CN108252087A - A kind of ultra-fine yarn spinning oil agent and preparation method thereof - Google Patents
A kind of ultra-fine yarn spinning oil agent and preparation method thereof Download PDFInfo
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- CN108252087A CN108252087A CN201711327016.3A CN201711327016A CN108252087A CN 108252087 A CN108252087 A CN 108252087A CN 201711327016 A CN201711327016 A CN 201711327016A CN 108252087 A CN108252087 A CN 108252087A
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/005—Compositions containing perfumes; Compositions containing deodorants
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- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/144—Alcohols; Metal alcoholates
- D06M13/148—Polyalcohols, e.g. glycerol or glucose
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- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/282—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing phosphorus
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- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
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- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
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- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
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- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/18—Synthetic fibres consisting of macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
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Abstract
The invention discloses a kind of ultra-fine yarn spinning oil agent and preparation method thereof, the ultra-fine yarn spinning oil agent is made of the raw material of following parts by weight：10 20 parts of vegetable oil, 57 parts of polyglyceryl fatty acid ester, 57 parts of antistatic agent, 5 10 parts of wetting agent, 35 parts of collecting agent, 35 parts of smooth agent, 35 parts of emulsifier, 35 parts of function ingredients, 13 parts of antifoaming agent, 57 parts of sodium carbonate, 20 30 parts of deionized water.The present invention ultra-fine yarn spinning oil agent application after can assign fiber good antistatic property, reduce friction coefficient, can overcome the problems, such as finish to high speed spinning, particularly with the addition of the fibroin after Masterbatch surface flatness it is inadequate.The ultra-fine yarn spinning oil agent effect of the present invention is good, and at low cost, the holding time is long.
Description
Technical field
The invention belongs to field of fabric producing technology, specifically relate to a kind of ultra-fine yarn spinning oil agent and preparation method thereof.
Background technology
At present, since the biological degradability of conventional mineral finish is poor, containing harmful substances such as polycyclic aromatic hydrocarbons, environmental pollution is tight
Weight, therefore it is imperative to develop the environmental-friendly finish of a new generation.
Invention content
The purpose of the present invention is to provide a kind of ultra-fine yarn spinning oil agent and preparation method thereof, to solve above-mentioned background technology
The problem of middle proposition.
To achieve the above object, the present invention provides following technical solution：
A kind of ultra-fine yarn spinning oil agent, according to parts by weight, including following components：10-20 parts of vegetable oil, polyglycereol fat
5-7 parts of acid esters, 5-7 parts of antistatic agent, 5-10 parts of wetting agent, 3-5 parts of collecting agent, 3-5 parts of smooth agent, 3-5 parts of emulsifier, function
3-5 parts of component, 1-3 parts of antifoaming agent, 5-7 parts of sodium carbonate, 20-30 parts of deionized water.
Preferably, the vegetable oil is peanut oil, in soya-bean oil, linseed oil, castor oil, rape seed oil, cottonseed oil, aloe
It is one or more than one kinds of.
Preferably, the wetting agent be soybean lecithin, glycerine, Span 60, in Span 80 it is a kind of or a kind of with
On.
Preferably, the antistatic agent for lauryl alcohol polyethylene glycol oxide ester, D-sorbite, one kind in glycollic amide or
More than one.
Preferably, the antifoaming agent is one or more than one kinds of in tributyl phosphate, aqueous silicone oil.
Preferably, the collecting agent is a kind of or a kind of in Polyethylene Glycol Oleate, polyoxyethylene carboxylate
More than.
Preferably, the smooth agent is one or more than one kinds of in white oil, fatty acid polyethylene glycol ester.
Preferably, the emulsifier is paregal O, in neopelex, polysorbate40, polysorbate60, Tween 80
It is one or more than one kinds of.
Preferably, the function ingredients are folium artemisiae argyi, peppermint, keep away one or several kinds in mosquito grass, lavender, cordate telosma
One or several kinds of natural sesame oil such as natural extract or rose, jasmine, bergamot, santal.
