KR950701957A - 고온에서 조작하는 냉동압축기용 폴리올 에스테르 윤활제(polyol ester lubricats for refrigerating compressors operating at high temperatures) - Google Patents

고온에서 조작하는 냉동압축기용 폴리올 에스테르 윤활제(polyol ester lubricats for refrigerating compressors operating at high temperatures)

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Publication number
KR950701957A
KR950701957A KR1019940704426A KR19940704426A KR950701957A KR 950701957 A KR950701957 A KR 950701957A KR 1019940704426 A KR1019940704426 A KR 1019940704426A KR 19940704426 A KR19940704426 A KR 19940704426A KR 950701957 A KR950701957 A KR 950701957A
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South Korea
Prior art keywords
acyl groups
mixture
group
carbon atoms
acyl
Prior art date
Application number
KR1019940704426A
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English (en)
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KR100240193B1 (en
Inventor
이.쉬너 니콜라스
알. 질러 유겐
Original Assignee
웨인 씨.제쉬크
헨켈 코포레이션
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Publication date
Priority claimed from PCT/US1992/004438 external-priority patent/WO1993024585A1/en
Priority claimed from PCT/US1993/004890 external-priority patent/WO1993025629A2/en
Application filed by 웨인 씨.제쉬크, 헨켈 코포레이션 filed Critical 웨인 씨.제쉬크
Publication of KR950701957A publication Critical patent/KR950701957A/ko
Application granted granted Critical
Publication of KR100240193B1 publication Critical patent/KR100240193B1/ko

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    • C09K5/00—Heat-transfer, heat-exchange or heat-storage materials, e.g. refrigerants; Materials for the production of heat or cold by chemical reactions other than by combustion
    • C09K5/02—Materials undergoing a change of physical state when used
    • C09K5/04—Materials undergoing a change of physical state when used the change of state being from liquid to vapour or vice versa
    • C09K5/041—Materials undergoing a change of physical state when used the change of state being from liquid to vapour or vice versa for compression-type refrigeration systems
    • C09K5/044—Materials undergoing a change of physical state when used the change of state being from liquid to vapour or vice versa for compression-type refrigeration systems comprising halogenated compounds
    • C09K5/045—Materials undergoing a change of physical state when used the change of state being from liquid to vapour or vice versa for compression-type refrigeration systems comprising halogenated compounds containing only fluorine as halogen
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Abstract

본 발명은, 장애된 폴리올, 가장 바람직하게는 일반적으로 약산의 펜타에리트리톨과 혼합된 디-펜타에리트리톨 및 이소-펜탄산 및 이소-노산산 각각을 최소한 약간 포함하는 카르복실산의 혼합물의 혼합된 에스테르에 의해 제공되는, 염소가 없는 하이드로플루오로카아본 냉매작용유체를 사용하는 대형 공기조화기 및 냉동 압축기에 대한 고품질 윤활제에 관한 것이다.

Description

고온에서 조작하는 냉동압축기용 폴리올 에스테르 윤활제(POLYOL ESTER LUBRICATS FOR REFRIGERATING COMPRESSORS OPERATING AT HIGH TEMPERATURES)
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (20)

