MX2018007988A - Metodo para producir fibras de carbono de fibras comerciales multiproposito. - Google Patents

Metodo para producir fibras de carbono de fibras comerciales multiproposito.

Info

Publication number
MX2018007988A
MX2018007988A MX2018007988A MX2018007988A MX2018007988A MX 2018007988 A MX2018007988 A MX 2018007988A MX 2018007988 A MX2018007988 A MX 2018007988A MX 2018007988 A MX2018007988 A MX 2018007988A MX 2018007988 A MX2018007988 A MX 2018007988A
Authority
MX
Mexico
Prior art keywords
tows
filaments
stabilized
precursor fiber
carbon fibers
Prior art date
Application number
MX2018007988A
Other languages
English (en)
Inventor
K Naskar Amit
D Jackson Connie
Original Assignee
Ut Battelle Llc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ut Battelle Llc filed Critical Ut Battelle Llc
Publication of MX2018007988A publication Critical patent/MX2018007988A/es

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Classifications

    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F9/00Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
    • D01F9/08Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
    • D01F9/12Carbon filaments; Apparatus specially adapted for the manufacture thereof
    • D01F9/14Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
    • D01F9/20Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products
    • D01F9/21Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D01F9/22Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from polyacrylonitriles
    • D01F9/225Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from polyacrylonitriles from stabilised polyacrylonitriles

Landscapes

  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Textile Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Inorganic Fibers (AREA)
  • Artificial Filaments (AREA)

Abstract

Se describe un método para producir fibras de carbono, incluye el paso de proporcionar filamentos de fibra de polímero precursores de poliacrilonitrilo. Los filamentos precursores de poliacrilonitrilo incluyen de 87-97% en mol de acrilonitrilo, y menor que 0.5% en mol de grupos funcionales aceleradores. Los filamentos no son más de 3 deniers por filamento. Los filamentos de fibra precursora de poliacrilonitrilo se pueden disponer en estopas de al menos 150,000 deniers por 2.54 cm (pulgada) de ancho. Las estopas de fibra precursora de poliacrilonitrilo dispuestas se estabilizan al calentar las estopas en al menos una zona de oxidación que contiene gas oxígeno y se mantiene en una primera temperatura T1 mientras se estiran las estopas al menos 10% para producir una estopa de fibra precursora estabilizada. Las estopas de fibra precursoras estabilizadas se carbonizan al hacer pasar las estopas de fibra precursoras estabilizadas a través una zona de carbonización. También se describen fibras de carbono conocidas por el proceso.
MX2018007988A 2015-12-31 2016-12-30 Metodo para producir fibras de carbono de fibras comerciales multiproposito. MX2018007988A (es)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201562273559P 2015-12-31 2015-12-31
US201662305232P 2016-03-08 2016-03-08
PCT/US2016/069537 WO2017117544A1 (en) 2015-12-31 2016-12-30 Method of producing carbon fibers from multipurpose commercial fibers

Publications (1)

Publication Number Publication Date
MX2018007988A true MX2018007988A (es) 2018-11-09

Family

ID=59225459

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2018007988A MX2018007988A (es) 2015-12-31 2016-12-30 Metodo para producir fibras de carbono de fibras comerciales multiproposito.

Country Status (10)

Country Link
US (3) US10407802B2 (es)
EP (1) EP3397797B1 (es)
JP (1) JP2019500511A (es)
KR (1) KR20180098666A (es)
CN (1) CN108431310A (es)
AU (1) AU2016381341B2 (es)
CA (1) CA3008672A1 (es)
MX (1) MX2018007988A (es)
RU (1) RU2018126669A (es)
WO (1) WO2017117544A1 (es)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2018083734A1 (ja) * 2016-11-01 2018-05-11 日産自動車株式会社 複合材料用強化基材、複合材料および複合材料用強化基材の製造方法
TWI654240B (zh) 2017-11-22 2019-03-21 財團法人工業技術研究院 碳纖維前驅物組合物以及碳纖維前驅物之製備方法
KR102197333B1 (ko) * 2020-08-04 2021-01-04 효성첨단소재 주식회사 폴리아크릴로니트릴계 내염화 섬유, 탄소섬유 및 그의 제조방법
CN112708971B (zh) * 2021-01-13 2022-11-25 荣成碳纤维科技有限公司 一种碳纤维氧化炉的自动防火、灭火方法及装置
WO2023234956A2 (en) * 2021-06-04 2023-12-07 University Of Tennessee Research Foundation Thermoplastic impregnation of large tow textile grade carbon fiber
CN113186718B (zh) * 2021-06-10 2022-11-22 浙江工商大学 一种螯合纤维pan-daam、其制备方法及其应用
US20230001618A1 (en) * 2021-06-30 2023-01-05 Connie Jackson Carbon-fiber fuel tank
WO2023023640A1 (en) * 2021-08-20 2023-02-23 Hexcel Corporation Carbon fibers having improved strength and modulus and an associated method and apparatus for preparing same
WO2023094650A2 (en) * 2021-11-29 2023-06-01 Teijin Carbon Europe Gmbh Continuous oven

