CN115787146A - High-temperature-resistant industrial silk spinning oil agent and production process thereof - Google Patents
High-temperature-resistant industrial silk spinning oil agent and production process thereof Download PDFInfo
- Publication number
- CN115787146A CN115787146A CN202211713066.6A CN202211713066A CN115787146A CN 115787146 A CN115787146 A CN 115787146A CN 202211713066 A CN202211713066 A CN 202211713066A CN 115787146 A CN115787146 A CN 115787146A
- Authority
- CN
- China
- Prior art keywords
- agent
- parts
- oil
- industrial yarn
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000009987 spinning Methods 0.000 title claims abstract description 81
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 28
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 96
- 239000003921 oil Substances 0.000 claims abstract description 69
- 239000002270 dispersing agent Substances 0.000 claims abstract description 25
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 25
- 239000002994 raw material Substances 0.000 claims abstract description 25
- 239000003146 anticoagulant agent Substances 0.000 claims abstract description 24
- 229940127219 anticoagulant drug Drugs 0.000 claims abstract description 24
- 239000002216 antistatic agent Substances 0.000 claims abstract description 24
- 239000002199 base oil Substances 0.000 claims abstract description 23
- 239000002518 antifoaming agent Substances 0.000 claims abstract description 19
- 239000008367 deionised water Substances 0.000 claims abstract description 18
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 18
- 230000005415 magnetization Effects 0.000 claims abstract description 15
- 238000001816 cooling Methods 0.000 claims abstract description 8
- 238000000034 method Methods 0.000 claims abstract description 7
- 238000006243 chemical reaction Methods 0.000 claims description 25
- 238000003756 stirring Methods 0.000 claims description 25
- 239000000203 mixture Substances 0.000 claims description 23
- 238000005303 weighing Methods 0.000 claims description 17
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical group CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 15
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 15
- 239000004359 castor oil Substances 0.000 claims description 15
- 235000019438 castor oil Nutrition 0.000 claims description 15
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims description 15
- 230000014759 maintenance of location Effects 0.000 claims description 13
- 238000002156 mixing Methods 0.000 claims description 12
- MUHFRORXWCGZGE-KTKRTIGZSA-N 2-hydroxyethyl (z)-octadec-9-enoate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCCO MUHFRORXWCGZGE-KTKRTIGZSA-N 0.000 claims description 10
- 239000002202 Polyethylene glycol Substances 0.000 claims description 10
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 10
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 10
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 10
- 239000000194 fatty acid Substances 0.000 claims description 10
- 229930195729 fatty acid Natural products 0.000 claims description 10
- 229940095098 glycol oleate Drugs 0.000 claims description 10
- 229920001223 polyethylene glycol Polymers 0.000 claims description 10
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 10
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 10
- 239000004721 Polyphenylene oxide Substances 0.000 claims description 8
- 229920000570 polyether Polymers 0.000 claims description 8
- BNIILDVGGAEEIG-UHFFFAOYSA-L disodium hydrogen phosphate Chemical compound [Na+].[Na+].OP([O-])([O-])=O BNIILDVGGAEEIG-UHFFFAOYSA-L 0.000 claims description 7
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 claims description 7
- 230000001105 regulatory effect Effects 0.000 claims description 6
- RZRNAYUHWVFMIP-KTKRTIGZSA-N 1-oleoylglycerol Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC(O)CO RZRNAYUHWVFMIP-KTKRTIGZSA-N 0.000 claims description 5
- FMNZBNCPTJEVDS-KVVVOXFISA-N 2-ethyl-2-(hydroxymethyl)propane-1,3-diol;(z)-octadec-9-enoic acid Chemical compound CCC(CO)(CO)CO.CCCCCCCC\C=C/CCCCCCCC(O)=O FMNZBNCPTJEVDS-KVVVOXFISA-N 0.000 claims description 5
- CZBZUDVBLSSABA-UHFFFAOYSA-N butylated hydroxyanisole Chemical group COC1=CC=C(O)C(C(C)(C)C)=C1.COC1=CC=C(O)C=C1C(C)(C)C CZBZUDVBLSSABA-UHFFFAOYSA-N 0.000 claims description 5
- 230000001276 controlling effect Effects 0.000 claims description 5
- 239000000645 desinfectant Substances 0.000 claims description 5
- MIMDHDXOBDPUQW-UHFFFAOYSA-N dioctyl decanedioate Chemical compound CCCCCCCCOC(=O)CCCCCCCCC(=O)OCCCCCCCC MIMDHDXOBDPUQW-UHFFFAOYSA-N 0.000 claims description 5
- -1 fatty acid triethanolamine ester Chemical class 0.000 claims description 5
- 150000004665 fatty acids Chemical class 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 5
