CN106939514A - A kind of terylene FDY spinning oil - Google Patents
A kind of terylene FDY spinning oil Download PDFInfo
- Publication number
- CN106939514A CN106939514A CN201710279964.8A CN201710279964A CN106939514A CN 106939514 A CN106939514 A CN 106939514A CN 201710279964 A CN201710279964 A CN 201710279964A CN 106939514 A CN106939514 A CN 106939514A
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- Prior art keywords
- agent
- spinning oil
- fdy spinning
- smooth
- acid
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/02—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with hydrocarbons
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/282—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing phosphorus
- D06M13/292—Mono-, di- or triesters of phosphoric or phosphorous acids; Salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Artificial Filaments (AREA)
Abstract
The present invention provides a kind of terylene FDY spinning oil, is made up of components such as smooth agent, emulsifying agent, collecting agent, antistatic additive.The percentage by weight of each component is：Smooth agent 55~65%, emulsifying agent 15~25%, collecting agent 10~20%, antistatic additive 2~10%.Terylene FDY spinning oil of the present invention is used for during polyester FDY spinning processing and post-processing, and good spinnability, hot property is excellent, can meet every technical requirements of polyester FDY spinning technique, effectively improves polyester FDY fiber product quality.
Description
Technical field
The present invention relates to a kind of terylene FDY spinning oil, during polyester FDY spinning processing and post-processing, belong to
Spinning oil manufacture field in synthetic fibers process technology.
Background technology
In polyester FDY fibre spinning production process, in order that fiber has appropriate flatness, convergence and antistatic
Property, it is necessary to a kind of spinning oil is added, frictional coefficient of fiber is reduced, eliminated because of the electrostatic that friction is produced, so that fiber has
Good spinnability and aft-loaded airfoil performance.
With the continuous improvement of spining technology, process velocity is more and more faster, processing temperature also more and more higher, and this is to spinning oil
The heat endurance of agent proposes higher requirement.Both required that finish volatilized in use few, dirt had not been caused to workshop condition
Dye, requires finish in macrocyclic running, coking is few on drawing-off hot-rolling, easy to clean again.
The content of the invention
It is stable it is an object of the invention to provide a kind of hot property in order to solve above-mentioned finish temperature resistance problem, smog knot
Jiao is few, the terylene FDY spinning oil of good spinning property.
To achieve these goals, technical scheme is as follows：A kind of terylene FDY spinning oil, comprising smooth agent,
Emulsifying agent, collecting agent, antistatic additive, the percentage by weight of each component is：Smooth agent 55~65%, emulsifying agent 15~25%, collection
Beam agent 10~20%, antistatic additive 2~10%.
Preferably, smooth agent 58~62%, emulsifying agent 18~23%, collecting agent 12~18%, antistatic additive 3~8%.
Preferably, smooth agent is using mineral oil, decanedioic acid -2- Octyl Nitrites, di-n-octyl sebacate, trimethylolpropane oil
Acid esters, pentadiol coconut oleate, one kind in thio-2 acid polyethenoxy ether (n) laurate or any several mixing
At least need to include thio-2 acid polyethenoxy ether (n) laurate in thing, and the smooth agent.
Preferably, thio-2 acid polyethenoxy ether (n) laurate weight shared in whole terylene FDY spinning oil
Measure percentage and be not less than 10%.
Smooth agent effect is regulation frictional coefficient of fiber, increases film strength, protects fiber surface, it is to avoid fiber is adding
Sustained damage during work.Wherein thio-2 acid polyethenoxy ether (n) laurate volatilization is few, and coking is few, with anti-oxidant
Function, can prevent or reduce the oxidation cross-linked or decomposition of other compounds at high temperature, improve the heat endurance of finish.
Preferably, emulsifying agent is used in AEO, aliphatic acid polyethenoxy ether, castor oil polyoxyethylene ether
One kind or any several mixtures.
The effect of emulsifying agent is that each component in finish is reached into balance by physical and chemical process, make finish when in use into
For uniform, stable oily liquids.
Preferably, collecting agent uses polyethylene glycol Glycol Oleic Acid Ester, polyethylene glycol bay acid diester, aliphatic acid polyethenoxy
One kind or any several mixtures in ether, castor oil polyoxyethylene ether.
The effect of collecting agent is the cluster performance for improving fiber, makes fiber not fluffy in process, not at random, processing
During uniform force, silk is simultaneously molded good.
Preferably, antistatic additive uses C10~C18 aliphatic alcohol polyoxyvinethene phosphates sylvite, C10~C18 fatty alcohols
One kind or any several mixtures in phosphate kalium salt.
The effect of antistatic additive is the hygroscopicity and electric conductivity for improving fiber, suppresses the generation of electrostatic, the product of minimizing electrostatic
It is tired, prevent broken end, the generation of lousiness.
Stable it is an object of the invention to provide a kind of hot property, smog coking is few, the polyester FDY spinning of good spinning property
The manufacture method of finish.
To achieve these goals, technical scheme is as follows：A kind of manufacture method of terylene FDY spinning oil,
It is characterized in that the manufacture method comprises the following steps：By each component percentage by weight, wherein smooth agent 55~65%, emulsification
Emulsifying agent, collecting agent, antistatic additive are first added and allocated by agent 15~25%, collecting agent 10~20%, antistatic additive 2~10%
Kettle, is warming up to 40~60 DEG C and stirs, then smooth agent is added into compounding kettle, continues to stir 30~60 minutes, cool down, filter,
The barrelling that discharges is that can obtain the excellent terylene FDY spinning oil of hot property.
The technical characterstic of the present invention：The terylene FDY spinning oil of the present invention is used in polyester FDY spinning production, broken end, hair
Silk is few, and cluster performance is good, and coiling and molding is good.Finish hot property is excellent, and no obvious smoke, hot-rolling coking is few, good spinning property,
Fiber quality is significantly improved.
Embodiment
【Embodiment 1】
The percentage by weight of the present embodiment each component is：(a) smooth agent：Mineral oil 20%, di-n-octyl sebacate 20%, sulphur
For dipropionic acid polyethenoxy ether (10) laurate 20%；(b) emulsifying agent：AEO (7) 10%, castor oil gathers
Oxygen vinethene (20) 10%；(c) collecting agent：Polyethylene glycol Glycol Oleic Acid Ester 5%, castor oil polyoxyethylene ether (30) 10% (d) resists
Electrostatic agent：C18 AEOs (5) phosphate kalium salt 5%.
Preparation method：By each component percentage by weight, emulsifying agent, collecting agent, antistatic additive are accurately measured, under stirring successively
Compounding kettle is added, 40~60 DEG C is warming up to and stirs, then smooth agent is added, continues to stir 30~60 minutes, cooling, mistake
Filter, discharging barrelling are that can obtain the excellent terylene FDY spinning oil of hot property.
【Embodiment 2】
The percentage by weight of the present embodiment each component is：(a) smooth agent：Mineral oil 15%, tricarboxymethyl propane oleate
30%, thio-2 acid polyethenoxy ether (7) laurate 13%；(b) emulsifying agent：AEO (7) 10%, castor
Sesame oil APEO (20) 12%；(c) collecting agent：Polyethylene glycol bay acid diester 8%, castor oil polyoxyethylene ether (30)
9% (d) antistatic additive：C12 fatty alcohol phosphates sylvite 3%.
Preparation method：By each component percentage by weight, emulsifying agent, collecting agent, antistatic additive are accurately measured, under stirring successively
Compounding kettle is added, 40~60 DEG C is warming up to and stirs, then smooth agent is added, continues to stir 30~60 minutes, cooling, mistake
Filter, discharging barrelling are that can obtain the excellent terylene FDY spinning oil of hot property.
【Comparative example 1】
The percentage by weight of the present embodiment each component is：(a) smooth agent：Mineral oil 30%, di-n-octyl sebacate 30%；
(b) emulsifying agent：AEO (7) 10%, castor oil polyoxyethylene ether (20) 12%；(c) collecting agent：Polyethylene glycol
Glycol Oleic Acid Ester 5%, castor oil polyoxyethylene ether (30) 9% (d) antistatic additive：C18 AEOs (5) phosphate potassium
Salt 4%.
Preparation method：By each component percentage by weight, emulsifying agent, collecting agent, antistatic additive are accurately measured, under stirring successively
Compounding kettle is added, 40~60 DEG C is warming up to and stirs, then smooth agent is added, continues to stir 30~60 minutes, cooling, mistake
Filter, discharging barrelling are that can obtain ordinary polyester FDY spinning oils.
