CN107333804A - Insecticide of composite essential oil compounding and preparation method thereof - Google Patents
Insecticide of composite essential oil compounding and preparation method thereof Download PDFInfo
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- CN107333804A CN107333804A CN201710660602.3A CN201710660602A CN107333804A CN 107333804 A CN107333804 A CN 107333804A CN 201710660602 A CN201710660602 A CN 201710660602A CN 107333804 A CN107333804 A CN 107333804A
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- essential oil
- composite essential
- insecticide
- agent
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/30—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests characterised by the surfactants
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N61/00—Biocides, pest repellants or attractants, or plant growth regulators containing substances of unknown or undetermined composition, e.g. substances characterised only by the mode of action
- A01N61/02—Mineral oils; Tar oils; Tar; Distillates, extracts or conversion products thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N63/00—Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
- A01N63/10—Animals; Substances produced thereby or obtained therefrom
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/20—Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Wood Science & Technology (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Agronomy & Crop Science (AREA)
- Environmental Sciences (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Pest Control & Pesticides (AREA)
- Mycology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- General Chemical & Material Sciences (AREA)
- Virology (AREA)
- Chemical & Material Sciences (AREA)
- Toxicology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
Insecticide of a kind of composite essential oil compounding and preparation method thereof, belongs to crop pests Prevention Technique field, it is intended to and solve existing physical pest killing agent component and design unreasonable, residual harmful composition, the problem of causing secondary pollution.Component that it is used and weight proportion for：50~99 parts of composite essential oil, 1~5 part of nonionic emulsifier, 0.2~2 part of bleeding agent, 0.1~2 part of spreader-sticker, 0.1~1.5 part of wetting agent, preparation method are：Start stirring apparatus for reaction kettle, composite essential oil is added into reactor, emulsifying agent stirring at normal temperature is added to emulsify 8~15 minutes, sequentially add bleeding agent, spreader-sticker, wetting agent, uniform stirring 18~30 minutes, through levigate 180~300 mesh of colloid mill, then through homogenizer homogeneous to 500~800 mesh, through after the assay was approved, that is, being made for insecticide finished product.Its component is reasonable in design, and preparation method is simple, is prevented and treated suitable for crop pests, also can serve as producing the insecticide of food.
Description
Technical field
The invention belongs to a kind of physical pest killing agent in crop pests Prevention Technique field and preparation method thereof.
Background technology
With the continuous development of agriculture production technology and being showing improvement or progress day by day for control of insect technology, to crop pests dispensary
With the technical requirements of article particularly physical control article also more and more higher.In known technology, existing physical pest killing agent master
If the desinsection agent aid being re-dubbed with mineral oil used, its component design compatibility is unreasonable, and preparation method is cumbersome, and it is lacked
Point is must to need to be used cooperatively with insecticides such as other chemical classes, and it is exceeded to there are content of beary metal, insecticide granule size
Scattered uneven, insecticidal effect is poor, in actual applications, there are the residual of the harmful components such as heavy metal again, easily causes
Secondary pollution, influence environment and be detrimental to health, using being restricted, i.e., brought inconvenience to practical application.
The content of the invention
For overcome the deficiencies in the prior art, it is unreasonable to solve existing physical pest killing agent component design, residual harmful into
Point, the problem of causing secondary pollution.It is reasonable in design it is an object of the present invention to provide a kind of component, environmental pollution is not caused, can be single
Desinsection solely is used, insecticide granule is tiny to be uniformly dispersed, and enhances adhesive force, penetration, good disinsection effect, the crop applied
It is in extensive range, and insect will not produce resistance, new-type physical pest killing agent easy to use and its application method.
Technical scheme is used by the present invention solves the above problems：
A kind of insecticide of composite essential oil compounding, component that it is used and weight proportion for：It is 50~99 parts of composite essential oil, non-
1~5 part of ionic emulsifying agent, 0.2~2 part of bleeding agent, 0.1~2 part of spreader-sticker, 0.1~1.5 part of wetting agent.
