CN113841711A - Method for using mixture of biological preparation containing eucalyptus globulus oil and biological insecticide - Google Patents
Method for using mixture of biological preparation containing eucalyptus globulus oil and biological insecticide Download PDFInfo
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- 239000000294 eucalyptus globulus labille leaf/twig oil Substances 0.000 title claims abstract description 34
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 239000000203 mixture Substances 0.000 title claims description 23
- 238000000034 method Methods 0.000 title claims description 12
- 239000002917 insecticide Substances 0.000 title description 2
- QSOHVSNIQHGFJU-UHFFFAOYSA-L thiosultap disodium Chemical compound [Na+].[Na+].[O-]S(=O)(=O)SCC(N(C)C)CSS([O-])(=O)=O QSOHVSNIQHGFJU-UHFFFAOYSA-L 0.000 claims abstract description 29
- 244000166124 Eucalyptus globulus Species 0.000 claims abstract description 26
- 235000004692 Eucalyptus globulus Nutrition 0.000 claims abstract description 26
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims abstract description 24
- 150000003839 salts Chemical class 0.000 claims abstract description 24
- JSYPRLVDJYQMAI-ODZAUARKSA-N (z)-but-2-enedioic acid;prop-2-enoic acid Chemical compound OC(=O)C=C.OC(=O)\C=C/C(O)=O JSYPRLVDJYQMAI-ODZAUARKSA-N 0.000 claims abstract description 21
- 229920002126 Acrylic acid copolymer Polymers 0.000 claims abstract description 21
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims abstract description 21
- 229920000142 Sodium polycarboxylate Polymers 0.000 claims abstract description 21
- -1 succinate sulfonic acid sodium salt Chemical class 0.000 claims abstract description 21
- 150000001875 compounds Chemical class 0.000 claims abstract description 13
- 241000426497 Chilo suppressalis Species 0.000 claims abstract description 12
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims abstract description 12
- 235000017557 sodium bicarbonate Nutrition 0.000 claims abstract description 12
- 235000019333 sodium laurylsulphate Nutrition 0.000 claims description 20
- 239000004480 active ingredient Substances 0.000 claims description 19
- 235000007164 Oryza sativa Nutrition 0.000 claims description 8
- 235000009566 rice Nutrition 0.000 claims description 8
- 241000607479 Yersinia pestis Species 0.000 claims description 6
- 239000011173 biocomposite Substances 0.000 claims description 4
- 238000004821 distillation Methods 0.000 claims description 4
- 238000009472 formulation Methods 0.000 claims description 4
- 230000008569 process Effects 0.000 claims description 2
- 241000404037 Eucalyptus urophylla Species 0.000 claims 3
- 240000007594 Oryza sativa Species 0.000 claims 1
- 230000002147 killing effect Effects 0.000 abstract description 6
- 230000002195 synergetic effect Effects 0.000 abstract description 4
- 239000003814 drug Substances 0.000 description 23
- 239000003921 oil Substances 0.000 description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 16
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 description 9
- 241000209094 Oryza Species 0.000 description 7
- 230000000694 effects Effects 0.000 description 3
- 239000000575 pesticide Substances 0.000 description 3
- 239000007921 spray Substances 0.000 description 3
- WEEGYLXZBRQIMU-UHFFFAOYSA-N 1,8-cineole Natural products C1CC2CCC1(C)OC2(C)C WEEGYLXZBRQIMU-UHFFFAOYSA-N 0.000 description 2
- WEEGYLXZBRQIMU-WAAGHKOSSA-N Eucalyptol Chemical compound C1C[C@H]2CC[C@]1(C)OC2(C)C WEEGYLXZBRQIMU-WAAGHKOSSA-N 0.000 description 2
- FWKQNCXZGNBPFD-UHFFFAOYSA-N Guaiazulene Chemical compound CC(C)C1=CC=C(C)C2=CC=C(C)C2=C1 FWKQNCXZGNBPFD-UHFFFAOYSA-N 0.000 description 2
- 241000238631 Hexapoda Species 0.000 description 2
- UAHWPYUMFXYFJY-UHFFFAOYSA-N beta-myrcene Chemical compound CC(C)=CCCC(=C)C=C UAHWPYUMFXYFJY-UHFFFAOYSA-N 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 229960005233 cineole Drugs 0.000 description 2
- 230000000749 insecticidal effect Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000009885 systemic effect Effects 0.000 description 2
- 239000001169 1-methyl-4-propan-2-ylcyclohexa-1,4-diene Substances 0.000 description 1
- 239000002028 Biomass Substances 0.000 description 1
- 239000005886 Chlorantraniliprole Substances 0.000 description 1
- 206010059866 Drug resistance Diseases 0.000 description 1
- 208000004232 Enteritis Diseases 0.000 description 1
- 239000005901 Flubendiamide Substances 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- 206010024453 Ligament sprain Diseases 0.000 description 1
- 206010035664 Pneumonia Diseases 0.000 description 1
- 206010037597 Pyelonephritis acute Diseases 0.000 description 1
