CN105053084A - Plant essential oil preparation capable of preventing and controlling aleyrodidae adult pests as well as preparation method and application thereof - Google Patents
Plant essential oil preparation capable of preventing and controlling aleyrodidae adult pests as well as preparation method and application thereof Download PDFInfo
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- CN105053084A CN105053084A CN201510507313.0A CN201510507313A CN105053084A CN 105053084 A CN105053084 A CN 105053084A CN 201510507313 A CN201510507313 A CN 201510507313A CN 105053084 A CN105053084 A CN 105053084A
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Abstract
The invention discloses a plant essential oil preparation capable of preventing and controlling aleyrodidae adult pests as well as a preparation method and application thereof. The preparation comprises the following components by weight percent content: 40-60% of plant essential oil, 5% of a cosolvent, 10-15% of an emulsifier, 1-3% of an antifreezing agent and the balance of a solvent. The preparation has a good control effect on aleyrodidae adult pests, such as aleurocanthus spiniferus, aleurocanthus woglumi ashby, trialeurodes vaporariorum, bemisia tabaci and dialeurodes citri, and is especially quite good in fast-acting property, the control efficiency can reach 90% or above 0.5 h after application, and the natural enemies of ladybird, and the like, are not killed and hurt; the preparation is used for preventing and controlling aleyrodidae adult pests, can be sprayed in large fields with a conventional sprayer, can be directly applied in a greenhouse with a thermal aerosol sprayer, can be used as an environment-friendly smoke agent of the thermal aerosol sprayer, and is simple in processing technology, various in application methods, efficient, safe and environment-friendly.
Description
Technical field
The present invention relates to a kind of plants essential oil preparation (hereinafter referred to as GCS preparation) preventing and treating Aleyrodidae adult pest, particularly principle active component is mixed by two kinds and above any proportioning in citronella oil, birch oil,sweet and fruit of cubeb litsea tree oil and makes mass content preparation reaching 40-60% and preparation method thereof and application.
Background technology
Aleyrodidae insect is distributed widely on the plants such as grain and oil crop, fruit-bearing forest, vegetables and landscape flower, aleyrodid with sucking mouth parts sucking plant juice cause plant weak, secrete the Sooty mould that a large amount of honeydew brings out and then the photosynthesis badly influencing plant, cause plant undergrowth and reduce its economic worth and ornamental value; Propagation various plants virus; Not only individual little, breeding rapidly but also 1 year generation is many, generation overlap serious, the nymph of Partial Species is hidden in plant middle and lower part vacuum side of blade (as tea tree Aleurocanthus spiniferus) for Aleyrodidae insect, thus be difficult to control.
So control Aleyrodidae adult pest is the key of this type of control of insect; Current prevention and controls has chemical control and insects trap board control, in chemical control, because its generation is many, generation overlap serious, then needs repeatedly dispenser, chemical pesticide must be caused thus to remain and exceed standard, and easily produce resistance; And in insects trap board control, mu is large by insects trap board quantity, and need manually in a large number to install in field, its with plate cost and recruitment cost high, and when its outburst is caused disaster, the control efficiency of this measure is very micro-.
Summary of the invention
The object of this invention is to provide a kind of plants essential oil preparation preventing and treating Aleyrodidae adult pest and preparation method thereof and application.
The technical solution used in the present invention is, be called for short GCS preparation, this GCS preparation is formulated by plants essential oil, cosolvent, emulsifier, antifreezing agent and ethanol.
Preferably, the mass percentage of the component of described GCS preparation is as follows:
Preferably, described plants essential oil to be mainly in citronella oil, birch oil,sweet and fruit of cubeb litsea tree oil the mixture of two kinds and above arbitrary proportion; Described birch oil,sweet is obtained through steam distillation by the stem of fast-growing tree smoothbark birch.
Preferably, described cosolvent is the mixture of one or more arbitrary proportions in ethylene glycol, isopropyl alcohol, cyclohexanone, 1-METHYLPYRROLIDONE and DMF.
Preferably, described emulsifier is the mixture of one or more arbitrary proportions in alkylphenol polyoxyethylene, polyol fatty acid ester and ethylene oxide adduct thereof, Sulfonates, fatty alcohol-polyoxyethylene ether and Tea Saponin.
Preferably, described antifreezing agent is the mixture of one or more arbitrary proportions in propane diols, glycerine and polyethylene glycol; To be volume content be described solvent 75% and above ethanol.
