EP0711250A1 - Verfahren und vorrichtung zum sterilen abfüllen von getränken in flaschen - Google Patents
Verfahren und vorrichtung zum sterilen abfüllen von getränken in flaschenInfo
- Publication number
- EP0711250A1 EP0711250A1 EP94924821A EP94924821A EP0711250A1 EP 0711250 A1 EP0711250 A1 EP 0711250A1 EP 94924821 A EP94924821 A EP 94924821A EP 94924821 A EP94924821 A EP 94924821A EP 0711250 A1 EP0711250 A1 EP 0711250A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- bottles
- interior
- bottle
- filling
- sterilization
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 title claims abstract description 27
- 238000012859 sterile filling Methods 0.000 title claims abstract description 10
- 235000013361 beverage Nutrition 0.000 title claims abstract description 9
- 238000011049 filling Methods 0.000 claims abstract description 39
- 238000004659 sterilization and disinfection Methods 0.000 claims abstract description 39
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 32
- 238000004140 cleaning Methods 0.000 claims abstract description 19
- 230000001954 sterilising effect Effects 0.000 claims description 37
- 239000007921 spray Substances 0.000 claims description 15
- 238000007664 blowing Methods 0.000 claims description 5
- 238000007689 inspection Methods 0.000 claims description 4
- 239000000314 lubricant Substances 0.000 claims description 3
- 238000011109 contamination Methods 0.000 claims description 2
- 238000005461 lubrication Methods 0.000 claims description 2
- 238000009423 ventilation Methods 0.000 claims description 2
- 238000003780 insertion Methods 0.000 claims 1
- 230000037431 insertion Effects 0.000 claims 1
- 230000005855 radiation Effects 0.000 claims 1
- 238000011144 upstream manufacturing Methods 0.000 claims 1
- 208000035415 Reinfection Diseases 0.000 abstract description 4
- 238000007789 sealing Methods 0.000 abstract description 3
- 238000005265 energy consumption Methods 0.000 abstract description 2
- 244000052616 bacterial pathogen Species 0.000 description 9
- 239000011521 glass Substances 0.000 description 5
- 238000005406 washing Methods 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 4
- 230000002147 killing effect Effects 0.000 description 4
- 229920006395 saturated elastomer Polymers 0.000 description 4
- 238000005507 spraying Methods 0.000 description 4
- 238000010025 steaming Methods 0.000 description 4
- 241000607479 Yersinia pestis Species 0.000 description 3
- 238000011010 flushing procedure Methods 0.000 description 3
- 235000015203 fruit juice Nutrition 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 238000001816 cooling Methods 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 230000018109 developmental process Effects 0.000 description 2
- 238000005429 filling process Methods 0.000 description 2
- 239000013505 freshwater Substances 0.000 description 2
- 230000007257 malfunction Effects 0.000 description 2
- 241001507865 Aspergillus fischeri Species 0.000 description 1
- 241000030451 Byssochlamys fulva Species 0.000 description 1
- 241001134446 Niveas Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 230000003749 cleanliness Effects 0.000 description 1
- 210000001520 comb Anatomy 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000006735 deficit Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 239000000523 sample Substances 0.000 description 1
- 238000011146 sterile filtration Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B67—OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
- B67C—CLEANING, FILLING WITH LIQUIDS OR SEMILIQUIDS, OR EMPTYING, OF BOTTLES, JARS, CANS, CASKS, BARRELS, OR SIMILAR CONTAINERS, NOT OTHERWISE PROVIDED FOR; FUNNELS
- B67C7/00—Concurrent cleaning, filling, and closing of bottles; Processes or devices for at least two of these operations
- B67C7/0073—Sterilising, aseptic filling and closing
Definitions
- the invention relates to a method for the sterile filling of drinks into bottles according to the preamble of claim 1 and a device for carrying it out according to the preamble of claim 13.
- the invention has for its object to enable a sufficiently high kill rate even extremely heat-resistant beverage pests and a trouble-free operation with high performance in a method of the type mentioned with simple means.
- a device for performing this method is to be created.
- the sterilization of the inside of the bottle is therefore not concentrated in one station, but rather spatially and temporally offset in several phases or stations.
