JPS6141904B2 - - Google Patents

Info

Publication number: JPS6141904B2
Authority: JP; Japan
Prior art keywords: carbonate; unsaturated; inorganic adsorbent; oxidizing agent; coloring
Prior art date: 1978-10-30
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

JP13252878A

Other languages

English (en)

Japanese (ja)

Other versions

JPS5559144A (en

Inventor

Kazuo Yomo

Toshiaki Shigemune

Yoshinori Mizumoto

Osamu Nomura

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Tokuyama Corp

Original Assignee

Tokuyama Corp

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1978-10-30

Filing date

1978-10-30

Publication date

1986-09-18

1978-10-30 Application filed by Tokuyama Corp filed Critical Tokuyama Corp

1978-10-30 Priority to JP13252878A priority Critical patent/JPS5559144A/ja

1980-05-02 Publication of JPS5559144A publication Critical patent/JPS5559144A/ja

1986-09-18 Publication of JPS6141904B2 publication Critical patent/JPS6141904B2/ja

Status Granted legal-status Critical Current

Links

239000003463 adsorbent Substances 0.000 claims description 31
238000000034 method Methods 0.000 claims description 20
239000007800 oxidant agent Substances 0.000 claims description 17
-1 carbonate compound Chemical class 0.000 claims description 16
239000002253 acid Substances 0.000 claims description 10
229910052500 inorganic mineral Inorganic materials 0.000 claims description 9
239000011707 mineral Substances 0.000 claims description 9
150000001875 compounds Chemical class 0.000 claims description 2
150000004649 carbonic acid derivatives Chemical class 0.000 description 31
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 20
241001550224 Apha Species 0.000 description 15
238000004040 coloring Methods 0.000 description 12
239000000203 mixture Substances 0.000 description 12
239000012043 crude product Substances 0.000 description 11
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 9
235000010755 mineral Nutrition 0.000 description 8
239000012044 organic layer Substances 0.000 description 7
239000000243 solution Substances 0.000 description 7
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
239000005708 Sodium hypochlorite Substances 0.000 description 6
MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 6
230000000694 effects Effects 0.000 description 6
239000012535 impurity Substances 0.000 description 6
SUKJFIGYRHOWBL-UHFFFAOYSA-N sodium hypochlorite Chemical compound [Na+].Cl[O-] SUKJFIGYRHOWBL-UHFFFAOYSA-N 0.000 description 6
MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 5
JKJWYKGYGWOAHT-UHFFFAOYSA-N bis(prop-2-enyl) carbonate Chemical group C=CCOC(=O)OCC=C JKJWYKGYGWOAHT-UHFFFAOYSA-N 0.000 description 5
238000006243 chemical reaction Methods 0.000 description 5
JHQVCQDWGSXTFE-UHFFFAOYSA-N 2-(2-prop-2-enoxycarbonyloxyethoxy)ethyl prop-2-enyl carbonate Chemical compound C=CCOC(=O)OCCOCCOC(=O)OCC=C JHQVCQDWGSXTFE-UHFFFAOYSA-N 0.000 description 4
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 4
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 4
239000006103 coloring component Substances 0.000 description 4
238000000746 purification Methods 0.000 description 4
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 3
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 3
ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 3
239000007864 aqueous solution Substances 0.000 description 3
230000000052 comparative effect Effects 0.000 description 3
229910001873 dinitrogen Inorganic materials 0.000 description 3
238000010438 heat treatment Methods 0.000 description 3
238000006116 polymerization reaction Methods 0.000 description 3
239000000047 product Substances 0.000 description 3
239000012264 purified product Substances 0.000 description 3
239000002994 raw material Substances 0.000 description 3
238000001179 sorption measurement Methods 0.000 description 3
238000003756 stirring Methods 0.000 description 3
OSDWBNJEKMUWAV-UHFFFAOYSA-N Allyl chloride Chemical compound ClCC=C OSDWBNJEKMUWAV-UHFFFAOYSA-N 0.000 description 2
JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 2
229910000147 aluminium phosphate Inorganic materials 0.000 description 2
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
238000009835 boiling Methods 0.000 description 2
239000001569 carbon dioxide Substances 0.000 description 2
