JP2014527525A - 有効成分、油及びイオン性液体を含む組成物 - Google Patents
有効成分、油及びイオン性液体を含む組成物 Download PDFInfo
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- JP2014527525A JP2014527525A JP2014525435A JP2014525435A JP2014527525A JP 2014527525 A JP2014527525 A JP 2014527525A JP 2014525435 A JP2014525435 A JP 2014525435A JP 2014525435 A JP2014525435 A JP 2014525435A JP 2014527525 A JP2014527525 A JP 2014527525A
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- Prior art keywords
- oil
- alkyl
- acid
- active ingredient
- composition
- Prior art date
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- 239000000203 mixture Substances 0.000 title claims abstract description 167
- 239000003921 oil Substances 0.000 title claims abstract description 75
- 239000004480 active ingredient Substances 0.000 title claims abstract description 74
- 239000002608 ionic liquid Substances 0.000 title claims abstract description 50
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 27
- 150000001450 anions Chemical class 0.000 claims abstract description 20
- 239000007788 liquid Substances 0.000 claims abstract description 18
- 238000000034 method Methods 0.000 claims abstract description 6
- -1 N-substituted pyridinium Chemical class 0.000 claims description 69
- 125000000217 alkyl group Chemical group 0.000 claims description 39
- 239000000194 fatty acid Substances 0.000 claims description 35
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 34
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- 150000002148 esters Chemical class 0.000 claims description 22
- 150000007942 carboxylates Chemical class 0.000 claims description 16
- 150000001768 cations Chemical class 0.000 claims description 15
- 229910019142 PO4 Inorganic materials 0.000 claims description 13
- 229910052739 hydrogen Inorganic materials 0.000 claims description 12
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 10
- 239000001257 hydrogen Substances 0.000 claims description 10
- 125000005599 alkyl carboxylate group Chemical group 0.000 claims description 9
- 150000008052 alkyl sulfonates Chemical class 0.000 claims description 9
- 239000006185 dispersion Substances 0.000 claims description 9
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- 229920000570 polyether Polymers 0.000 claims description 8
- 239000003945 anionic surfactant Substances 0.000 claims description 7