A preparation method for GCS preparation, joins plants essential oil in cosolvent and solvent, is stirred to after dissolving completely, adds emulsifier and stir, then adding antifreezing agent, finally add residual solvent and stir and get final product.
An application for GCS preparation, is used as insecticide by this GCS preparation, the adult of the Aleyrodidae insect such as main control tea tree Aleurocanthus spiniferus, oranges and tangerines Aleurocanthus spiniferus, Trialeurodes vaporariorum Westwood, Bemisia tabaci, oranges and tangerines aleyrodid; Its application process is used by conventional nebulizers spraying and thermal aerosol generator.
Preferably, this GCS preparation can be used as the smoke agent of thermal aerosol generator.
Beneficial effect of the present invention is: various plants essential oil tool insecticidal activity, its mode of action of insect is mainly contained lure, repellent, food refusal, stifling and Growth inhibition; The features such as plants essential oil tool source is wide, smell is pleasant, low toxicity, environmental friendliness, volatility are good; Appliable plant essential oil, as insecticide, is repeatedly used generation because it derives from plant, low toxicity and its good volatility without the need to worry and is remained.
Embodiment
Below in conjunction with the embodiment of the present invention, be clearly and completely described the technical scheme in the embodiment of the present invention, obviously, described embodiment is only the present invention's part embodiment, instead of whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art, not making the every other embodiment obtained under creative work prerequisite, belong to the scope of protection of the invention.
The preparation of example 1:40%GCS preparation:
In this embodiment, describe the preparation of 5 kinds of 40%GCS preparations in detail, the content of its component is separately as shown in table 1.
The content of table 1.5 kind of each component of 40%GCS preparation
In GCS1 preparation, cosolvent is ethylene glycol and 1-METHYLPYRROLIDONE (mass ratio is 4:1), emulsifier is alkylphenol polyoxyethylene, Sulfonates and Tea Saponin (mass ratio is 5:2:3), and antifreezing agent is propane diols and polyethylene glycol (mass ratio is 1:1).In GCS2 preparation, cosolvent is ethylene glycol and DMF (mass ratio is 4:1), emulsifier is alkylphenol polyoxyethylene, Sulfonates and Tea Saponin (mass ratio is 5:2:3), and antifreezing agent is propane diols and polyethylene glycol (mass ratio is 1:1).In GCS3 preparation, cosolvent is ethylene glycol and DMF (mass ratio is 4:1), emulsifier is alkylphenol polyoxyethylene, Sulfonates and Tea Saponin (mass ratio is 5:2:3), and antifreezing agent is propane diols and polyethylene glycol (mass ratio is 1:2).In GCS4 preparation, cosolvent is ethylene glycol and DMF (mass ratio is 4:1), emulsifier is alkylphenol polyoxyethylene, Sulfonates and Tea Saponin (mass ratio is 6:3:3), and antifreezing agent is propane diols and polyethylene glycol (mass ratio is 1:1).In GCS4 preparation, cosolvent is isopropyl alcohol and cyclohexanone (mass ratio is 3:2), emulsifier is alkylphenol polyoxyethylene, polyol fatty acid ester and ethylene oxide adduct thereof, Sulfonates and fatty alcohol-polyoxyethylene ether (mass ratio is 5:2:2:3), and antifreezing agent is propane diols and polyethylene glycol (mass ratio is 1:1).The solvent of GCS1 to GCS5 preparation is 75% ethanol.
The preparation method of above-mentioned GCS1 to GCS5 preparation is as described below:
Each plants essential oil mixing (mixed essential oil is 40kg) is taken by proportioning, join 5kg cosolvent and 30kg solvent, be stirred to after dissolving completely, add emulsifier and stir, then add antifreezing agent, finally add residual solvent and stir and obtain GCS1 to the GCS5 preparation of 100kg.
The preparation of example 2:50%GCS preparation:
In this embodiment, describe the preparation of 3 kinds of 50%GCS preparations in detail, the content of its component is separately as shown in table 2.
