CN104556697B - A kind of golden yellow crystal bead blank and preparation method thereof - Google Patents
A kind of golden yellow crystal bead blank and preparation method thereof Download PDFInfo
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- CN104556697B CN104556697B CN201510003677.5A CN201510003677A CN104556697B CN 104556697 B CN104556697 B CN 104556697B CN 201510003677 A CN201510003677 A CN 201510003677A CN 104556697 B CN104556697 B CN 104556697B
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Abstract
The invention discloses a kind of golden yellow crystal bead blank and preparation method thereof, this golden yellow crystal bead blank is made up of following weight composition: quartz sand 150-220 part, soda ash 75-95 part, salt of wormwood 21-32 part, boric acid 1-3 part, aluminium hydroxide 2-5 part, salt 1-3.5 part, flour 0.3-0.6 part, sulphur 0.15-0.3 part and iron sulphide 0.001-0.003 part.The redox equilibrium that the present invention's golden yellow crystal bead blank makes cupric ion in melting process when preparing keeps stable, thus obtains good tint permanence; Adopt unleaded raw material, have glossiness good, bright-colored, neat, no color differnece, without decorative pattern, output is high, unleaded pollution-free, greatly reduces production cost, the advantage that productivity effect is good.
Description
Technical field
The present invention relates to a kind of golden yellow crystal bead blank and preparation method thereof.
Background technology
Golden yellow crystal bead blank is used to the work in-process preparing golden yellow crystal product, existing golden yellow crystal bead blank technique adopts crucible manufacture, there is aberration, color is uneven, have decorative pattern, unstable product quality, production efficiency is low, be not suitable for continuous production in enormous quantities, and cause environmental pollution by coal burning.And there is many problems in existing golden yellow crystal bead blank technical recipe, there is colour-change in pearl embryo integer process, cause aberration, i.e. the poor heat stability of color, have plenty of the consumptions such as tinting material sulphur excessive, cause cost too high.
Summary of the invention
It is good that technical problem to be solved by this invention is to provide a kind of color reproduction, and solid colour no color differnece, without decorative pattern, constant product quality, production efficiency is high, can be applicable to the production operation of continuous tank furnace, greatly reduces the golden yellow crystal bead blank of production cost.
For solving the problem, the present invention is achieved through the following technical solutions: a kind of golden yellow crystal bead blank, and this golden yellow crystal bead blank is made up of following weight composition: quartz sand 150-220 part, soda ash 75-95 part, salt of wormwood 21-32 part, boric acid 1-3 part, aluminium hydroxide 2-5 part, salt 1-3.5 part, flour 0.3-0.6 part, sulphur 0.15-0.3 part and iron sulphide 0.001-0.003 part.
Another technical problem to be solved by this invention is to provide a kind of preparation method of golden yellow crystal bead blank,
The present invention is achieved through the following technical solutions: the preparation process of described golden yellow crystal bead blank is as follows:
1) extract quartz sand 150-220 part, soda ash 75-95 part, salt of wormwood 21-32 part, boric acid 1-3 part, aluminium hydroxide 2-5 part, salt 1-3.5 part, flour 0.3-0.6 part, sulphur 0.15-0.3 part and iron sulphide 0.001-0.003 part by weight ratio to mix;
2) the golden yellow crystal bead blank raw material mixed is carried out granulation by tablets press;
3) granular golden yellow crystal bead blank raw material will be made put into glass quartz tank furnace and found, when founding, keep strongly reducing atmosphere and liquation liquid level stabilizing;
4) crystal liquation is molded into golden yellow crystal bead blank after the homogenizing cooling of material road;
5) shaping pearl embryo is put into fire and throw stove polishing, integer, uniform coloring, shaping pearl embryo is allowed at the uniform velocity to enter stainless steel pipes, pipe temperature controls at 800 DEG C-900 DEG C, rotating speed 180 revolutions per seconds, in pipeline 5 minutes, pipeline was out just through integer, solid colour, no color differnece, golden yellow crystal bead blank without decorative pattern.
Further, described in the preparation process 3 of golden yellow crystal bead blank, when founding, temperature controls at 1320 DEG C-1380 DEG C.
Further, described in the preparation process 4 of golden yellow crystal bead blank, cooling temperature controls at 800 DEG C-1000 DEG C.
The beneficial effect of the golden yellow crystal bead blank of the present invention is: the redox equilibrium making cupric ion in melting process time prepared by described golden yellow crystal bead blank keeps stable, thus obtains good tint permanence; Adopt unleaded raw material, have glossiness good, bright-colored, neat, no color differnece, without decorative pattern, output is high, unleaded pollution-free, greatly reduces production cost, the advantage that productivity effect is good.
Embodiment
Following examples for illustration of the present invention, but are not used for limiting the scope of the invention.
