CN108252098A - A kind of polyester fiber spinning oil and preparation method thereof - Google Patents

A kind of polyester fiber spinning oil and preparation method thereof Download PDF

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Publication number
CN108252098A
CN108252098A CN201711364873.0A CN201711364873A CN108252098A CN 108252098 A CN108252098 A CN 108252098A CN 201711364873 A CN201711364873 A CN 201711364873A CN 108252098 A CN108252098 A CN 108252098A
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Prior art keywords
parts
polyester fiber
agent
spinning oil
fiber spinning
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CN201711364873.0A
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Inventor
储平
徐有琦
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Jiangsu New Lucky Polytron Technologies Inc
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Jiangsu New Lucky Polytron Technologies Inc
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Priority to CN201711364873.0A priority Critical patent/CN108252098A/en
Publication of CN108252098A publication Critical patent/CN108252098A/en
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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/53Polyethers
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/188Monocarboxylic acids; Anhydrides, halides or salts thereof
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/192Polycarboxylic acids; Anhydrides, halides or salts thereof
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/244Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
    • D06M13/282Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing phosphorus
    • D06M13/292Mono-, di- or triesters of phosphoric or phosphorous acids; Salts thereof
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/643Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16Synthetic fibres, other than mineral fibres
    • D06M2101/30Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/32Polyesters
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/40Reduced friction resistance, lubricant properties; Sizing compositions

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The invention discloses a kind of polyester fiber spinning oil and preparation method thereof, the polyester fiber is made of with spinning oil the raw material of following parts by weight:5 10 parts of emulsifier, 35 parts of smooth agent, 5 10 parts of antistatic agent, 37 parts of collecting agent, 13 parts of preservative, 13 parts of antifoaming agent, 35 parts of pH adjusting agent, 20 30 parts of deionized water.The good flatness of fiber and convergence, good hot property are imparted after the polyester fiber spinning oil application of the present invention.The polyester fiber spinning oil of the present invention has excellent oil effect and antistatic effect.The polyester fiber spinning oil of the present invention causes fiber, and lousiness little breakage, item is done and even dyeing, and smoke amount is few, and coking is few, and the cleaning frequency is long, and product stability is good in rear road drafting process.