- the temperature increase in the following phase based on the heating carried out in the previous phase, results in a synergy effect which enormously increases the killing effect.
- the particularly heat-resistant spores of the dreaded molds Byssochlamys fulva, 3yssochlamys nivea and Neosartorya fischeri can be destroyed with very high kill rates.
- the method according to the invention is thus ideally suited for the sterile filling of beverages in modern high-performance systems with several separate machines and intermediate conveyors.
- a device according to the invention is as simple and manageable as a device without Sterilization. It is easily accessible, particularly in the area of the bottle conveyors, so that malfunctions can be remedied at any time and the efficiency can thereby be kept high. Nevertheless, the interior sterilization of the bottles several times results in an extremely high killing effect.
- Empty bottle inspection machine can be integrated if the bottles are reusable and should be checked for cleanliness and damage. It is only 'to ensure that through a sterile holding the engaging on the bottle mouth centering bells there is no excessive reinfection.
- the lubrication of the conveyor belts with a heated lubricant, as specified in claim 29, enables the bottle bottom, which is particularly at risk, to be warmed up.
- Fig. 1 is a schematic plan view of a plant for the sterile filling of fruit juice in returnable glass bottles with a brief description of the procedural s
- Fig. 2 shows the vertical section through
- FIG. 3 shows a schematic representation of the four
- Fig. 4 shows the vertical section through a filling element of the filling machine of the system according to Fig. 1 during the internal sterilization.
- 1 to 4 is set up for the sterile filling of fruit juice in reusable bottles 24 made of glass. It has a cleaning machine 1, a rinser 4, a filling machine 2 and a sealing machine 3.
- the cleaning machine 1 is a double-end version which, following the last lye bath 21 and a hot water spray 22, has a pressure chamber 18 in the form of a box which is open at the bottom.
- the pressure chamber 18 is immersed in a tank 25 filled with hot water and is subjected to an overpressure of 0.1 bar in its interior, for example by means of a compressor 26 which, controlled by a control device (not shown), presses sterile air into the pressure chamber 18.
- a water level which is one meter lower than in the tank 25.
- the two side walls of the pressure chamber 18 lying in the running direction together with the tar. 25 form a siphon-type inlet lock 19 and a siphon-type outlet lock 20.
- the bottles 24 are passed through the bottle cells 28 suspended from endless, continuously driven chains 27 after passing through the hot water spray 22 down into the tank 25, horizontally through the inlet lock 19 through, up into the interior of the pressure chamber 18 above the water level, a short distance horizontally, then down again into the water bath, in a horizontal direction through the outlet lock 20 and finally up out of the tank 25 for a final hot water spray 23 transported.
- the bottles then run to the dispensing device 29, where they are led out of the bottle cells 28 and placed on a bottle conveyor 5.
- three parallel spray tubes 8 with a number of nozzle openings corresponding to the number of bottles 24 per ' bottle cell 28 are arranged below the horizontal movement path of the bottles 24 above the water level transversely to the direction of rotation.
- the spray tubes 8 are rotatably supported and are rotated synchronously with the movement of the bottles 24 by means not shown, so that the nozzles first jet obliquely into the bottle, then hit the floor vertically upwards and finally again downwards along the bottle wall shine.
- the three spray tubes 8 are connected via a line 11 to a generator 16 for superheated water of 105 degrees Celsius, including a high pressure pump.
- the superheated water Due to the overpressure prevailing in the pressure chamber 18, the superheated water is injected into the bottles 24 through the spray tubes 8 without excessive vapor formation and largely hits the bottom of the bottle. As a result, a large amount of heat is introduced into the bottle in the shortest possible time and in a short way, so that a temperature in the entire interior of the bottles 24 is well above 100 degrees Celsius sets.
- the water flowing out of the bottles 24 is collected in a tub 44 and returned to the generator 16 for superheated water. Some of the superheated water turns into steam during the injection and condenses within the pressure chamber 18, as a result of which the amount of water in the tank 25 increases. This is compensated for by an overflow, not shown. Accordingly, the tub 44 is also connected to a fresh water line 30, via which the condensed water is automatically replenished.