- 229910000403 monosodium phosphate Inorganic materials 0.000 claims description 5
- 235000019799 monosodium phosphate Nutrition 0.000 claims description 5
- 229940049964 oleate Drugs 0.000 claims description 5
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 claims description 5
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 claims description 5
- 229920003023 plastic Polymers 0.000 claims description 5
- 239000004033 plastic Substances 0.000 claims description 5
- 229920002401 polyacrylamide Polymers 0.000 claims description 5
- 229920001522 polyglycol ester Polymers 0.000 claims description 5
- 235000017557 sodium bicarbonate Nutrition 0.000 claims description 5
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims description 5
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 5
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 claims description 5
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 claims description 5
- 235000019982 sodium hexametaphosphate Nutrition 0.000 claims description 5
- 235000019832 sodium triphosphate Nutrition 0.000 claims description 5
- BSWXAWQTMPECAK-UHFFFAOYSA-N 6,6-diethyloctyl dihydrogen phosphate Chemical compound CCC(CC)(CC)CCCCCOP(O)(O)=O BSWXAWQTMPECAK-UHFFFAOYSA-N 0.000 claims description 4
- QNVRIHYSUZMSGM-UHFFFAOYSA-N hexan-2-ol Chemical compound CCCCC(C)O QNVRIHYSUZMSGM-UHFFFAOYSA-N 0.000 claims description 4
- 238000004806 packaging method and process Methods 0.000 claims description 4
- 238000007789 sealing Methods 0.000 claims description 4
- 238000011049 filling Methods 0.000 claims description 2
- 150000004760 silicates Chemical class 0.000 claims description 2
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 claims description 2
- 229940048086 sodium pyrophosphate Drugs 0.000 claims description 2
- 235000019818 tetrasodium diphosphate Nutrition 0.000 claims description 2
- 239000000463 material Substances 0.000 claims 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract description 5
- 239000010687 lubricating oil Substances 0.000 abstract description 5
- 238000005516 engineering process Methods 0.000 abstract description 2
- 229910052742 iron Inorganic materials 0.000 abstract description 2
- 230000033228 biological regulation Effects 0.000 abstract 1
- 239000006185 dispersion Substances 0.000 abstract 1
- 230000001050 lubricating effect Effects 0.000 abstract 1
- 230000003647 oxidation Effects 0.000 abstract 1
- 238000007254 oxidation reaction Methods 0.000 abstract 1
- 230000001172 regenerating effect Effects 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 description 7
- 239000013530 defoamer Substances 0.000 description 4
- 239000002480 mineral oil Substances 0.000 description 4
- 235000010446 mineral oil Nutrition 0.000 description 4
- 239000002105 nanoparticle Substances 0.000 description 4
- 108010022355 Fibroins Proteins 0.000 description 3
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 3
- PHYFQTYBJUILEZ-UHFFFAOYSA-N Trioleoylglycerol Natural products CCCCCCCCC=CCCCCCCCC(=O)OCC(OC(=O)CCCCCCCC=CCCCCCCCC)COC(=O)CCCCCCCC=CCCCCCCCC PHYFQTYBJUILEZ-UHFFFAOYSA-N 0.000 description 3
- 238000010923 batch production Methods 0.000 description 3
- QXLPXWSKPNOQLE-UHFFFAOYSA-N methylpentynol Chemical compound CCC(C)(O)C#C QXLPXWSKPNOQLE-UHFFFAOYSA-N 0.000 description 3
- 229920002545 silicone oil Polymers 0.000 description 3
- JOLVYUIAMRUBRK-UTOQUPLUSA-N Cardanol Chemical class OC1=CC=CC(CCCCCCC\C=C/C\C=C/CC=C)=C1 JOLVYUIAMRUBRK-UTOQUPLUSA-N 0.000 description 2
- 238000005299 abrasion Methods 0.000 description 2
- 235000019800 disodium phosphate Nutrition 0.000 description 2
- 229910000397 disodium phosphate Inorganic materials 0.000 description 2
- 238000005461 lubrication Methods 0.000 description 2
- 239000004094 surface-active agent Substances 0.000 description 2
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 1
- 235000017491 Bambusa tulda Nutrition 0.000 description 1
- 241001330002 Bambuseae Species 0.000 description 1
- 239000004255 Butylated hydroxyanisole Substances 0.000 description 1
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 1
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 description 1
- GTVWRXDRKAHEAD-UHFFFAOYSA-N Tris(2-ethylhexyl) phosphate Chemical compound CCCCC(CC)COP(=O)(OCC(CC)CCCC)OCC(CC)CCCC GTVWRXDRKAHEAD-UHFFFAOYSA-N 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 239000011425 bamboo Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229940043253 butylated hydroxyanisole Drugs 0.000 description 1
- 235000019282 butylated hydroxyanisole Nutrition 0.000 description 1
- XPPKVPWEQAFLFU-UHFFFAOYSA-J diphosphate(4-) Chemical compound [O-]P([O-])(=O)OP([O-])([O-])=O XPPKVPWEQAFLFU-UHFFFAOYSA-J 0.000 description 1