- 206010037601 Pyelonephritis chronic Diseases 0.000 description 1
- 206010057190 Respiratory tract infections Diseases 0.000 description 1
- 208000010040 Sprains and Strains Diseases 0.000 description 1
- 206010046306 Upper respiratory tract infection Diseases 0.000 description 1
- 230000001154 acute effect Effects 0.000 description 1
- 201000001555 acute pyelonephritis Diseases 0.000 description 1
- 239000002386 air freshener Substances 0.000 description 1
- VYBREYKSZAROCT-UHFFFAOYSA-N alpha-myrcene Natural products CC(=C)CCCC(=C)C=C VYBREYKSZAROCT-UHFFFAOYSA-N 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 206010006451 bronchitis Diseases 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 229940112822 chewing gum Drugs 0.000 description 1
- 235000015218 chewing gum Nutrition 0.000 description 1
- PSOVNZZNOMJUBI-UHFFFAOYSA-N chlorantraniliprole Chemical compound CNC(=O)C1=CC(Cl)=CC(C)=C1NC(=O)C1=CC(Br)=NN1C1=NC=CC=C1Cl PSOVNZZNOMJUBI-UHFFFAOYSA-N 0.000 description 1
- 201000006368 chronic pyelonephritis Diseases 0.000 description 1
- 244000038559 crop plants Species 0.000 description 1
- 238000012258 culturing Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000003467 diminishing effect Effects 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 208000001848 dysentery Diseases 0.000 description 1
- 210000005069 ears Anatomy 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- ZGNITFSDLCMLGI-UHFFFAOYSA-N flubendiamide Chemical compound CC1=CC(C(F)(C(F)(F)F)C(F)(F)F)=CC=C1NC(=O)C1=CC=CC(I)=C1C(=O)NC(C)(C)CS(C)(=O)=O ZGNITFSDLCMLGI-UHFFFAOYSA-N 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 229960002350 guaiazulen Drugs 0.000 description 1
- 238000003306 harvesting Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 206010022000 influenza Diseases 0.000 description 1
- PHTQWCKDNZKARW-UHFFFAOYSA-N isoamylol Chemical compound CC(C)CCO PHTQWCKDNZKARW-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 208000004296 neuralgia Diseases 0.000 description 1
- 239000000825 pharmaceutical preparation Substances 0.000 description 1
- 229940127557 pharmaceutical product Drugs 0.000 description 1
- 150000007875 phellandrene derivatives Chemical class 0.000 description 1
- NAYYNDKKHOIIOD-UHFFFAOYSA-N phthalamide Chemical compound NC(=O)C1=CC=CC=C1C(N)=O NAYYNDKKHOIIOD-UHFFFAOYSA-N 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 208000020029 respiratory tract infectious disease Diseases 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000001256 steam distillation Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- KDYFGRWQOYBRFD-UHFFFAOYSA-L succinate(2-) Chemical compound [O-]C(=O)CCC([O-])=O KDYFGRWQOYBRFD-UHFFFAOYSA-L 0.000 description 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
- 229930006978 terpinene Natural products 0.000 description 1
- 150000003507 terpinene derivatives Chemical class 0.000 description 1
- 229940034610 toothpaste Drugs 0.000 description 1
- 239000000606 toothpaste Substances 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01G—HORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
- A01G13/00—Protecting plants
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N41/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom
- A01N41/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom containing a sulfur-to-oxygen double bond
- A01N41/04—Sulfonic acids; Derivatives thereof
- A01N41/08—Sulfonic acid halides; alpha-Hydroxy-sulfonic acids; Amino-sulfonic acids; Thiosulfonic acids; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/28—Myrtaceae [Myrtle family], e.g. teatree or clove
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Environmental Sciences (AREA)
- Wood Science & Technology (AREA)
- Agronomy & Crop Science (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Zoology (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Botany (AREA)
- Toxicology (AREA)
- Pest Control & Pesticides (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a biological compound preparation containing eucalyptus globulus oil and a preparation method thereof, which comprises 0.01-100 parts by weight of eucalyptus globulus oil, 0.01-100 parts by weight of dimehypo, 0.5-20 parts by weight of sodium polycarboxylate, 4.5-20 parts by weight of maleic acid-acrylic acid copolymer salt, 0.5-20 parts by weight of dialkyl succinate sulfonic acid sodium salt, 1-20 parts by weight of sodium dodecyl sulfate and 10-20 parts by weight of sodium bicarbonate. The biological compound preparation containing the eucalyptus globulus tail oil has a synergistic killing effect, and is particularly suitable for killing rice stem borers.
