CO2020001376A2 - Solución de sal de leucoíndigo con muy bajo contenido de anilina y método para realizar la misma - Google Patents

Solución de sal de leucoíndigo con muy bajo contenido de anilina y método para realizar la misma

Info

Publication number
CO2020001376A2
CO2020001376A2 CONC2020/0001376A CO2020001376A CO2020001376A2 CO 2020001376 A2 CO2020001376 A2 CO 2020001376A2 CO 2020001376 A CO2020001376 A CO 2020001376A CO 2020001376 A2 CO2020001376 A2 CO 2020001376A2
Authority
CO
Colombia
Prior art keywords
leukoindigo
solution
perform
same
salt solution
Prior art date
Application number
CONC2020/0001376A
Other languages
English (en)
Inventor
Erwin Lucic
Jörg Hübner
David Hyett
Michèle Catherine Christianne Janssen
Karin Hendrika Maria Bessembinder
Pierre L Woestenborghs
Marinus Petrus Wilhelmus Maria Rijkers
Original Assignee
Archroma Ip Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from EP17185971.3A external-priority patent/EP3441429B1/en
Priority claimed from EP17185980.4A external-priority patent/EP3441431B1/en
Priority claimed from EP17185976.2A external-priority patent/EP3441430B1/en
Priority claimed from EP18173343.7A external-priority patent/EP3569660B1/en
Application filed by Archroma Ip Gmbh filed Critical Archroma Ip Gmbh
Publication of CO2020001376A2 publication Critical patent/CO2020001376A2/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
    • C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
    • C09B67/0083—Solutions of dyes
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
    • C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
    • C09B67/0077—Preparations with possibly reduced vat, sulfur or indigo dyes
    • C09B67/0078—Preparations of vat, sulfur or indigo dyes in liquid form
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
    • C09B67/0096—Purification; Precipitation; Filtration
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B7/00—Indigoid dyes
    • C09B7/02—Bis-indole indigos
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/22—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using vat dyestuffs including indigo
    • D06P1/228—Indigo
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Indole Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Coloring (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Peptides Or Proteins (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

Solución de leucoíndigo acuosa estable que comprende una amina aromática en forma de anilina o anilina y N–metilanilina, en donde dicho leucoíndigo está en forma de una sal de metal alcalino; en donde la concentración de la amina aromática está por debajo de 40 ppm determinada de acuerdo con ISO 14362–1: 2017 (E); y en donde la concentración de la sal de leucoíndigo está en un intervalo de concentración de 10 a 45% en peso basado en el peso total de la solución, y en donde la estabilidad de la solución se mide a una temperatura de 23ºC; o en donde la concentración de la sal de leucoíndigo está en un intervalo de concentración de 45 a 65% en peso basado en el peso total de la solución, y en donde la estabilidad de la solución se mide a una temperatura de 60ºC.
CONC2020/0001376A 2017-08-11 2020-02-07 Solución de sal de leucoíndigo con muy bajo contenido de anilina y método para realizar la misma CO2020001376A2 (es)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
EP17185971.3A EP3441429B1 (en) 2017-08-11 2017-08-11 Purified concentrated aqueous leucoindigo salt solutions
EP17185980.4A EP3441431B1 (en) 2017-08-11 2017-08-11 Methods of making leucoindigo salt solutions with very low aniline content
EP17185976.2A EP3441430B1 (en) 2017-08-11 2017-08-11 Leucoindigo salt solution with very low content of aniline and method of making same
EP18173343.7A EP3569660B1 (en) 2018-05-18 2018-05-18 Method for making aniline-free leucoindigo salt solutions
PCT/EP2018/071791 WO2019030391A1 (en) 2017-08-11 2018-08-10 SALT SOLUTION OF LEUCOINDIGO HAVING VERY LOW ANILINE CONTENT AND PROCESS FOR PREPARING THE SAME

Publications (1)

Publication Number Publication Date
CO2020001376A2 true CO2020001376A2 (es) 2020-05-29

Family

ID=63108593

Family Applications (3)