The content of table 2.3 kind of each component of 50%GCS preparation
In GCS6 preparation, cosolvent is ethylene glycol, and emulsifier is alkylphenol polyoxyethylene, Sulfonates and Tea Saponin (mass ratio is 6:2:3), and antifreezing agent is propane diols and polyethylene glycol (mass ratio is 2:1).In GCS7 preparation, cosolvent is ethylene glycol and isopropyl alcohol (mass ratio is 4:1), and emulsifier is alkylphenol polyoxyethylene, Sulfonates and Tea Saponin (mass ratio is 6:6:3), and antifreezing agent is glycerine.In GCS8 preparation, cosolvent is ethylene glycol and cyclohexanone (mass ratio is 4:1), emulsifier is alkylphenol polyoxyethylene, Sulfonates and Tea Saponin (mass ratio is 8:2:3), and antifreezing agent is propane diols and polyethylene glycol (mass ratio is 1:2).The solvent of GCS6 to GCS8 preparation is 80% ethanol.
The preparation method of above-mentioned GCS6 to GCS8 preparation is as described below:
Each plants essential oil mixing (mixed essential oil is 50kg) is taken by proportioning, join 5kg cosolvent and 25kg solvent, be stirred to after dissolving completely, add emulsifier and stir, then add antifreezing agent, finally add residual solvent and stir and obtain GCS6 to the GCS8 preparation of 100kg.
The preparation of example 3:60%GCS preparation:
In this embodiment, describe the preparation of 7 kinds of 60%GCS preparations in detail, the content of its component is separately as shown in table 3.
The content of table 3.7 kind of each component of 60%GCS preparation
In GCS9 preparation, cosolvent is ethylene glycol and 1-METHYLPYRROLIDONE (mass ratio is 4:1), emulsifier is alkylphenol polyoxyethylene, Sulfonates and Tea Saponin (mass ratio is 7:3:3), and antifreezing agent is propane diols and polyethylene glycol (mass ratio is 1:1).In GCS10 and GCS11 preparation, cosolvent is ethylene glycol and DMF (mass ratio is 4:1), emulsifier is alkylphenol polyoxyethylene, polyol fatty acid ester and ethylene oxide adduct thereof, Sulfonates and Tea Saponin (mass ratio is 5:3:2:5), and antifreezing agent is propane diols and polyethylene glycol (mass ratio is 1:1).In GCS12 and GCS13 preparation, cosolvent is ethylene glycol and DMF (mass ratio is 4:1), emulsifier is alkylphenol polyoxyethylene, Sulfonates, fatty alcohol-polyoxyethylene ether and Tea Saponin (mass ratio is 5:3:2:4), and antifreezing agent is propane diols and polyethylene glycol (mass ratio is 1:2).In GCS14 and GCS13 preparation, cosolvent is ethylene glycol and cyclohexanone (mass ratio is 4:1), emulsifier is alkylphenol polyoxyethylene, Sulfonates and Tea Saponin (mass ratio is 6:2:3), and antifreezing agent is propane diols and polyethylene glycol (mass ratio is 1:1).The solvent of GCS9 to GCS13 preparation is 90% ethanol.The solvent of GCS14 and GCS13 preparation is 95% ethanol.
The preparation method of above-mentioned GCS9 to GCS15 preparation is as described below:
Each plants essential oil mixing (mixed essential oil is 60kg) is taken by proportioning, join 5kg cosolvent and 15kg solvent, be stirred to after dissolving completely, add emulsifier and stir, then add antifreezing agent, finally add residual solvent and stir and obtain GCS9 to the GCS15 preparation of 100kg.
Invention formulation is to the efficiency test of relevant adult whitefly
1: invention formulation sprayer spray-on process is to the efficiency test of tea tree Aleurocanthus spiniferus imago
(1) reagent agent and concentration thereof: GCS1 to GCS15 of the present invention is totally 15 preparations, the equal 600mg/L of concentration is; 10% Biphenthrin missible oil (100mg/L), 5% Imidacloprid missible oil (50mg/L) and 5% aqueous matrine solution (100mg/L).
(2) test method: implement when Aleurocanthus spiniferus imago on tea tree is contained and sent out.Often 4 repetitions are established in process, plot area 15m2, the group arrangement of random district, after being watered for examination concentration by each medicament, manual sprayer is sprayed, if spray clear water is contrast, before medicine, after medicine 0.5,2 and 24h investigate Aleurocanthus spiniferus imago adhesion amount on 1 bud 2 leaf tea shoot, every community random searching 20 tea shoots.Calculate Revision insect recluced rate and preventive effect, and carry out significance of difference analysis (the multiple range method of new Deng Kenshi).
(3) preventive effect result: 4 be the results are shown in Table to the preventive effect of Aleurocanthus spiniferus imago on tea tree.
