CN102428973A - Agricultural pesticide with essential oil and application thereof - Google Patents
Agricultural pesticide with essential oil and application thereof Download PDFInfo
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- CN102428973A CN102428973A CN2011103159923A CN201110315992A CN102428973A CN 102428973 A CN102428973 A CN 102428973A CN 2011103159923 A CN2011103159923 A CN 2011103159923A CN 201110315992 A CN201110315992 A CN 201110315992A CN 102428973 A CN102428973 A CN 102428973A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
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Abstract
The invention relates to agricultural pesticide with essential oil and an application thereof. The agricultural pesticide comprises the following components: 5-90% of the essential oil with insecticidal active components, and 5-90% of solvent, 5-90% of pesticide adjuvant. The essential oil is one or mixture made one from wintergreen oil, camphor tree oil, clove oil, peppermint oil, eucalyptus oil, citronella oil or tea tree oil. The solvent is one or a mixture made of formic acid, acetic acid, propionic acid, methyl alcohol, ethyl alcohol or propyl alcohol. The pesticide adjuvant is one or mixture made of dodecyl benzenesulfonic acid, Tween-80, Span-80 (SPAN) or OP-10. The invention has low toxin for animals, safety for environment, efficiency for pests at each life stage and good effects for killing mites and pests. The agricultural pesticide has simple use method and low manufacturing cost, and is suitable for killing the mites and the pests in agriculture and forestry.
Description
Technical field
The invention belongs to technical field of pesticide preparations, be specially the agricultural chemicals and the pesticidal applications thereof that contain plants essential oil.
Background technology
Because losing, the agricultural product that agricultural pest caused reach 15-25% every year; Use chemical pesticide to have certain positive role on a large scale for stablizing farm output, still, because the insecticidal spectrum of chemical pesticide is wide; The field longevity of residure is longer; Bring out insect easily it is developed immunity to drugs, particularly chemical pesticide is to the pollution of agricultural product and environment, causes that the women miscarries, baby's distortion and bring out various diseases such as human cancer.Therefore, use the biopesticide pest control more and more to receive people's attention.Along with the enhancing of human environment protection consciousness, the biopesticide of high-efficiency low-toxicity has become the developing direction of current agricultural chemicals.Biopesticide has mode of action uniqueness, and controlling object is single-minded, and to beneficial organism safety such as natural enemies, consumption is little, and degraded is fast, and is dangerous low to people, animal, ambient wind, is applicable to characteristics such as disease, worm, crop smothering integrated control.1992; World environments once spelt out with the development conference; The sale and the use of inner control chemical pesticide in the world by 2000, the consumption of biopesticide reaches 60%, yet; Biopesticide only accounts for 2% the market share in global agricultural chemicals total sales volume at present, differs greatly with re-set target.Therefore, greatly develop biopesticide and become the great task that countries in the world face jointly.China relevant department proposes 2015, requires the use of biopesticide to account for the 30-50% of agricultural chemicals total amount, and China's biopesticide annual production at present only accounts for about 10% of agricultural chemicals gross yield, applies area and accounts for agricultural chemicals and always use about 12% of area.It is thus clear that the development biopesticide has become one of China's significant problem anxious to be solved.
There is kind surplus the mite class about 500 in China, endanger bigger have 40 surplus kind, be mainly spider mite kind, goitre mite class, crops such as main harm fruit tree, cotton, wheat class, vegetables, tobacco and tea tree, wherein receiving harm the most seriously is mandarin tree, apple tree and cotton.The harmful mite class of agricultural is had characteristics such as volume is little, breeding is fast, adaptability is strong and be prone to develop immunity to drugs, and is one of pest group of the most difficult control of generally acknowledging.The miticide kind accounts for about 10% of insecticide sum at present.Expect 2010, Lepidoptera, nematode, mite, aphid and springtail still are the insects of main control, and the insecticide that is used to prevent and treat above 5 class pests will account for more than 60% of the whole insecticide market share.The mite evil of China takes place the most serious with fruit tree.Wherein the most serious will count mandarin tree, is apple tree secondly, and field crop mainly is a cotton.At present external pesticide development is very fast, because China is large agricultural country, external agricultural chemicals company has an optimistic view of China market, one after another its product is squeezed into China market.From the miticide of current use, though great majority are compounds efficient, low toxicity, also be prone to decompose, most of products are never poisons, and mammiferous toxicity can not be ignored, and environment is also had certain influence, mite is easy to generate pesticide resistance simultaneously.In the long run; Acaricidal development should develop to non-killing livestock property noval chemical compound and biotype compound direction; Minimizing alleviates the pollution to environment to the toxicity of animal, solves the pesticide resistance problem of mite; Therefore it is few, little to the natural enemy injury, to each life stage of evil mite all effectively and be difficult for producing the novel miticide of safety of resistance to develop efficient, long-acting, wide spectrum, environmental pollution, also is the task of top priority.