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- 239000012868 active agrochemical ingredient Substances 0.000 claims description 6
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 5
- ZRALSGWEFCBTJO-UHFFFAOYSA-N Guanidine Chemical class NC(N)=N ZRALSGWEFCBTJO-UHFFFAOYSA-N 0.000 claims description 5
- 150000004945 aromatic hydrocarbons Chemical class 0.000 claims description 5
- UUEVFMOUBSLVJW-UHFFFAOYSA-N oxo-[[1-[2-[2-[2-[4-(oxoazaniumylmethylidene)pyridin-1-yl]ethoxy]ethoxy]ethyl]pyridin-4-ylidene]methyl]azanium;dibromide Chemical compound [Br-].[Br-].C1=CC(=C[NH+]=O)C=CN1CCOCCOCCN1C=CC(=C[NH+]=O)C=C1 UUEVFMOUBSLVJW-UHFFFAOYSA-N 0.000 claims description 5
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 5
- RAXXELZNTBOGNW-UHFFFAOYSA-O Imidazolium Chemical compound C1=C[NH+]=CN1 RAXXELZNTBOGNW-UHFFFAOYSA-O 0.000 claims description 3
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 3
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- QWJNFFYFEKXZBF-UHFFFAOYSA-N cyanocyanamide Chemical compound N#CNC#N QWJNFFYFEKXZBF-UHFFFAOYSA-N 0.000 claims description 3
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- UEZVMMHDMIWARA-UHFFFAOYSA-M phosphonate Chemical compound [O-]P(=O)=O UEZVMMHDMIWARA-UHFFFAOYSA-M 0.000 claims description 3
- KPZGRMZPZLOPBS-UHFFFAOYSA-N 1,3-dichloro-2,2-bis(chloromethyl)propane Chemical compound ClCC(CCl)(CCl)CCl KPZGRMZPZLOPBS-UHFFFAOYSA-N 0.000 claims description 2
- VVRKSAMWBNJDTH-UHFFFAOYSA-N difluorophosphane Chemical compound FPF VVRKSAMWBNJDTH-UHFFFAOYSA-N 0.000 claims description 2
- 229910052736 halogen Inorganic materials 0.000 claims description 2
- 150000002367 halogens Chemical class 0.000 claims description 2
- 125000002768 hydroxyalkyl group Chemical group 0.000 claims description 2
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- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 9
- 239000000843 powder Substances 0.000 description 9
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- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 8
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- BARWIPMJPCRCTP-CLFAGFIQSA-N oleyl oleate Chemical compound CCCCCCCC\C=C/CCCCCCCCOC(=O)CCCCCCC\C=C/CCCCCCCC BARWIPMJPCRCTP-CLFAGFIQSA-N 0.000 description 8
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- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 7