- 235000011180 diphosphates Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000009499 grossing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229920001296 polysiloxane Polymers 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 229940048084 pyrophosphate Drugs 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Landscapes
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a high-temperature-resistant industrial yarn spinning oil agent and a production process thereof, and relates to the field of spinning auxiliaries. The high-temperature-resistant industrial yarn spinning oil comprises 40-80 parts of base oil, 8-18 parts of emulsifier, 2-8 parts of bundling agent, 2-10 parts of anticoagulant, 1-3 parts of dispersant, 3-9 parts of water retention agent, 1-5 parts of defoaming agent, 5-9 parts of antistatic agent, 1-3 parts of pH regulator and 6-10 parts of deionized water. This production technology of industry silk spinning finish of high temperature resistant type, weigh through the raw materials, constant temperature mixes, the cooling dispersion, pH value regulation and five steps of magnetization, pungent smell can not appear at the in-process of preparing the spinning finish, the spinning finish after the magnetization, can effectually carry over the iron fillings that come back after lubricating to repel, thereby purify lubricating oil, avoid regenerating the vicious circle of more wearing and tearing, the effectual spinning finish of avoiding is located in high temperature environment for a long time, can the oxidation failure, appear blackening, the phenomenon of becoming thick, increase its life.
Description
Technical Field
The invention relates to the technical field of spinning auxiliaries, in particular to a high-temperature-resistant industrial silk spinning oil agent and a production process thereof.
Background
The high-temperature-resistant wear-resistant spinning oil with the publication number of CN114687212A and the preparation method thereof are characterized in that a cardanol derivative surfactant is introduced into an emulsifier, and the cardanol derivative surfactant is compounded and cooperated with a smoothing agent, an antistatic agent, a bundling agent and other components, so that the use amount of the emulsifier is greatly reduced compared with that of the prior art on the basis of ensuring excellent emulsibility and emulsion stability, the heat resistance is obviously superior to that of good swallow oil in the market, and the wear resistance is obviously superior to that of the good swallow oil and bamboo oil.
According to the high-temperature-resistant wear-resistant spinning oil and the preparation method thereof, nano-scale particles are easy to agglomerate in the use process of the prepared spinning oil, and the agglomerated nano-scale particles are difficult to disperse by the dispersing agent, so that the wear resistance of the lubricating oil is reduced.
Disclosure of Invention
Technical problem to be solved
The invention aims to provide a high-temperature-resistant industrial silk spinning oil agent and a production process thereof, so as to solve the problems in the background technology.
(II) technical scheme
In order to achieve the purpose, the invention provides the following technical scheme: a high-temperature-resistant industrial yarn spinning oil agent comprises the following raw materials in parts by weight: 40-80 parts of base oil, 8-18 parts of emulsifier, 2-8 parts of bundling agent, 2-10 parts of anticoagulant, 1-3 parts of dispersant, 3-9 parts of water retention agent, 1-5 parts of defoaming agent, 5-9 parts of antistatic agent, 1-3 parts of pH regulator and 6-10 parts of deionized water.
Preferably, the base oil is one or a mixture of several of dioctyl sebacate, trimethylolpropane oleate, pentaerythritol oleate, glycerol oleate and polyethylene glycol oleate.
Preferably, the emulsifier is one or a mixture of more of sulfated castor oil, hydrogenated castor oil polyoxyethylene ether and polyethylene glycol oleate.
Preferably, the bundling agent is formed by mixing hydrogenated castor oil polyoxyethylene ether and fatty acid triethanolamine ester.
Preferably, the anticoagulant is butylated hydroxyanisole.
Preferably, the dispersing agent is one or a mixture of silicate, triethylhexyl phosphoric acid, methyl amyl alcohol, polyacrylamide and fatty acid polyglycol ester.
Preferably, the water retention agent is one or a mixture of more of sodium tripolyphosphate, sodium hexametaphosphate, sodium pyrophosphate, disodium hydrogen phosphate and sodium dihydrogen phosphate.
Preferably, the defoaming agent is one of mineral oil, silicone and polyether.
Preferably, the antistatic agent is a propylene glycol block polyether.
Preferably, the PH regulator is one of sodium carbonate, sodium bicarbonate and sodium hydroxide.