229910002092 carbon dioxide Inorganic materials 0.000 description 2
239000004927 clay Substances 0.000 description 2
238000001816 cooling Methods 0.000 description 2
239000007789 gas Substances 0.000 description 2
239000001301 oxygen Substances 0.000 description 2
229910052760 oxygen Inorganic materials 0.000 description 2
229920000642 polymer Polymers 0.000 description 2
239000000126 substance Substances 0.000 description 2
238000003786 synthesis reaction Methods 0.000 description 2
VZSRBBMJRBPUNF-UHFFFAOYSA-N 2-(2,3-dihydro-1H-inden-2-ylamino)-N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]pyrimidine-5-carboxamide Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C(=O)NCCC(N1CC2=C(CC1)NN=N2)=O VZSRBBMJRBPUNF-UHFFFAOYSA-N 0.000 description 1
BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
239000005909 Kieselgur Substances 0.000 description 1
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
229910021536 Zeolite Inorganic materials 0.000 description 1
XMUZQOKACOLCSS-UHFFFAOYSA-N [2-(hydroxymethyl)phenyl]methanol Chemical compound OCC1=CC=CC=C1CO XMUZQOKACOLCSS-UHFFFAOYSA-N 0.000 description 1
150000007513 acids Chemical class 0.000 description 1
230000004913 activation Effects 0.000 description 1
229910000288 alkali metal carbonate Inorganic materials 0.000 description 1
150000008041 alkali metal carbonates Chemical class 0.000 description 1
PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
CIPHOUPBLAOEKY-UHFFFAOYSA-N azepane-1-carbodithioate;azepan-1-ium Chemical compound C1CCCNCC1.SC(=S)N1CCCCCC1 CIPHOUPBLAOEKY-UHFFFAOYSA-N 0.000 description 1
WPBUMSXOUUWUAL-UHFFFAOYSA-N benzyl prop-2-enyl carbonate Chemical compound C=CCOC(=O)OCC1=CC=CC=C1 WPBUMSXOUUWUAL-UHFFFAOYSA-N 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
238000004061 bleaching Methods 0.000 description 1
239000006227 byproduct Substances 0.000 description 1
229910052799 carbon Inorganic materials 0.000 description 1
239000011203 carbon fibre reinforced carbon Substances 0.000 description 1
239000003054 catalyst Substances 0.000 description 1
239000003153 chemical reaction reagent Substances 0.000 description 1
230000007423 decrease Effects 0.000 description 1
HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 1
238000004821 distillation Methods 0.000 description 1
BGSFCOHRQUBESL-UHFFFAOYSA-N ethyl prop-2-enyl carbonate Chemical compound CCOC(=O)OCC=C BGSFCOHRQUBESL-UHFFFAOYSA-N 0.000 description 1
230000002349 favourable effect Effects 0.000 description 1
238000004817 gas chromatography Methods 0.000 description 1
239000011521 glass Substances 0.000 description 1
150000004820 halides Chemical class 0.000 description 1
230000002209 hydrophobic effect Effects 0.000 description 1
239000011261 inert gas Substances 0.000 description 1
239000007788 liquid Substances 0.000 description 1
239000007791 liquid phase Substances 0.000 description 1
238000004519 manufacturing process Methods 0.000 description 1
230000010534 mechanism of action Effects 0.000 description 1
YHLVIDQQTOMBGN-UHFFFAOYSA-N methyl prop-2-enyl carbonate Chemical compound COC(=O)OCC=C YHLVIDQQTOMBGN-UHFFFAOYSA-N 0.000 description 1
239000011259 mixed solution Substances 0.000 description 1
229930014626 natural product Natural products 0.000 description 1
229910017604 nitric acid Inorganic materials 0.000 description 1
230000003287 optical effect Effects 0.000 description 1
230000003647 oxidation Effects 0.000 description 1
238000007254 oxidation reaction Methods 0.000 description 1
230000001590 oxidative effect Effects 0.000 description 1
238000012856 packing Methods 0.000 description 1
239000012286 potassium permanganate Substances 0.000 description 1
CAEWJEXPFKNBQL-UHFFFAOYSA-N prop-2-enyl carbonochloridate Chemical compound ClC(=O)OCC=C CAEWJEXPFKNBQL-UHFFFAOYSA-N 0.000 description 1
UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
238000007670 refining Methods 0.000 description 1
238000004904 shortening Methods 0.000 description 1
229910000029 sodium carbonate Inorganic materials 0.000 description 1
235000017550 sodium carbonate Nutrition 0.000 description 1
239000007787 solid Substances 0.000 description 1
230000002194 synthesizing effect Effects 0.000 description 1
238000005292 vacuum distillation Methods 0.000 description 1
238000005406 washing Methods 0.000 description 1
239000010457 zeolite Substances 0.000 description 1