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- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 6
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- 229940045714 alkyl sulfonate alkylating agent Drugs 0.000 description 6
- 150000001408 amides Chemical class 0.000 description 6
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- 239000006260 foam Substances 0.000 description 6
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 6
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- 239000002917 insecticide Substances 0.000 description 6
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 6
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- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 5
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- JGUMTYWKIBJSTN-UHFFFAOYSA-N 2-ethylhexyl 4-[[4,6-bis[4-(2-ethylhexoxycarbonyl)anilino]-1,3,5-triazin-2-yl]amino]benzoate Chemical compound C1=CC(C(=O)OCC(CC)CCCC)=CC=C1NC1=NC(NC=2C=CC(=CC=2)C(=O)OCC(CC)CCCC)=NC(NC=2C=CC(=CC=2)C(=O)OCC(CC)CCCC)=N1 JGUMTYWKIBJSTN-UHFFFAOYSA-N 0.000 description 4
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- GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 description 4
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- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
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- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
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- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Medicinal Preparation (AREA)
Abstract
Description
国際公開第2007/144286号パンフレットには、陽イオンとしてのN-カルボキシアルキルイミダゾリウム基、及び陰イオンとしてのアルキルスルホネート、アルキルホスフェート又はアルキルカルボキシレートを含むイオン性液体を含む抗微生物組成物が記載されている。組成物は、炭化水素油又は抗微生物性有効成分を含み得る。
A)難水溶性及び難油溶性である溶解形態の有機有効成分と、
B)20℃の水に最大で20g/lまで溶解可能な油と、
C)陽イオン及び陰イオンを含むイオン性液体であって、
陽イオンが、式(I)
N+R1R2R3R4 (I)
(式中、R1、R2、R3及びR4は互いに独立してアルキル基であり、該基は、ヘテロ官能基で置換されていてもよく、互いに脂肪族環系を形成し得る)のアンモニウム、
式(II)
N-置換ピリジニウム誘導体、
N,N'-二置換ピラゾリウム誘導体、又は
グアニジウム誘導体、
を含むイオン性液体とを含む液体組成物により達成された。
- p-アミノ安息香酸誘導体、例えば2-エチルヘキシル4-ジメチルアミノベンゾエート、
- サリチル酸誘導体、例えば2-エチルヘキシルサリチレート、
- ベンゾフェノン誘導体、例えば2-ヒドロキシ-4-メトキシベンゾフェノン、ジエチルアミノヒドロキシベンゾイルヘキシルベンゾエート(Uvinul A Plus)及び式
- ジベンゾイルメタン誘導体、例えば1-(4-tert-ブチルフェニル)-3-(4-メトキシフェニル)プロパン-1,3-ジオン、
- ジフェニルアクリレート、例えば2-エチルヘキシル2-シアノ-3,3-ジフェニルアクリレート及び3-(ベンゾフラニル)2-シアノアクリレート、
- 3-イミダゾール-4-イルアクリル酸及びエステル、