Preferably, the preparation method of the ultra-fine yarn spinning oil agent, specific steps include：
Step 1,10-20 parts of vegetable oil, 3-5 parts of emulsifier are added in a kettle, increase temperature to 100-120 DEG C,
It 500-1000 revs/min, stirs 10-15 minutes；
Step 2,20-30 parts of deionized water, rate of addition 10-20mL/min, 500- are slowly added to by constant pressure funnel
It 1000 revs/min, stirs 30-40 minutes；
Step 3, temperature is reduced to 60-80 DEG C, adds in 5-7 parts of polyglyceryl fatty acid ester, 5-7 parts of antistatic agent, wetting agent
It 5-10 parts, 500-1000 revs/min, stirs 10-20 minutes；
Step 4, temperature is reduced to 40-60 DEG C, 3-5 parts of collecting agent of addition, 3-5 parts of smooth agent, 500-1000 revs/min,
Stirring 10-20 minutes；
Step 5,3-5 parts of function ingredients, 1-3 parts of antifoaming agent, 5-7 parts of sodium carbonate are added in, 500-1000 revs/min, is stirred
30-40 minutes；
Step 6, stirring is shut down, obtains prepared liquid super-fine yarn spinning oil agent；
Step 7, it stands and is cooled in reaction kettle liquid super-fine yarn spinning oil agent and is less than 20 DEG C, blowing encapsulation, finished product.
Compared with prior art, the beneficial effects of the invention are as follows：
1st, it can assign fiber good antistatic property after ultra-fine yarn spinning oil agent of the invention application, reduce friction system
Number, can overcome the problems, such as finish to high speed spinning, particularly with the addition of the fibroin after Masterbatch surface flatness it is inadequate.
2nd, ultra-fine yarn spinning oil agent effect of the invention is good, and at low cost, the holding time is long.
3rd, fiber can be made well to be molded after ultra-fine yarn spinning oil agent of the invention application, easily unwinds, have extremely strong
Antistatic property.
4th, ultra-fine yarn spinning oil agent of the invention has good heat resistance, the feature of environmental protection based on vegetable oil, in spinning
Smoke is few in technical process, carbonizing matter easy-clear.
5th, ultra-fine yarn spinning oil agent manufacturing process of the invention is simple to operation, and low in raw material price easily obtains, and environmental protection,
Being easy to degradation, there are no pollution to the environment.
6th, mutual compatibility, synergistic effect, collectively constituting property between various raw materials used in ultra-fine yarn spinning oil agent of the invention
The excellent product of energy.
7th, ultrafine wire has the performance of mosquito-proof antibacterial after ultra-fine yarn spinning oil agent of the invention application, has light clear
It is fragrant.
Example is embodied
The invention discloses a kind of ultra-fine yarn spinning oil agent, according to parts by weight, including following components：Vegetable oil 10-20
Part, 5-7 parts of polyglyceryl fatty acid ester, 5-7 parts of antistatic agent, 5-10 parts of wetting agent, 3-5 parts of collecting agent, 3-5 parts of smooth agent, breast
3-5 parts of agent, 3-5 parts of function ingredients, 1-3 parts of antifoaming agent, 5-7 parts of sodium carbonate, 20-30 parts of deionized water.
The present invention also provides a kind of preparation method of ultra-fine yarn spinning oil agent, specific steps include：
Step 1,10-20 parts of vegetable oil, 3-5 parts of emulsifier are added in a kettle, increase temperature to 100-120 DEG C,
It 500-1000 revs/min, stirs 10-15 minutes；
Step 2,20-30 parts of deionized water, rate of addition 10-20mL/min, 500- are slowly added to by constant pressure funnel
It 1000 revs/min, stirs 30-40 minutes；
Step 3, temperature is reduced to 60-80 DEG C, adds in 5-7 parts of polyglyceryl fatty acid ester, 5-7 parts of antistatic agent, wetting agent
It 5-10 parts, 500-1000 revs/min, stirs 10-20 minutes；
Step 4, temperature is reduced to 40-60 DEG C, 3-5 parts of collecting agent of addition, 3-5 parts of smooth agent, 500-1000 revs/min,
Stirring 10-20 minutes；
Step 5,3-5 parts of function ingredients, 1-3 parts of antifoaming agent, 5-7 parts of sodium carbonate are added in, 500-1000 revs/min, is stirred
30-40 minutes；
Step 6, stirring is shut down, obtains prepared liquid super-fine yarn spinning oil agent；
Step 7, it stands and is cooled in reaction kettle liquid super-fine yarn spinning oil agent and is less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 1
The invention discloses a kind of ultra-fine yarn spinning oil agent, according to parts by weight, including following components：10 parts of vegetable oil,
5 parts of polyglyceryl fatty acid ester, 5 parts of antistatic agent, 5 parts of wetting agent, 3 parts of collecting agent, 3 parts of smooth agent, 3 parts of emulsifier, function group
Points 3 parts, 1 part of antifoaming agent, 5 parts of sodium carbonate, 20 parts of deionized water.