  1. 40℃에서 45내지 157센티스토크의 절도를 갖는 액체이고, 폴리올에스테르 분사의 혼합물로 구성되는, 윤활제 또는 윤활제 원료로서 사용하기 위해 적합한 물질의 조성물로서, 플리을 에스테르 분자의 혼합물에서, PE, DPE 및 TPE로 부터 유도된 알콜올 부분으로 구성된 군으로 부터 알코올 부분의 85%이상이 선택되고, DPE 및 TPE로 부터 유도된 알코올 부분으로 구성된 군으로 부터 알코올 부분의 20% 이상이 선택되고, 각각 C4내지 C12의 모든 직쇄 및 촉쇄 1염기 및 2염기 카르복실단의 아실기로 구성된 군으로 부터 아실기의 92%이상이 선택되며, 알코올 부분 및 아실기는, (a)혼합물중에서 총 3%이상의 아실기는 i-C5산의 아실기이고; (b)8개 이상의 탄소원자를 함유하고 가지가 달리지 않는 혼합물중의 아실기의 % 대 6개 이하의 탄소원자를 함유하고 가지가 달린 혼합물중의 아실기의 %의 비는 1.56이하이고; (C)가지가 달리거나 또한 그렇지 않은 9개 이상의 탄소원자를 함유하는 혼합물중의 아실기의 %는 81%이하이고; (d)에스테르 혼합물중의 아실기의 2%이하는 2개 이상의 카르복실기를 갖는 산분자의 일부이고; (e)혼합물의 20%이상의 아실기는 트리메틸 헥사노일 아실기 중 하나이고, 에스테르 혼합물중의 7.5%이하의 아실기는 2염기성인 것으로 제한되도록 선택됨을 특징으로 하는 조성물.
  2. 제1항에 있어서, 40℃에서 51 내지 145센티스토크의 점도를 갖고 폴리올 에스테르 분자의 혼합물로 구성되는 조성물로서, 여기에서 DPE 및 TPE로 부터 유도된 알코올 부분으로 구성된 군으로 부터 알코올 부분의 26%이상이 선택 되고, 알코올 부분 및 아실기는, (a)혼합물에서 아실기의 총 7%이상은 i-C5산의 아실기이고; (b)8개 이상의 탄소원자를 함유하고 가지가 달리지 않은 혼합물중의 아실기의 % 대 6개 이하의 탄소원자를 함유하고 가지가 달린 혼합물중의 아실기의 %의 비는 1.56이하이고; (C)가지가 달리거나 또는 그렇지 않은 9개 이상의 탄소 원자를 함유하는 혼합물중의 아실기의 %를 67%이하이고; (e)혼합물중의 아실기의 29%이상은 트리메틸 헥산산중 하나이고, 산혼합물중의 아실기는 6.0%이하는 2염기성인 것으로 제한되도록 선택됨을 특징으로 하는 조성물.
  3. 제2항에 있어서, 40℃에서 51 내지 134센티스토크의 점도를 갖고, 폴리올 에스테르 분자의 혼합물로 구성되는 조성물로서, 여기에서, PE, DPE 및 TPE로 부터 유로된 알코올 부분으로 구성된 군으로 부터 알코올 부분의 95%이상이 선택되고, DPE 및 TPE로 부터 유도된 알코올 부분으로 구성된 군으로 부터 알코올 부분의 32%이상이 선택되고, 각각 4내지 12개의 탄소원자를 갖는 모든 직쇄 및 측쇄 1염기성 카르복실산의 아실기로 구성된 군으로부터 아실기의 95%이상이 선택되며, 상기 알코올 부분 및 아실기는, (a)혼합물중에서 총 10%이상의 아실기는 i-C5산의 아기실이고; (b)8개 이상의 탄소원자를 함유하고 가지가 달리지 않은 혼합물중의 아실기의 %대 6개 이하의 탄소원자를 함유하고 가지가 달린 혼합물중의 아실기의 %의 비는 1.21이하이고; (C)가지가 달리거나 또는 그렇지 않은 적어도 9개의 탄소원자를 함유하는 에스테르 혼합물중의 아실기의 %는 67%이하이고; (d)에스테르 혼합물중의 아실기의 1%이하는 각각 2개 이상의 카르복실기를 함유하고; (e)혼합물중의 총 35%이상의 아실기는 트리메틸 핵산산의 아실기중 하나이고 에스테르 혼합물중의 3%이하는 2염기성 인 것으로 제한되도록 선택됨을 특징으로 하는 조성물.
