AR127380A2 - Método para elaborar una solución acuosa de leucoíndigo libre de anilina o libre de anilina y n-metilanilina, solución estable acuosa de leucoindigo, método para su elaboración, aparato y uso - Google Patents
Método para elaborar una solución acuosa de leucoíndigo libre de anilina o libre de anilina y n-metilanilina, solución estable acuosa de leucoindigo, método para su elaboración, aparato y usoInfo
- Publication number
- AR127380A2 AR127380A2 ARP220102811A ARP220102811A AR127380A2 AR 127380 A2 AR127380 A2 AR 127380A2 AR P220102811 A ARP220102811 A AR P220102811A AR P220102811 A ARP220102811 A AR P220102811A AR 127380 A2 AR127380 A2 AR 127380A2
- Authority
- AR
- Argentina
- Prior art keywords
- aniline
- leucoindigo
- free
- aqueous solution
- methylaniline
- Prior art date
Links
- AFBPFSWMIHJQDM-UHFFFAOYSA-N N-methylaniline Chemical compound CNC1=CC=CC=C1 AFBPFSWMIHJQDM-UHFFFAOYSA-N 0.000 title abstract 8
- VIFKLIUAPGUEBV-UHFFFAOYSA-N 2-(3-hydroxy-1h-indol-2-yl)-1h-indol-3-ol Chemical compound N1C2=CC=CC=C2C(O)=C1C1=C(O)C2=CC=CC=C2N1 VIFKLIUAPGUEBV-UHFFFAOYSA-N 0.000 title abstract 5
- 239000007864 aqueous solution Substances 0.000 title abstract 4
- 238000000034 method Methods 0.000 title abstract 4
- 238000002360 preparation method Methods 0.000 title 1
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 abstract 6
- 239000007788 liquid Substances 0.000 abstract 2
- 238000000746 purification Methods 0.000 abstract 2
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- -1 alkali metal salt Chemical class 0.000 abstract 1
- 150000001412 amines Chemical class 0.000 abstract 1
- SQISUZWPWJHTEP-UHFFFAOYSA-N aniline Chemical compound NC1=CC=CC=C1.NC1=CC=CC=C1 SQISUZWPWJHTEP-UHFFFAOYSA-N 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/0083—Solutions of dyes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B7/00—Indigoid dyes
- C09B7/02—Bis-indole indigos
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/0077—Preparations with possibly reduced vat, sulfur or indigo dyes
- C09B67/0078—Preparations of vat, sulfur or indigo dyes in liquid form
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0096—Purification; Precipitation; Filtration
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/22—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using vat dyestuffs including indigo
- D06P1/228—Indigo
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Indole Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Coloring (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Peptides Or Proteins (AREA)
Abstract
Método para elaborar una solución acuosa de leucoíndigo libre de anilina o libre de anilina y N-metilanilina a partir de una solución acuosa de leucoíndigo que comprende anilina o anilina y N-metilanilina, la concentración de anilina o anilina y N-metilanilina se determina de acuerdo con la norma ISO 14362-1:2017(E), donde dicho leucoíndigo está en forma de una sal de metal alcalino, el método comprende al menos los pasos (A) a (C): (A) proporcionar una corriente líquida que comprende dicha solución acuosa de leucoíndigo que comprende dicha(s) amina(s); (B) proporcionar una corriente de purificación; (C) poner en contacto dicha corriente líquida con dicha corriente de purificación.