Plants essential oil is one type of very important natural perfume material, general adopt that physical methods such as distillation, squeezing, extraction (lixiviate) or absorption extract from flower, grass, leaf, branch, skin, root, stem, fruit, seed or the secretion of fragrant plant have certain fragrance and a volatile oily mater.The contained chemical composition more complicated of plants essential oil can be divided into aliphatic, aromatic series and terpene three major types compound and their containing oxygen derivative by the difference of its chemical constitution.Plants essential oil content has Cupressaceae, Magnoliaceae, Lauraceae, Carrot family, Labiatae, composite family, Rutaceae, Zingiber, Myrtaceae, Dipterocarpaceae and grass family etc. than the plant of horn of plenty.Plants essential oil is one type of natural plant additive, has painted, anti-inflammation, effect such as anticorrosion, anti-oxidant, antitumor, can correct the peculiar smell of food, gives fragrance.Therefore, plants essential oil is widely used in the food manufacturing industries such as meat products, fruit and vegetable product, dairy products, aquatic products, baked goods.Plants essential oil also is the important source material of medicine, spices and chemical industry, also is the food additives of using always, antibiotic, anti-oxidant, anti-inflammatory is arranged, shortly oozes, desinsection mosquito repellent and effect such as anticorrosion.Yet so far, the document announcement that is used for plants essential oil pesticide research is also seldom seen, and rarely seenly is used for stifling sterilization expelling parasite and is used for purposes such as the fresh-keeping of grain and storage.
Summary of the invention
To the problems referred to above that exist in the prior art; The objective of the invention is to design provides a kind of low toxicity, no extended residual, environmentally safe, the biopesticide preparation that kills the mite good disinsection effect; Its manufacture process environmental protection, method for using are simple, and consumption is low, is applicable to various crop.
Described a kind of agricultural insecticide that contains plants essential oil and preparation method thereof; It is characterized in that containing active insecticidal components plants essential oil 5-90%; Solvent 5-90%; Insecticides adjuvant 5-90%, described plants essential oil are one or more mixtures of wintergreen, camphor tree oil, caryophyllus oil, peppermint oil, eucalyptus oil, citronella oil or tea oil, and described solvent is for being formic acid, acetate, propionic acid; One or more mixtures of methyl alcohol, ethanol or propyl alcohol, described insecticides adjuvant are one or more mixtures of DBSA, Tween-80, Si Ban-80 (SPAN) or OP-10.
Described plants essential oil content is 20-70%, preferred 20-40%.
Described solvent is 16-65%, preferred 20-50%.
Described insecticides adjuvant content is 5-20%, preferred 10-15%.
The above-mentioned agricultural insecticide that contains plants essential oil can be used as in miticide and the insecticide and uses.
Said worm and mite comprise tetranychid, rice fulgorid, aphid, striped rice borer, paddy stem borer, leaf roll snout moth's larva, Bemisia tabaci, false eye leafhopper, diamond-back moth and cabbage caterpillar.
The present invention is main active with the plants essential oil, and as the auxiliary activity composition solvent of holding concurrently, the preparation that makes is low to animal toxicity with solvent; Environmental compatibility is good; Environmentally safe, all effective and difficult resistance that produces is killed the mite good disinsection effect to each life stage of insect; And method for using is simple, low cost of manufacture, and what be applicable to various crop kills the mite desinsection.
Embodiment
Combine the embodiments of the invention and the test of pesticide effectiveness at present, further specify effect of the present invention, percentage composition is weight percentage in the present specification.
Embodiment 1
In the 1000L agitated reactor, drop into wintergreen 25kg, formic acid 450kg stirs, and after whole dissolvings, slowly drops into 25kg emulsifier DBSA again, stir, finished product wintergreen preparation.
Embodiment 2
In the 1000L agitated reactor, drop into camphor tree oil 250kg, ethanol 200kg stirs, and after whole dissolvings, slowly drops into 50kg emulsifier tween-80 again, stir, finished product camphor tree oil formulation.
Embodiment 3
In the 1000L agitated reactor, drop into caryophyllus oil 450kg, acetate 25kg stirs, and after whole dissolvings, slowly drops into 25kg emulsifier neopelex again, stir, finished product caryophyllus oil preparation.
Embodiment 4
In the 1000L agitated reactor, drop into peppermint oil 25kg, methyl alcohol 25kg stirs, and after whole dissolvings, slowly drops into the 450kg emulsifier op-10 again, stir, the finished product menthence preparation.