  4. 제3항에 있어서, 40에서 51 내지 123센티스토크의 점도는 갖고, 폴리올 에스테르 분자의 혼합물로 구성되는 조성물로서, 알코올 부분 및 아실기는, (a)혼합물중에서 총 14%이상의 i-C5산의 아실기이고; (b)8개 이상의 탄소원자를 함유하고 가지가 달리치 않은 혼합물중의 아실기의 % 대 6개 이하의 탄소원자를 함유하고 가지가 달린 아실기의 %의 비는 1.00이하이고; (c)가지 달리거나 또는 그렇지 않은 9개 이상의 탄소원자를 함유하는 혼합물중의 아실기의 %는 49%이하이고; (d)에스테르 혼합물중의 아실기의 0.4%이하는 각각 2개 이상의 카드복실기를 함유하고; (e)혼합물중의 아실기의 총 35%이상은 트리메틸 핵산산중 하나의 아실기이고, 혼합물 중의 아실기의 총 35%이상은 3,3,5-트리메틸 헥사노일기이고, 에스테르 혼합물중의 아실기의 1.7%이하는 2염기성인 것으로 제한되도록 선택됨을 특징으로 하는 조성물.
  5. 제4항에 있어서, 폴리올에스테르 분자의 혼합물로 구성되는 조성물로서, 각각 4내지 12개의 탄소원자를 갖는 모든 직쇄 및 측쇄 1염기성 및 2염기성 카르복실산의 아실기로 구성된 군으로 부터 아실기의 95%이상이 선택되고, DPE 및 TPE로 부터 유도된 알코올 분자로 구성된 군으로 부터 알코올 부분의 35%이상이 선택되며, 알코올 부분 및 아실기는, (a)에스테르 혼합물중의 아실기의 총 16%이상은 i-C5의 아실기이고 (b)8개 이상의 탄소원자를 함유하고 가지달리지 않은 혼합물중의 아실기의 %대 5개 이하의 탄소원자를 함유하고 가지달린 혼합물중의 아실기의 %의 비는 1.00이하이고; (c)가지달리거나 또는 그렇지 않은 9개 이상의 탄소원자를 함유하는 혼합물중의 아실기의 %는 49%이하이고; (e)에스테르 혼합물중의 아실기의 41%이상은 트리메틸 헥산산의 아실기이고, 혼합물중의 아실기의 29%이상은 3,3,5-트리메틸헥사노일기인 것으로 제한되도록 선택됨을 특징으로 하는 조성물.
  6. 95중향%이상의 제5항에 따르는 조성물, 및 산화 방지성 및 열안정성 개량제, 부식억제제, 금속 탈활성화제, 윤활성 첨가제, 점도지수 개량제, 용융점 강하제, 청량제, 분산제, 발포방지제, 내마멸제 및 극압 저항성 첨가제로 구성된 군으로 부터 선택되는 5중량%이하의 하나 이상의 첨가제로 구성되는 배합된 윤활제.
  7. 92중향%이상의 제3항에 따르는 조성물, 및 산화 방지성 및 열안정성 개량제, 부식억제제, 금속 탈활성화제, 윤활성 첨가제, 점도지수 개량제, 용융점 강하제, 청량제, 분산제, 발포방지제, 내마멸제 및 극압 저항성 첨가제로 구성된 군으로 부터 선택되는 8중량%이하의 하나 이상의 첨가제로 구성되는 배합된 윤활제.
  8. 92중향%이상의 제2항에 따르는 조성물, 및 산화 방지성 및 열안정성 개량제, 부식억제제, 금속 탈활성화제, 윤활성 첨가제, 점도지수 개량제, 용융점 강하제, 청량제, 분산제, 발포방지제, 내마멸제 및 극압 저항성 첨가제로 구성된 군으로 부터 선택되는 5중량%이하의 하나 이상의 첨가제로 구성되는 배합된 윤활제.
  9. 92중향%이상의 제1항에 따르는 조성물, 및 산화 방지성 및 열안정성 개량제, 부식억제제, 금속 탈활성화제, 윤활성 첨가제, 점도지수 개량제, 용융점 강하제, 청량제, 분산제, 발포방지 제, 내마멸제 및 극압 저항성 첨가제로 구성된 군으로 부터 선택되는 8중량%이하의 하나 이상의 첨가제로 구성되는 배합된 윤활제.
  10. 펜타플루오로에탄, 1,1-디플루오로에탄, 1,1,1-트리플루오로에탄, 테트라 플루오로에탄 및 이들의 혼합물로 구성된 군으로 부터 선택된 85%이상의 1차 열전달 유체, 긴 15중량%이하의 제9항에 따르는 윤활제로 구성되는 냉매작용유체.
  11. 펜타플루오로에탄, 1,1-디플루오로에탄, 1,1,1-트리플루오로에탄, 테트라 플루오로에탄 및 이들의 혼합물로 구성된 군으로 부터 선택된 85%이상의 1차 열전달 유체, 긴 15중량%이하의 제8항에 따르는 윤활제로 구성되는 냉매작용유체,
  12. 펜타플루오로에탄, 1,1-디플루오로에탄, 1,1,1-트리플루오로에탄, 테트라 플루오로에탄 및 이들의 혼합물로 구성된 군으로 부터 선택된 85%이상의 1차 열전달 유체, 긴 15중량%이하의 제7항에 따르는 윤활제로 구성되는 냉매작용유체.