Description
Technical Field
The invention relates to the field of agricultural application, and in particular relates to a biological compound preparation containing eucalyptus globulus tail oil and a using method thereof.
Background
Rice is a main food crop for human, and is planted in all countries in the world and has a wide area. The rice stem borer is one of important insect pests of rice, and can damage the tillering stage, the booting stage and the heading stage of the rice to cause withered seedlings, withered sheaths, withered booting or white ears, thereby causing yield reduction and even no harvest. Because the chilo suppressalis is a boring pest, it is very important to control the key control period, and farmers generally begin to spray pesticide only when the chilo suppressalis is withered or withered, which requires that the pesticide has stronger systemic property. In recent years, reports on the resistance of chilo suppressalis to more and more drugs are on the rise. After being popularized on the market, the chlorantraniliprole and the flubendiamide medicaments become main medicaments for preventing and treating the rice stem borer. The phthalic diamide medicament has high activity and strong killing effect and has certain osmosis; however, the traditional Chinese medicine composition has the defects of low dead insect speed and easy generation of drug resistance, so that the traditional Chinese medicine composition needs to be mixed with a medicament with good quick-acting property and strong systemic property to enhance the effect and delay the resistance.
Eucalyptus globulus Labill, whose bark is grayish blue, exfoliates and has slightly arrises; in China, it is distributed in Guangxi, Yunnan and Sichuan provinces, and the north most can be found in Chengdu and Han. The Eucalyptus globulus Labill leaf and fruit can be used as medicine, has effects of invigorating stomach, relieving neuralgia, treating rheumatism, sprain, and diminishing inflammation, and can be used for preventing influenza, and treating upper respiratory infection, pharyngolaryngitis, bronchitis, pneumonia, acute and chronic pyelonephritis, enteritis, dysentery, etc.
The eucalyptus globulus oil is colorless to yellow liquid at normal temperature, the relative density is 0.906-0.925, the refractive index is 1.459-1.467, and the effective components of the eucalyptus globulus oil are mainly volatile oil, such as eucalyptol, phellandrene, terpinene, pinene, isoamylol and the like. The Eucalyptus globulus Labill oil has bactericidal effect, can be widely used in pharmaceutical products, and can also be used in essence such as chewing gum, toothpaste, gargle and air freshener, and has the main functions of perfuming and sterilizing. At present, eucalyptus globulus oil is mainly prepared by steam distillation of eucalyptus globulus branches and leaves, and byproducts (namely distillation residual oil, namely eucalyptus globulus tail oil in application) in the production process mainly contain guaiazulene, myrcene, eucalyptol and the like; most of these byproducts are discarded or used as biomass fuel, and cannot be fully utilized.
Disclosure of Invention
In view of the above problems, in one aspect, the present invention provides a bio-composite preparation containing eucalyptus globulus tail oil, which has a synergistic effect of killing rice stem borer.
A biological compound preparation containing eucalyptus globulus oil comprises:
0.01-100 parts of eucalyptus globulus oil, 0.01-100 parts of dimehypo, 0.5-20 parts of sodium polycarboxylate, 4.5-20 parts of maleic acid-acrylic acid copolymer salt, 0.5-20 parts of dialkyl succinate sulfonic acid sodium salt, 1-20 parts of sodium dodecyl sulfate and 10-20 parts of sodium bicarbonate.
In one or more specific embodiments herein, the eucalyptus globulus oil is 0.1 to 10 parts by weight, the dimehypo 0.1 to 10 parts by weight, the sodium polycarboxylate salt 0.5 parts by weight, the maleic acid-acrylic acid copolymer salt 4.5 parts by weight, the dialkyl succinate sulfonic acid sodium salt 0.5 parts by weight, the sodium lauryl sulfate 1 part by weight, and the sodium bicarbonate 10 parts by weight.