A production process of a high-temperature-resistant industrial yarn spinning oil agent comprises the following steps:
s1, weighing raw materials; weighing the base oil, the emulsifier, the bundling agent, the anticoagulant, the dispersant, the water retention agent, the defoamer, the antistatic agent, the pH regulator and the deionized water according to the raw material ratio, and weighing for later use;
s2, mixing at constant temperature; adding the base oil weighed in the step S1 into a reaction kettle, adding an emulsifier, a bundling agent, an anticoagulant and a moisture retention agent into the reaction kettle, then controlling the temperature in the reaction kettle to rise to 30-40 ℃, stirring for 10-20 minutes at a constant temperature, wherein the stirring speed is 300r/min until the raw materials in the reaction kettle are uniformly mixed;
s3, cooling and dispersing; reducing the temperature in the reaction kettle in the S2 to room temperature, then sequentially adding a dispersing agent, a defoaming agent and an antistatic agent, and continuously stirring for 10-20 minutes at the stirring speed of 600r/min to obtain a semi-finished yarn spinning oil;
s4, regulating the pH value; adding a pH regulator and deionized water into the S3, stirring for 5-10 minutes, filtering the stirred solution, and removing filter residues to obtain a silk spinning oil;
s5, magnetizing; and (5) putting the silk spinning oil agent obtained in the step (S4) into special magnetizing equipment for magnetizing for 24 hours, then, inspecting the magnetization, inspecting whether the characteristics of the silk spinning oil agent are qualified or not, packaging the qualified silk spinning oil agent, filling and sealing with a disinfectant plastic bottle, externally packaging, then, inspecting the sealing performance of the silk spinning oil agent again, and storing qualified products in a finished product warehouse.
(III) advantageous effects
Compared with the prior art, the invention provides the high-temperature-resistant industrial silk spinning oil agent and the production process thereof, and the high-temperature-resistant industrial silk spinning oil agent has the following beneficial effects:
1. this high temperature resistant type industrial yarn spinning finish, raw materials are through having added base oil, emulsifier, bundling agent, anticoagulant, dispersant, moisture retention agent, defoaming agent, antistatic agent, PH regulator and deionized water in the preparation process, the silk finish of preparation not only has better heat resistance and wearability, and the while is little at high temperature heat volatilization, it is more excellent to compare traditional spinning finish comprehensive properties, and stability is better, more can be accepted by consumers, and the production that drops into simultaneously is low, can batch production, facilitate promotion and use.
2. The production process of the high-temperature-resistant industrial yarn spinning oil agent comprises five steps of weighing raw materials, mixing at constant temperature, cooling and dispersing, regulating pH value and magnetizing, is simple in production mode and easy to operate, can not generate pungent smell in the process of preparing the spinning oil agent, further cannot influence the health of production personnel, implements production safety protection measures, and can effectively repel iron scrap brought back after lubrication, purify lubricating oil, avoid severe cycle of greater abrasion, effectively avoid the phenomenon that the spinning oil agent is in a high-temperature environment for a long time and is oxidized to lose efficacy, blacken and thicken, and prolong the service life of the spinning oil agent.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The first embodiment is as follows:
a high-temperature-resistant industrial yarn spinning oil agent comprises the following raw materials in parts by weight: 40-parts of base oil, 8 parts of emulsifier, 2 parts of bundling agent, 2 parts of anticoagulant, 1 part of dispersant, 3 parts of moisture retention agent, 1 part of defoaming agent, 5 parts of antistatic agent, 1 part of pH regulator and 6 parts of deionized water, wherein the base oil is one or a mixture of more of dioctyl sebacate, trimethylolpropane oleate, pentaerythritol oleate, glyceryl oleate and polyethylene glycol oleate, the emulsifier is one or a mixture of more of sulfated castor oil, hydrogenated castor oil polyoxyethylene ether and polyethylene glycol oleate, the bundling agent is one or a mixture of hydrogenated castor oil polyoxyethylene ether and fatty acid triethanolamine ester, the anticoagulant is butyl hydroxy anisole, the dispersant is one or a mixture of more of silicate, triethylhexyl phosphoric acid, methylpentanol, polyacrylamide and fatty acid polyglycol ester, the moisture retention agent is one or a mixture of more of sodium tripolyphosphate, sodium hexametaphosphate, sodium hydrogen phosphate, disodium hydrogen phosphate and sodium dihydrogen phosphate, the anticoagulant is one of mineral oil, silicone oil and polyether, the antistatic agent is propylene glycol block, the pH regulator is sodium carbonate, sodium bicarbonate and sodium hydroxide, the prepared silk fibroin pyrophosphate is better than the defoamer and is more suitable for mass production.