- the bottles 24 are thus subjected to a first internal sterilization by injecting superheated water, which together with the preceding cleaning by hot lye results in a virtually complete killing of all germs inside the bottle.
- a slight cooling then takes place in the area of the outlet lock 20 and, if present, the subsequent hot water spray 23, so that the bottles 24 leave the cleaning machine 1 at a temperature of approximately 80 to 90 degrees Celsius. Cooling down is also possible.
- This can already be initiated by the water spray 22 in front of the pressure chamber 18, since, as already mentioned, the bottle walls are only partially heated by the spray tubes 8. The outer wall can therefore easily have a temperature that is significantly below 100 degrees Celsius.
- the bottle conveyor 5 taking over the bottles 24 from the Reinigur.gsmaschine 1 is formed in the usual way by a number of motor-driven hinged belt chains, which the bottles 24 in several rows and in 10
- bottles 24 on the bottle conveyor 5 gradually cool down and have a temperature of around 60 degrees Celsius during normal operation in the area of the merging.
- the temperature in the floor area can be kept somewhat higher by heating the usual chain lubricant before spraying on the flat top chains.
- a rinser 4 is connected to the bottle conveyor 5, which at the same time has a certain buffer function as a mass conveyor.
- This has an inlet screw, an inlet star, a rotor provided with pivotable and controllable grippers 31 for the bottles 24 and an outlet star.
- the grippers 31 By means of the grippers 31, the bottles 24 fed in the upright normal position (FIG. 3a) are pivoted by 180 degrees, so that their mouth points downward.
- nozzles formed in the neck of the bottles 2 - are formed by vertical, open-top rinsing pipes 9. introduced.
- the flushing pipes 9 rotate together with the rotor and are connected to a ring line 12 via individually controllable control valves 14. This contains saturated steam of approx. 105 degrees Celsius, which is opened for a time-controlled opening of the control valve 14 11
- Each flushing pipe 9 is also connected via a further control valve 32 to a further ring line 33 which contains sterile air. This is blown into the interior of the bottle by time-controlled opening of the control valve 32 after steaming for a period of, for example, 3 seconds (FIG. 3c). As a result, the condensate formed during steaming is rinsed out and the bottle 24 is dried on the inside. The bottles 24 are then pivoted back into their normal position by the grippers 31, in which they run out of the rinser 4 (FIG. 3d).
- the bottles 24 are thus subjected to a second interior sterilization by blowing in saturated steam.
- the inner wall of the bottles 24, which approach at a temperature of around 60 degrees Celsius, is heated in all areas to a sterilization temperature above 100 degrees Celsius.
- the germs that have penetrated into the bottle 24 through the open mouth in the course of the bottle transport on the bottle conveyor 5 are largely killed again.
- the bottles 24 are transported from the rinser 4 to a filling machine 2 by a short, single-lane screw conveyor 6. Instead, direct blocking is also possible in which the discharge star of the rinser 4 is connected directly or with the interposition of a transfer star 12
- a tunnel 34 with a steam feed line 35 can therefore be arranged in the area of the bottle mouths, which largely prevents germs from penetrating into the bottle openings (FIG. 3d).
- the filling machine 2 provided with an inlet star, a rotor and an outlet star corresponds to the construction of the filling machine from German Offenlegungsschrift 40 36 290. It therefore has a plurality of similar filling elements 17 arranged on the circumference of the rotor and associated with rotating lifting elements 36 associated therewith.
- the empty bottles 24 coming from the rinser '4 are first partially raised by the lifting members 36 to the filling members 17.
- a return gas tube 10 penetrates into the bottle neck. This is connected by time-controlled opening of a control valve 15 via channels in the filling element 17 to a line 13 which contains saturated steam of, for example, 105 degrees Celsius.
- each bottle 24 is thus subjected to a third and final internal sterilization by blowing in saturated steam. Those germs and beverage pests that "survived" the first internal sterilization in the cleaning machine 1 and the second internal sterilization in the rinser 4 are also killed with high certainty. All in all, the "fractional sterilization" according to the invention can achieve a significantly higher kill rate than with the same sterilization time and the same energy input in a single station.