The present invention also provides a kind of preparation method of ultra-fine yarn spinning oil agent, specific steps include：
Step 1,10 parts of vegetable oil, 3 parts of emulsifier are added in a kettle, increase temperature to 100 DEG C, 500 revs/min,
Stirring 15 minutes；
Step 2,20 parts of deionized water is slowly added to by constant pressure funnel, rate of addition 10mL/min, is stirred by 500 revs/min
It mixes 40 minutes；
Step 3, temperature is reduced to 60 DEG C, 5 parts of polyglyceryl fatty acid ester of addition, 5 parts of antistatic agent, 5 parts of wetting agent, 500
Rev/min, it stirs 10 minutes；
Step 4, temperature is reduced to 40 DEG C, is added in 3 parts of collecting agent, 3 parts of smooth agent, 500 revs/min, is stirred 10 minutes；
Step 5,3 parts of function ingredients, 1 part of antifoaming agent, 5 parts of sodium carbonate are added in, 500 revs/min, is stirred 30 minutes；
Step 6, stirring is shut down, obtains prepared liquid super-fine yarn spinning oil agent；
Step 7, it stands and is cooled in reaction kettle liquid super-fine yarn spinning oil agent and is less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 2
The invention discloses a kind of ultra-fine yarn spinning oil agent, according to parts by weight, including following components：15 parts of vegetable oil,
6 parts of polyglyceryl fatty acid ester, 6 parts of antistatic agent, 8 parts of wetting agent, 4 parts of collecting agent, 4 parts of smooth agent, 4 parts of emulsifier, function group
Points 4 parts, 2 parts of antifoaming agent, 6 parts of sodium carbonate, 25 parts of deionized water.
The present invention also provides a kind of preparation method of ultra-fine yarn spinning oil agent, specific steps include：
Step 1,15 parts of vegetable oil, 4 parts of emulsifier are added in a kettle, increase temperature to 110 DEG C, 800 revs/min,
Stirring 13 minutes；
Step 2,25 parts of deionized water is slowly added to by constant pressure funnel, rate of addition 15mL/min, is stirred by 800 revs/min
It mixes 35 minutes；
Step 3, temperature is reduced to 70 DEG C, 6 parts of polyglyceryl fatty acid ester of addition, 6 parts of antistatic agent, 8 parts of wetting agent, 800
Rev/min, it stirs 15 minutes；
Step 4, temperature is reduced to 50 DEG C, is added in 4 parts of collecting agent, 4 parts of smooth agent, 800 revs/min, is stirred 15 minutes；
Step 5,4 parts of function ingredients, 2 parts of antifoaming agent, 6 parts of sodium carbonate are added in, 800 revs/min, is stirred 35 minutes；
Step 6, stirring is shut down, obtains prepared liquid super-fine yarn spinning oil agent；
Step 7, it stands and is cooled in reaction kettle liquid super-fine yarn spinning oil agent and is less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 3
The invention discloses a kind of ultra-fine yarn spinning oil agent, according to parts by weight, including following components：20 parts of vegetable oil,
7 parts of polyglyceryl fatty acid ester, 7 parts of antistatic agent, 10 parts of wetting agent, 5 parts of collecting agent, 5 parts of smooth agent, 5 parts of emulsifier, function group
Points 5 parts, 3 parts of antifoaming agent, 7 parts of sodium carbonate, 30 parts of deionized water.