In one or more specific embodiments herein, the eucalyptus globulus oil is a distillation residue in a process for producing eucalyptus globulus oil.
In one aspect, the invention also provides a use method of the biological compound preparation containing the eucalyptus globulus oil.
The application method of the biological compound preparation containing the eucalyptus globulus tailing oil comprises the step of spraying the biological compound preparation containing the eucalyptus globulus tailing oil on crops to kill pests of the crops.
In one or more specific embodiments of the present application, the crop plant is rice.
In one or more specific embodiments of the present application, the crop pest is chilo suppressalis.
In one or more specific embodiments of the present application, the application amount of the eucalyptus globulus oil-containing biocomposite formulation is 0.1 to 200 g/acre on an active ingredient basis.
The invention principle and the beneficial effects of the application are as follows:
the invention discloses a biological compound preparation prepared by mixing bisultap and eucalyptus globulus tail oil, and surprisingly discovers that a synergistic effect of killing rice stem borers is achieved.
Detailed Description
The present invention will be further explained below.
The examples provided herein are merely to further illustrate the invention and should not be construed as limiting the invention in any way.
It will be apparent to those skilled in the art that the materials and methods of operation used in the present invention are well known in the art, unless otherwise specified, in the following.
In the present invention, parts by weight means measured in units of weight, such as 1 part by weight means: when the weight is Kg, 1 part by weight means 1 Kg; when the weight is g, 1 part by weight means 1g, and the like, and is not limited to a specific Kg or g.
In the application, the active ingredients are bisultap and eucalyptus globulus oil,
in the following examples, dimehypo, sodium polycarboxylate salts, maleic acid-acrylic acid copolymer salts, sodium salt of dialkyl succinate sulfonate, sodium lauryl sulfate and sodium bicarbonate were all commercially available, and eucalyptus globulus oil was the distillation residue oil in the production of eucalyptus globulus oil and was obtained from the eucalyptus globulus oil manufacturer.
Example 1
Taking 10 parts by weight of dimehypo, 0.1 part by weight of eucalyptus globulus tailing oil, 0.5 part by weight of sodium polycarboxylate, 4.5 parts by weight of maleic acid-acrylic acid copolymer salt, 0.5 part by weight of dialkyl succinate sulfonic acid sodium salt, 1 part by weight of sodium dodecyl sulfate and 10 parts by weight of sodium bicarbonate, uniformly mixing, adding the mixture into water, and preparing the medicament 1 with 10ppm of active ingredients of dimehypo and 0.1ppm of eucalyptus globulus tailing oil for later use.
Example 2
Taking 10 parts by weight of dimehypo, 0.5 part by weight of sodium polycarboxylate, 4.5 parts by weight of maleic acid-acrylic acid copolymer salt, 0.5 part by weight of dialkyl succinate sulfonic acid sodium salt, 1 part by weight of sodium dodecyl sulfate and 10 parts by weight of sodium bicarbonate, uniformly mixing, adding the mixture into water, and preparing the medicament 2 with 10ppm of active ingredient dimehypo for later use.
Example 3
Taking 0.1 part by weight of eucalyptus globulus oil, 0.5 part by weight of sodium polycarboxylate, 4.5 parts by weight of maleic acid-acrylic acid copolymer salt, 0.5 part by weight of dialkyl succinate sulfonic acid sodium salt, 1 part by weight of sodium dodecyl sulfate and 10 parts by weight of sodium bicarbonate, uniformly mixing, adding the mixture into water, and preparing a medicament 3 with 0.1ppm of eucalyptus globulus oil as an active ingredient for later use.
Example 4
8 parts by weight of dimehypo, 0.4 part by weight of eucalyptus globulus labill tail oil, 0.5 part by weight of sodium polycarboxylate, 4.5 parts by weight of maleic acid-acrylic acid copolymer salt, 0.5 part by weight of dialkyl succinate sulfonic acid sodium salt, 1 part by weight of sodium dodecyl sulfate and 10 parts by weight of sodium bicarbonate are taken and uniformly mixed, and the mixture is added into water to prepare a medicament 4 with 10ppm of dimehypo and 1ppm of eucalyptus globulus labill tail oil as active ingredients for standby.