Landscapes

Eyeglasses (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

JP13252878A 1978-10-30 1978-10-30 Purification of carbonate Granted JPS5559144A (en)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP13252878A JPS5559144A (en)	1978-10-30	1978-10-30	Purification of carbonate

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP13252878A JPS5559144A (en)	1978-10-30	1978-10-30	Purification of carbonate

Related Child Applications (1)

Application Number	Title	Priority Date	Filing Date
JP28939985A Division JPS61210057A (ja)	1985-12-24	1985-12-24	カ−ボネ−ト化合物の精製方法

Publications (2)

Publication Number	Publication Date
JPS5559144A JPS5559144A (en)	1980-05-02
JPS6141904B2 true JPS6141904B2 (ko)	1986-09-18

Family

ID=15083390

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP13252878A Granted JPS5559144A (en)	1978-10-30	1978-10-30	Purification of carbonate

Country Status (1)

Country	Link
JP (1)	JPS5559144A (ko)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE4414121A1 (de) *	1994-04-22	1995-10-26	Bayer Ag	Verfahren zur Reinigung von Ethylenglykolcarbonat (EGC) durch Adsorption an Aktivkohle

1978
- 1978-10-30 JP JP13252878A patent/JPS5559144A/ja active Granted

Also Published As

Publication number	Publication date
JPS5559144A (en)	1980-05-02

Publication	Publication Date	Title
JP2001114729A (ja)	2001-04-24	エステル可塑剤の製造方法
JPH07206757A (ja)	1995-08-08	ポリフルオルクロル−及びペルフルオルカルボン酸クロリドの製法
JPS6141904B2 (ko)	1986-09-18
JPS6218539B2 (ko)	1987-04-23
JPS5914017B2 (ja)	1984-04-02	多官能性アクリレ−トの製造方法
EP1501818B8 (en)	2006-02-01	Alkylene carbonate purification method
JPS61165349A (ja)	1986-07-26	多官能エステルの製法
JPH01242554A (ja)	1989-09-27	ピルビン酸アルキルの製造方法
JP2000256265A (ja)	2000-09-19	メタクリル酸メチルの製造方法
JPH0316937B2 (ko)	1991-03-06
JPS6133014B2 (ko)	1986-07-31
JPH0225449A (ja)	1990-01-26	酢酸アリルの製造法
JPS6023099B2 (ja)	1985-06-05	粗有機カ−ボネ−トの精製方法
EP0183160A1 (en)	1986-06-04	Preparation process of indole
JPS59108734A (ja)	1984-06-23	グルタルアルデヒドの製造方法
JPH01151534A (ja)	1989-06-14	アルデヒドの製造方法
SU842016A1 (ru)	1981-06-30	Способ очистки хлористого водорода
JPH0366294B2 (ko)	1991-10-16
JPH0534350B2 (ko)	1993-05-21
RU2149867C1 (ru)	2000-05-27	Способ очистки ацетонитрила
JPH01180848A (ja)	1989-07-18	ジクロロアセチルクロライドの製造法
KR0145730B1 (ko)	1998-08-17	다가알콜의(메트) 아크릴산 에스테르의 제조방법(ⅲ)
JPH0366680A (ja)	1991-03-22	ラクトン類の精製方法
JPH07278053A (ja)	1995-10-24	メタクリル酸エステルの精製法
JPS6075448A (ja)	1985-04-27	芳香環を有する多価アルコ−ルのアリルカ−ボネ−トの製造方法