A production process of a high-temperature-resistant industrial yarn spinning oil agent comprises the following steps: step one, weighing raw materials; weighing the base oil, the emulsifier, the bundling agent, the anticoagulant, the dispersant, the water retention agent, the defoamer, the antistatic agent, the pH regulator and the deionized water according to the raw material ratio, and weighing for later use; step two, mixing at constant temperature; adding the base oil weighed in the step one into a reaction kettle, adding an emulsifier, a bundling agent, an anticoagulant and a moisture retention agent into the reaction kettle, then controlling the temperature in the reaction kettle to rise to 30-40 ℃, stirring for 10-20 minutes at a constant temperature, wherein the stirring speed is 300r/min, and mixing the raw materials in the reaction kettle uniformly; step three, cooling and dispersing; reducing the temperature in the reaction kettle in the step two to room temperature, then sequentially adding a dispersing agent, a defoaming agent and an antistatic agent, and continuously stirring for 10-20 minutes at the stirring speed of 600r/min to obtain a semi-finished yarn spinning oil; step four, regulating the pH value; adding a pH regulator and deionized water into the third step, stirring for 5-10 minutes, filtering the stirred solution, and removing filter residues to obtain a silk spinning oil; step five, magnetization; the silk spinning oil agent obtained in the fourth step is placed into special magnetization equipment for magnetization for 24 hours, then magnetization is checked, whether the characteristics of the silk spinning oil agent are qualified or not is checked, the qualified silk spinning oil agent is packaged, encapsulated and externally packaged by a disinfectant plastic bottle, then the tightness of the silk spinning oil agent is checked again, and qualified products are stored in a finished product warehouse.
The second embodiment:
a high-temperature-resistant industrial yarn spinning oil agent comprises the following raw materials in parts by weight: 60 parts of base oil, 13 parts of emulsifier, 6 parts of bundling agent, 6 parts of anticoagulant, 2 parts of dispersant, 6 parts of moisture retention agent, 3 parts of defoaming agent, 7 parts of antistatic agent, 2 parts of pH regulator and 8 parts of deionized water, wherein the base oil is one or a mixture of more of dioctyl sebacate, trimethylolpropane oleate, pentaerythritol oleate, glyceryl oleate and polyethylene glycol oleate, the emulsifier is one or a mixture of more of sulfated castor oil, hydrogenated castor oil polyoxyethylene ether and polyethylene glycol oleate, the bundling agent is one or a mixture of hydrogenated castor oil polyoxyethylene ether and fatty acid triethanolamine ester, the anticoagulant is butyl hydroxy anisole, the dispersant is one or a mixture of more of silicate, triethylhexyl phosphoric acid, methylpentanol, polyacrylamide and fatty acid polyglycol ester, the moisture retention agent is one or a mixture of more of sodium tripolyphosphate, sodium hexametaphosphate, sodium hydrogen phosphate, disodium hydrogen phosphate and sodium dihydrogen phosphate, the defoaming agent is one of mineral oil, organosilicone of silicone oil and polyether, the antistatic agent is propylene glycol block polyether, the pH regulator is sodium carbonate, sodium bicarbonate and sodium hydroxide, the prepared silk fibroin oil has better heat resistance and better comprehensive heat resistance and can be popularized and used in batches, and is more suitable for production.
A production process of a high-temperature-resistant industrial yarn spinning oil agent comprises the following steps: step one, weighing raw materials; weighing the base oil, the emulsifier, the bundling agent, the anticoagulant, the dispersant, the water retention agent, the defoamer, the antistatic agent, the pH regulator and the deionized water according to the raw material ratio, and weighing for later use; step two, mixing at constant temperature; adding the base oil weighed in the step one into a reaction kettle, adding an emulsifier, a bundling agent, an anticoagulant and a moisture retention agent into the reaction kettle, then controlling the temperature in the reaction kettle to rise to 30-40 ℃, stirring for 10-20 minutes at a constant temperature, wherein the stirring speed is 300r/min, and mixing the raw materials in the reaction kettle uniformly; step three, cooling and dispersing; reducing the temperature in the reaction kettle in the step two to room temperature, then sequentially adding a dispersing agent, a defoaming agent and an antistatic agent, and continuously stirring for 10-20 minutes at the stirring speed of 600r/min to obtain a semi-finished yarn spinning oil; step four, adjusting the pH value; adding a pH regulator and deionized water into the step three, stirring for 5-10 minutes, filtering the stirred solution, and removing filter residues to obtain a silk spinning oil; step five, magnetization; the silk spinning oil agent obtained in the fourth step is placed into special magnetization equipment to be magnetized for 24 hours, then magnetization is checked, whether the characteristics of the silk spinning oil agent are qualified is checked, the qualified silk spinning oil agent is packaged, encapsulated and externally packaged by a disinfectant plastic bottle, the tightness of the silk spinning oil agent is checked again, qualified products are stored in a finished product warehouse, the production mode is simple, operation is easy, meanwhile, sharp smell cannot occur in the process of preparing the spinning oil agent, the body health of production personnel cannot be affected, production safety protection measures are implemented, the prepared spinning oil agent is excellent in comprehensive performance and high in high temperature resistance, and the magnetized spinning oil agent can effectively repel iron chips brought back after lubrication, so that the lubricating oil is purified, vicious circle of larger abrasion is avoided, the phenomenon that the spinning oil agent is oxidized and loses efficacy and blackened and thickened is avoided when being in a high-temperature environment for a long time, and the service life of the spinning oil agent is prolonged.