Example 5
8 parts by weight of dimehypo, 0.5 part by weight of sodium polycarboxylate, 4.5 parts by weight of maleic acid-acrylic acid copolymer salt, 0.5 part by weight of dialkyl succinate sulfonic acid sodium salt, 1 part by weight of sodium dodecyl sulfate and 10 parts by weight of sodium bicarbonate are taken and uniformly mixed, and the mixture is added into water to prepare a medicament 5 with 10ppm of active ingredient dimehypo for standby.
Example 6
Taking 0.4 weight part of eucalyptus globulus oil, 0.5 weight part of sodium polycarboxylate, 4.5 weight parts of maleic acid-acrylic acid copolymer salt, 0.5 weight part of dialkyl succinate sulfonic acid sodium salt, 1 weight part of sodium dodecyl sulfate and 10 weight parts of sodium bicarbonate, uniformly mixing, adding the mixture into water, and preparing a medicament 6 with 1ppm of eucalyptus globulus oil as an active ingredient for later use.
Example 7
Taking 4 parts by weight of dimehypo, 4 parts by weight of eucalyptus globulus labill tail oil, 0.5 part by weight of sodium polycarboxylate, 4.5 parts by weight of maleic acid-acrylic acid copolymer salt, 0.5 part by weight of dialkyl succinate sulfonic acid sodium salt, 1 part by weight of sodium dodecyl sulfate and 10 parts by weight of sodium bicarbonate, uniformly mixing, adding the mixture into water, and preparing a medicament 7 with 10ppm of active ingredients of dimehypo and 5ppm of eucalyptus globulus labill tail oil for later use.
Example 8
Taking 4 parts by weight of dimehypo, 0.5 part by weight of sodium polycarboxylate, 4.5 parts by weight of maleic acid-acrylic acid copolymer salt, 0.5 part by weight of dialkyl succinate sulfonic acid sodium salt, 1 part by weight of sodium dodecyl sulfate and 10 parts by weight of sodium bicarbonate, uniformly mixing, adding the mixture into water, and preparing the medicament 8 with 10ppm of active ingredient dimehypo for later use.
Example 9
Taking 4 parts by weight of eucalyptus globulus tailing oil, 0.5 part by weight of sodium polycarboxylate, 4.5 parts by weight of maleic acid-acrylic acid copolymer salt, 0.5 part by weight of dialkyl succinate sulfonic acid sodium salt, 1 part by weight of sodium dodecyl sulfate and 10 parts by weight of sodium bicarbonate, uniformly mixing, adding the mixture into water, and preparing a medicament 9 with 5ppm of eucalyptus globulus tailing oil as an active ingredient for later use.
Example 10
0.4 part by weight of dimehypo, 8 parts by weight of eucalyptus globulus labill tail oil, 0.5 part by weight of sodium polycarboxylate, 4.5 parts by weight of maleic acid-acrylic acid copolymer salt, 0.5 part by weight of dialkyl succinate sulfonic acid sodium salt, 1 part by weight of sodium dodecyl sulfate and 10 parts by weight of sodium bicarbonate are taken and uniformly mixed, and the mixture is added into water to prepare a medicament 10 with 1ppm of dimehypo and 10ppm of eucalyptus globulus labill tail oil as active ingredients for standby.
Example 11
0.4 part by weight of dimehypo, 0.5 part by weight of sodium polycarboxylate, 4.5 parts by weight of maleic acid-acrylic acid copolymer salt, 0.5 part by weight of dialkyl succinate sulfonic acid sodium salt, 1 part by weight of sodium dodecyl sulfate and 10 parts by weight of sodium bicarbonate are taken and uniformly mixed, and the mixture is added into water to prepare a medicament 11 with 1ppm of active ingredient dimehypo for standby.
Example 12
Taking 8 parts by weight of eucalyptus globulus oil, 0.5 part by weight of sodium polycarboxylate, 4.5 parts by weight of maleic acid-acrylic acid copolymer salt, 0.5 part by weight of dialkyl succinate sulfonic acid sodium salt, 1 part by weight of sodium dodecyl sulfate and 10 parts by weight of sodium bicarbonate, uniformly mixing, adding the mixture into water, and preparing a medicament 12 with 10ppm of eucalyptus globulus oil as an active ingredient for later use.