Description

A kind of polyester fiber spinning oil and preparation method thereof
Technical field
The invention belongs to field of fabric producing technology, specifically relate to a kind of polyester fiber spinning oil and its preparation side Method.
Background technology
Polyester fiber (polyester fiber) abbreviation PET fiber, Chinese trade name is referred to as terylene, is by organic The polyester that binary acid and dihydric alcohol polycondensation form mainly uses poly terephthalic acid second through the synthetic fibers obtained by spinning, polyester fiber Diol ester is made, and is the first big kind of current synthetic fibers.In addition to this there is a small amount of poly terephthalic acid (third) diol ester Fiber, abbreviation PTT polyester fibers.Its biggest advantage is that wrinkle resistance and conformality are fine, it is extensive with higher intensity and elasticity Reactivation power.
Spinning oil be chemical fibre or synthetic fibers before spinned fiber, the liquid substance that is added in into spinning solution, It forms cohesion and wetability needed for fiber assigning so that post-processing process (boundling, stretching, combing) be able to smoothly into Row, while can also make the fiber to be formed that there are smooth pliable and the performances such as antistatic.But general finish in use can Occur coating fiber bad so that fibre frictoin is larger, and the yarn of production is caused bifurcated, broken end etc. occur, leads to pure polyester The quality of yarn declines.
Invention content
The purpose of the present invention is to provide a kind of polyester fiber spinning oil and preparation method thereof, to solve above-mentioned background The problem of being proposed in technology.
To achieve the above object, the present invention provides following technical solution:
A kind of polyester fiber spinning oil, according to parts by weight, including following components:5-10 parts of emulsifier, smooth agent 3-5 parts, 5-10 parts of antistatic agent, 3-7 parts of collecting agent, 1-3 parts of preservative, 1-3 parts of antifoaming agent, 3-5 parts of pH adjusting agent, deionization 20-30 parts of water.
Preferably, the emulsifier is ethoxylated dodecyl alcohol, paregal O, polyoxyethylene oleic acid ester, stearic acid gather Ethylene oxide ester, polysorbas20, polysorbate40, polysorbate60, Tween 80, Span 20, Span 40, Span 60, Span 80, detergent alkylate sulphur It is one or more than one kinds of in sour sodium.
Preferably, the smooth agent is a kind of or a kind of in white oil, fatty acid polyethylene glycol ester, C16-C18 alcohol More than.
Preferably, the antistatic agent is lauryl alcohol polyethylene glycol oxide ester, D-sorbite, glycollic amide, anhydrous sorbitol It is one or more than one kinds of in ester.
Preferably, the collecting agent is a kind of or a kind of in Polyethylene Glycol Oleate, oleic acid polyethylene glycol dibasic acid esters More than.
Preferably, the preservative is one or more than one kinds of in sorbic acid, sodium Diacetate, sodium lactate.
Preferably, the antifoaming agent is one or more than one kinds of in aqueous silicone oil, tributyl phosphate.
Preferably, the pH adjusting agent be acetic acid, citric acid, sodium carbonate, in sodium bicarbonate it is a kind of or a kind of with On.
Preferably, the preparation method of the polyester fiber spinning oil, specific steps include:
Step 1,20-30 parts of deionized water, 50-60 DEG C of oil bath heating, condensing reflux are added in a kettle;
Step 2,5-10 parts of emulsifier, 5-10 parts of antistatic agent, rate of addition 10- are slowly added to by constant pressure funnel 20mL/min, 500-700 rev/min are stirred 10-20 minutes;
Step 3, temperature is reduced to 30-40 DEG C, adds in pH adjusting agent, and adjusting pH is 5-7;
Step 4,3-5 parts of smooth agent, 3-7 parts of collecting agent are added in, 500-1000 revs/min, is stirred 20-30 minutes;
Step 5, pH adjusting agent is added in, adjusting pH is 7-8;
Step 6,1-3 parts of preservative, 1-3 parts of antifoaming agent are added in, 500-1000 revs/min, is stirred 30-40 minutes;
Step 7, stirring is shut down, obtains prepared liquid polyester fiber spinning oil;
Step 8, it stands and is cooled in reaction kettle liquid polyester fiber spinning oil and is less than 20 DEG C, blowing encapsulation is made Finished product.
Compared with prior art, the beneficial effects of the invention are as follows:
1st, the good flatness of fiber and convergence are imparted after polyester fiber spinning oil of the invention application, it is good Good hot property.
2nd, polyester fiber spinning oil of the invention has excellent oil effect and antistatic effect.The present invention's is poly- Ester fiber spinning oil causes fiber, and lousiness little breakage, item is done and even dyeing, and smoke amount is few in rear road drafting process, Coking is few, and the cleaning frequency is long, and product stability is good.
3rd, there is good spinnability, smooth under the high temperature conditions after polyester fiber of the invention is applied with spinning oil Property, coherent it is good, no lousiness, end breakage rate is low, waste silk rate be less than import finish.
4th, polyester fiber of the invention is simple to operation with spinning oil manufacturing process, and low in raw material price easily obtains, and It is nontoxic, human body is not stimulated, volatility is low.
5th, mutual compatibility, synergistic effect between various raw materials used in polyester fiber spinning oil of the invention, common group Into the product haveing excellent performance.
6th, simplify technique, safe operation is simple, is easy to industrialized production.
7th, use of the invention can receive good economic benefit.
Example is embodied
The invention discloses a kind of polyester fiber spinning oil, according to parts by weight, including following components:Emulsifier 5- 10 parts, 3-5 parts of smooth agent, 5-10 parts of antistatic agent, 3-7 parts of collecting agent, 1-3 parts of preservative, 1-3 parts of antifoaming agent, pH adjusting agent 3-5 parts, 20-30 parts of deionized water.
The present invention also provides a kind of preparation method of polyester fiber spinning oil, specific steps include:
Step 1,20-30 parts of deionized water, 50-60 DEG C of oil bath heating, condensing reflux are added in a kettle;
Step 2,5-10 parts of emulsifier, 5-10 parts of antistatic agent, rate of addition 10- are slowly added to by constant pressure funnel 20mL/min, 500-700 rev/min are stirred 10-20 minutes;
Step 3, temperature is reduced to 30-40 DEG C, adds in pH adjusting agent, and adjusting pH is 5-7;
Step 4,3-5 parts of smooth agent, 3-7 parts of collecting agent are added in, 500-1000 revs/min, is stirred 20-30 minutes;