- ベンゾフラン誘導体、特に欧州特許出願公開第582,189号、米国特許第5,338,539号、米国特許第5,518,713号及び欧州特許出願公開第613,893号に記載された2-(p-アミノフェニル)ベンゾフラン誘導体、
- ポリマーUV吸収剤、例えば欧州特許出願公開第709,080号に記載されたベンジリデンマロネート誘導体、
- 桂皮酸誘導体、例えば4-メトキシ桂皮酸2-エチルヘキシルエステル若しくはイソアミルエステル、又は米国特許第5,601,811号及び国際公開第97/00851号パンフレットに開示された桂皮酸誘導体、
- ショウノウ誘導体、例えば3-(4'-メチル)ベンジリデン-ボルナン-2-オン、3-ベンジリデン-ボルナン-2-オン、N-[2(及び4)-2-オキシボルン-3-イリデンメチル)ベンジル]アクリルアミドポリマー、3-(4'-トリメチルアンモニウム)ベンジリデン-ボルナン-2-オンメチルスルフェート、3,3'-(1,4-フェニレンジメチン)-ビス(7,7-ジメチル-2-オキソ-ビシクロ-[2.2.1]ヘプタン-1-メタンスルホン酸)及びその塩、3-(4'-スルホ)ベンジリデン-ボルナン-2-オン及びその塩; ショウノウベンザルコニウムメトスルフェート、
- ヒドロキシフェニルトリアジン化合物、例えば2-(4'-メトキシフェニル)-4,6-ビス(2'-ヒドロキシ-4'-n-オクチルオキシフェニル)-1,3,5-トリアジン;2,4-ビス{[4-(3-(2-プロピルオキシ)-2-ヒドロキシプロピルオキシ)-2-ヒドロキシ]フェニル}-6-(4-メトキシフェニル)-1,3,5-トリアジン;2,4-ビス{[4-(2-エチルヘキシルオキシ)-2-ヒドロキシ]フェニル}-6-[4-(2-メトキシエチルカルボキシル)フェニルアミノ]-1,3,5-トリアジン;2,4-ビス{[4-(トリス(トリメチルシロキシシリルプロピルオキシ)-2-ヒドロキシ]フェニル}-6-(4-メトキシフェニル)-1,3,5-トリアジン;2,4-ビス{[4-(2''メチルプロペニルオキシ)-2-ヒドロキシ]フェニル}-6-(4-メトキシフェニル)-1,3,5-トリアジン;2,4-ビス{[4-(1',1',1',3',5',5',5'-ヘプタメチルトリシリル-2''-メチルプロピルオキシ)-2-ヒドロキシ]フェニル}-6-(4-メトキシフェニル)-1,3,5-トリアジン;2,4-ビス{[4-(3-(2-プロピルオキシ)-2-ヒドロキシプロピルオキシ)-2-ヒドロキシ]フェニル}-6-[4-エチルカルボキシル)フェニルアミノ]-1,3,5-トリアジン;及びビス-エチルヘキシルオキシフェノールメトキシフェニルトリアジン(Tinosorb S)、
- ポリフェニル置換トリアジン化合物、例えばトリス-ビフェニルトリアジン(Tinosorb A2B)、
- ベンゾトリアゾール化合物、例えば2,2'-メチレンビス(6-(2H-ベンゾトリアゾール-2-イル)-4-(1,1,3,3-テトラメチルブチル)フェノール
- 2-フェニルベンゾイミダゾール-5-スルホン酸及びその塩、
- メンチルo-アミノベンゾエート
- メロシアニン化合物、
である。
N+R1R2R3R4 (I)
(式中、R1、R2、R3及びR4は互いに独立してアルキル基であり、該基は、ヘテロ官能基で置換されていてもよく、互いに脂肪族環系を形成し得る)のアンモニウムを含む。好ましくはR1、R2、R3及びR4は互いに独立して、アルキル及び/又はヒドロキシアルキルである。特に好ましくはR1、R2、R3及びR4は互いに独立して、C1〜C20-アルキル及び/又はC1〜C20-ヒドロキシアルキルである。非常に特に好ましくはR1、R2、R3及びR4は互いに独立して、C1〜C8-アルキル及び/又はC1〜C8-ヒドロキシアルキルである。例は、テトラブチルアンモニウム(TBA)又はコリニウム(N,N,N-トリメチル-N-ヒドロキシエチルアンモニウム)である。
(RaO(CH2CH2O)nCH2CO2 - (III)
(式中、nは、0〜3の値を有し、Raは、C1〜C8-アルキル又はアセテート基である)又は式(IV)
Rb-O-CH2CO2 - (IV)
(式中、Rbは、C1〜C18-アルキルである)を有する。Rbは、好ましくは、C3〜C12-アルキル、特にヘキシルである。
- グリセロール;
- アルキレングリコール、例えばエチレングリコール、ジエチレングリコール、プロピレングリコール、ブチレングリコール、ヘキシレングリコール、及び100〜1,000ダルトンの平均分子量を有するポリエチレングリコール;
- 自己縮合度1.5〜10を有する工業銘柄のオリゴグリセロール混合物、例えば40〜50重量%のジグリセロール含量を有する工業銘柄のジグリセロール混合物;
- メチロール化合物、例えば特にトリメチロールエタン、トリメチロールプロパン、トリメチロールブタン、ペンタエリトリトール及びジペンタエリトリトール;
- 低級アルキルグルコシド、特にアルキル基中に1〜8個の炭素原子を有するもの、例えば、メチルグルコシド及びブチルグルコシド;
- 5〜12個の炭素原子を有する糖アルコール、例えばソルビトール又はマンニトール;
- 5〜12個の炭素原子を有する糖、例えばグルコース又はスクロース;
- アミノ糖、例えばグルカミン;
- ジアルコールアミン、例えばジエタノールアミン又は2-アミノ1,3-プロパンジオール、
である。
- スキンケア用の組成物、例えば棒状若しくは液体石鹸、合成洗剤又は洗浄ペーストの形態の皮膚洗浄及び浄化組成物;