Family Cites Families (90)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2913802A (en) 1953-07-16 1959-11-24 Johns Manville Thermal modification of acrylonitrile yarns
US3296341A (en) 1963-07-15 1967-01-03 Dow Chemical Co Method for impregnating acrylonitrile polymer fibers to improve dyeability
GB1110791A (en) 1964-04-24 1968-04-24 Nat Res Dev The production of carbon fibres
GB1196599A (en) 1966-11-24 1970-07-01 Courtaulds Ltd Polyacrylonitrile and carbon fibre production
US3607817A (en) 1967-03-09 1971-09-21 Celanese Corp Production of dyeable polyacrylonitrile compositions and articles
US3466716A (en) * 1967-06-02 1969-09-16 Du Pont Twisted chute for improved tow stacking
US3533743A (en) 1968-05-28 1970-10-13 Great Lakes Carbon Corp Process for the manufacture of continuous high modulus carbon yarns and monofilaments
US3539295A (en) 1968-08-05 1970-11-10 Celanese Corp Thermal stabilization and carbonization of acrylic fibrous materials
JPS527796B1 (es) 1968-10-04 1977-03-04
NL165611B (nl) 1968-10-04 Accumulateurs Fixes Elektrochemische cel met een lithiumelektrode.
US3607059A (en) 1969-04-02 1971-09-21 Great Lakes Carbon Corp Process for the manufacture of filamentary carbon products
GB1324041A (en) 1969-10-31 1973-07-18 Nippon Carbon Co Ltd Method of producing carbon fibres
US3716331A (en) 1970-04-10 1973-02-13 Union Carbide Corp Process for producing carbon fibers having a high young's modulus of elasticity
GB1354880A (en) 1970-09-23 1974-06-05 Nat Res Dev Carbon fibre tow production
US3917776A (en) 1970-12-12 1975-11-04 Mitsubishi Rayon Co Process for producing carbon fiber
GB1370366A (en) 1970-12-12 1974-10-16 Mitsubishi Rayon Co Production of carbon fibres
US4002426A (en) 1971-01-25 1977-01-11 Celanese Corporation Production of stabilized non-burning acrylic fibers and films
US3965227A (en) 1971-06-22 1976-06-22 Ceskoslovenska Akademie Ved Method of simultaneously manufacturing acrylic fibers and nitrates
US3914394A (en) 1973-02-15 1975-10-21 Japan Exlan Co Ltd Process for producing carbon fibers
JPS5133211B2 (es) 1974-02-04 1976-09-18
US3945093A (en) 1974-06-10 1976-03-23 Hitco Method and apparatus for producing high modulus bixial fabric
GB1498721A (en) 1975-02-17 1978-01-25 Morganite Modmor Ltd Production of carbon fibre
JPS51119833A (en) 1975-04-08 1976-10-20 Toho Rayon Co Ltd A process for manufacturing carbon fibers
JPS5231124A (en) 1975-09-01 1977-03-09 Japan Exlan Co Ltd Improved preparation of carbon fiber
US4100004A (en) 1976-05-11 1978-07-11 Securicum S.A. Method of making carbon fibers and resin-impregnated carbon fibers
JPS5920004B2 (ja) * 1977-03-23 1984-05-10 日本エクスラン工業株式会社 炭素繊維の製造方法
GB2014971A (en) * 1977-12-14 1979-09-05 Securicum Sa Carbon Fibre
US4336022A (en) 1979-08-01 1982-06-22 E. I. Du Pont De Nemours And Company Acrylic precursor fibers suitable for preparing carbon or graphite fibers
US4698413A (en) 1979-08-01 1987-10-06 E. I. Du Pont De Nemours And Company Acrylic fiber suitable for preparing carbon or graphite fibers
JPS5663014A (en) 1979-10-25 1981-05-29 Toho Rayon Co Ltd Flameproofing and carbonizing method of acrylonitrile fiber
CA1156409A (en) 1980-10-02 1983-11-08 Roger T. Pepper Method of producing carbon fiber and product thereof
US4526770A (en) 1980-10-02 1985-07-02 Fiber Materials, Inc. Method of producing carbon fiber and product thereof