Embodiment 5
In the 1000L agitated reactor, drop into eucalyptus oil 100kg, double solvents 325kg (methyl alcohol 125kg+ acetate 200kg) stirring; Composite pesticide auxiliary agent 75kg (Si Ban-80 25kg+ Tween-80 50kg); Stir, finished product tea tree citronella oil composite plant essential oil preparation.
Embodiment 6
In the 1000L agitated reactor, drop into citronella oil 150kg, double solvents 300kg (methyl alcohol 200kg+ acetate 300kg) stirring; Composite pesticide auxiliary agent 50kg (Si Ban-80 20kg+ Tween-80 10kg+OP-1010kg+ DBSA 10kg); Stir, the fragrant lemon composite plant of finished product tea essential oil preparation.
Embodiment 7
In the 1000L agitated reactor, drop into tea oil 350kg, double solvents 80kg (methyl alcohol 20kg+ ethanol 30kg+ formic acid 10kg+ acetate 15kg+ propionic acid 5kg) stirring; Composite pesticide auxiliary agent 70kg (Si Ban-80 50kg+ Tween-80 10kg+OP-105kg+ DBSA 5kg); Stir, the fragrant lemon eucalyptus of finished product tea composite plant essential oil preparation.
Embodiment 8
In the 1000L agitated reactor, drop into plants essential oil 200kg (wintergreen 20kg+ camphor tree oil 30kg+ caryophyllus oil 30kg+ peppermint oil 30kg+ eucalyptus oil 30kg+ citronella oil 30kg+ tea oil 30kg), double solvents 250kg (methyl alcohol 50kg+ ethanol 100kg+ propyl alcohol 50kg+ formic acid 20kg+ acetate 20kg+ propionic acid 10kg) stirring; Composite pesticide auxiliary agent 50kg (Si Ban-80 20kg+ Tween-80 10kg+OP-10 10kg+ DBSA 10kg); Stir, the fragrant lemon eucalyptus of finished product tea composite plant essential oil preparation.
Below through the above-mentioned control efficiency of killing the mite insecticide of test explanation.
Each chemical control tea tree tetranychid result of the test of table 1.
Table 2. control sweet orange spider result of the test (concentration of treatment is essential oil content 750mg/L)
Table 3. control apple result of the test (concentration of treatment is essential oil content 750mg/L)
Table 1-3 data show: embodiment 1-8 all has effect preferably to the tetranychid of control tealeaves, citrus and apple; In the agent of essential oil list; Drug effect order from big to small is: embodiment 7＞embodiment 6＞embodiment 5＞embodiment 4＞embodiment 3＞embodiment 2＞embodiment 1, same preparation to the drug effect order from big to small of 3 kinds of tetranychids is: tealeaves＞citrus＞apple.
Embodiment 1-8 extension rate is advisable with activity component concentration 500-1000mg/L.
Table 4. control tealeaves (wild cabbage) aphid result of the test
Table 4 data show: embodiment 1-8 all has effect preferably to control tealeaves and cabbage aphid; The control efficiency of embodiment 1-8 does not have significant difference; Also do not have significant difference with commercially available medicine 10% Imidacloprid, promptly the effect of embodiment 1-8 and commercially available medicine 10% Imidacloprid is suitable.Same preparation to the drug effect order from big to small of 2 kinds of aphids is: tealeaves＞wild cabbage.Embodiment 1-8 extension rate is advisable with activity component concentration 750mg/L.
Table 5 embodiment 1-8 prevents and treats tealeaves false eye leafhopper effect (essential oil concentration 500mg/L)
The result of the test of table 5 shows that embodiment 1-8 has higher control efficiency to the false eye leafhopper insect at activity component concentration 500mg/L.Wherein, the best results of embodiment 4, embodiment 1-8 extension rate is advisable with activity component concentration 500mg/L.
Table 6 embodiment 1-8 prevents and treats wild cabbage diamond-back moth effect (essential oil concentration 500mg/L)
| Embodiment | 3 days schools behind the medicine | 7 days schools behind the medicine | Proofreaied and correct in 15 days behind the medicine |
| Positive preventive effect (%) | Positive preventive effect (%) | Preventive effect (%) | |
| Embodiment 1 | 81.5 | 87.6 | 80.3 |
| Embodiment 2 | 82.7 | 89.0 | 82.6 |
| Embodiment 3 | 85.4 | 91.3 | 84.5 |
| Embodiment 4 | 87.0 | 95.0 | 88.0 |
| Embodiment 5 | 75.6 | 82.3 | 73.6 |
| Embodiment 6 | 72.7 | 85.6 | 78.9 |
| Embodiment 7 | 78.5 | 82.0 | 81.3 |
| Embodiment 8 | 78.0 | 87.6 | 82.1 |
| 5% presses down 800 times of hooligan's missible oil | 69.8 | 75.8 | 73.6 |
Table 7 embodiment 1-8 prevents and treats cabbage pieris effect (essential oil concentration 500mg/L)
Table 8 embodiment 1-8 prevents and treats wild cabbage Bemisia tabaci effect (essential oil concentration 500mg/L)
The result of the test of table 6-8 shows that embodiment 1-8 has higher control efficiency to pest such as Bemisia tabaci, diamond-back moth, cabbage caterpillars at activity component concentration 500mg/L.Wherein, embodiment 4 the bests.