- 入浴剤、例えば液体(フォームバス、ミルク、シャワー剤)又は固形入浴剤、例えばバスキューブ及びバスソルト;
- スキンケア組成物、例えばスキンエマルジョン、マルチエマルジョン又はスキンオイル;
- 化粧用ボティーケア組成物、例えばデイクリーム、パウダークリーム、フェイスパウダー(粉状又は固形)、頬紅ルージュ又はクリームメイクアップの形態の顔用メイクアップ、アイケア組成物、例えばアイシャドー剤、マスカラ、アイライナー、アイクリーム又はアイフィックスクリーム;リップケア組成物、例えば口紅、リップグロス、リップライナーペンシル、ネイルケア組成物、例えばマニキュア、マニキュアリムーバー、ネイルハードナー又はキューティクルリムーバー;
- フットケア組成物、例えばフットバス、フットパウダー、フットクリーム及びフットバルサム、特に脱臭剤及び制汗剤又はタコ除去組成物;
- 光保護組成物、例えばサンミルク、ローション、クリーム、オイル、サンブロック又はトロピカル、プレタンニング剤又はアフターサン剤;
- スキンタンニング組成物、例えばセルフタンニングクリーム;
- 脱色組成物、例えば皮膚漂白剤又は皮膚増白組成物;
- 防虫組成物(「忌避剤」)、例えば防虫オイル、ローション、スプレー又はスティック;
- 脱臭剤、例えば脱臭スプレー、ポンプスプレー、脱臭ゲル、スティック又はロール-オン;
- 制汗剤、例えば制汗スティック、クリーム又はロール-オン;
- 皮膚のシミをクレンジング及びケアするための組成物、例えば合成洗剤(固体又は液体)、ピーリング若しくはスクラブ剤又はピーリングマスク;
- 化学的形態の脱毛組成物(除毛)、例えば脱毛パウダー、除毛液、クリーム又はペースト状除毛剤、ゲル形態又はエアゾールフォームの脱毛剤;
- シェービング組成物、例えばシェービング石鹸、発泡シェービングクリーム、非発泡シェービングクリーム、フォーム、ゲル、ドライシェービング用のプレシェーブ剤、アフターシェーブ剤又はアフターシェーブローション;
- 着香した組成物、例えば着香液(オーデコロン、オードトワレ、オードパルファム、パルファムドトワレ、香水)、パヒュームオイル又はパヒュームクリーム;
- ヘアトリートメント用の化粧品組成物、例えばシャンプーの形態の洗髪組成物、ヘアコンディショナー、ヘアケア組成物、例えばプレトリートメント組成物、ヘアトニック、スタイリングクリーム、スタイリングゲル、ポマード、ヘアリンス、トリートメントパック、インテンシブヘアトリートメント、ヘア成形用組成物、例えばパーマネントウェーブ(ホットウェーブ、マイルドウェーブ、コールドウェーブ)を形成するためのウェービング組成物、ヘアストレートニング剤、液体ヘアセッティング組成物、ヘアフォーム、ヘアスプレー、漂白組成物、例えば過酸化水素溶液、増白シャンプー、脱色クリーム、脱色パウダー、脱色スラリー若しくはオイル、一時的、半永久的若しくは永久的な染髪剤、自己酸化染料を含む製剤、又は天然染髪剤、例えばヘナ又はカミツレ。
- W/O、O/W、O/W/O、W/O/W、PIT及び全てのタイプのマイクロエマルジョンとして液体製剤の形態で、
- ゲルの形態で、
- オイル、クリーム、ミルク若しくはローションの形態で、
- パウダー、ラッカー、タブレット若しくはメイクアップの形態で、
- スティックの形態で、
- スプレー(噴射ガスを含むスプレー又はポンプ式スプレー)若しくはエアゾールの形態で、
- フォームの形態で、又は
- ペーストの形態で、
存在し得る。
フルキサピロキサド:殺菌剤、3-(ジフルオロメチル)-1-メチル-N-(3',4',5'-トリフルオロビフェニル-2-イル)ピラゾール-4-カルボキサミド
Uvinul(登録商標)T150:BASF SEから市販される2,4,6-トリアニリノ-p-(カルボ-2'-エチルヘキシル-1'-オキシ)-1,3,5-トリアジン;CAS No. 88122-99-0。
Surf B: ポリオキシル40水素化ひまし油
Surf C: エトキシル化トリスチリルフェノール
Surf D: エトキシル化ポリアリールフェノール硫酸アンモニウム塩
Surf E: C10-ゲルベアルコールエトキシレート(7 EO)
Surf F: C10-ゲルベアルコールエトキシレート(3 EO)
Surf G C13C15 -オキソアルコールエトキシレート(3 EO)
Surf H: イソC12アルキルベンゼンスルホン酸Ca塩
Surf I: C13-オキソアルコールエトキシレート(+3EO)
Surf J: C13-オキソアルコールエトキシレート(+7EO)
Surf K: C13-オキソアルコールエトキシレート(+10EO)
Surf L: C13-オキソアルコールエトキシレート(+12EO)
Surf M: C10C18-アルコールエトキシレート(+5EO)。
農薬有効成分の溶解度上昇
溶解度を21℃で検査した。このために、最大の溶解度に達するまで、増加量の有効成分を、イオン性液体を含む油(Cetiol(登録商標)B又はSolvesso(登録商標))に少しずつ添加した。或いはイオン性液体を含む油を有効成分で飽和させて、有効成分の可溶性画分をHPLCにより定量した。
水性希釈物
8重量%のN-ブチル-N'-メチルイミダゾリウム(BMIM)アセテートと20重量%のフルキサピロキサドと72重量%のCetiol(登録商標)Bと表6に列挙された界面活性剤との混合物を調製した。混合物を、混合物1部対水100部の重量比で水を用いて室温で希釈して、均質な分散液を生成させた。