Application Number Title Priority Date Filing Date
CONC2020/0001377A CO2020001377A2 (es) 2017-08-11 2020-02-07 Método y dispositivo para elaborar soluciones de sal de leucoíndigo libres de anilina
CONC2020/0001376A CO2020001376A2 (es) 2017-08-11 2020-02-07 Solución de sal de leucoíndigo con muy bajo contenido de anilina y método para realizar la misma
CONC2020/0001381A CO2020001381A2 (es) 2017-08-11 2020-02-07 Métodos para fabricar soluciones de sal de leucoíndigo con muy bajo contenido de anilina

Family Applications Before (1)

Application Number Title Priority Date Filing Date
CONC2020/0001377A CO2020001377A2 (es) 2017-08-11 2020-02-07 Método y dispositivo para elaborar soluciones de sal de leucoíndigo libres de anilina

Family Applications After (1)

Application Number Title Priority Date Filing Date
CONC2020/0001381A CO2020001381A2 (es) 2017-08-11 2020-02-07 Métodos para fabricar soluciones de sal de leucoíndigo con muy bajo contenido de anilina

Country Status (15)

Country Link
US (4) US11299633B2 (es)
EP (4) EP3665229A1 (es)
JP (5) JP7250762B2 (es)
KR (5) KR102636591B1 (es)
CN (5) CN111108156A (es)
AR (2) AR126783A2 (es)
BR (4) BR112019018494B1 (es)
CO (3) CO2020001377A2 (es)
MA (1) MA48430B1 (es)
MX (4) MX2020001517A (es)
PE (2) PE20201188A1 (es)
SG (4) SG11202001155UA (es)
TN (4) TN2020000013A1 (es)
TW (4) TWI763903B (es)
WO (4) WO2019030396A1 (es)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111108156A (zh) 2017-08-11 2020-05-05 昂高知识产权有限公司 具有很低苯胺含量的靛白盐溶液及其制备方法
CN110016816A (zh) * 2019-03-13 2019-07-16 广东前进牛仔布有限公司 一种靛蓝染色方法
BR102019025172A2 (pt) 2019-11-28 2021-06-08 Bann Química Ltda. processo de purificação de soluções de sal de leucoíndigo e uso de um gás inerte

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2130878A (en) 1933-04-10 1938-09-20 Ici Ltd Leucoindigo
US4992143A (en) 1989-06-09 1991-02-12 Mobay Corporation Continuous process for the separation of a partially water soluble component from a slurry
US5116996A (en) * 1991-07-17 1992-05-26 Basf Aktiengesellschaft Purification of indigo
US6169218B1 (en) 1992-02-10 2001-01-02 Catalytic Distillation Technologies Selective hydrogenation of highly unsaturated compounds in hydrocarbon streams
DE4220804A1 (de) * 1992-06-25 1994-01-05 Basf Ag Verfahren zur Reinigung von Indigo
TW251325B (es) 1993-03-30 1995-07-11 Basf Ag
DE4327221A1 (de) * 1993-08-13 1995-02-16 Basf Ag Leukoindigo-Präparation in Granulatform
DE4336032A1 (de) 1993-10-22 1995-04-27 Basf Ag Verfahren zur Reinigung von Indigo
DE19502968A1 (de) * 1995-01-31 1996-08-01 Basf Ag Leukoküpenfarbstoff-Präparationen in Granulatform
DE19624208A1 (de) 1996-06-18 1998-01-02 Basf Ag Leukoküpenfarbstoff-Präparationen in Granulatform
JPH10111633A (ja) 1996-10-04 1998-04-28 Denso Corp ホログラム感光剤，ホログラム感光材料及びホログラム，並びにこれらの製造方法
DE19831291A1 (de) 1998-07-13 2000-01-20 Basf Ag Konzentrierte Lekoindigolösungen
DE19919746A1 (de) 1999-04-29 2000-11-02 Basf Ag Verfahren zur Herstellung von wäßrig-alkalischen Lösungen reduzierter indigoider Farbstoffe
WO2004024826A2 (de) * 2002-08-31 2004-03-25 Dystar Textilfarben Gmbh & Co. Deutschland Kg Verfahren zur herstellung von hochreinem indigo
JP4941891B2 (ja) 2006-11-13 2012-05-30 株式会社Ｉｈｉ フィルム冷却構造
JP2009197353A (ja) 2008-02-20 2009-09-03 Asahi Breweries Ltd インヂゴの染色増強剤および増強方法
CN111108156A (zh) 2017-08-11 2020-05-05 昂高知识产权有限公司 具有很低苯胺含量的靛白盐溶液及其制备方法

