 DEG C, rotating speed 180 revolutions per seconds, in pipeline 5 minutes, pipeline was out just through integer, solid colour, no color differnece, red-purple crystal bead blank without decorative pattern.
Embodiment 2
Its difference from Example 1 is, this red-purple crystal bead blank is made up of following weight composition: quartz sand 160 parts, 15.5 parts, zinc oxide, soda ash 51 parts, 30 parts, salt of wormwood, boric acid 16 parts, 5.5 parts, calcium carbonate, 3.5 parts, aluminium hydroxide, salt 2 parts, antimonous oxide 3.5 parts, 27 parts, saltpetre, gold trichloride 0.035 part, cerium oxide 5 parts and 0.002 part, potassium permanganate.
Embodiment 3
Its difference from Example 1 is, this red-purple crystal bead blank is made up of following weight composition: quartz sand 80 parts, 7 parts, zinc oxide, soda ash 27 parts, 16 parts, salt of wormwood, boric acid 7 parts, 2.5 parts, calcium carbonate, 0.8 part, aluminium hydroxide, salt 1 part, antimonous oxide 1.5 parts, 12 parts, saltpetre, gold trichloride 0.01 part, cerium oxide 1 part and 0.001 part, potassium permanganate.
Embodiment 4
Its difference from Example 1 is, this red-purple crystal bead blank is made up of following weight composition: quartz sand 90 parts, 9 parts, zinc oxide, soda ash 31 parts, 19 parts, salt of wormwood, boric acid 9 parts, 2.8 parts, calcium carbonate, 1.1 parts, aluminium hydroxide, salt 1.2 parts, antimonous oxide 1.8 parts, 14 parts, saltpetre, gold trichloride 0.019 part, cerium oxide 1.3 parts and 0.0014 part, potassium permanganate.
Embodiment 5
Its difference from Example 1 is, this red-purple crystal bead blank is made up of following weight composition: quartz sand 155 parts, 14 parts, zinc oxide, soda ash 47 parts, 28 parts, salt of wormwood, boric acid 14 parts, 5.1 parts, calcium carbonate, 3.1 parts, aluminium hydroxide, salt 1.8 parts, antimonous oxide 3.2 parts, 25 parts, saltpetre, gold trichloride 0.03 part, cerium oxide 4.6 parts and 0.0018 part, potassium permanganate.
Embodiment 6
Its difference from Example 1 is, this red-purple crystal bead blank is made up of following weight composition: quartz sand 125 parts, 11 parts, zinc oxide, soda ash 33 parts, 23 parts, salt of wormwood, boric acid 12 parts, 3.5 parts, calcium carbonate, 2.5 parts, aluminium hydroxide, salt 1.5 parts, antimonous oxide 2 parts, 20 parts, saltpetre, gold trichloride 0.021 part, cerium oxide 3.1 parts and 0.0015 part, potassium permanganate.
Embodiment 7
Its difference from Example 1 is, this red-purple crystal bead blank is made up of following weight composition: quartz sand 100 parts, 9.5 parts, zinc oxide, soda ash 40 parts, 21 parts, salt of wormwood, boric acid 13 parts, 4 parts, calcium carbonate, 2 parts, aluminium hydroxide, salt 1 part, antimonous oxide 2 parts, 17 parts, saltpetre, gold trichloride 0.03 part, cerium oxide 2 parts and 0.0013 part, potassium permanganate.
Embodiment 8
Its difference from Example 1 is, this red-purple crystal bead blank is made up of following weight composition: quartz sand 115 parts, 13.5 parts, zinc oxide, soda ash 39 parts, 25 parts, salt of wormwood, boric acid 13 parts, 4.3 parts, calcium carbonate, 2.9 parts, aluminium hydroxide, salt 1.7 parts, antimonous oxide 1.9 parts, 21 parts, saltpetre, gold trichloride 0.027 part, cerium oxide 1.5 parts and 0.0018 part, potassium permanganate.
The present invention is not limited to above-mentioned preferred forms, anyone other any or akin products identical with the present invention drawn under enlightenment of the present invention, all drops within protection scope of the present invention.