Step 5, pH adjusting agent is added in, adjusting pH is 7-8;
Step 6,1-3 parts of preservative, 1-3 parts of antifoaming agent are added in, 500-1000 revs/min, is stirred 30-40 minutes;
Step 7, stirring is shut down, obtains prepared liquid polyester fiber spinning oil;
Step 8, it stands and is cooled in reaction kettle liquid polyester fiber spinning oil and is less than 20 DEG C, blowing encapsulation is made Finished product.
Embodiment 1
The invention discloses a kind of polyester fiber spinning oil, according to parts by weight, including following components:Emulsifier 5 Part, 3 parts of smooth agent, 5 parts of antistatic agent, 3 parts of collecting agent, 1 part of preservative, 1 part of antifoaming agent, 3 parts of pH adjusting agent, deionized water 20 Part.
The present invention also provides a kind of preparation method of polyester fiber spinning oil, specific steps include:
Step 1,20 parts of deionized water, 50 DEG C of oil bath heating, condensing reflux are added in a kettle;
Step 2,5 parts of emulsifier, 5 parts of antistatic agent are slowly added to by constant pressure funnel, rate of addition 10mL/min, It 500 revs/min, stirs 10 minutes;
Step 3, temperature is reduced to 30 DEG C, adds in pH adjusting agent, and it is 5 to adjust pH;
Step 4,3 parts of smooth agent, 3 parts of collecting agent are added in, 500 revs/min, is stirred 20 minutes;
Step 5, pH adjusting agent is added in, it is 7 to adjust pH;
Step 6,1 part of preservative, 1 part of antifoaming agent are added in, 500 revs/min, is stirred 30 minutes;
Step 7, stirring is shut down, obtains prepared liquid polyester fiber spinning oil;
Step 8, it stands and is cooled in reaction kettle liquid polyester fiber spinning oil and is less than 20 DEG C, blowing encapsulation is made Finished product.
Embodiment 2
The invention discloses a kind of polyester fiber spinning oil, according to parts by weight, including following components:Emulsifier 8 Part, 4 parts of smooth agent, 8 parts of antistatic agent, 5 parts of collecting agent, 2 parts of preservative, 2 parts of antifoaming agent, 4 parts of pH adjusting agent, deionized water 25 Part.
The present invention also provides a kind of preparation method of polyester fiber spinning oil, specific steps include:
Step 1,25 parts of deionized water, 55 DEG C of oil bath heating, condensing reflux are added in a kettle;
Step 2,8 parts of emulsifier, 8 parts of antistatic agent are slowly added to by constant pressure funnel, rate of addition 15mL/min, It 700 revs/min, stirs 15 minutes;
Step 3, temperature is reduced to 35 DEG C, adds in pH adjusting agent, and it is 6 to adjust pH;
Step 4,4 parts of smooth agent, 5 parts of collecting agent are added in, 800 revs/min, is stirred 25 minutes;
Step 5, pH adjusting agent is added in, it is 7 to adjust pH;
Step 6,2 parts of preservative, 2 parts of antifoaming agent are added in, 900 revs/min, is stirred 35 minutes;
Step 7, stirring is shut down, obtains prepared liquid polyester fiber spinning oil;
Step 8, it stands and is cooled in reaction kettle liquid polyester fiber spinning oil and is less than 20 DEG C, blowing encapsulation is made Finished product.
Embodiment 3
The invention discloses a kind of polyester fiber spinning oil, according to parts by weight, including following components:Emulsifier 10 Part, 5 parts of smooth agent, 10 parts of antistatic agent, 7 parts of collecting agent, 3 parts of preservative, 3 parts of antifoaming agent, 5 parts of pH adjusting agent, deionized water 30 parts.
The present invention also provides a kind of preparation method of polyester fiber spinning oil, specific steps include:
Step 1,30 parts of deionized water, 60 DEG C of oil bath heating, condensing reflux are added in a kettle;
Step 2,10 parts of emulsifier, 10 parts of antistatic agent are slowly added to by constant pressure funnel, rate of addition 20mL/min, It 700 revs/min, stirs 10 minutes;
Step 3, temperature is reduced to 40 DEG C, adds in pH adjusting agent, and it is 7 to adjust pH;
Step 4,5 parts of smooth agent, 7 parts of collecting agent are added in, 1000 revs/min, is stirred 20 minutes;
Step 5, pH adjusting agent is added in, it is 8 to adjust pH;
Step 6,3 parts of preservative, 3 parts of antifoaming agent are added in, 1000 revs/min, is stirred 40 minutes;
Step 7, stirring is shut down, obtains prepared liquid polyester fiber spinning oil;
Step 8, it stands and is cooled in reaction kettle liquid polyester fiber spinning oil and is less than 20 DEG C, blowing encapsulation is made Finished product.
Embodiment 4
The invention discloses a kind of polyester fiber spinning oil, according to parts by weight, including following components:Emulsifier 8 Part, 4 parts of smooth agent, 10 parts of antistatic agent, 7 parts of collecting agent, 2 parts of preservative, 2 parts of antifoaming agent, 4 parts of pH adjusting agent, deionized water 20 parts.
The present invention also provides a kind of preparation method of polyester fiber spinning oil, specific steps include:
Step 1,20 parts of deionized water, 60 DEG C of oil bath heating, condensing reflux are added in a kettle;
Step 2,8 parts of emulsifier, 10 parts of antistatic agent are slowly added to by constant pressure funnel, rate of addition 10mL/min, It 700 revs/min, stirs 10 minutes;
Step 3, temperature is reduced to 35 DEG C, adds in pH adjusting agent, and it is 7 to adjust pH;
Step 4,4 parts of smooth agent, 7 parts of collecting agent are added in, 1000 revs/min, is stirred 20 minutes;
Step 5, pH adjusting agent is added in, it is 7 to adjust pH;
Step 6,2 parts of preservative, 2 parts of antifoaming agent are added in, 800 revs/min, is stirred 35 minutes;
Step 7, stirring is shut down, obtains prepared liquid polyester fiber spinning oil;
Step 8, it stands and is cooled in reaction kettle liquid polyester fiber spinning oil and is less than 20 DEG C, blowing encapsulation is made Finished product.
Test case
Polyester fiber is handled using the polyester fiber spinning oil of embodiment 1,2,3,4, test result is as follows:
Embodiment Smoke amount Coking is removed Lousiness number Centrifugal stability
It is untreated It is more It is difficult It is more Layering
1 It is less Easily It is less Stablize
2 Seldom It is easy to Seldom Stablize
3 It is micro It is easy to It is micro Stablize
4 Seldom It is easy to Seldom Stablize
The above-mentioned various embodiments enumerated, under the premise of reconcilable, can be combined with each other implementation, those skilled in the art It can combine above to the explanation of embodiment, as the foundation being combined to the technical characteristic in different embodiments.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace And modification, the scope of the present invention is defined by the appended.