The present invention also provides a kind of preparation method of ultra-fine yarn spinning oil agent, specific steps include：
Step 1,20 parts of vegetable oil, 5 parts of emulsifier are added in a kettle, increase temperature to 120 DEG C, 1000 revs/min,
Stirring 15 minutes；
Step 2,30 parts of deionized water is slowly added to by constant pressure funnel, rate of addition 20mL/min, 1000 revs/min,
Stirring 30 minutes；
Step 3, temperature is reduced to 80 DEG C, adds in 7 parts of polyglyceryl fatty acid ester, 7 parts of antistatic agent, 10 parts of wetting agent,
It 1000 revs/min, stirs 20 minutes；
Step 4, temperature is reduced to 60 DEG C, is added in 5 parts of collecting agent, 5 parts of smooth agent, 1000 revs/min, is stirred 20 minutes；
Step 5,5 parts of function ingredients, 3 parts of antifoaming agent, 7 parts of sodium carbonate are added in, 1000 revs/min, is stirred 40 minutes；
Step 6, stirring is shut down, obtains prepared liquid super-fine yarn spinning oil agent；
Step 7, it stands and is cooled in reaction kettle liquid super-fine yarn spinning oil agent and is less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 4
The invention discloses a kind of ultra-fine yarn spinning oil agent, according to parts by weight, including following components：20 parts of vegetable oil,
5 parts of polyglyceryl fatty acid ester, 6 parts of antistatic agent, 8 parts of wetting agent, 4 parts of collecting agent, 4 parts of smooth agent, 5 parts of emulsifier, function group
Points 4 parts, 2 parts of antifoaming agent, 7 parts of sodium carbonate, 20 parts of deionized water.
The present invention also provides a kind of preparation method of ultra-fine yarn spinning oil agent, specific steps include：
Step 1,20 parts of vegetable oil, 5 parts of emulsifier are added in a kettle, increase temperature to 100 DEG C, 1000 revs/min,
Stirring 15 minutes；
Step 2,20 parts of deionized water is slowly added to by constant pressure funnel, rate of addition 20mL/min, 1000 revs/min,
Stirring 30 minutes；
Step 3, temperature is reduced to 70 DEG C, 5 parts of polyglyceryl fatty acid ester of addition, 6 parts of antistatic agent, 8 parts of wetting agent, 800
Rev/min, it stirs 10 minutes；
Step 4, temperature is reduced to 40 DEG C, is added in 4 parts of collecting agent, 4 parts of smooth agent, 800 revs/min, is stirred 20 minutes；
Step 5,4 parts of function ingredients, 2 parts of antifoaming agent, 7 parts of sodium carbonate are added in, 900 revs/min, is stirred 30 minutes；
Step 6, stirring is shut down, obtains prepared liquid super-fine yarn spinning oil agent；
Step 7, it stands and is cooled in reaction kettle liquid super-fine yarn spinning oil agent and is less than 20 DEG C, blowing encapsulation, finished product.
The above-mentioned various embodiments enumerated, under the premise of reconcilable, can be combined with each other implementation, those skilled in the art
It can combine above to the explanation of embodiment, as the foundation being combined to the technical characteristic in different embodiments.
Test case
Acrylic fiber is handled using the ultra-fine yarn spinning oil agent of embodiment 1,2,3,4, test result is as follows：
| Embodiment | Smoke amount (%) | Waste silk rate (%) | Spinnability |
| It is untreated | It is more | 10.1 | There is broken end |
| 1 | It is few | 5 | Well |
| 2 | Seldom | 3.5 | Well |
| 3 | Almost without | 2.5 | Well |
| 4 | Seldom | 3.2 | Well |
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace
And modification, the scope of the present invention is defined by the appended.
Claims (10)
1. a kind of ultra-fine yarn spinning oil agent, it is characterised in that：The ultra-fine yarn spinning oil agent includes the raw material of following parts by weight：
It is 10-20 parts of vegetable oil, 5-7 parts of polyglyceryl fatty acid ester, 5-7 parts of antistatic agent, 5-10 parts of wetting agent, 3-5 parts of collecting agent, smooth
3-5 parts of agent, 3-5 parts of emulsifier, 3-5 parts of function ingredients, 1-3 parts of antifoaming agent, 5-7 parts of sodium carbonate, 20-30 parts of deionized water.
2. ultra-fine yarn spinning oil agent according to claim 1, it is characterised in that：The vegetable oil for peanut oil, soya-bean oil,
It is one or more than one kinds of in linseed oil, castor oil, rape seed oil, cottonseed oil, aloe.