JPS58139645A (ja) 1982-02-10 1983-08-19 三菱電機株式会社 発電所母線切換装置
JPS59199809A (ja) 1983-04-20 1984-11-13 Japan Exlan Co Ltd 高強力ポリアクリロニトリル系繊維及びその製造法
US5004590A (en) * 1983-08-05 1991-04-02 Hercules Incorporated Carbon fibers
WO1985001752A1 (en) 1983-10-13 1985-04-25 Mitsubishi Rayon Co., Ltd. Carbon fibers with high strength and high modulus, and process for their production
US4610860A (en) * 1983-10-13 1986-09-09 Hitco Method and system for producing carbon fibers
US5078926A (en) 1984-03-07 1992-01-07 American Cyanamid Company Rapid stabilization process for carbon fiber precursors
US4874563A (en) 1984-03-15 1989-10-17 Basf Structural Materials Inc. Process for preparing tows from composite fiber blends
US4728395A (en) 1984-10-12 1988-03-01 Stackpole Fibers Company, Inc. Controlled resistivity carbon fiber paper and fabric sheet products and method of manufacture
US4726770A (en) 1985-01-12 1988-02-23 Kurer Hans G Tooth restoration and means for use therein
KR890005273B1 (ko) 1985-10-09 1989-12-20 미쓰비시레이욘 가부시끼가이샤 탄소 섬유의 제조방법
EP0223199B1 (en) 1985-11-18 1992-05-27 Toray Industries, Inc. Process for producing high-strenght, high-modulus carbon fibers
US4661336A (en) 1985-11-25 1987-04-28 Hitco Pretreatment of pan fiber
JPS62257422A (ja) 1986-04-25 1987-11-10 Mitsubishi Rayon Co Ltd 炭素繊維の製法
US5268158A (en) 1987-03-11 1993-12-07 Hercules Incorporated High modulus pan-based carbon fiber
JPS6445830A (en) 1987-08-13 1989-02-20 Toray Industries High performance carbon fiber cord
US5066433A (en) 1988-02-16 1991-11-19 Hercules Incorporated Method of manufacturing carbon fiber using preliminary stretch
CA1327258C (en) 1988-02-16 1994-03-01 James Toner Paul Jr. Method of manufacturing carbon fiber using preliminary stretch
US4935180A (en) 1988-08-25 1990-06-19 Basf Aktiengesellschaft Formation of melt-spun acrylic fibers possessing a highly uniform internal structure which are particularly suited for thermal conversion to quality carbon fibers
CA2007067A1 (en) * 1989-01-11 1990-07-11 Martin E. Ketterer Composite metal-loaded carbon fibers
US5256344A (en) 1989-02-23 1993-10-26 Hercules Incorporated Process of thermally stabilizing pan fibers
US4933128A (en) 1989-07-06 1990-06-12 Basf Aktiengesellschaft Formation of melt-spun acrylic fibers which are well suited for thermal conversion to high strength carbon fibers
CA2044268A1 (en) 1989-11-01 1991-05-02 Francis P. Mccullough, Jr. Linear carbonaceous fiber with improved elongatability
JPH0633531A (ja) 1992-07-17 1994-02-08 Shigekiyo Tsuge プラスチック発泡体パネルおよび三層構造パネル
JPH10121325A (ja) 1996-10-14 1998-05-12 Toray Ind Inc 炭素繊維用前駆体繊維束とその製造方法および炭素繊維の製造方法
US5804108A (en) 1996-10-31 1998-09-08 Wilkinson; Kenneth Process for the preparation of carbon fiber
US6054214A (en) 1996-10-31 2000-04-25 Wilkinson; Kenneth Process for the preparation of carbon fiber
JPH10167564A (ja) 1996-12-05 1998-06-23 Toray Ind Inc 炭素繊維パッケージおよび炭素繊維梱包体
US6268450B1 (en) 1998-05-11 2001-07-31 Solutia Inc. Acrylic fiber polymer precursor and fiber
DE69928436T2 (de) 1998-07-22 2006-08-03 Mitsubishi Rayon Co., Ltd. Vorlaüferfaser aus acrylonitril für kohlenstofffaser und herstellungsverfahren
JP2000336529A (ja) 1999-05-28 2000-12-05 Toray Ind Inc 炭素繊維の製造方法