Embodiment 1
The golden yellow crystal bead blank of one of the present invention, this golden yellow crystal bead blank is made up of following weight composition: quartz sand 220 parts, soda ash 95 parts, 32 parts, salt of wormwood, boric acid 3 parts, 5 parts, aluminium hydroxide, salt 3.5 parts, 0.6 part, flour, 0.3 part, sulphur and 0.003 part, iron sulphide.
The preparation process of described golden yellow crystal bead blank is as follows:
1) extract quartz sand 220 parts, soda ash 95 parts, 32 parts, salt of wormwood, boric acid 3 parts, 5 parts, aluminium hydroxide, salt 3.5 parts, 0.6 part, flour, 0.3 part, sulphur and 0.003 part, iron sulphide by weight ratio to mix;
2) the golden yellow crystal bead blank raw material mixed is carried out granulation by tablets press;
3) will make granular golden yellow crystal bead blank raw material to put into glass quartz tank furnace and found, keep strongly reducing atmosphere and liquation liquid level stabilizing when founding, glass melting temperature controls at 1320 DEG C-1380 DEG C;
4) crystal liquation is molded into golden yellow crystal bead blank after the homogenizing cooling of material road, cooling temperature controls at 800 DEG C-1000 DEG C;
5) shaping pearl embryo is put into fire and throw stove polishing, integer, uniform coloring, shaping pearl embryo is allowed at the uniform velocity to enter stainless steel pipes, pipe temperature controls at 800 DEG C-900 DEG C, rotating speed 180 revolutions per seconds, in pipeline 5 minutes, pipeline was out just through integer, solid colour, no color differnece, golden yellow crystal bead blank without decorative pattern.
Embodiment 2
Its difference from Example 1 is, this golden yellow crystal bead blank is made up of following weight composition: quartz sand 150 parts, soda ash 75 parts, 21 parts, salt of wormwood, boric acid 1 part, 2 parts, aluminium hydroxide, salt 1 part, 0.3 part, flour, 0.15 part, sulphur and 0.001 part, iron sulphide.
Embodiment 3
Its difference from Example 1 is, this golden yellow crystal bead blank is made up of following weight composition: quartz sand 160 parts, soda ash 80 parts, 23 parts, salt of wormwood, boric acid 1.5 parts, 2.6 parts, aluminium hydroxide, salt 1.4 parts, 0.38 part, flour, 0.17 part, sulphur and 0.002 part, iron sulphide.
Embodiment 4
Its difference from Example 1 is, this golden yellow crystal bead blank is made up of following weight composition: quartz sand 210 parts, soda ash 90 parts, 30 parts, salt of wormwood, boric acid 2.7 parts, 4.3 parts, aluminium hydroxide, salt 3.2 parts, 0.5 part, flour, 0.2 part, sulphur and 0.0027 part, iron sulphide.
Embodiment 5
Its difference from Example 1 is, this golden yellow crystal bead blank is made up of following weight composition: quartz sand 180 parts, soda ash 85 parts, 27 parts, salt of wormwood, boric acid 2 parts, 4 parts, aluminium hydroxide, salt 2 parts, 0.4 part, flour, 0.2 part, sulphur and 0.002 part, iron sulphide.
Embodiment 6
Its difference from Example 1 is, this golden yellow crystal bead blank is made up of following weight composition: quartz sand 195 parts, soda ash 88 parts, 34 parts, salt of wormwood, boric acid 1.9 parts, 3.7 parts, aluminium hydroxide, salt 2.6 parts, 0.46 part, flour, 0.24 part, sulphur and 0.0021 part, iron sulphide.
Embodiment 7
Its difference from Example 1 is, this golden yellow crystal bead blank is made up of following weight composition: quartz sand 165 parts, soda ash 91 parts, 26 parts, salt of wormwood, boric acid 1.4 parts, 2.8 parts, aluminium hydroxide, salt 1.7 parts, 0.33 part, flour, 0.17 part, sulphur and 0.0015 part, iron sulphide.
Embodiment 8
Its difference from Example 1 is, this golden yellow crystal bead blank is made up of following weight composition: quartz sand 205 parts, soda ash 88 parts, 31 parts, salt of wormwood, boric acid 2.1 parts, 4.3 parts, aluminium hydroxide, salt 3.3 parts, 0.52 part, flour, 0.25 part, sulphur and 0.0026 part, iron sulphide.
The present invention is not limited to above-mentioned preferred forms, anyone other any or akin products identical with the present invention drawn under enlightenment of the present invention, all drops within protection scope of the present invention.
Claims (1)
1. a golden yellow crystal bead blank, is characterized in that: be made up of following weight composition: quartz sand 220 parts, soda ash 95 parts, 32 parts, salt of wormwood, boric acid 3 parts, 5 parts, aluminium hydroxide, salt 3.5 parts, 0.6 part, flour, 0.3 part, sulphur and 0.003 part, iron sulphide; The preparation process of described golden yellow crystal bead blank is as follows: 1) extract quartz sand 220 parts, soda ash 95 parts, 32 parts, salt of wormwood, boric acid 3 parts, 5 parts, aluminium hydroxide, salt 3.5 parts, 0.6 part, flour, 0.3 part, sulphur and 0.003 part, iron sulphide by weight ratio and mix; 2) the golden yellow crystal bead blank raw material mixed is carried out granulation by tablets press; 3) will make granular golden yellow crystal bead blank raw material to put into glass quartz tank furnace and found, keep strongly reducing atmosphere and liquation liquid level stabilizing when founding, glass melting temperature controls at 1320 DEG C-1380 DEG C; 4) crystal liquation is molded into golden yellow crystal bead blank after the homogenizing cooling of material road, cooling temperature controls at 800 DEG C-1000 DEG C; 5) shaping pearl embryo is put into fire and throw stove polishing, integer, uniform coloring, shaping pearl embryo is allowed at the uniform velocity to enter stainless steel pipes, pipe temperature controls at 800 DEG C-900 DEG C, rotating speed 180 revolutions per seconds, in pipeline 5 minutes, pipeline was out just through integer, solid colour, no color differnece, golden yellow crystal bead blank without decorative pattern.
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| CN201510003677.5A CN104556697B (en) | 2015-01-06 | 2015-01-06 | A kind of golden yellow crystal bead blank and preparation method thereof |
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| CN201510003677.5A CN104556697B (en) | 2015-01-06 | 2015-01-06 | A kind of golden yellow crystal bead blank and preparation method thereof |
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| CN104556697A CN104556697A (en) | 2015-04-29 |
| CN104556697B true CN104556697B (en) | 2016-03-23 |
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| CN105859136B (en) * | 2016-06-15 | 2018-05-11 | 浙江伟兴水晶有限公司 | A kind of crystal bead blank of amber color and preparation method thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4988376A (en) * | 1989-08-02 | 1991-01-29 | Western Research Institute | Glassification of lead and silica solid waste |
| US5656559A (en) * | 1994-06-23 | 1997-08-12 | Saint-Gobain Vitrage | Clear glass composition intended for the production of panes |
| CN102372433A (en) * | 2011-10-08 | 2012-03-14 | 浙江伟兴水晶有限公司 | Preparation method of yellow crystal ball blank |
| CN102503126A (en) * | 2011-10-08 | 2012-06-20 | 浙江伟兴水晶有限公司 | Preparation method for smoky yellow crystal bead blanks |
| CN102838277A (en) * | 2012-09-17 | 2012-12-26 | 江苏锦程集团科技有限公司 | Production process of honey peach CZ diamond |
| CN102837251A (en) * | 2012-09-17 | 2012-12-26 | 江苏锦程集团科技有限公司 | Diamond bead blank fire polishing furnace |
-
2015
- 2015-01-06 CN CN201510003677.5A patent/CN104556697B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4988376A (en) * | 1989-08-02 | 1991-01-29 | Western Research Institute | Glassification of lead and silica solid waste |
| US5656559A (en) * | 1994-06-23 | 1997-08-12 | Saint-Gobain Vitrage | Clear glass composition intended for the production of panes |
| CN102372433A (en) * | 2011-10-08 | 2012-03-14 | 浙江伟兴水晶有限公司 | Preparation method of yellow crystal ball blank |
| CN102503126A (en) * | 2011-10-08 | 2012-06-20 | 浙江伟兴水晶有限公司 | Preparation method for smoky yellow crystal bead blanks |
| CN102838277A (en) * | 2012-09-17 | 2012-12-26 | 江苏锦程集团科技有限公司 | Production process of honey peach CZ diamond |
| CN102837251A (en) * | 2012-09-17 | 2012-12-26 | 江苏锦程集团科技有限公司 | Diamond bead blank fire polishing furnace |
Non-Patent Citations (1)
| Title |
|---|
| 介绍几种加速玻璃熔化的助熔剂;林元;《建筑材料工业》;19600614(第11期);第33-34页 * |
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Effective date of registration: 20220211 Address after: 321000 No. 668, Xuecheng East Road, Hanxiang Industrial Park, Tangya Town, Jindong District, Jinhua City, Zhejiang Province Patentee after: Zhejiang xinweixing crystal Co.,Ltd. Address before: 321000 Jindong comprehensive development park, Jinhua City, Zhejiang Province Patentee before: ZHEJIANG WEIXING CRYSTAL Co.,Ltd. |