3. ultra-fine yarn spinning oil agent according to claim 1, it is characterised in that：The wetting agent for soybean lecithin,
It is one or more than one kinds of in glycerine, Span 60, Span 80.
4. ultra-fine yarn spinning oil agent according to claim 1, it is characterised in that：The antistatic agent is laruyl alcohol polyoxy
It is one or more than one kinds of in vinyl acetate, D-sorbite, glycollic amide.
5. ultra-fine yarn spinning oil agent according to claim 1, it is characterised in that：The antifoaming agent for tributyl phosphate,
It is one or more than one kinds of in aqueous silicone oil.
6. ultra-fine yarn spinning oil agent according to claim 1, it is characterised in that：The collecting agent is oleic acid polyethylene glycol
It is one or more than one kinds of in ester, polyoxyethylene carboxylate.
7. ultra-fine yarn spinning oil agent according to claim 1, it is characterised in that：The smooth agent is white oil, aliphatic acid
It is one or more than one kinds of in macrogol ester.
8. ultra-fine yarn spinning oil agent according to claim 1, it is characterised in that：The emulsifier is paregal O, 12
It is one or more than one kinds of in sodium alkyl benzene sulfonate, polysorbate40, polysorbate60, Tween 80.
9. ultra-fine yarn spinning oil agent according to claim 1, it is characterised in that：The function ingredients for folium artemisiae argyi, peppermint,
Keep away one or several kinds of natural extracts or rose, jasmine, bergamot, santal in mosquito grass, lavender, cordate telosma etc.
One or several kinds of natural sesame oil.
10. a kind of preparation method using any one of the claims 1-9 ultra-fine yarn spinning oil agents, feature exists
In：Specific steps include：
Step 1,10-20 part of vegetable oil, 3-5 parts of emulsifier are added in a kettle, increase temperature to 100-120 DEG C, 500-
It 1000 revs/min, stirs 10-15 minutes；
Step 2,20-30 parts of deionized water being slowly added to by constant pressure funnel, rate of addition 10-20mL/min, 500-1000 turn/
Minute, it stirs 30-40 minutes；
Step 3, temperature is reduced to 60-80 DEG C, adds in 5-7 parts of polyglyceryl fatty acid ester, 5-7 parts of antistatic agent, wetting agent 5-10
Part, it 500-1000 revs/min, stirs 10-20 minutes；
Step 4, temperature is reduced to 40-60 DEG C, is added in 3-5 parts of collecting agent, 3-5 parts of smooth agent, 500-1000 revs/min, is stirred
10-20 minutes；
Step 5,3-5 parts of function ingredients, 1-3 parts of antifoaming agent, 5-7 parts of sodium carbonate are added in, 500-1000 revs/min, stirs 30-40
Minute；
Step 6, stirring is shut down, obtains prepared liquid super-fine yarn spinning oil agent；
Step 7, it stands and is cooled in reaction kettle liquid super-fine yarn spinning oil agent and is less than 20 DEG C, blowing encapsulation, finished product.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108998979A (en) * | 2018-07-27 | 2018-12-14 | 南通凯大纺织有限公司 | A kind of preparation method of terylene spinning finish |
| CN112281261A (en) * | 2020-09-15 | 2021-01-29 | 如皋市雨润纤维科技有限公司 | High-speed spinning oil with high permeability and preparation process thereof |
| CN114351450A (en) * | 2022-01-13 | 2022-04-15 | 沈阳浩博实业有限公司 | Oil agent for semi-continuous spinning viscose filament yarn and preparation method and application thereof |
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| CN112281261A (en) * | 2020-09-15 | 2021-01-29 | 如皋市雨润纤维科技有限公司 | High-speed spinning oil with high permeability and preparation process thereof |
| CN114351450A (en) * | 2022-01-13 | 2022-04-15 | 沈阳浩博实业有限公司 | Oil agent for semi-continuous spinning viscose filament yarn and preparation method and application thereof |
| CN115896982A (en) * | 2022-11-21 | 2023-04-04 | 上海丰泽源科技有限公司 | Preparation process of environment-friendly spinning oil |
| CN115896982B (en) * | 2022-11-21 | 2024-06-14 | 上海丰泽源科技有限公司 | Environment-friendly spinning oil preparation process |
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Application publication date: 20180706 |