The insecticide of above-mentioned composite essential oil compounding, the composite essential oil is by the composite essential oil of plant extract, by mineral oil
In the composite essential oil of extraction, the composite essential oil of livestock and poultry animal oil extract, the composite essential oil of leather-solid waste extraction, fishes and shrimps aquatic products
Any composite essential oil of the composite essential oil of extraction, and other applicable composite essential oils, the composite essential oil of plant extract be from
The composite essential oil extracted in the fruit of plant, flower, leaf, stem, root.
The insecticide of above-mentioned composite essential oil compounding, described emulsifying agent is compound nonionic emulsifier.
The insecticide of above-mentioned composite essential oil compounding, the bleeding agent is anion surfactant.
The insecticide of above-mentioned composite essential oil compounding, the spreader-sticker is casein ionized calcium.
The insecticide of above-mentioned composite essential oil compounding, described wetting agent are sulfonated oil, wetting agent (PE100), food-grade
Soften NMF, soap, Nekal BX, soybean lecithin, thio-alcohol, hydrazides class, mercaptan acetals, the polyoxyethylene of alkyl phenol
Any nonionic surface active agent in ether, and other applicable wetting agents (NMF).
The insecticide of above-mentioned composite essential oil compounding, the described process for preparing insecticide are：According to component and weight proportion
After weighing, start the agitating device of reactor, first composite essential oil is added in reactor, add emulsifying agent progress normal temperature and stir
After mixing emulsification 8~15 minutes, bleeding agent, spreader-sticker, wetting agent, uniform stirring 18~30 minutes, through colloid mill are sequentially added
Levigate 180~300 mesh, then through homogenizer homogeneous to 500~800 mesh, described answer is made for through after the assay was approved, entering storage tank
Close the insecticide finished product (product) of essential oil compounding.
The composite essential oil compounded pesticides finished product of the present invention in use, according to design requirement and according to insect pest actual conditions,
This composite essential oil compounded pesticides finished product is watered into 50~400 times to be sprayed.Due to the droplet being sprayed onto on crops
The graininess oil film that shape oil is formed, the wax coat of insect body surface is dissolved rapidly, make the uniform confining bed of stomatal limiting value of insect body surface,
Make insect death by suffocation, and plant growth is had no effect.
Because present invention design employs above-mentioned technical proposal, effectively solves the existing existing thing of physical pest killing agent
Manage insecticide component and design unreasonable, residual harmful composition, the problem of causing secondary pollution.Also pass through for several times on Hebei province, mountain
The ground such as Dong Sheng actual tests result on trial shows that it has, and component design and compatibility are reasonable, and preparation method is simple, does not cause environment
Pollution, can be used alone desinsection, and insecticide granule is tiny to be uniformly dispersed, and good disinsection effect, the crop applied is in extensive range, and
The advantages that insect will not produce resistance, and practical application facilitates, suitable for the preventing and treating of crop pests trialeurodes vaporariorum etc., it can also use
Make the insecticide of production food.
Embodiment
Embodiment 1
The present embodiment is to be by weight ratio by following component：The food-grade plant composite essential oil extracted by soybean, peanut
6kg, 774 non-ionic composite emulsifying agent 0.4kg, bleeding agent (JFC) 0.1kg, agricultural organosilicon spreader-sticker 0.2kg, sulfonated oil
Wetting agent 0.1kg；Preparation method is：After being weighed according to said components and weight proportion, start the agitating device of reactor, first
Food-grade plant composite essential oil is added in reactor, 774 non-ionic composite emulsifying agents is added and carries out stirring at normal temperature breast
After changing 12 minutes, bleeding agent (JFC), agricultural organosilicon spreader-sticker, the wetting agent of sulfonated oil are sequentially added, uniform stirring 25 divides
Clock, 300 mesh are milled down to through colloid mill, then through homogenizer homogeneous to excessively domestic screen cloth up to 580 mesh, through after the assay was approved, entering storage tank
The insecticide finished product (I) of described composite essential oil compounding is made for, its mechanism of action is the food-level white oil warp of plant extract
The insecticide finished product (I) that composite essential oil compounds is watered 100 times in greenhouse by emulsifier, the present embodiment in Cangzhou City Yanshan County
On cucumber after spray application, medicament forms one layer of graininess oil film on polypide, chorion, mycelia or weeds surface, makes pest body, ovum
Shell, hyphal surface stomata are closed, and cause its death by suffocation；The oil emu of distribution blade or fruit surface can also prevent other evils
Worm just hatches the land of nymph, and the spawning to insect has repellent action；In nature, this medicament oxidation-degradable is right
People and animals and natural enemies security, and resistance will not be produced to insect.
Embodiment 2
The present embodiment is to be by weight ratio by following component：By the cosmetics-stage composite essential oil 90kg of mineral oil extract,
The non-ionic composite emulsifying agents of NP -10 5kg, bleeding agent (JFC-S) 0.8kg, wetting agent (PE100) 1.4kg；The present embodiment should
The flow of process for preparing insecticide is：After being weighed according to said components and weight proportion, start the agitating device of reactor, first
Composite essential oil is added in reactor, add emulsifying agent carry out stirring at normal temperature emulsify 10 minutes, sequentially add bleeding agent,
Spreader-sticker, wetting agent, uniform stirring 20 minutes, through levigate 200 mesh of colloid mill, then through homogenizer homogeneous to import screen cloth reach
350 mesh, the pesticide product (II) for being made for described composite essential oil through after the assay was approved, entering storage tank and compounding, it acts on machine
Reason is to synthesize basic essential oil through emulsifier, and the pesticide product for compounding composite essential oil in Hejian City of Hebei province (II) is watered
80 times, on Elizabethan's melon after spray application, medicament forms one layer of graininess oil on polypide, chorion, mycelia or weeds surface
Film, pest body surface pores is closed, cause insect death by suffocation, it can also be prevented by being distributed the oil emu of blade or fruit surface
Its insect just hatches the land of nymph, and the spawning to insect has repellent action；In nature, this oxidable drop of medicament
Solution, thus residual life, is short；Therefore it is that a kind of preferably physical control insect persistently controls pesticide control；And insect will not produce it is anti-
Property.
Embodiment 3
The present embodiment is to be by weight ratio by following component：By pigskin, ox-hide leftover bits and pieces extract composite essential oil 52kg,
TX-4 nonionic emulsifier 1.6kg, OP-10 nonionic penetrants 1.0kg, casein ionized calcium spreader-sticker 1.6kg, food-grade are soft
Change NMF 0.9kg；Preparation method is：After being weighed according to said components and weight proportion, start the agitating device of reactor, first
The composite essential oil that leather-solid waste extracts is added in reactor, TX-4 nonionic emulsifiers is added and carries out stirring at normal temperature breast
After changing 12 minutes, OP-10 nonionic penetrants, casein ionized calcium spreader-sticker, food-grade softening NMF are sequentially added,
Even stirring 25 minutes, through levigate 280 mesh of colloid mill, then through homogenizer homogeneous to passing through screen cloth up to 480 mesh, through after the assay was approved,
Enter the insecticide finished product (III) that storage tank is made for described composite essential oil compounding.Compounded in Dezhou City Shandong Province with composite essential oil
Insecticide finished product (III) be watered 100 times sprayed on tomato after, medicament polypide, chorion, mycelia or weeds surface formed one
Layer microparticle shape oil film, closes insect stomata, and insect death by suffocation rate is up to 91%；It is distributed the oil emu of blade or fruit surface
Other insects can be also prevented just to hatch the land of nymph, and the spawning to insect has repellent action；In nature, this medicine
Agent oxidation-degradable, and insect will not produce resistance.