The preventive effect of table 4. pair tea tree Aleurocanthus spiniferus imago
As shown in Table 4,15 GCS preparations prepared by example 1-3, to the good preventive effect of the equal tool of Aleurocanthus spiniferus imago on tea tree, after medicine, the preventive effect of 0.5h all reaches more than 90%, and its quick-acting is fine.In 5 40%GCS preparations of example 1, best with GCS3 preventive effect, after medicine, the preventive effect of 0.5h reaches 95.64%.In 3 50%GCS preparations of example 2, best with GCS8 preventive effect, after medicine, the preventive effect of 0.5h reaches 96.88%.In 7 60%GCS preparations of example 3, best with GCS15 preventive effect, after medicine, the preventive effect of 0.5h reaches 98.25%.Given this, the GCS15 in GCS8 and the 60%GCS preparation during following efficiency test then uses in 40%GCS preparation GCS3,50%GCS preparation.
Invention formulation thermal aerosol generator application method is to the efficiency test of eggplant trialeurodes vaporariorum adult in plastic greenhouse
(1) reagent agent and concentration thereof: GCS3, GCS8, GCS15 of the present invention be totally 3 preparations, the equal 600mg/L of concentration is; 10% Biphenthrin missible oil (100mg/L).
(2) test method: implement when the trialeurodes vaporariorum adult on eggplant in plastic greenhouse is contained and sends out.Often 4 repetitions are established in process, often repeat 20 strain eggplant Potted orchard, and are moved in plant tent, make its relative closure and isolation.After being watered for examination concentration by each medicament, thermal aerosol generator is used, if spray clear water is contrast.Before medicine, after medicine 0.5,2 and 24h investigate trialeurodes vaporariorum adult adhesion amount on eggplant seedling, every strain eggplant seedling investigates 5 blades.Calculate Revision insect recluced rate and preventive effect, and carry out significance of difference analysis (the multiple range method of new Deng Kenshi).
(3) preventive effect result: 5 be the results are shown in Table to the preventive effect of trialeurodes vaporariorum adult on eggplant in plastic greenhouse.
As shown in Table 5, GCS3, GCS8, GCS15 are to the good preventive effect of the equal tool of trialeurodes vaporariorum adult on eggplant in plastic greenhouse, and after medicine, the preventive effect of 0.5h all reaches more than 96%, and its quick-acting is fine.
The preventive effect of trialeurodes vaporariorum adult on eggplant in table 5. pair plastic greenhouse
Invention formulation sprayer spray-on process is to the efficiency test of tomato Bemisia tabaci adults
(1) reagent agent and concentration thereof: GCS3, GCS8, GCS15 of the present invention be totally 3 preparations, the equal 600mg/L of concentration is; 10% Biphenthrin missible oil (100mg/L).
(2) test method: implement when the Bemisia tabaci adults on tomato is contained and sent out.Often 4 repetitions are established in process, often repeat 20 strain tomato seedlings, and after being watered for examination concentration by each medicament, manual sprayer is sprayed, if spray clear water is contrast.Before medicine, after medicine 0.5,2 and 24h investigate Bemisia tabaci adults adhesion amount on tomato, every strain tomato investigates 5 blades.Calculate Revision insect recluced rate and preventive effect, and carry out significance of difference analysis (the multiple range method of new Deng Kenshi).
(3) preventive effect result: 6 be the results are shown in Table to the preventive effect of the Bemisia tabaci adults on tomato.
As shown in Table 6, GCS3, GCS8, GCS15 are to the good preventive effect of the equal tool of the Bemisia tabaci adults on tomato, and after medicine, the preventive effect of 0.5h all reaches more than 93%, and its quick-acting is fine.
The preventive effect of Bemisia tabaci adults on table 6. pair tomato
Invention formulation sprayer spray-on process is to the efficiency test of oranges and tangerines adult whitefly
(1) reagent agent and concentration thereof: GCS3, GCS8, GCS15 of the present invention be totally 3 preparations, the equal 600mg/L of concentration is; 10% Biphenthrin missible oil (100mg/L).
(2) test method: implement when the oranges and tangerines adult whitefly on oranges and tangerines is contained and sent out.Often 4 repetitions are established in process, often repeat 1 strain oranges and tangerines, and after being watered for examination concentration by each medicament, manual sprayer is sprayed, if spray clear water is contrast.Before medicine, after medicine 0.5,2 and 24h investigate oranges and tangerines adult whiteflies adhesion amount, 20 blades investigated by every strain oranges and tangerines.Calculate Revision insect recluced rate and preventive effect, and carry out significance of difference analysis (the multiple range method of new Deng Kenshi).