- the tensioning gas valve 38 of the filling member 17 is opened and thereby introduced into the bottle 24 from a duct 39 CO. Via the return gas pipe 10.
- the sterilization steam and the resulting condensate are largely flushed out of the bottle 24 into the open.
- the bottle 24 is pressed completely and tightly against the filling member 17 by further lifting the lifting member 36, so that it fills up to the set counterpressure of, for example, 3 bar with C0_ while the tensioning gas valve 38 is still open.
- C0 ⁇ sterile air can of course also be used as the span gas and purge gas.
- the tensioning gas valve 38 is closed and then the return gas valve 40 and the liquid valve 41 are opened simultaneously.
- the fruit juice to be filled previously sterilized for example by sterile filtration, can enter the bottle 24 via the product line 42 and the outlet opening of the filling element 17.
- the liquid valve 41 is closed and the filling process is thus ended.
- the lifting element 36 is then lowered with the filled bottle 24.
- the bottles 24 are taken over by transport stars 7 at normal transport height and passed on to the closing machine 3.
- the ingress of germs can be prevented.
- the bottles 24 are then sealed with crown caps or the like previously sterilized by steam. locked.
- a conventional electronic empty bottle inspection machine can be easily integrated into the system according to FIGS. 1 to 4, preferably between the bottle conveyor 5 and the rinser 4. It is expedient to sterilize the centering bells of the empty bottle inspection machine which attack in the area of the bottle mouth shape. This can e.g. by means of an integrated heater that keeps the centering bell constantly at a temperature of over ICO degrees. It is also possible, at certain time intervals, to carry out chemical sterilization or heat eriiization by flaming or irradiation by supplying sr. •
- Vessels in the cleaning machine 1 can also be done by acid instead of Lau ⁇ e or in addition to the Lau ⁇ e.
Landscapes
- Filling Of Jars Or Cans And Processes For Cleaning And Sealing Jars (AREA)
- Apparatus For Disinfection Or Sterilisation (AREA)
Abstract
Description
Claims
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE4326601 | 1993-08-07 | ||
DE4326601A DE4326601A1 (de) | 1993-08-07 | 1993-08-07 | Verfahren und Vorrichtung zum sterilen Abfüllen von Getränken in Flaschen |
PCT/EP1994/002522 WO1995004699A1 (de) | 1993-08-07 | 1994-07-29 | Verfahren und vorrichtung zum sterilen abfüllen von getränken in flaschen |
Publications (2)
Publication Number | Publication Date |
---|---|
EP0711250A1 true EP0711250A1 (de) | 1996-05-15 |
EP0711250B1 EP0711250B1 (de) | 1997-05-21 |
Family
ID=6494707
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP94924821A Expired - Lifetime EP0711250B1 (de) | 1993-08-07 | 1994-07-29 | Verfahren und vorrichtung zum sterilen abfüllen von getränken in flaschen |
Country Status (8)
Country | Link |
---|---|
US (1) | US5896899A (de) |
EP (1) | EP0711250B1 (de) |
JP (1) | JPH09507453A (de) |
CN (1) | CN1128526A (de) |
AU (1) | AU7497094A (de) |
BR (1) | BR9407186A (de) |
DE (2) | DE4326601A1 (de) |
WO (1) | WO1995004699A1 (de) |
Families Citing this family (28)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE29611297U1 (de) * | 1996-06-28 | 1996-09-05 | Rico-Maschinenbau Max Appel KG, 73431 Aalen | Pasteurisiervorrichtung |