Embodiment 4
The present embodiment is to be by weight ratio by following component：By cottonseed, rapeseed extract plant composite essential oil 50kg,
TX-4 nonionic emulsifier 1.6kg, OP-10 nonionic penetrants 1.05kg, casein ionized calcium spreader-sticker 1.52kg, food-grade
Soften NMF 0.96kg；Preparation method is：After being weighed according to said components and weight proportion, start the stirring dress of reactor
Put, first add plant composite essential oil in a kettle, add TX-4 nonionic emulsifiers and carry out stirring at normal temperature emulsification 12 minutes
Afterwards, OP-10 nonionic penetrants, casein ionized calcium spreader-sticker, the wetting agent of food-grade softening NMF are sequentially added,
Even stirring 21 minutes, through levigate 300 mesh of colloid mill, then through homogenizer homogeneous to passing through screen cloth up to 560 mesh, through after the assay was approved,
Enter the insecticide finished product (IV) that storage tank is made for described composite essential oil compounding.
Embodiment 5
The present embodiment is to be by weight ratio by following component：By extracted in fishes and shrimps aquatic products composite essential oil 5.8kg,
774 non-ionic composite emulsifying agent 0.5kg, bleeding agent (JFC) 0.12kg, agricultural organosilicon spreader-sticker 0.25kg, sulfonated oil
Wetting agent 0.13kg；Preparation method is：After being weighed according to said components and weight proportion, start the agitating device of reactor,
Composite essential oil is first added in reactor, add emulsifying agent carry out stirring at normal temperature emulsify 15 minutes after, sequentially add bleeding agent,
Add spreader-sticker, add wetting agent, uniform stirring 30 minutes, 300 mesh are milled down to through colloid mill, then state was arrived through homogenizer homogeneous
Screen cloth is produced up to 800 mesh, the insecticide finished product (V) for being made for described composite essential oil through after the assay was approved, entering storage tank and compounding.
After the insecticide practical probation of the composite essential oil compounding of the present invention, favorable comment and the accreditation of users is obtained, is put into practice
Prove, it belongs to the physical control insect product of green, energy autoxidation, and will not produce any toxic residue, and it produces system
Do not have to fuel and heating in work, meet the requirement of environmental protection, cost of goods manufactured valency is less than other biological pesticide products, production
It is moderate with use cost, it is easy to the promotion and application of large area, a wide range of crops and food production.
Claims (7)
1. a kind of insecticide of composite essential oil compounding, it is characterised in that the component and weight proportion that it is used is composite essential oils 50
~99 parts, 1~5 part of nonionic emulsifier, 0.2~2 part of bleeding agent, 0.1~2 part of spreader-sticker, 0.1~1.5 part of wetting agent.
2. the insecticide of composite essential oil compounding according to claim 1, it is characterised in that the composite essential oil is by plant
The composite essential oil of extraction, by the composite essential oil of mineral oil extract, the composite essential oil of livestock and poultry animal oil extract, leather-solid waste extract
Composite essential oil, any composite essential oil of the composite essential oil extracted in fishes and shrimps aquatic products, the composite essential oil of plant extract be from
The composite essential oil extracted in the fruit of plant, flower, leaf, stem, root.
3. the insecticide of composite essential oil according to claim 1 compounding, it is characterised in that described nonionic emulsifier is
Compound nonionic emulsifier.
4. the insecticide of composite essential oil compounding according to claim 1, it is characterised in that described bleeding agent is anion table
Face activating agent.
5. according to claim 1 composite essential oil compounding insecticide, it is characterised in that described spreader-sticker be casein from
Sub- calcium.
6. the insecticide of composite essential oil compounding according to claim 1, it is characterised in that the moistening described in described wetting agent
Agent is sulfonated oil, wetting agent (PE100), food-grade softening NMF, soap, Nekal BX, soybean lecithin, thio-alcohol, acyl
Hydrazine, mercaptan acetals, alkyl phenol APEO in any nonionic surface active agent wetting agent.
7. the insecticide of composite essential oil compounding according to claim 1, it is characterised in that the process for preparing insecticide is：
After being weighed according to component and weight proportion, after the agitating device for starting reactor, first composite essential oil is added in reactor, then
After adding the emulsification of emulsifying agent progress stirring at normal temperature 8~15 minutes, bleeding agent, spreader-sticker, wetting agent, uniform stirring are sequentially added
18~30 minutes, 180~300 mesh are milled down to through colloid mill, then through homogenizer homogeneous to 500~800 mesh, through after the assay was approved,
Enter the insecticide finished product that storage tank is made for described composite essential oil compounding.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710660602.3A CN107333804A (en) | 2017-08-04 | 2017-08-04 | Insecticide of composite essential oil compounding and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710660602.3A CN107333804A (en) | 2017-08-04 | 2017-08-04 | Insecticide of composite essential oil compounding and preparation method thereof |
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| Publication Number | Publication Date |
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| CN107333804A true CN107333804A (en) | 2017-11-10 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201710660602.3A Pending CN107333804A (en) | 2017-08-04 | 2017-08-04 | Insecticide of composite essential oil compounding and preparation method thereof |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1164333A (en) * | 1997-05-23 | 1997-11-12 | 贾宏山 | Synergistic plant insecticide |
| CN101057590A (en) * | 2006-04-23 | 2007-10-24 | 孟祥宁 | Pesticide additive |
| CN101420848A (en) * | 2006-02-15 | 2009-04-29 | 博塔诺凯普有限公司 | Applications of microencapsulated essential oils |
| CN102428973A (en) * | 2011-10-18 | 2012-05-02 | 浙江农林大学 | Agricultural pesticide with essential oil and application thereof |
| CN102485000A (en) * | 2010-12-02 | 2012-06-06 | 江苏丘陵地区镇江农业科学研究所 | Composition for insecticide and bactericide |
-
2017
- 2017-08-04 CN CN201710660602.3A patent/CN107333804A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1164333A (en) * | 1997-05-23 | 1997-11-12 | 贾宏山 | Synergistic plant insecticide |
| CN101420848A (en) * | 2006-02-15 | 2009-04-29 | 博塔诺凯普有限公司 | Applications of microencapsulated essential oils |
| CN101057590A (en) * | 2006-04-23 | 2007-10-24 | 孟祥宁 | Pesticide additive |
| CN102485000A (en) * | 2010-12-02 | 2012-06-06 | 江苏丘陵地区镇江农业科学研究所 | Composition for insecticide and bactericide |
| CN102428973A (en) * | 2011-10-18 | 2012-05-02 | 浙江农林大学 | Agricultural pesticide with essential oil and application thereof |
Non-Patent Citations (8)
| Title |
|---|
| 丁锦华等: "《农业昆虫学 南方本》", 30 June 2002, 中国农业出版社 * |
| 上海市农业技术推广服务中心: "《农药安全使用手册》", 30 September 2009, 上海科学技术出版社 * |
| 刘步林: "《农药剂型加工技术（第二版）》", 31 October 1998, 化学工业出版 * |
| 华乃震: "油类助剂及油类在农药中的应用和前景(Ⅱ)", 《农药》 * |
| 李建中等: "《生物技术》", 31 October 2013, 中国科学技术出版社 * |
| 湖南省长沙农业学校: "《植物保护基础》", 30 September 1984, 农业出版社 * |
| 福建省粮食厅《粮油保管》编写组: "《粮油保管》", 31 December 1983, 福建科学技术出版社 * |
| 费有春: "《简明农药词典》", 31 October 1985, 化学工业出版 * |
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Application publication date: 20171110 |
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