(3) preventive effect result: 7 be the results are shown in Table to the preventive effect of the Bemisia tabaci adults on tomato.
As shown in Table 7, GCS3, GCS8, GCS15 are to the good preventive effect of the equal tool of the Bemisia tabaci adults on tomato, and after medicine, the preventive effect of 0.5h all reaches more than 94%, and its quick-acting is fine.
The preventive effect of Bemisia tabaci adults on table 7. pair tomato
Finally it should be noted that, above embodiment is the unrestricted technical scheme of the present invention in order to explanation only, although with reference to above-described embodiment to invention has been detailed description, those skilled in the art are to be understood that, still can modify to the present invention or equivalent replacement, and not departing from any modification or partial replacement of the spirit and scope of the present invention, it all should be encompassed in right of the present invention.
Claims (9)
1. can prevent and treat a plants essential oil preparation for Aleyrodidae adult pest, be called for short GCS preparation, it is characterized in that: this GCS preparation is formulated by plants essential oil, cosolvent, emulsifier, antifreezing agent and ethanol.
2. according to GCS preparation according to claim 1, it is characterized in that: the mass percentage of the component of described GCS preparation is as follows:
3. according to the GCS preparation described in any one of claim 1 ~ 2, it is characterized in that: described plants essential oil to be mainly in citronella oil, birch oil,sweet and fruit of cubeb litsea tree oil the mixture of two kinds and above arbitrary proportion; Described birch oil,sweet is obtained through steam distillation by the stem of fast-growing tree smoothbark birch.
4. according to the GCS preparation described in any one of claims 1 to 3, it is characterized in that: described cosolvent is the mixture of one or more arbitrary proportions in ethylene glycol, isopropyl alcohol, cyclohexanone, 1-METHYLPYRROLIDONE and DMF.
5. according to the GCS preparation described in any one of Claims 1 to 4, it is characterized in that: described emulsifier is the mixture of one or more arbitrary proportions in alkylphenol polyoxyethylene, polyol fatty acid ester and ethylene oxide adduct thereof, Sulfonates, fatty alcohol-polyoxyethylene ether and Tea Saponin.
6. according to the GCS preparation described in any one of Claims 1 to 5, it is characterized in that: described antifreezing agent is the mixture of one or more arbitrary proportions in propane diols, glycerine and polyethylene glycol; To be volume content be described solvent 75% and above ethanol.
7. according to the preparation method of the GCS preparation described in any one of claim 1 ~ 6, it is characterized in that: plants essential oil is joined in cosolvent and solvent, be stirred to after dissolving completely, add emulsifier and stir, then add antifreezing agent, finally add residual solvent and stir and get final product.
8. an application for GCS preparation, is characterized in that: this GCS preparation is used as insecticide, the adult of the Aleyrodidae insect such as main control tea tree Aleurocanthus spiniferus, oranges and tangerines Aleurocanthus spiniferus, Trialeurodes vaporariorum Westwood, Bemisia tabaci, oranges and tangerines aleyrodid; Its application process is used by conventional nebulizers spraying and thermal aerosol generator.
9. according to the application of GCS preparation according to claim 8, it is characterized in that: this GCS preparation can be used as the smoke agent of thermal aerosol generator.
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Cited By (1)
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Inventor after: Yang Wen Inventor after: Zhou Yufeng Inventor after: Meng Zehong Inventor after: Chen Yao Inventor after: Yao Yongjing Inventor after: Lei Zhiwei Inventor after: Gao Xiubing Inventor after: Lv Zhaoyun Inventor before: Zhou Yufeng Inventor before: Yang Wen Inventor before: Meng Zehong Inventor before: Chen Yao Inventor before: Yao Yongjing Inventor before: Lei Zhiwei Inventor before: Gao Xiubing Inventor before: Lv Zhaoyun |
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Effective date of registration: 20201202 Address after: Room 308, building 147, 500 Zhennan Road, Putuo District, Shanghai Patentee after: RELIACHEM INDUSTRY Corp. Address before: 550000, Guizhou, Guiyang Province Creek District Kim community Patentee before: GUIZHOU TEA Research Institute |