Claims (9)

1. a kind of polyester fiber spinning oil, it is characterised in that:The polyester fiber includes following parts by weight with spinning oil Several raw materials:5-10 parts of emulsifier, 3-5 parts of smooth agent, 5-10 parts of antistatic agent, 3-7 parts of collecting agent, 1-3 parts of preservative, defoaming 1-3 parts of agent, 3-5 parts of pH adjusting agent, 20-30 parts of deionized water.
2. polyester fiber spinning oil according to claim 1, it is characterised in that:The emulsifier gathers for laruyl alcohol Ethylene oxide ether, paregal O, polyoxyethylene oleic acid ester, polyoxyethylene stearic acid ester, polysorbas20, polysorbate40, polysorbate60, Tween 80, It is one or more than one kinds of in Span 20, Span 40, Span 60, Span 80, neopelex.
3. polyester fiber spinning oil according to claim 1, it is characterised in that:The smooth agent is white oil, fat It is one or more than one kinds of in fat acid polyethylene glycol ester, C16-C18 alcohol.
4. polyester fiber spinning oil according to claim 1, it is characterised in that:The antistatic agent is laruyl alcohol It is one or more than one kinds of in polyoxyethylene ester, D-sorbite, glycollic amide, sorbitan ester.
5. polyester fiber spinning oil according to claim 1, it is characterised in that:The collecting agent is the poly- second of oleic acid It is one or more than one kinds of in diol ester, oleic acid polyethylene glycol dibasic acid esters.
6. polyester fiber spinning oil according to claim 1, it is characterised in that:The preservative for sorbic acid, It is one or more than one kinds of in sodium Diacetate, sodium lactate.
7. polyester fiber spinning oil according to claim 1, it is characterised in that:The antifoaming agent is aqueous silicon It is one or more than one kinds of in oil, tributyl phosphate.
8. polyester fiber spinning oil according to claim 1, it is characterised in that:The pH adjusting agent for acetic acid, It is one or more than one kinds of in citric acid, sodium carbonate, sodium bicarbonate.
9. a kind of preparation method using any one of the claims 1-8 polyester fiber spinning oils, feature It is:Specific steps include:
Step 1,20-30 parts of deionized water, 50-60 DEG C of oil bath heating, condensing reflux are added in a kettle;
Step 2,5-10 parts of emulsifier, 5-10 parts of antistatic agent, rate of addition 10-20mL/ are slowly added to by constant pressure funnel Min, 500-700 rev/min are stirred 10-20 minutes;
Step 3, temperature is reduced to 30-40 DEG C, adds in pH adjusting agent, and adjusting pH is 5-7;
Step 4,3-5 parts of smooth agent, 3-7 parts of collecting agent are added in, 500-1000 revs/min, is stirred 20-30 minutes;
Step 5, pH adjusting agent is added in, adjusting pH is 7-8;
Step 6,1-3 parts of preservative, 1-3 parts of antifoaming agent are added in, 500-1000 revs/min, is stirred 30-40 minutes;
Step 7, stirring is shut down, obtains prepared liquid polyester fiber spinning oil;
Step 8, it stands and is cooled in reaction kettle liquid polyester fiber spinning oil and is less than 20 DEG C, blowing encapsulation, finished product.
CN201711364873.0A 2017-12-18 2017-12-18 A kind of polyester fiber spinning oil and preparation method thereof Pending CN108252098A (en)