Example three:
a high-temperature-resistant industrial yarn spinning oil agent comprises the following raw materials in parts by weight: the anti-foaming agent comprises, by weight, 80 parts of base oil, 18 parts of an emulsifier, 8 parts of a bundling agent, 10 parts of an anticoagulant, 3 parts of a dispersant, 9 parts of a moisture retention agent, 5 parts of an antifoaming agent, 9 parts of an antistatic agent, 3 parts of a pH regulator and 10 parts of deionized water, wherein the base oil is one or a mixture of more of dioctyl sebacate, trimethylolpropane oleate, pentaerythritol oleate, glyceryl oleate and polyethylene glycol oleate, the emulsifier is one or a mixture of more of sulfated castor oil, hydrogenated castor oil polyoxyethylene ether and polyethylene glycol oleate, the bundling agent is one or a mixture of hydrogenated castor oil polyoxyethylene ether and fatty acid triethanolamine ester, the anticoagulant is butyl hydroxy anisole, the dispersant is one or a mixture of more of silicates, triethylhexyl phosphate, methylpentanol, polyacrylamide and fatty acid polyglycol ester, the moisture retention agent is one or a mixture of more of sodium tripolyphosphate, sodium hexametaphosphate, sodium bicarbonate, disodium hydrogen phosphate and sodium dihydrogen phosphate, the antifoaming agent is one of mineral oil, silicone oil and polyether, the antistatic agent is propylene glycol block polyether, the pH regulator is sodium carbonate, sodium bicarbonate and sodium hydroxide, the prepared silk fibroin oil has better heat resistance and better comprehensive heat resistance and can be used in batch production, and is more suitable for mass production.
A production process of a high-temperature-resistant industrial yarn spinning oil agent comprises the following steps: step one, weighing raw materials; weighing base oil, an emulsifier, a bundling agent, an anticoagulant, a dispersant, a water retention agent, a defoaming agent, an antistatic agent, a pH regulator and deionized water according to the raw material ratio, and weighing for later use; step two, mixing at constant temperature; adding the base oil weighed in the step one into a reaction kettle, adding an emulsifier, a bundling agent, an anticoagulant and a moisture retention agent into the reaction kettle, then controlling the temperature in the reaction kettle to rise to 30-40 ℃, stirring for 10-20 minutes at a constant temperature, wherein the stirring speed is 300r/min, and mixing the raw materials in the reaction kettle uniformly; step three, cooling and dispersing; reducing the temperature in the reaction kettle in the step two to room temperature, then sequentially adding a dispersing agent, a defoaming agent and an antistatic agent, and continuously stirring for 10-20 minutes at the stirring speed of 600r/min to obtain a semi-finished yarn spinning oil; step four, regulating the pH value; adding a pH regulator and deionized water into the step three, stirring for 5-10 minutes, filtering the stirred solution, and removing filter residues to obtain a silk spinning oil; step five, magnetization; the silk spinning oil agent obtained in the fourth step is placed into special magnetization equipment for magnetization for 24 hours, then magnetization is checked, whether the characteristics of the silk spinning oil agent are qualified or not is checked, the qualified silk spinning oil agent is packaged, encapsulated and externally packaged by a disinfectant plastic bottle, then the tightness of the silk spinning oil agent is checked again, and qualified products are stored in a finished product warehouse.
It can be seen from this that: according to the traditional high-temperature-resistant wear-resistant spinning oil and the preparation method thereof, nano-scale particles are easy to agglomerate in the use process of the prepared spinning oil, and the agglomerated nano-scale particles are difficult to disperse by a dispersing agent, so that the wear resistance of lubricating oil is reduced. This high temperature resistant type industrial yarn spinning finish, raw materials are through having added base oil, emulsifier, bundling agent, anticoagulant, dispersant, moisture retention agent, defoaming agent, antistatic agent, PH regulator and deionized water in the preparation process, the silk finish of preparation not only has better heat resistance and wearability, and the while is little at high temperature heat volatilization, it is more excellent to compare traditional spinning finish comprehensive properties, and stability is better, more can be accepted by consumers, and the production that drops into simultaneously is low, can batch production, facilitate promotion and use. The production process of the high-temperature-resistant industrial yarn spinning oil agent comprises five steps of weighing raw materials, mixing at constant temperature, cooling and dispersing, regulating pH value and magnetizing, is simple in production mode and easy to operate, can not generate pungent smell in the process of preparing the spinning oil agent, further cannot influence the health of production personnel, implements production safety protection measures, and the prepared spinning oil agent is excellent in comprehensive performance and high in high-temperature resistance.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims
And equivalents thereof.