Also Published As

Publication number Publication date
JP7011042B2 (ja) 2022-01-26
TWI760544B (zh) 2022-04-11
CN111065690A (zh) 2020-04-24
WO2019030397A1 (en) 2019-02-14
JP2020530516A (ja) 2020-10-22
KR102636594B1 (ko) 2024-02-13
KR102636591B1 (ko) 2024-02-13
US11384245B2 (en) 2022-07-12
WO2019030391A1 (en) 2019-02-14
KR20200037854A (ko) 2020-04-09
AR126783A2 (es) 2023-11-15
JP2020530517A (ja) 2020-10-22
US20200247999A1 (en) 2020-08-06
JP2023076433A (ja) 2023-06-01
SG11202001151PA (en) 2020-03-30
TN2020000011A1 (en) 2021-10-04
CO2020001377A2 (es) 2020-05-29
CN111108156A (zh) 2020-05-05
SG11202001155UA (en) 2020-03-30
CN111133057A (zh) 2020-05-08
JP2020530518A (ja) 2020-10-22
TW201920499A (zh) 2019-06-01
US11299633B2 (en) 2022-04-12
WO2019030396A1 (en) 2019-02-14
EP3665230A1 (en) 2020-06-17
BR112019018494A2 (pt) 2020-04-14
MA48430A1 (fr) 2020-04-30
BR112019018497B1 (pt) 2023-12-19
KR20210114958A (ko) 2021-09-24
JP2020537700A (ja) 2020-12-24
JP7295844B2 (ja) 2023-06-21
TWI763903B (zh) 2022-05-11
SG11202001153RA (en) 2020-03-30
CN111094460A (zh) 2020-05-01
BR112019018497A2 (pt) 2020-04-14
SG11202001152YA (en) 2020-03-30
CN111133057B (zh) 2022-09-13
TWI763904B (zh) 2022-05-11
BR112019018490A2 (pt) 2020-04-14
JP7245227B2 (ja) 2023-03-23
WO2019030389A1 (en) 2019-02-14
JP2023014157A (ja) 2023-01-26
BR112019018494B1 (pt) 2024-01-30
CN111065690B (zh) 2022-06-28
JP7250762B2 (ja) 2023-04-03
US20210009810A1 (en) 2021-01-14
MA48430B1 (fr) 2020-11-30
MX2020001518A (es) 2020-03-20
US20200216674A1 (en) 2020-07-09
EP3665229A1 (en) 2020-06-17
EP3665227A1 (en) 2020-06-17
TWI755558B (zh) 2022-02-21
PE20201187A1 (es) 2020-11-06
CN115627081A (zh) 2023-01-20
AR127380A2 (es) 2024-01-17
TN2020000013A1 (en) 2021-10-04
MX2020001519A (es) 2020-03-20
BR112019018498A2 (pt) 2020-04-14
TN2020000012A1 (en) 2021-10-04
CO2020001381A2 (es) 2020-05-29
KR20200037853A (ko) 2020-04-09
MX2020001516A (es) 2020-03-20
TW201925357A (zh) 2019-07-01
TN2020000014A1 (en) 2021-10-04
TW201920498A (zh) 2019-06-01
KR20230010673A (ko) 2023-01-19
EP3665228A1 (en) 2020-06-17
BR112019018490B1 (pt) 2023-12-19
MX2020001517A (es) 2020-08-03
PE20201188A1 (es) 2020-11-06
KR20200040278A (ko) 2020-04-17
KR20200040279A (ko) 2020-04-17
TW201920497A (zh) 2019-06-01
WO2019030396A8 (en) 2019-12-05
US20200172734A1 (en) 2020-06-04

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