  13. 85중량%이상의 1,1,1,2-테트라 플루오로에탄 및 15중량%이하의 제6항에 따르는 윤활제로 구성되는 냉매작용유체.
  14. 펜타플루오로에탄, 1,1-디플로오로에탄, 1,1,1-트리플로오로에탄, 테트라 플루오로에탄 및 이들의 혼합물로 구성된 군으로 부터 선택된 85%이상의 1차 열전달 유체, 긴 15중량%이하의 제5항에 따르는 윤활제로 구성되는 냉매작용유체.
  15. 펜타플루오로에탄, 1,1-디플루오로에탄, 1,1,1-트리플루오로에탄, 테트라 플루오로에탄 및 이들의 혼합물로 구성된 군으로 부터 선택된 85%이상의 1차 열전달 유체, 긴 15중량%이하의 제4항에 따르는 윤활제로 구성되는 냉매작용유체.
  16. 펜타플루오로에탄, 1.1-디플루오로에탄, 1,1,1-트리플루오로에탄, 테트라 플루오로에탄 및 이들의 혼합물로 구성된 군으로 부터 선택된 85%이상의 1차 열전달 유체, 긴 15S중량%이하의 제3항에 따르는 윤활제로 구성되는 냉매작용유체.
  17. 펜타플루오로에탄, 1,1-디플루오로에탄, 1.1,1-트리플루오로에탄, 테트라 플루오로에탄 및 이들의 혼합물로 구성된 군으로 분터 선택된 85%이상의 1차 열전달 유체, 긴 15중량%이하의 제2항에 따르는 윤활제로 구성되는 냉매작용유체.
  18. 펜타플루오로에탄, 1,1-디플루오로에탄, 1.1.1-트리플루오로에탄, 테트라 플루오로에탄 및 이들의 혼합물로 구성된 군으로 부터 선택된 85%이상의 1차 열전달 유체, 및 15중량%이하의 재1항에 따르는 윤활제로 구성되는 냉매작용유체.
  19. 85중량%이상의 1,1,2,2-테트라플루오로에탄 및 15중량%이하의 제6항에 따르는 윤활제로 구성된 열전달 유체의 순환식 압축, 액화, 팽창 및 증발로 이루어지는 냉동기를 조작하기 위한 방법.
  20. 펜타플루오로에탄, 1,1-디플루오로에탄, 1,1,1-트리플루오로에탄, 테트라 플루오로에탄 및 이들의 혼합물로 구성된 군으로 부터 선택된 85%이상의 1차 열전달 유체, 및 15중량%이하의 제1항에 따르는 윤활제로 구성된 열전달 유체의 순환실, 압축, 액화, 팽창 및 증발로 이루어지는, 냉동기를 조작하기 위한 방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019940704426A 1992-06-03 1994-12-03 Polyol ester lubricants for refrigerating compessors operating at high temperatures KR100240193B1 (en)

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US2919493A 1993-03-10 1993-03-10
US08/029,194 1993-03-10
PCT/US1993/004890 WO1993025629A2 (en) 1992-06-03 1993-05-27 Polyol ester lubricants for refrigerating compressors operating at high temperatures

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CA2137263A1 (en) 1993-12-23
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DE69329028D1 (de) 2000-08-17
CA2137263C (en) 2003-10-14
US5906769A (en) 1999-05-25
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US6267906B1 (en) 2001-07-31

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