水性希釈物
9重量%のコリニウムオクタノエートと10重量%のフルキサピロキサドと81重量%のCetiol(登録商標)Bと表6に列挙された界面活性剤との混合物を調製した。混合物を、混合物1部対水100部の重量比で水を用いて室温で希釈して、均質な分散液を生成させた。
水性希釈物
8.5重量%のN-エチル-N'-メチルイミダゾリウム(EMIM)アセテートと15重量%のフルキサピロキサドと76.5重量%のCetiol(登録商標)Bと表6に列挙された界面活性剤との混合物を調製した。混合物を、混合物1部対水100部の重量比で水を用いて室温で希釈して、均質な分散液を生成させた。
Claims (15)
- A)難水溶性及び難油溶性である溶解形態の有機有効成分と、
B)20℃の水に最大で20g/lまで溶解可能な油と、
C)陽イオン及び陰イオンを含むイオン性液体であって、
陽イオンが、式(I)
N+R1R2R3R4 (I)
(式中、R1、R2、R3及びR4は互いに独立してアルキル基であり、該基は、ヘテロ官能基で置換されていてもよく、互いに脂肪族環系を形成し得る)のアンモニウム、
式(II)
N-置換ピリジニウム誘導体、
N,N'-二置換ピラゾリウム誘導体、又は
グアニジウム誘導体、
を含むイオン性液体とを含む液体組成物。 - 陽イオンが、式(I)のアンモニウム又は式(II)のイミダゾリウムを含む、請求項1に記載の組成物。
- 油のイオン性液体に対する重量比が、100/1〜1/1の範囲内である、請求項1又は2に記載の組成物。
- R1、R2、R3及びR4が互いに独立して、C1〜C20アルキル及び/又はC1〜C20ヒドロキシアルキルである、請求項1〜3のいずれか1項に記載の組成物。
- R5が水素又はC1〜C20アルキルであり、R6がC1〜C20アルキルであり、R7がC1〜C20アルキルである、請求項1〜4のいずれか1項に記載の組成物。
- 1〜25重量%の少なくとも1種の界面活性剤を含む、請求項1〜5のいずれか1項に記載の組成物。
- 有効成分が、農薬有効成分である、請求項1〜6のいずれか1項に記載の組成物。
- 界面活性剤が、アルコキシレートから選択される少なくとも1種の非イオン性界面活性剤、及び場合により、スルフェートから選択される陰イオン性界面活性剤を含む、請求項1〜7のいずれか1項に記載の組成物。
- 油が、芳香族炭化水素、アルキルアルカノエート、脂肪酸アミド、又はアルキル二酸のジアルキルエステルである、請求項1〜8のいずれか1項に記載の組成物。
- 陰イオンが、カルボキシレート、スルホネート、スルフェート、ホスホネート、ホスフェート、ハロゲン、ビス(トリフルオロスルホニル)イミド、四塩化アルミニウム、フッ化リン、又はジシアニミドを含む、請求項1〜9のいずれか1項に記載の組成物。
- 陰イオンが、アルキルカルボキシレート、ポリエーテル含有カルボキシレート、又はアルキルスルホネートを含む、請求項1〜10のいずれか1項に記載の組成物。
- 溶液又は分散液であり、最大で5重量%の水を含む、請求項1〜11のいずれか1項に記載の組成物。
- 分散液であり、少なくとも5重量%の水を含む、請求項1〜11のいずれか1項に記載の組成物。
- 有効成分、油及びイオン性液体を接触させる、請求項1〜13のいずれか1項に記載の液体組成物の調製方法。
- 請求項1〜13のいずれか1項に記載の油に対する請求項1〜13のいずれか1項に記載の有効成分の溶解度を上昇させるための、請求項1〜14のいずれか1項に記載のイオン性液体の使用。
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DE102014212522A1 (de) * | 2014-06-27 | 2015-12-31 | Beiersdorf Ag | Stabile kosmetische und dermatologische Zubereitung mit hohem Lichtschutzfaktor |
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KR101984330B1 (ko) | 2019-05-30 |
US20150004109A1 (en) | 2015-01-01 |
EP2744335B1 (en) | 2018-10-10 |
CN103929962A (zh) | 2014-07-16 |
EP2744335A1 (en) | 2014-06-25 |
CN103929962B (zh) | 2016-12-07 |
BR112014003566A2 (pt) | 2017-03-21 |
BR112014003566B8 (pt) | 2020-08-18 |
AR087556A1 (es) | 2014-04-03 |
WO2013024099A1 (en) | 2013-02-21 |
US9949475B2 (en) | 2018-04-24 |
JP6050354B2 (ja) | 2016-12-21 |
KR20140057608A (ko) | 2014-05-13 |
BR112014003566B1 (pt) | 2020-07-28 |
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