DE19731796A1 (de) * | 1997-07-24 | 1999-01-28 | Kronseder Maschf Krones | Verfahren und Vorrichtung zum hochreinen Abfüllen von Getränken in Flaschen |
DE19741242C1 (de) * | 1997-09-18 | 1999-07-08 | Diversey Lever Gmbh | Anlage zum Reinigen einer Abfüllanlage |
EP1059237A1 (de) * | 1999-06-07 | 2000-12-13 | Graham Engineering Corporation | Verbesserte Lebensmittelverpackung und Methode |
US7851458B2 (en) * | 1999-06-22 | 2010-12-14 | Joint Juice, Inc. | Cartilage enhancing food supplements and methods of preparing the same |
US20020085971A1 (en) * | 2001-01-03 | 2002-07-04 | Raniwala Subodh K. | Bottle sterilizing system and method |
US20020116644A1 (en) * | 2001-01-30 | 2002-08-22 | Galea Secured Networks Inc. | Adapter card for wirespeed security treatment of communications traffic |
DE10326618A1 (de) * | 2003-06-13 | 2005-01-05 | Khs Maschinen- Und Anlagenbau Ag, Patentabteilung | Behälterbehandlungsmaschine |
ITBO20030411A1 (it) * | 2003-07-03 | 2005-01-04 | Stk Stocchi Progetti S R L | Rubinetto per il riempimento sterile di liquidi alimentari. |
CN100503060C (zh) * | 2004-12-29 | 2009-06-24 | 广州泰成生化科技有限公司 | 一种瓶装饮用水瓶子的洗涤消毒方法 |
ITBO20050010A1 (it) * | 2005-01-12 | 2006-07-13 | Ima Spa | Impianto compatto per il confezionamento in ambiente sterile di prodotti liquidi iniettabili in contenitori |
US8181429B2 (en) * | 2005-12-21 | 2012-05-22 | Toyo Seikan Kaisha, Ltd. | Method of producing contents filed in a container |
DE102006002633B4 (de) * | 2006-01-19 | 2009-08-20 | Khs Ag | Verfahren sowie Vorrichtung zur Inspektion von Flaschen oder dgl. Behältern |
JP2008151771A (ja) | 2006-11-22 | 2008-07-03 | Fujifilm Corp | マイクロ流体チップ |
JP4940944B2 (ja) * | 2006-12-28 | 2012-05-30 | 澁谷工業株式会社 | 容器充填システム |
US8479784B2 (en) * | 2007-03-15 | 2013-07-09 | The Coca-Cola Company | Multiple stream filling system |
US9394153B2 (en) * | 2007-03-15 | 2016-07-19 | The Coca-Cola Company | Multiple stream filling system |
US8147616B2 (en) * | 2007-10-22 | 2012-04-03 | Stokely-Van Camp, Inc. | Container rinsing system and method |
US9168569B2 (en) | 2007-10-22 | 2015-10-27 | Stokely-Van Camp, Inc. | Container rinsing system and method |
DE102008026043A1 (de) | 2008-05-30 | 2009-12-03 | Khs Ag | Verfahren und Vorrichtung zur kombinierten Herstellung und Abfüllung von Behältern aus Kunststoff |
DE102008048812A1 (de) | 2008-09-24 | 2010-04-01 | Khs Ag | Verfahren und Vorrichtung zur kombinierten Herstellung und Abfüllung von Behältern aus Kunststoff |
DE102009040924A1 (de) * | 2009-09-11 | 2011-03-24 | Khs Gmbh | Anlage zum sterilen Abfüllen von Produkten, insbesondere von Getränken in Flaschen oder dergleichen Behälter |
CN102455116A (zh) * | 2010-10-25 | 2012-05-16 | 王振涛 | 氧气湿化瓶烘干消毒承载架 |
CN102838072A (zh) * | 2011-06-24 | 2012-12-26 | 山东工大机械有限公司 | 无菌灌封一体机 |
JP5998539B2 (ja) * | 2012-03-12 | 2016-09-28 | シブヤマシナリー株式会社 | 洗浄充填装置 |
DE102013102916A1 (de) * | 2013-03-21 | 2014-09-25 | Krones Ag | Vorrichtung und Verfahren zur Reinigung von Behältern |
US11390466B1 (en) | 2018-01-17 | 2022-07-19 | James P. Gallagher | Apparatus for use in molecular transfer and delivery of substances such as vapors, gases, liquids, and sprays |
SE2051547A1 (en) * | 2020-12-22 | 2022-06-23 | Wayout Int Ab | Tracking beverage containers in a filling station |