Claims (2)
1. a red-purple crystal bead blank, is characterized in that: this red-purple crystal bead blank is made up of following weight composition: quartz sand 80-160 part, zinc oxide 7-15.5 part, soda ash 27-51 part, salt of wormwood 16-30 part, boric acid 7-16 part, calcium carbonate 2.5-5.5 part, aluminium hydroxide 0.8-3.5 part, salt 1-2 part, antimonous oxide 1.5-3.5 part, saltpetre 12-27 part, gold trichloride 0.01-0.035 part, cerium oxide 1-5 part and potassium permanganate 0.001-0.002 part.
2. prepare a preparation method for red-purple crystal bead blank according to claim 1, it is characterized in that: the method comprises the following steps:
1) extract quartz sand 80-160 part, zinc oxide 7-15.5 part, soda ash 27-51 part, salt of wormwood 16-30 part, boric acid 7-16 part, calcium carbonate 2.5-5.5 part, aluminium hydroxide 0.8-3.5 part, salt 1-2 part, antimonous oxide 1.5-3.5 part, saltpetre 12-27 part, gold trichloride 0.01-0.035 part, cerium oxide 1-5 part and potassium permanganate 0.001-0.002 part by weight ratio to mix;
2) the red-purple crystal bead blank raw material mixed is carried out granulation by tablets press;
3) granular red-purple crystal bead blank raw material will be made put into glass quartz tank furnace and found, when founding, keep strong oxidizing atmosphere and liquation liquid level stabilizing;
4) crystal liquation is molded into red-purple crystal bead blank after the homogenizing cooling of material road;
5) shaping pearl embryo is put into fire and throw stove polishing, integer, uniform coloring, shaping pearl embryo is allowed at the uniform velocity to enter stainless steel pipes, pipe temperature controls at 800 DEG C-900 DEG C, rotating speed 180 revolutions per seconds, in pipeline 5 minutes, pipeline was out just through integer, solid colour, no color differnece, red-purple crystal bead blank without decorative pattern;
Described in the preparation process 3 of red-purple crystal bead blank, when founding, temperature controls at 1380 DEG C-1450 DEG C, and described in the preparation process 4 of red-purple crystal bead blank, cooling temperature controls at 800 DEG C-1000 DEG C.
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| CN106396375B (en) * | 2016-06-15 | 2018-09-25 | 浙江伟兴水晶有限公司 | A kind of crystal bead blank and preparation method thereof of violet color |
| CN108558219A (en) * | 2018-04-18 | 2018-09-21 | 浙江工业大学 | Noctilucent crystal bead blank and preparation method thereof |
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| US5656559A (en) * | 1994-06-23 | 1997-08-12 | Saint-Gobain Vitrage | Clear glass composition intended for the production of panes |
| CN102320747A (en) * | 2011-06-27 | 2012-01-18 | 浙江伟兴水晶有限公司 | Preparation method of shallow crystal and yellow crystal bead blank |
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| CN102837251A (en) * | 2012-09-17 | 2012-12-26 | 江苏锦程集团科技有限公司 | Diamond bead blank fire polishing furnace |
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2015
- 2015-01-06 CN CN201510003836.1A patent/CN104556699B/en active Active
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|---|---|---|---|---|
| US5656559A (en) * | 1994-06-23 | 1997-08-12 | Saint-Gobain Vitrage | Clear glass composition intended for the production of panes |
| CN102320747A (en) * | 2011-06-27 | 2012-01-18 | 浙江伟兴水晶有限公司 | Preparation method of shallow crystal and yellow crystal bead blank |
| CN102372433A (en) * | 2011-10-08 | 2012-03-14 | 浙江伟兴水晶有限公司 | Preparation method of yellow crystal ball blank |
| CN102503126A (en) * | 2011-10-08 | 2012-06-20 | 浙江伟兴水晶有限公司 | Preparation method for smoky yellow crystal bead blanks |
| CN102838277A (en) * | 2012-09-17 | 2012-12-26 | 江苏锦程集团科技有限公司 | Production process of honey peach CZ diamond |
| CN102837251A (en) * | 2012-09-17 | 2012-12-26 | 江苏锦程集团科技有限公司 | Diamond bead blank fire polishing furnace |
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Effective date of registration: 20220215 Address after: 321000 No. 668, Xuecheng East Road, Hanxiang Industrial Park, Tangya Town, Jindong District, Jinhua City, Zhejiang Province Patentee after: Zhejiang xinweixing crystal Co.,Ltd. Address before: 321000 Jindong comprehensive development park, Jinhua City, Zhejiang Province Patentee before: ZHEJIANG WEIXING CRYSTAL Co.,Ltd. |