Example 13
0.1 part by weight of dimehypo, 10 parts by weight of eucalyptus globulus tailing oil, 0.5 part by weight of sodium polycarboxylate, 4.5 parts by weight of maleic acid-acrylic acid copolymer salt, 0.5 part by weight of dialkyl succinate sulfonic acid sodium salt, 1 part by weight of sodium dodecyl sulfate and 10 parts by weight of sodium bicarbonate are taken and uniformly mixed, and the mixture is added into water to prepare a medicament 13 with 0.1ppm of dimehypo and 10ppm of eucalyptus globulus tailing oil as active ingredients for later use.
Example 14
0.1 part by weight of dimehypo, 0.5 part by weight of sodium polycarboxylate, 4.5 parts by weight of maleic acid-acrylic acid copolymer salt, 0.5 part by weight of dialkyl succinate sulfonic acid sodium salt, 1 part by weight of sodium dodecyl sulfate and 10 parts by weight of sodium bicarbonate are taken and uniformly mixed, and the mixture is added into water to prepare a medicament 14 with 0.1ppm of active ingredient dimehypo for standby.
Example 15
Taking 10 parts by weight of eucalyptus globulus oil, 0.5 part by weight of sodium polycarboxylate, 4.5 parts by weight of maleic acid-acrylic acid copolymer salt, 0.5 part by weight of dialkyl succinate sulfonic acid sodium salt, 1 part by weight of sodium dodecyl sulfate and 10 parts by weight of sodium bicarbonate, uniformly mixing, adding the mixture into water, and preparing a medicament 15 with 10ppm of eucalyptus globulus oil as an active ingredient for later use.
Example 16
Transplanting 2-3 weeks old rice seedlings into trays with length, width and height of 100cm × 100cm × 20cm, and culturing conventionally. When the rice seedlings grow to 6-8 true leaf stages, 50 rice chilo suppressalis larvae are inoculated to each tray, and then the pesticide 1-15 and pure water (as blank control) are respectively sprayed. Wherein each agent is a treatment, which is repeated 3 times per treatment. The spray rate was consistent from treatment to treatment (the spray rate equates to about 300 liters per hectare). After 7 days of each treatment, the mortality was investigated and finally calculated (3 replicates were taken as an average), and the results are shown in table 1 below, where in table 1 the theoretical insecticidal rate is the insecticidal rate calculated using the Colby formula.
TABLE 1
As can be seen from Table 1, the active ingredient bisultap and the eucalyptus globulus tail oil are mixed to have a synergistic killing effect on chilo suppressalis of rice.
The above description is only a preferred embodiment of the present invention and is not intended to limit the present invention, and various modifications and changes may be made by those skilled in the art. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (7)
1. A biological compound preparation containing eucalyptus globulus oil comprises:
0.01-100 parts of eucalyptus globulus oil, 0.01-100 parts of dimehypo, 0.5-20 parts of sodium polycarboxylate, 4.5-20 parts of maleic acid-acrylic acid copolymer salt, 0.5-20 parts of dialkyl succinate sulfonic acid sodium salt, 1-20 parts of sodium dodecyl sulfate and 10-20 parts of sodium bicarbonate.
2. The bio-composite preparation containing eucalyptus globulus oil as set forth in claim 1, wherein the eucalyptus globulus oil is 0.1 to 10 parts by weight, dimehypo 0.1 to 10 parts by weight, a sodium polycarboxylate salt 0.5 part by weight, a maleic acid-acrylic acid copolymer salt 4.5 parts by weight, a dialkyl succinate sulfonic acid sodium salt 0.5 part by weight, sodium lauryl sulfate 1 part by weight, and sodium hydrogen carbonate 10 parts by weight.
3. The bio-composite formulation comprising eucalyptus urophylla oil according to claim 1 or 2, wherein said eucalyptus urophylla oil is distillation residue oil in the process of producing eucalyptus urophylla oil.
4. A method for using a biological compound preparation containing eucalyptus globulus Labill oil is characterized in that the biological compound preparation containing eucalyptus globulus Labill oil of any claim 1-3 is sprayed on crops to kill pests of the crops.
5. The use method of the bio-complex formulation containing eucalyptus globulus oil according to claim 4, wherein the crop is rice.
6. The use method of the bio-complex formulation containing eucalyptus globulus oil according to any one of claims 4 to 5, wherein the crop pest is chilo suppressalis.
7. The use method of the eucalyptus globulus oil-containing biological compound preparation according to any one of claims 4 to 6, wherein the application amount of the eucalyptus globulus oil-containing biological compound preparation is 0.1 to 200 g/mu in terms of active ingredients.
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