WO2012121496A3 - 백금족 금속 함유 산업폐기물로부터 백금족 금속을 회수하는 방법 - Google Patents

백금족 금속 함유 산업폐기물로부터 백금족 금속을 회수하는 방법 Download PDF

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Publication number
WO2012121496A3
WO2012121496A3 PCT/KR2012/001219 KR2012001219W WO2012121496A3 WO 2012121496 A3 WO2012121496 A3 WO 2012121496A3 KR 2012001219 W KR2012001219 W KR 2012001219W WO 2012121496 A3 WO2012121496 A3 WO 2012121496A3
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WIPO (PCT)
Prior art keywords
platinum group
platinum
group metals
group metal
metal ions
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PCT/KR2012/001219
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English (en)
French (fr)
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WO2012121496A2 (ko
Inventor
신장식
한상철
곽인섭
구정분
김영애
권현지
오경준
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(주)알티아이엔지니어링
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Priority to CN201280012351.3A priority Critical patent/CN103502484A/zh
Publication of WO2012121496A2 publication Critical patent/WO2012121496A2/ko
Publication of WO2012121496A3 publication Critical patent/WO2012121496A3/ko

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    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B7/00—Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
    • C22B7/006—Wet processes
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B11/00—Obtaining noble metals
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/42—Treatment or purification of solutions, e.g. obtained by leaching by ion-exchange extraction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/90—Regeneration or reactivation
    • B01J23/96—Regeneration or reactivation of catalysts comprising metals, oxides or hydroxides of the noble metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/02—Heat treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J41/00—Anion exchange; Use of material as anion exchangers; Treatment of material for improving the anion exchange properties
    • B01J41/04—Processes using organic exchangers
    • B01J41/05—Processes using organic exchangers in the strongly basic form
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B11/00—Obtaining noble metals
    • C22B11/04—Obtaining noble metals by wet processes
    • C22B11/042—Recovery of noble metals from waste materials
    • C22B11/044—Recovery of noble metals from waste materials from pyrometallurgical residues, e.g. from ashes, dross, flue dust, mud, skim, slag, sludge
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/22—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition
    • C22B3/24—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition by adsorption on solid substances, e.g. by extraction with solid resins
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B7/00—Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00—Technologies related to metal processing
    • Y02P10/20—Recycling

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Mechanical Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Processing Of Solid Wastes (AREA)

Abstract

본 발명은 백금족 금속(백금(Pt), 루테늄(Ru), 오스뮴(Os), 로듐(Rh), 이리듐(Ir), 팔라듐(Pd))을 함유한 산업폐기물로부터 백금족을 침출하여, 침출액 내 백금족 금속이온을 흡착제에 흡착한 후 흡착제에 붙어 있는 백금족 금속이온을 탈착제로 탈착하여 고농도 백금족 금속이온 혼합용액으로 회수할 수 있으며, 또한, 백금족 금속이온이 붙어 있는 흡착제를 회화(灰化, ashing)하여 백금족 금속이온을 금속형태(Metallic form)로 회수할 수도 있다. 또한, 회화공정 후 백금족 금속으로 혼합되어 있는 재(Ash)로부터 용해과정을 통해 용해되는 백금은 고농도의 백금 이온으로 회수되고 용해되지 않는 루테늄은 금속형태로 분리할 수 있다.
PCT/KR2012/001219 2011-03-09 2012-02-17 백금족 금속 함유 산업폐기물로부터 백금족 금속을 회수하는 방법 WO2012121496A2 (ko)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201280012351.3A CN103502484A (zh) 2011-03-09 2012-02-17 用于从含有铂族金属的工业废弃物回收铂族金属的方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR20110021116A KR101224503B1 (ko) 2011-03-09 2011-03-09 백금족 금속 함유 산업폐기물로부터 백금족 금속을 회수하는 방법
KR10-2011-0021116 2011-03-09

Publications (2)

Publication Number Publication Date
WO2012121496A2 WO2012121496A2 (ko) 2012-09-13
WO2012121496A3 true WO2012121496A3 (ko) 2012-11-15

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KR (1) KR101224503B1 (ko)
CN (1) CN103502484A (ko)
WO (1) WO2012121496A2 (ko)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101392179B1 (ko) 2013-02-08 2014-05-08 강희남 백금족 금속의 회수방법 및 이에 사용되는 백금족 금속의 회수장치
KR101454645B1 (ko) 2013-02-20 2014-10-27 한국생산기술연구원 배기 가스 정화 장치의 폐촉매에 포함된 금속 정량 방법
KR101452809B1 (ko) * 2013-04-22 2014-10-22 (주)알티아이엔지니어링 폐촉매에서 회수한 백금을 이용한 연료전지용 백금 담지 촉매 제조방법
KR101579498B1 (ko) * 2015-02-24 2015-12-22 (주) 유천테크 팔라듐함유 폐 페이스트로부터 팔라듐의 회수방법
CN108579695A (zh) * 2018-01-22 2018-09-28 江苏欣诺科催化剂有限公司 一种吸附铱的吸附剂及脱附方法
CN112029998B (zh) * 2020-08-27 2022-03-18 湖南高鑫铂业有限公司 一种从颗粒状废催化剂中溶-吸-脱联合回收铂族金属的方法
CN113957244A (zh) * 2021-10-26 2022-01-21 中钢集团南京新材料研究院有限公司 一种含铂料液中铂族金属的富集方法

Citations (4)

* Cited by examiner, † Cited by third party
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KR20030036749A (ko) * 2000-09-05 2003-05-09 존슨 맛쎄이 퍼블릭 리미티드 컴파니 금속을 함유하는 염기성 이온교환수지의 회화에 의한금속의 회수방법
KR20030041841A (ko) * 2001-11-21 2003-05-27 쉬플리 캄파니, 엘.엘.씨. 촉매 금속의 회수방법
JP2005002414A (ja) * 2003-06-12 2005-01-06 Maezawa Ind Inc 溶液中の貴金属の回収方法
KR20100113678A (ko) * 2009-04-14 2010-10-22 전북대학교산학협력단 유가금속의 회수방법

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1038199C (zh) * 1994-11-30 1998-04-29 核工业北京化工冶金研究院 从废催化剂中回收铂族金属的方法

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20030036749A (ko) * 2000-09-05 2003-05-09 존슨 맛쎄이 퍼블릭 리미티드 컴파니 금속을 함유하는 염기성 이온교환수지의 회화에 의한금속의 회수방법
KR20030041841A (ko) * 2001-11-21 2003-05-27 쉬플리 캄파니, 엘.엘.씨. 촉매 금속의 회수방법
JP2005002414A (ja) * 2003-06-12 2005-01-06 Maezawa Ind Inc 溶液中の貴金属の回収方法
KR20100113678A (ko) * 2009-04-14 2010-10-22 전북대학교산학협력단 유가금속의 회수방법

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KR20120103082A (ko) 2012-09-19
KR101224503B1 (ko) 2013-02-04
WO2012121496A2 (ko) 2012-09-13
CN103502484A (zh) 2014-01-08

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