Claims (10)
1. A high-temperature-resistant industrial yarn spinning oil agent is characterized in that: the material comprises the following raw materials in parts by weight: 40-80 parts of base oil, 8-18 parts of emulsifier, 2-8 parts of bundling agent, 2-10 parts of anticoagulant, 1-3 parts of dispersant, 3-9 parts of water retention agent, 1-5 parts of defoaming agent, 5-9 parts of antistatic agent, 1-3 parts of pH regulator and 6-10 parts of deionized water.
2. The high temperature resistant industrial yarn spin finish of claim 1, wherein: the base oil is one or a mixture of several of dioctyl sebacate, trimethylolpropane oleate, pentaerythritol oleate, glycerol oleate and polyethylene glycol oleate.
3. The high temperature resistant industrial yarn spin finish of claim 1, wherein: the emulsifier is one or a mixture of more of sulfated castor oil, hydrogenated castor oil polyoxyethylene ether and polyethylene glycol oleate.
4. The high temperature resistant industrial yarn spin finish of claim 1, wherein: the bundling agent is formed by mixing hydrogenated castor oil polyoxyethylene ether and fatty acid triethanolamine ester.
5. The industrial yarn spinning finish of claim 1, wherein the industrial yarn spinning finish comprises: the anticoagulant is butyl hydroxy anisole.
6. The high temperature resistant industrial yarn spin finish of claim 1, wherein: the dispersing agent is one or a mixture of more of silicates, triethylhexyl phosphoric acid, methyl amyl alcohol, polyacrylamide and fatty acid polyglycol ester.
7. The industrial yarn spinning finish of claim 1, wherein the industrial yarn spinning finish comprises: the water retention agent is one or a mixture of more of sodium tripolyphosphate, sodium hexametaphosphate, sodium pyrophosphate, disodium hydrogen phosphate and sodium dihydrogen phosphate.
8. The industrial yarn spinning finish of claim 1, wherein the industrial yarn spinning finish comprises: the antistatic agent is propylene glycol block polyether.
9. The high temperature resistant industrial yarn spin finish of claim 1, wherein: the pH regulator is one of sodium carbonate, sodium bicarbonate and sodium hydroxide.
10. A production process of a high-temperature-resistant industrial yarn spinning oil agent is characterized by comprising the following steps: the method comprises the following steps:
s1, weighing raw materials; weighing base oil, an emulsifier, a bundling agent, an anticoagulant, a dispersant, a water retention agent, a defoaming agent, an antistatic agent, a pH regulator and deionized water according to the raw material ratio, and weighing for later use;
s2, mixing at constant temperature; adding the base oil weighed in the step S1 into a reaction kettle, adding an emulsifier, a bundling agent, an anticoagulant and a moisture retention agent into the reaction kettle, then controlling the temperature in the reaction kettle to rise to 30-40 ℃, stirring for 10-20 minutes at a constant temperature, wherein the stirring speed is 300r/min until the raw materials in the reaction kettle are uniformly mixed;
s3, cooling and dispersing; reducing the temperature in the reaction kettle in the S2 to room temperature, then sequentially adding a dispersing agent, a defoaming agent and an antistatic agent, and continuously stirring for 10-20 minutes at the stirring speed of 600r/min to obtain a semi-finished yarn spinning oil;
s4, regulating the PH value; adding a pH regulator and deionized water into S3, stirring for 5-10 minutes, filtering the stirred solution, and removing filter residues to obtain a silk spinning oil;
s5, magnetizing; and (3) putting the silk spinning oil agent obtained in the step (4) into special magnetizing equipment for magnetizing for 24 hours, then, inspecting the magnetization, inspecting whether the characteristics of the silk spinning oil agent are qualified, packaging the qualified silk spinning oil agent, filling and sealing by using a disinfectant plastic bottle, carrying out external packaging, then, inspecting the sealing performance of the silk spinning oil agent again, and storing the qualified products in a finished product warehouse.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211713066.6A CN115787146A (en) | 2022-12-30 | 2022-12-30 | High-temperature-resistant industrial silk spinning oil agent and production process thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211713066.6A CN115787146A (en) | 2022-12-30 | 2022-12-30 | High-temperature-resistant industrial silk spinning oil agent and production process thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN115787146A true CN115787146A (en) | 2023-03-14 |
Family
ID=85428202