GB2367031B (en) 1999-06-15 2003-09-03 Mitsubishi Rayon Co Acrylic yarn as thick carbon fiber precursor and method for producing the same
JP3552953B2 (ja) 1999-07-05 2004-08-11 日本電信電話株式会社 予備vp設計装置、予備vp設計方法及び記録媒体
US6210622B1 (en) 1999-07-19 2001-04-03 Arteva North America S.A.R.L. Process of making polymeric fibers
US7223376B2 (en) 2000-02-10 2007-05-29 Industrial Technology And Equipment Company Apparatus and method for making carbon fibers
US6641915B1 (en) 2000-05-09 2003-11-04 Mitsubishi Rayon Co., Ltd. Acrylonitrile-based fiber bundle for carbon fiber precursor and method for preparation thereof
JP2001355120A (ja) 2000-06-12 2001-12-26 Toho Tenax Co Ltd ラージトウプリカーサー、その製造方法及び炭素繊維の製造方法
JP4630193B2 (ja) 2004-02-13 2011-02-09 三菱レイヨン株式会社 炭素繊維前駆体繊維束の製造方法及び製造装置
JP4360233B2 (ja) 2004-03-11 2009-11-11 東レ株式会社 ゴルフシャフト
KR101335140B1 (ko) 2005-12-13 2013-12-03 도레이 카부시키가이샤 탄소 섬유, 탄소 섬유 제조용 폴리아크릴로니트릴계 전구체섬유의 제조 방법, 및 탄소 섬유의 제조 방법
CA2782617C (en) 2006-09-06 2014-03-11 Mitsubishi Rayon Co., Ltd. Carbon fiber package and process for producing the same
US7749479B2 (en) 2006-11-22 2010-07-06 Hexcel Corporation Carbon fibers having improved strength and modulus and an associated method and apparatus for preparing same
JP5012089B2 (ja) 2007-03-02 2012-08-29 東レ株式会社 炭素繊維前駆体繊維束およびその製造方法
JP5207796B2 (ja) * 2008-03-28 2013-06-12 三菱レイヨン株式会社 耐炎化処理装置および前駆体繊維束の耐炎化処理方法
CN101560701B (zh) 2009-05-13 2010-12-08 北京化工大学 一种高强度炭纤维的制备方法
US8608992B2 (en) * 2010-09-24 2013-12-17 The Board Of Trustees Of The University Of Illinois Carbon nanofibers derived from polymer nanofibers and method of producing the nanofibers
EP2628827B1 (en) 2010-10-13 2020-07-08 Mitsubishi Chemical Corporation Carbon fiber bundle, and uses thereof
WO2013015210A1 (ja) 2011-07-22 2013-01-31 三菱レイヨン株式会社 ポリアクリロニトリル系共重合体、炭素繊維用ポリアクリロニトリル系前駆体繊維、炭素繊維束、耐炎化繊維束の製造方法、および炭素繊維束の製造方法
KR101528115B1 (ko) 2011-10-04 2015-06-10 도레이 카부시키가이샤 탄소 섬유 강화 열가소성 수지 조성물, 성형 재료, 프리프레그, 및 이들의 제조 방법
DE202012013359U1 (de) 2011-10-26 2016-07-15 Deutsche Institute Für Textil- Und Faserforschung Denkendorf Carbonfasern und Carbonfaser-Precursoren
CN102505189B (zh) * 2011-10-27 2013-05-01 北京化工大学 高强度高模量碳纤维的制备方法
KR101417217B1 (ko) 2011-11-22 2014-07-09 현대자동차주식회사 탄소섬유용 전구체 섬유의 제조방법
TWI527946B (zh) * 2012-04-12 2016-04-01 三菱麗陽股份有限公司 碳纖維前驅體丙烯酸纖維束及其製造方法、熱氧化處理爐以及碳纖維束的製造方法
KR101984362B1 (ko) 2012-04-18 2019-05-30 미쯔비시 케미컬 주식회사 탄소 섬유속 및 탄소 섬유속의 제조 방법
KR101813433B1 (ko) 2012-04-18 2017-12-28 미쯔비시 케미컬 주식회사 탄소 섬유속 및 탄소 섬유의 제조 방법
CN103572411B (zh) 2012-07-31 2015-09-23 金发科技股份有限公司 聚丙烯腈基碳纤维、制备方法及其应用
CN104372445B (zh) 2013-08-13 2018-03-09 中国石油化工股份有限公司 一种共聚序列分布均匀的聚丙烯腈碳纤维的制备方法
JP2015183165A (ja) * 2014-03-26 2015-10-22 東レ株式会社 アクリロニトリル系共重合体およびポリアクリロニトリル系炭素繊維前駆体繊維、炭素繊維の製造方法
JP6295890B2 (ja) 2014-08-27 2018-03-20 三菱ケミカル株式会社 炭素繊維束

Also Published As

Publication number Publication date
WO2017117544A1 (en) 2017-07-06
CN108431310A (zh) 2018-08-21
EP3397797A4 (en) 2019-07-31
US10961642B2 (en) 2021-03-30
US10407802B2 (en) 2019-09-10
EP3397797B1 (en) 2023-08-30
EP3397797A1 (en) 2018-11-07
AU2016381341A1 (en) 2018-07-05
JP2019500511A (ja) 2019-01-10
US20170191194A1 (en) 2017-07-06
AU2016381341B2 (en) 2021-06-03
CA3008672A1 (en) 2017-07-06
US20210198816A1 (en) 2021-07-01
KR20180098666A (ko) 2018-09-04
RU2018126669A (ru) 2020-02-03
US20190382925A1 (en) 2019-12-19

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