Table 9 embodiment 1-8 prevents and treats rice hoppers effect (essential oil concentration 750mg/L)
Table 10 embodiment 1-8 prevents and treats rice-stem borer effect (essential oil concentration 750mg/L)
Table 11 embodiment 1-8 prevents and treats paddy rice paddy stem borer effect (essential oil concentration 750mg/L)
Table 12 embodiment 1-8 prevents and treats rice leaf roll snout moth's larva effect (essential oil concentration 750mg/L)
The result of the test of table 9-12 shows that embodiment 1-8 has higher control efficiency to rice grubs such as rice fulgorid, striped rice borer, paddy stem borer, leaf roll snout moth's larvas at activity component concentration 750mg/L.Wherein, Different embodiment among the embodiment 1-8, same embodiment all show the insecticidal activity of different sizes to different insects; In the process of actual production and agricultural chemicals use, can reach the purpose of controlling above insect fully through the formulation (active constituent content) of adjustment agricultural chemicals and the multiple of dilution use.
Claims (6)
1. agricultural insecticide that contains plants essential oil; It is characterized in that containing the plants essential oil 5-90% of active insecticidal components; Solvent 5-90%; Insecticides adjuvant 5-90%, described plants essential oil are one or more mixtures of wintergreen, camphor tree oil, caryophyllus oil, peppermint oil, eucalyptus oil, citronella oil or tea oil, and described solvent is for being formic acid, acetate, propionic acid; One or more mixtures of methyl alcohol, ethanol or propyl alcohol, described insecticides adjuvant are one or more mixtures of DBSA, Tween-80, Si Ban-80 (SPAN) or OP-10.
2. like right 1 described a kind of agricultural insecticide that contains plants essential oil, it is characterized in that described plants essential oil content is 20-70%, be preferably 20-40%.
3. like right 1 described a kind of agricultural insecticide that contains plants essential oil, it is characterized in that described solvent is 16-65%, is preferably 20-50%.
4. like right 1 described a kind of agricultural insecticide that contains plants essential oil, it is characterized in that described insecticides adjuvant content is 5-20%, be preferably 10-15%.
5. like right 1 described a kind of agricultural insecticide that contains plants essential oil, it is characterized in that this agricultural insecticide is as the application in miticide and the insecticide.
6. like right 5 described a kind of agricultural insecticides that contain plants essential oil, it is characterized in that described worm and mite comprise tetranychid, rice fulgorid, aphid, striped rice borer, paddy stem borer, leaf roll snout moth's larva, Bemisia tabaci, false eye leafhopper, diamond-back moth and cabbage caterpillar.
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| CN103636690A (en) * | 2013-12-20 | 2014-03-19 | 重庆华宇园林股份有限公司 | Novel insecticide formula for landscape plants |
| CN103689006A (en) * | 2014-01-06 | 2014-04-02 | 清流县鸿翔农庄农业发展有限公司 | Method for preventing gerbera jamesonii bolus pests by melaleuca ahemifolia oil |
| CN103718815A (en) * | 2014-01-06 | 2014-04-16 | 清流县鸿翔农庄农业发展有限公司 | Biological pest control method for gerbera jamesonii bolus |
| CN104304331A (en) * | 2014-11-19 | 2015-01-28 | 李�杰 | Pesticide composite for killing rice planthopper and preparing method of pesticide composite |
| CN104673496A (en) * | 2015-02-12 | 2015-06-03 | 中国农业科学院兰州畜牧与兽药研究所 | Rhododendron nivale Hook. f. volatile oil and application thereof |
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| CN105123780A (en) * | 2015-08-24 | 2015-12-09 | 湖南中烟工业有限责任公司 | Botanical composition for controlling bemisiatabaci, botanical pesticide thereof, and application of botanical pesticide |
| CN105613606A (en) * | 2016-03-23 | 2016-06-01 | 国际竹藤中心 | Plant-source aphicide prepared from Cinnamomum camphora (L.) Presl. essential oil |
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| CN107156190A (en) * | 2017-05-10 | 2017-09-15 | 广西南宁黑泥巴农业科技有限公司 | A kind of botanical pesticide synergistic composition |
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| CN107212027A (en) * | 2017-05-10 | 2017-09-29 | 南宁为辰科技有限公司 | A kind of pesticide synergistic composition of leaf essential oil containing camphor tree and chlorfenapyr |
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