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP17185971.3A EP3441429B1 (en) | 2017-08-11 | 2017-08-11 | Purified concentrated aqueous leucoindigo salt solutions |
EP17185976.2A EP3441430B1 (en) | 2017-08-11 | 2017-08-11 | Leucoindigo salt solution with very low content of aniline and method of making same |
EP17185980.4A EP3441431B1 (en) | 2017-08-11 | 2017-08-11 | Methods of making leucoindigo salt solutions with very low aniline content |
EP18173343.7A EP3569660B1 (en) | 2018-05-18 | 2018-05-18 | Method for making aniline-free leucoindigo salt solutions |
Publications (1)
Publication Number | Publication Date |
---|---|
AR127380A2 true AR127380A2 (es) | 2024-01-17 |
Family
ID=63108593
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ARP220102183A AR126783A2 (es) | 2017-08-11 | 2022-08-12 | Métodos para fabricar soluciones de sal de leucoíndigo con muy bajo contenido de anilina |
ARP220102811A AR127380A2 (es) | 2017-08-11 | 2022-10-14 | Método para elaborar una solución acuosa de leucoíndigo libre de anilina o libre de anilina y n-metilanilina, solución estable acuosa de leucoindigo, método para su elaboración, aparato y uso |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ARP220102183A AR126783A2 (es) | 2017-08-11 | 2022-08-12 | Métodos para fabricar soluciones de sal de leucoíndigo con muy bajo contenido de anilina |
Country Status (15)
Country | Link |
---|---|
US (4) | US11299633B2 (es) |
EP (4) | EP3665228A1 (es) |
JP (6) | JP7245227B2 (es) |
KR (5) | KR102636591B1 (es) |
CN (5) | CN111108156A (es) |
AR (2) | AR126783A2 (es) |
BR (4) | BR112019018494B1 (es) |
CO (3) | CO2020001381A2 (es) |
MA (1) | MA48430B1 (es) |
MX (4) | MX2020001516A (es) |
PE (2) | PE20201188A1 (es) |
SG (4) | SG11202001151PA (es) |
TN (4) | TN2020000011A1 (es) |
TW (4) | TWI763903B (es) |
WO (4) | WO2019030396A1 (es) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
TWI763903B (zh) | 2017-08-11 | 2022-05-11 | 瑞士商亞齊羅馬Ip公司 | 製備無苯胺之靛白溶液的方法以及製得之穩定的水性靛白溶液、製備靛藍之方法、整合設備和一裝置之用途 |
CN110016816A (zh) * | 2019-03-13 | 2019-07-16 | 广东前进牛仔布有限公司 | 一种靛蓝染色方法 |
BR102019025172A2 (pt) * | 2019-11-28 | 2021-06-08 | Bann Química Ltda. | processo de purificação de soluções de sal de leucoíndigo e uso de um gás inerte |
Family Cites Families (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2130878A (en) * | 1933-04-10 | 1938-09-20 | Ici Ltd | Leucoindigo |
US4992143A (en) | 1989-06-09 | 1991-02-12 | Mobay Corporation | Continuous process for the separation of a partially water soluble component from a slurry |
US5116996A (en) | 1991-07-17 | 1992-05-26 | Basf Aktiengesellschaft | Purification of indigo |
US6169218B1 (en) | 1992-02-10 | 2001-01-02 | Catalytic Distillation Technologies | Selective hydrogenation of highly unsaturated compounds in hydrocarbon streams |
DE4220804A1 (de) * | 1992-06-25 | 1994-01-05 | Basf Ag | Verfahren zur Reinigung von Indigo |
TW251325B (es) | 1993-03-30 | 1995-07-11 | Basf Ag | |
DE4327221A1 (de) * | 1993-08-13 | 1995-02-16 | Basf Ag | Leukoindigo-Präparation in Granulatform |
DE4336032A1 (de) | 1993-10-22 | 1995-04-27 | Basf Ag | Verfahren zur Reinigung von Indigo |
DE19502968A1 (de) * | 1995-01-31 | 1996-08-01 | Basf Ag | Leukoküpenfarbstoff-Präparationen in Granulatform |
DE19624208A1 (de) | 1996-06-18 | 1998-01-02 | Basf Ag | Leukoküpenfarbstoff-Präparationen in Granulatform |
JPH10111633A (ja) | 1996-10-04 | 1998-04-28 | Denso Corp | ホログラム感光剤,ホログラム感光材料及びホログラム,並びにこれらの製造方法 |
DE19831291A1 (de) | 1998-07-13 | 2000-01-20 | Basf Ag | Konzentrierte Lekoindigolösungen |
DE19919746A1 (de) | 1999-04-29 | 2000-11-02 | Basf Ag | Verfahren zur Herstellung von wäßrig-alkalischen Lösungen reduzierter indigoider Farbstoffe |
AU2003260454A1 (en) | 2002-08-31 | 2004-04-30 | Dystar Textilfarben Gmbh And Co. Deutschland Kg | Method for the production of high-purity indigo |
JP4941891B2 (ja) | 2006-11-13 | 2012-05-30 | 株式会社Ihi | フィルム冷却構造 |
JP2009197353A (ja) | 2008-02-20 | 2009-09-03 | Asahi Breweries Ltd | インヂゴの染色増強剤および増強方法 |
TWI763903B (zh) | 2017-08-11 | 2022-05-11 | 瑞士商亞齊羅馬Ip公司 | 製備無苯胺之靛白溶液的方法以及製得之穩定的水性靛白溶液、製備靛藍之方法、整合設備和一裝置之用途 |
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2018
- 2018-08-10 TW TW107127915A patent/TWI763903B/zh active
- 2018-08-10 WO PCT/EP2018/071800 patent/WO2019030396A1/en unknown
- 2018-08-10 CN CN201880059267.4A patent/CN111108156A/zh active Pending
- 2018-08-10 WO PCT/EP2018/071805 patent/WO2019030397A1/en active Application Filing
- 2018-08-10 TW TW107127917A patent/TWI760544B/zh active
- 2018-08-10 SG SG11202001151PA patent/SG11202001151PA/en unknown
- 2018-08-10 MA MA48430A patent/MA48430B1/fr unknown
- 2018-08-10 US US16/637,874 patent/US11299633B2/en active Active
- 2018-08-10 CN CN201880059273.XA patent/CN111065690B/zh active Active
- 2018-08-10 MX MX2020001516A patent/MX2020001516A/es unknown
- 2018-08-10 MX MX2020001518A patent/MX2020001518A/es unknown
- 2018-08-10 PE PE2020000210A patent/PE20201188A1/es unknown
- 2018-08-10 JP JP2020507660A patent/JP7245227B2/ja active Active
- 2018-08-10 WO PCT/EP2018/071791 patent/WO2019030391A1/en unknown
- 2018-08-10 BR BR112019018494-5A patent/BR112019018494B1/pt active IP Right Grant
- 2018-08-10 TW TW107127916A patent/TWI755558B/zh active
- 2018-08-10 SG SG11202001153RA patent/SG11202001153RA/en unknown
- 2018-08-10 JP JP2020507600A patent/JP7011042B2/ja active Active
- 2018-08-10 US US16/637,889 patent/US20200216674A1/en not_active Abandoned
- 2018-08-10 TN TNP/2020/000011A patent/TN2020000011A1/en unknown
- 2018-08-10 JP JP2020507661A patent/JP7250762B2/ja active Active
- 2018-08-10 EP EP18750225.7A patent/EP3665228A1/en active Pending
- 2018-08-10 SG SG11202001155UA patent/SG11202001155UA/en unknown
- 2018-08-10 TW TW107127918A patent/TWI763904B/zh active
- 2018-08-10 BR BR112019018490-2A patent/BR112019018490B1/pt active IP Right Grant
- 2018-08-10 KR KR1020207007074A patent/KR102636591B1/ko active IP Right Grant
- 2018-08-10 EP EP18750226.5A patent/EP3665229A1/en active Pending
- 2018-08-10 MX MX2020001519A patent/MX2020001519A/es unknown
- 2018-08-10 KR KR1020207007071A patent/KR20200040278A/ko not_active IP Right Cessation
- 2018-08-10 PE PE2020000206A patent/PE20201187A1/es unknown
- 2018-08-10 JP JP2020507643A patent/JP7295844B2/ja active Active
- 2018-08-10 TN TNP/2020/000012A patent/TN2020000012A1/en unknown
- 2018-08-10 BR BR112019018498A patent/BR112019018498A2/pt not_active Application Discontinuation
- 2018-08-10 KR KR1020217023586A patent/KR20210114958A/ko not_active Application Discontinuation
- 2018-08-10 US US16/637,886 patent/US20200172734A1/en active Pending
- 2018-08-10 SG SG11202001152YA patent/SG11202001152YA/en unknown
- 2018-08-10 CN CN201880059274.4A patent/CN111133057B/zh active Active
- 2018-08-10 CN CN201880059304.1A patent/CN111094460A/zh active Pending
- 2018-08-10 TN TNP/2020/000013A patent/TN2020000013A1/en unknown
- 2018-08-10 WO PCT/EP2018/071783 patent/WO2019030389A1/en unknown
- 2018-08-10 KR KR1020207007084A patent/KR102636594B1/ko active IP Right Grant
- 2018-08-10 CN CN202211229474.4A patent/CN115627081A/zh active Pending
- 2018-08-10 US US16/637,862 patent/US11384245B2/en active Active
- 2018-08-10 KR KR1020227042817A patent/KR20230010673A/ko active IP Right Grant
- 2018-08-10 TN TNP/2020/000014A patent/TN2020000014A1/en unknown
- 2018-08-10 EP EP18750223.2A patent/EP3665227A1/en active Pending
- 2018-08-10 BR BR112019018497-0A patent/BR112019018497B1/pt active IP Right Grant
- 2018-08-10 MX MX2020001517A patent/MX2020001517A/es unknown
- 2018-08-10 EP EP18750227.3A patent/EP3665230A1/en active Pending
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2020
- 2020-02-07 CO CONC2020/0001381A patent/CO2020001381A2/es unknown
- 2020-02-07 CO CONC2020/0001377A patent/CO2020001377A2/es unknown
- 2020-02-07 CO CONC2020/0001376A patent/CO2020001376A2/es unknown
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2022
- 2022-08-12 AR ARP220102183A patent/AR126783A2/es unknown
- 2022-10-14 AR ARP220102811A patent/AR127380A2/es unknown
- 2022-11-21 JP JP2022185474A patent/JP2023014157A/ja active Pending
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2023
- 2023-02-28 JP JP2023029566A patent/JP2023076433A/ja active Pending
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