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202211713066.6A Pending CN115787146A (en) | 2022-12-30 | 2022-12-30 | High-temperature-resistant industrial silk spinning oil agent and production process thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN115787146A (en) |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN202808719U (en) * | 2012-07-02 | 2013-03-20 | 贾文亮 | Novel lubricant and additive magnetizing device |
| CN108252098A (en) * | 2017-12-18 | 2018-07-06 | 江苏新瑞贝科技股份有限公司 | A kind of polyester fiber spinning oil and preparation method thereof |
| CN111206427A (en) * | 2020-03-12 | 2020-05-29 | 金浦新材料股份有限公司 | High-temperature oil agent for polyester industrial yarn and preparation method thereof |
| CN114687212A (en) * | 2022-04-20 | 2022-07-01 | 浙江传化化学品有限公司 | High-temperature-resistant wear-resistant spinning oil and preparation method thereof |
| CN114892405A (en) * | 2022-06-29 | 2022-08-12 | 天津工大纺织助剂有限公司 | Polyester-nylon composite oiling agent for FDY spinning |
| CN115369649A (en) * | 2022-07-29 | 2022-11-22 | 桐乡市恒隆化工有限公司 | Special oil for low-oil-smoke high-speed spinning of heat-humidity comfortable polyester fiber and preparation process thereof |
-
2022
- 2022-12-30 CN CN202211713066.6A patent/CN115787146A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN202808719U (en) * | 2012-07-02 | 2013-03-20 | 贾文亮 | Novel lubricant and additive magnetizing device |
| CN108252098A (en) * | 2017-12-18 | 2018-07-06 | 江苏新瑞贝科技股份有限公司 | A kind of polyester fiber spinning oil and preparation method thereof |
| CN111206427A (en) * | 2020-03-12 | 2020-05-29 | 金浦新材料股份有限公司 | High-temperature oil agent for polyester industrial yarn and preparation method thereof |
| CN114687212A (en) * | 2022-04-20 | 2022-07-01 | 浙江传化化学品有限公司 | High-temperature-resistant wear-resistant spinning oil and preparation method thereof |
| CN114892405A (en) * | 2022-06-29 | 2022-08-12 | 天津工大纺织助剂有限公司 | Polyester-nylon composite oiling agent for FDY spinning |
| CN115369649A (en) * | 2022-07-29 | 2022-11-22 | 桐乡市恒隆化工有限公司 | Special oil for low-oil-smoke high-speed spinning of heat-humidity comfortable polyester fiber and preparation process thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101629383A (en) | Terylene FDY spinning oil and preparation method thereof | |
| CN106065527A (en) | Polyester filament FDY spinning oil and preparation method thereof | |
| CN105633404B (en) | A kind of method that modified oxidized iron prepares carbon-coated LiFePO 4 for lithium ion batteries | |
| CN111206427A (en) | High-temperature oil agent for polyester industrial yarn and preparation method thereof | |
| CN114687212B (en) | High-temperature-resistant wear-resistant spinning oil and preparation method thereof | |
| CN115787146A (en) | High-temperature-resistant industrial silk spinning oil agent and production process thereof | |
| CN106800963A (en) | A kind of water soluble oil metalworking fluid raw material and metalworking fluid | |
| CN101507000B (en) | Method of texturing silicon wafer for fabricating solar cells | |
| CN1272568A (en) | Conventional polyester spinning oil and preparation method thereof | |
| CN114532354A (en) | Antibacterial compound, antibacterial polycarbonate material, and preparation method and application thereof | |
| CN113698126A (en) | Efficient cement grinding aid and preparation method and application thereof | |
| CN113373006A (en) | Super-concentrated laundry detergent and preparation method thereof | |
| CN107994269B (en) | Lead-carbon battery with high cycle times and preparation method thereof | |
| CN112522016B (en) | Copper wire drawing agent and preparation method and application thereof | |
| CN115895756A (en) | Heterocyclic amine modified defoaming antioxidant corrosion inhibitor for wind power gear oil and preparation method thereof | |
| CN110318056A (en) | A kind of water-base metal galvanic corrosion inhibitor and preparation method | |
| CN104672896B (en) | A kind of high temperature resistant type case for circuit breaker | |
| CN103437186A (en) | Preparation method of high-speed polyester POY (Pre-Oriented Yarn) spinning oil agent | |
| CN111560278A (en) | Environment-friendly composite aluminum-based lubricating grease and preparation method thereof | |
| CN111117627A (en) | Production formula of emulsion type antioxidant | |
| CN1451728A (en) | Communication optical cable and electric cable filled factis | |
| CN112538395B (en) | Wide-range multi-soap-base self-repairing lubricating grease and preparation method thereof | |
| CN105895288B (en) | The sintering method of neodymium iron boron magnetic body | |
| CN107394281A (en) | A kind of additive package of lead storage battery electrolytic solution and preparation method thereof | |
| CN107611496A (en) | A kind of combined additive for lead accumulator and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination |