CN106365446A - Light-blue colored crystal bead blank and preparation method thereof - Google Patents
Light-blue colored crystal bead blank and preparation method thereof Download PDFInfo
- Publication number
- CN106365446A CN106365446A CN201610745217.4A CN201610745217A CN106365446A CN 106365446 A CN106365446 A CN 106365446A CN 201610745217 A CN201610745217 A CN 201610745217A CN 106365446 A CN106365446 A CN 106365446A
- Authority
- CN
- China
- Prior art keywords
- parts
- bead blank
- crystal bead
- color crystal
- shallow orchid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B19/00—Other methods of shaping glass
- C03B19/10—Forming beads
- C03B19/1005—Forming solid beads
- C03B19/1035—Forming solid beads by pressing
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B19/00—Other methods of shaping glass
- C03B19/10—Forming beads
- C03B19/1095—Thermal after-treatment of beads, e.g. tempering, crystallisation, annealing
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
- C03C1/002—Use of waste materials, e.g. slags
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
- C03C1/04—Opacifiers, e.g. fluorides or phosphates; Pigments
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C4/00—Compositions for glass with special properties
- C03C4/0028—Compositions for glass with special properties for crystal glass, e.g. lead-free crystal glass
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C4/00—Compositions for glass with special properties
- C03C4/02—Compositions for glass with special properties for coloured glass
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Geochemistry & Mineralogy (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Crystallography & Structural Chemistry (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Glass Compositions (AREA)
Abstract
The invention discloses a light-blue colored crystal bead blank and a preparation method thereof. The light-blue colored crystal bead blank is prepared from the following components in parts by weight: 100 to 300 parts of quartz sand, 100 to 300 parts of flame polishing powder, 100 to 300 parts of sodium carbonate, 150 to 300 parts of glass, 25 to 65 parts of sodium nitrate, 10 to 50 parts of borax decahydrate, 10 to 45 parts of calcium carbonate, 3.5 to 15 parts of table salt, 7 to 25 parts of potassium nitrate and 0.08 to 1.2 parts of cobalt oxide. When the light-blue colored crystal bead blank is prepared, the cobalt oxide is used as a coloring agent, so that the light-blue colored crystal bead blank has a good coloring property; raw materials containing lead are not used, and the light-blue colored crystal bead blank has the advantages of good glossiness, bright color, orderliness, no color difference, no spots, high yield, no lead, no dust pollution, good production benefits and capability of being produced in a large batch; a plurality of recyclable wastes are used as the raw materials, so that the production cost is greatly reduced, and energy source consumption and environmental pollution are also reduced.
Description
Technical field
The present invention relates to a kind of shallow orchid color crystal bead blank and preparation method thereof.
Background technology
Shallow orchid color crystal bead blank is used to prepare the semi-finished product of shallow orchid color crystal product, existing shallow orchid color crystal
Pearl embryo technique adopts crucible manufacture, there is aberration, spottiness, unstable product quality, low production efficiency, is not suitable for continuously big
Batch production, in addition leaded harmful, and burnt with coal and cause environmental pollution.
Content of the invention
The technical problem to be solved is to provide a kind of color reproduction good, solid colour no color differnece, immaculate,
Unleaded, no dust pollution, product quality is stable, and production efficiency is high, can be suitable for the shallow orchid color water of the production operation of continuous tank furnace
Brilliant pearl embryo.
For solving the above problems, the present invention is achieved through the following technical solutions: a kind of shallow orchid color crystal bead blank,
This shallow orchid color crystal bead blank is made up of following weight composition: quartz sand 100-300 part, fiery polishing powder 100-300 part,
Soda 100-300 part, glass 150-300 part, sodium nitrate 25-65 part, borax decahydrate 10-50 part, Calcium Carbonate 10-45 part, Sal
3.5-15 part, potassium nitrate 7-25 part and cobalt oxide 0.08-1.2 part.
Another technical problem to be solved by this invention is to provide a kind of preparation method of shallow orchid color crystal bead blank,
The present invention is achieved through the following technical solutions: the preparation process of described shallow orchid color crystal bead blank is as follows:
1) quartz sand 100-300 part, fiery polishing powder 100-300 part, soda 100-300 part, glass are extracted by weight ratio
150-300 part, sodium nitrate 25-65 part, borax decahydrate 10-50 part, Calcium Carbonate 10-45 part, Sal 3.5-15 part, potassium nitrate 7-25
Part and cobalt oxide 0.08-1.2 part mix homogeneously；
2) the shallow orchid color crystal bead blank raw material of mix homogeneously is carried out pelletize by comminutor；
3) granular shallow orchid color crystal bead blank raw material will be made to put in glass quartz tank furnace and found, put into by several times,
Put into per hour once, when founding, keep oxidizing atmosphere and liquid level of solution stable；
4) crystal solution is molded into after the cooling of material road homogenizing shallow orchid color crystal bead blank；
5) molding pearl embryo is put into fire and throws stove polishing, integer, uniform coloring, during polishing, first allow blank be stained with composite,
Molding pearl embryo is allowed at the uniform velocity to enter stainless steel pipes again, pipe temperature controls at 870 DEG C -1000 DEG C, 150 revolutions per seconds of rotating speed, and pipeline is long
Spend for 7.5 meters, 7 minutes in pipeline；
6) pipeline out enters tank of giving a dinner of welcome, and is exactly out through integer, beautiful, no color differnece, no decorative pattern is shallow from tank of giving a dinner of welcome
Blue color crystal bead blank.
Further, described shallow orchid color crystal bead blank preparation process 3 in, when founding temperature control 1360 DEG C-
1420℃.
Further, in the described preparation process 4 in shallow orchid color crystal bead blank, chilling temperature controls at 870 DEG C -980
℃.
The beneficial effect of the present invention shallow orchid color crystal bead blank is: using oxidation during described shallow orchid color crystal bead blank preparation
Cobalt is coloring agent, thus obtaining good coloring；Do not adopt leaded raw material, it is good to have a glossiness, bright-colored, neat,
No color differnece, immaculate, yield is high, unleaded no dust pollution, and productivity effect is good, the advantage that can be mass；Using much can returning
The waste material received, as raw material, greatly reduces production cost and decreases energy resource consumption and environmental pollution.
Specific embodiment
Following examples are used for the present invention is described, but are not limited to the scope of the present invention.
Embodiment 1
One kind shallow orchid color crystal bead blank of the present invention, this shallow orchid color crystal bead blank is by following weight composition
Composition: 100 parts of quartz sand, fiery 100 parts of polishing powder, 100 parts of soda, 150 parts of glass, 25 parts of sodium nitrate, 10 parts of borax decahydrate, carbonic acid
10 parts of calcium, 3.5 parts of Sal, 7 parts of potassium nitrate and 0.08 part of cobalt oxide.
The preparation process of described shallow orchid color crystal bead blank is as follows:
1) 100 parts of quartz sand, fiery 100 parts of polishing powder, 100 parts of soda, 150 parts of glass, sodium nitrate are extracted by weight ratio
25 parts, 10 parts of borax decahydrate, 10 parts of Calcium Carbonate, 3.5 parts of Sal, 7 parts of potassium nitrate and 0.08 part of mix homogeneously of cobalt oxide；
2) the shallow orchid color crystal bead blank raw material of mix homogeneously is carried out pelletize by comminutor；
3) granular shallow orchid color crystal bead blank raw material will be made to put in glass quartz tank furnace and found, put into by several times,
Put into per hour once, keep oxidizing atmosphere and liquid level of solution to stablize when founding, temperature control is at 1360 DEG C -1420 DEG C；
4) by crystal solution through material road homogenizing cooling after be molded into shallow orchid color crystal bead blank, temperature control 870 DEG C-
980℃；
5) molding pearl embryo is put into fire and throws stove polishing, integer, uniform coloring, during polishing, first allow blank be stained with composite,
Molding pearl embryo is allowed at the uniform velocity to enter stainless steel pipes again, pipe temperature controls at 870 DEG C -1000 DEG C, 150 revolutions per seconds of rotating speed, and pipeline is long
Spend for 7.5 meters, 7 minutes in pipeline；
6) pipeline out enters tank of giving a dinner of welcome, and is exactly out through integer, beautiful, no color differnece, no decorative pattern is shallow from tank of giving a dinner of welcome
Blue color crystal bead blank.
Embodiment 2
Its difference from Example 1 is, this shallow orchid color crystal bead blank is made up of following weight composition:
300 parts of quartz sand, fiery 300 parts of polishing powder, 300 parts of soda, 300 parts of glass, 65 parts of sodium nitrate, 50 parts of borax decahydrate, carbonic acid Ca45
Part, 15 parts of Sal, 25 parts of potassium nitrate and 1.2 parts of cobalt oxide.
Embodiment 3
Its difference from Example 1 is, this shallow orchid color crystal bead blank is made up of following weight composition:
200 parts of quartz sand, fiery 200 parts of polishing powder, 180 parts of soda, 220 parts of glass, 45 parts of sodium nitrate, 30 parts of borax decahydrate, Calcium Carbonate 25
Part, 8 parts of Sal, 17 parts of potassium nitrate and 0.65 part of cobalt oxide.
Embodiment 4
Its difference from Example 1 is, this shallow orchid color crystal bead blank is made up of following weight composition:
112 parts of quartz sand, fiery 135 parts of polishing powder, 121 parts of soda, 166 parts of glass, 28 parts of sodium nitrate, 17 parts of borax decahydrate, Calcium Carbonate 14
Part, 5.1 parts of Sal, 9 parts of potassium nitrate and 0.23 part of cobalt oxide.
Embodiment 5
Its difference from Example 1 is, this shallow orchid color crystal bead blank is made up of following weight composition:
288 parts of quartz sand, fiery 265 parts of polishing powder, 290 parts of soda, 258 parts of glass, 61 parts of sodium nitrate, 44 parts of borax decahydrate, Calcium Carbonate 39
Part, 13 parts of Sal, 22 parts of potassium nitrate and 1 part of cobalt oxide.
Embodiment 6
Its difference from Example 1 is, this shallow orchid color crystal bead blank is made up of following weight composition:
120 parts of quartz sand, fiery 130 parts of polishing powder, 150 parts of soda, 150 parts of glass, 30 parts of sodium nitrate, 33 parts of borax decahydrate, Calcium Carbonate 13
Part, 4 parts of Sal, 11 parts of potassium nitrate and 0.39 part of cobalt oxide.
Embodiment 7
Its difference from Example 1 is, this shallow orchid color crystal bead blank is made up of following weight composition:
177 parts of quartz sand, fiery 234 parts of polishing powder, 251 parts of soda, 199 parts of glass, 46 parts of sodium nitrate, 27 parts of borax decahydrate, Calcium Carbonate 31
Part, 9.3 parts of Sal, 16 parts of potassium nitrate and 0.82 part of cobalt oxide.
Embodiment 8
Its difference from Example 1 is, this shallow orchid color crystal bead blank is made up of following weight composition:
215 parts of quartz sand, fiery 155 parts of polishing powder, 265 parts of soda, 166 parts of glass, 37 parts of sodium nitrate, 25 parts of borax decahydrate, Calcium Carbonate 30
Part, 10 parts of Sal, 15 parts of potassium nitrate and 0.55 part of cobalt oxide.
The present invention is not limited to above-mentioned preferred forms, anyone draw under the enlightenment of the present invention other any with
Product as the present invention is same or like, is within the scope of the present invention.
Claims (4)
1. a kind of shallow orchid color crystal bead blank it is characterised in that: this shallow orchid color crystal bead blank is to be become by following weight
Part composition: quartz sand 100-300 part, fiery polishing powder 100-300 part, soda 100-300 part, glass 150-300 part, sodium nitrate 25-
65 parts, borax decahydrate 10-50 part, Calcium Carbonate 10-45 part, Sal 3.5-15 part, potassium nitrate 7-25 part and cobalt oxide 0.08-1.2
Part.
2. a kind of prepare described in claim 1 shallow orchid color crystal bead blank preparation method it is characterised in that: the method includes
Following steps:
1) quartz sand 100-300 part, fiery polishing powder 100-300 part, soda 100-300 part, glass 150- are extracted by weight ratio
300 parts, sodium nitrate 25-65 part, borax decahydrate 10-50 part, Calcium Carbonate 10-45 part, Sal 3.5-15 part, potassium nitrate 7-25 part and
Cobalt oxide 0.08-1.2 part mix homogeneously；
2) the shallow orchid color crystal bead blank raw material of mix homogeneously is carried out pelletize by comminutor；
3) granular shallow orchid color crystal bead blank raw material will be made to put in glass quartz tank furnace and found, put into by several times, often little
When put into once, keep oxidizing atmosphere and liquid level of solution stable when founding；
4) crystal solution is molded into after the cooling of material road homogenizing shallow orchid color crystal bead blank；
5) molding pearl embryo is put into fire and throw stove polishing, integer, uniform coloring, first allow blank be stained with composite during polishing, then allow
Molding pearl embryo at the uniform velocity enters stainless steel pipes, and pipe temperature controls at 870 DEG C -1000 DEG C, 150 revolutions per seconds of rotating speed, and duct length is
7.5 meters, 7 minutes in pipeline；
6) pipeline out enters tank of giving a dinner of welcome, from tank of giving a dinner of welcome be exactly out through integer, beautiful, no color differnece, no decorative pattern shallow orchid face
Color crystal bead blank.
3. according to claim 2 shallow orchid color crystal bead blank preparation method it is characterised in that: described shallow orchid color water
In the preparation process 3 of brilliant pearl embryo, when founding, temperature control is at 1360 DEG C -1420 DEG C.
4. according to claim 2 shallow orchid color crystal bead blank preparation method it is characterised in that: described shallow orchid color water
In the preparation process 4 of brilliant pearl embryo, chilling temperature controls at 870 DEG C -980 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610745217.4A CN106365446A (en) | 2016-08-29 | 2016-08-29 | Light-blue colored crystal bead blank and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610745217.4A CN106365446A (en) | 2016-08-29 | 2016-08-29 | Light-blue colored crystal bead blank and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106365446A true CN106365446A (en) | 2017-02-01 |
Family
ID=57903634
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610745217.4A Pending CN106365446A (en) | 2016-08-29 | 2016-08-29 | Light-blue colored crystal bead blank and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106365446A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102503127A (en) * | 2011-10-08 | 2012-06-20 | 浙江伟兴水晶有限公司 | Preparation method for light blue crystal bead blanks |
| CN102838277A (en) * | 2012-09-17 | 2012-12-26 | 江苏锦程集团科技有限公司 | Production process of honey peach CZ diamond |
| CN105859136A (en) * | 2016-06-15 | 2016-08-17 | 浙江伟兴水晶有限公司 | Amber crystal bead blank and preparation method thereof |
-
2016
- 2016-08-29 CN CN201610745217.4A patent/CN106365446A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102503127A (en) * | 2011-10-08 | 2012-06-20 | 浙江伟兴水晶有限公司 | Preparation method for light blue crystal bead blanks |
| CN102838277A (en) * | 2012-09-17 | 2012-12-26 | 江苏锦程集团科技有限公司 | Production process of honey peach CZ diamond |
| CN105859136A (en) * | 2016-06-15 | 2016-08-17 | 浙江伟兴水晶有限公司 | Amber crystal bead blank and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 西北轻工业学院主编: "《玻璃工艺学》", 31 January 2000, 中国轻工业出版社 * |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105859136B (en) | A kind of crystal bead blank of amber color and preparation method thereof | |
| CN106278176B (en) | A kind of high-strength ceramic granule and preparation method thereof | |
| CN103922594B (en) | A kind of large red color crystal bead blank and preparation method thereof | |
| CN110922058A (en) | Preparation method for sintering microcrystalline glass plate by using multi-tube distribution | |
| CN104556698B (en) | A kind of cigarette yellow crystal pearl embryo and preparation method thereof | |
| CN108545934B (en) | Iron-titanium-carbon colored medical water-resistant glass | |
| CN104014720A (en) | Quartz sand/fire clay composite alcohol group casting coating and preparation method thereof | |
| CN102503127A (en) | Preparation method for light blue crystal bead blanks | |
| CN104478214B (en) | A kind of pale pink look crystal bead blank and preparation method thereof | |
| CN104496178B (en) | A kind of rose crystal bead blank and preparation method thereof | |
| CN103936282B (en) | A kind of shallow large red color crystal bead blank and preparation method thereof | |
| CN106365446A (en) | Light-blue colored crystal bead blank and preparation method thereof | |
| CN104761207A (en) | High-strength brick and preparation method of high-strength brick | |
| CN104556699B (en) | A kind of red-purple crystal bead blank and preparation method thereof | |
| CN104556696B (en) | A kind of rosy quartz pearl embryo and preparation method thereof | |
| CN103922593B (en) | A kind of deep-red coloration crystal bead blank and preparation method thereof | |
| CN103922592B (en) | A kind of orange color crystal bead blank and preparation method thereof | |
| CN106380074A (en) | Cymbidium sinensis-color crystal ball blank and preparation method thereof | |
| CN104556697B (en) | A kind of golden yellow crystal bead blank and preparation method thereof | |
| CN104496179B (en) | A kind of transparent black crystal ball blank and preparation method thereof | |
| CN106396376A (en) | Capri blue crystal bead rough and preparation method thereof | |
| CN106277780A (en) | A kind of Flos Nelumbinis color purple crystal bead blank and preparation method thereof | |
| CN106082648B (en) | A kind of crystal bead blank of lake water orchid color and preparation method thereof | |
| CN106082643B (en) | A kind of crystal bead blank of black color and preparation method thereof | |
| CN106365447A (en) | Peacock blue crystal bead blank and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170201 |
|
| RJ01 | Rejection of invention patent application after publication |