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108998979A (en) * 2018-07-27 2018-12-14 南通凯大纺织有限公司 A kind of preparation method of terylene spinning finish
CN109763335A (en) * 2019-01-12 2019-05-17 厦门东纶股份有限公司 A kind of nylon spinning oil and preparation method thereof
CN109957861A (en) * 2019-02-28 2019-07-02 常州凯途纺织品有限公司 A kind of heat-resisting oxidation-resistance spinning oil
CN110965331A (en) * 2018-09-30 2020-04-07 中国石油化工股份有限公司 Polyvinyl alcohol water-soluble short fiber spinning oil and preparation method thereof
CN112647284A (en) * 2020-12-17 2021-04-13 太仓旭云特种纤维科技有限公司 PBO fiber carding oil
CN115369649A (en) * 2022-07-29 2022-11-22 桐乡市恒隆化工有限公司 Special oil for low-oil-smoke high-speed spinning of heat-humidity comfortable polyester fiber and preparation process thereof
CN115787146A (en) * 2022-12-30 2023-03-14 江苏索力得新材料集团有限公司 High-temperature-resistant industrial silk spinning oil agent and production process thereof

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CN104179005A (en) * 2014-08-15 2014-12-03 上海中孚特种油品有限公司 Fiber fully drawn yarn (FDY) spinning oil and preparation method thereof
CN106065527A (en) * 2016-07-08 2016-11-02 苏州夏尔植物油脂科技有限公司 Polyester filament FDY spinning oil and preparation method thereof
CN107227612A (en) * 2017-06-28 2017-10-03 常州通和建筑工程有限公司 A kind of spinning oil of resistance to volatile-type

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Publication number Priority date Publication date Assignee Title
CN101629383A (en) * 2009-08-27 2010-01-20 上虞市皇马化学有限公司 Terylene FDY spinning oil and preparation process thereof
CN104179005A (en) * 2014-08-15 2014-12-03 上海中孚特种油品有限公司 Fiber fully drawn yarn (FDY) spinning oil and preparation method thereof
CN106065527A (en) * 2016-07-08 2016-11-02 苏州夏尔植物油脂科技有限公司 Polyester filament FDY spinning oil and preparation method thereof
CN107227612A (en) * 2017-06-28 2017-10-03 常州通和建筑工程有限公司 A kind of spinning oil of resistance to volatile-type

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108998979A (en) * 2018-07-27 2018-12-14 南通凯大纺织有限公司 A kind of preparation method of terylene spinning finish
CN110965331A (en) * 2018-09-30 2020-04-07 中国石油化工股份有限公司 Polyvinyl alcohol water-soluble short fiber spinning oil and preparation method thereof
CN110965331B (en) * 2018-09-30 2022-06-21 中国石油化工股份有限公司 Polyvinyl alcohol water-soluble short fiber spinning oil and preparation method thereof
CN109763335A (en) * 2019-01-12 2019-05-17 厦门东纶股份有限公司 A kind of nylon spinning oil and preparation method thereof
CN109763335B (en) * 2019-01-12 2021-03-02 厦门东纶股份有限公司 Nylon spinning oil and preparation method thereof
CN109957861A (en) * 2019-02-28 2019-07-02 常州凯途纺织品有限公司 A kind of heat-resisting oxidation-resistance spinning oil
CN112647284A (en) * 2020-12-17 2021-04-13 太仓旭云特种纤维科技有限公司 PBO fiber carding oil
CN115369649A (en) * 2022-07-29 2022-11-22 桐乡市恒隆化工有限公司 Special oil for low-oil-smoke high-speed spinning of heat-humidity comfortable polyester fiber and preparation process thereof
CN115787146A (en) * 2022-12-30 2023-03-14 江苏索力得新材料集团有限公司 High-temperature-resistant industrial silk spinning oil agent and production process thereof

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Application publication date: 20180706