Family Cites Families (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2029303A (en) * | 1930-08-27 | 1936-02-04 | American Can Co | Apparatus for and method of canning |
FR748104A (fr) * | 1932-02-10 | 1933-06-29 | Seitz Werke Gmbh | Procédé et dispositif pour le remplissage aseptique de bouteilles |
DE733623C (de) * | 1936-09-27 | 1943-03-31 | Seitz Werke Gmbh | Reinigungs- und Sterilisiermaschine |
US3143120A (en) * | 1963-01-28 | 1964-08-04 | In Crate Bottling Co Proprieta | Apparatus for washing bottles or the like |
FR1405493A (fr) * | 1964-06-19 | 1965-07-09 | Graham Enock Mfg Company Ltd | Procédé et installation pour la mise en bouteilles de liquides complètement stérilisés, notamment du lait |
US3839843A (en) * | 1970-09-09 | 1974-10-08 | A Stewart | Acid-steam sterilization |
DE2622434A1 (de) * | 1976-05-20 | 1977-12-01 | Seitz Werke Gmbh | Reinigungsmaschine fuer behaelter, insbesondere flaschen |
US4409775A (en) * | 1977-08-22 | 1983-10-18 | The Mead Corporation | Apparatus for the aseptic packing of high acid food |
ZA812347B (en) * | 1980-04-11 | 1982-04-28 | Fenner Co Ltd J H | Endless conveyors |
US4635662A (en) * | 1982-11-29 | 1987-01-13 | Industrial Automation Corporation | Inline bottle rinser with quick bottle size changeover capability |
US4643330A (en) * | 1986-03-27 | 1987-02-17 | Owens-Illinois, Inc. | Container systems |
US4917267A (en) * | 1986-11-12 | 1990-04-17 | Laverdure Roland J A | Self-closing valve with tamper evident lip seal tab for liquids, pastes or solids |
DE3902432A1 (de) * | 1989-01-27 | 1990-08-02 | Bosch Gmbh Robert | Verfahren und vorrichtung zum reinigen und sterilisieren von behaeltern |
DE4008847A1 (de) * | 1990-03-20 | 1991-09-26 | Granini Gmbh | Anlage zum aseptischen fuellen und zum aseptischen verschliessen von flaschen |
DE4036290A1 (de) * | 1990-06-06 | 1991-12-12 | Kronseder Maschf Krones | Verfahren und vorrichtung zum sterilen abfuellen von getraenkefluessigkeiten |
US5251424A (en) * | 1991-01-11 | 1993-10-12 | American National Can Company | Method of packaging products in plastic containers |
DE9110492U1 (de) * | 1991-08-24 | 1992-09-24 | Krones Ag Hermann Kronseder Maschinenfabrik, 93073 Neutraubling | Maschine zum Reinigen von Flaschen o.dgl. |
-
1993
- 1993-08-07 DE DE4326601A patent/DE4326601A1/de not_active Withdrawn
-
1994
- 1994-07-29 DE DE59402843T patent/DE59402843D1/de not_active Expired - Fee Related
- 1994-07-29 JP JP7506203A patent/JPH09507453A/ja active Pending
- 1994-07-29 EP EP94924821A patent/EP0711250B1/de not_active Expired - Lifetime
- 1994-07-29 US US08/592,365 patent/US5896899A/en not_active Expired - Fee Related
- 1994-07-29 WO PCT/EP1994/002522 patent/WO1995004699A1/de active IP Right Grant
- 1994-07-29 BR BR9407186A patent/BR9407186A/pt not_active Application Discontinuation
- 1994-07-29 AU AU74970/94A patent/AU7497094A/en not_active Abandoned
- 1994-07-29 CN CN94193009A patent/CN1128526A/zh active Pending
Non-Patent Citations (1)
Title |
---|
See references of WO9504699A1 * |
Also Published As
Publication number | Publication date |
---|---|
BR9407186A (pt) | 1996-07-30 |
US5896899A (en) | 1999-04-27 |
AU7497094A (en) | 1995-02-28 |
DE4326601A1 (de) | 1995-02-09 |
DE59402843D1 (de) | 1997-06-26 |
JPH09507453A (ja) | 1997-07-29 |
EP0711250B1 (de) | 1997-05-21 |
CN1128526A (zh) | 1996-08-07 |
WO1995004699A1 (de) | 1995-02-16 |
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