Oil performance is tested：Embodiment 1, embodiment 2 and comparative example 1 are subjected to oil performance test evaluation, as a result such as table 1
It is shown.
The test evaluation result of table 1.
Note：Lousiness, break situations, with during spin-drawing lousiness occur number and end breakage rate height, with ◎ it is excellent,
◎-zero is between excellent and good, zero good, zero-△ between good and slightly worse, △ is slightly worse, △-× between it is slightly worse between difference,
× poor, totally seven grades are represented
Can be seen that finish of the present invention (embodiment 1, embodiment 2) from the test evaluation result of table 1 has good heat steady
Qualitative energy, smoke, coking are few, and site environment is improved, lousiness, little breakage in spinning production process, and processing is good by property,
Spinnability is excellent.
Claims (8)
1. a kind of terylene FDY spinning oil, it is characterised in that：By the component group such as smooth agent, emulsifying agent, collecting agent, antistatic additive
Into.
2. the percentage by weight of each component is：Smooth agent 55~65%, emulsifying agent 15~25%, collecting agent 10~20% is antistatic
Agent 2~10%.
3. terylene FDY spinning oil according to claim 1, the preferential percentage by weight of each component：Smooth agent 58~
62%, emulsifying agent 18~23%, collecting agent 12~18%, antistatic additive 3~8%.
4. terylene FDY spinning oil according to claim 1 or 2, it is characterised in that：Smooth agent uses mineral oil, the last of the ten Heavenly stems two
Acid -2- Octyl Nitrites, di-n-octyl sebacate, tricarboxymethyl propane oleate, pentadiol coconut oleate, thio-2 acid gather
Oxypropylene ether（n）One or more of mixtures in laurate, and at least needed in the smooth agent poly- comprising thio-2 acid
Oxypropylene ether（n）Laurate.
5. terylene FDY spinning oil according to claim 1 or 2, it is characterised in that：Emulsifying agent uses fatty alcohol polyoxy second
One or more of mixtures in alkene ether, aliphatic acid polyethenoxy ether, castor oil polyoxyethylene ether.
6. terylene FDY spinning oil according to claim 1 or 2, it is characterised in that：Collecting agent uses polyethylene glycol oleic acid
One or more of mixing in dibasic acid esters, polyethylene glycol bay acid diester, aliphatic acid polyethenoxy ether, castor oil polyoxyethylene ether
Thing.
7. terylene FDY spinning oil according to claim 1 or 2, it is characterised in that：Antistatic additive uses C10~C18 fat
One or more of mixtures in fat alcohol polyoxyethylene ether phosphate sylvite, C10~C18 fatty alcohol phosphate sylvite.
8. terylene FDY spinning oil according to claim 1 or 2, its manufacturing step is：By each component percentage by weight,
The components such as emulsifying agent, collecting agent, antistatic additive are first added into compounding kettle, 40~60 DEG C is warming up to and stirs, then by smooth agent
Compounding kettle is added, continues to stir 30~60 minutes, cooling, filtering, discharging barrelling are that can obtain the excellent polyester FDY of hot property to spin
Silk oiling agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710279964.8A CN106939514A (en) | 2017-04-25 | 2017-04-25 | A kind of terylene FDY spinning oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710279964.8A CN106939514A (en) | 2017-04-25 | 2017-04-25 | A kind of terylene FDY spinning oil |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106939514A true CN106939514A (en) | 2017-07-11 |
Family
ID=59463810
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710279964.8A Pending CN106939514A (en) | 2017-04-25 | 2017-04-25 | A kind of terylene FDY spinning oil |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109281176A (en) * | 2018-09-07 | 2019-01-29 | 浙江新胜油脂科技有限公司 | A kind of extrusion spinning finish |
| CN109763335A (en) * | 2019-01-12 | 2019-05-17 | 厦门东纶股份有限公司 | A kind of nylon spinning oil and preparation method thereof |
| CN110629546A (en) * | 2019-10-31 | 2019-12-31 | 如皋市雨润纤维科技有限公司 | Green and environment-friendly oil agent for tencel fiber weaving and preparation method thereof |
| CN111074552A (en) * | 2019-11-30 | 2020-04-28 | 江苏双江能源科技股份有限公司 | Environment-friendly antioxidant polyester DTY oil agent and preparation method thereof |
| CN111206427A (en) * | 2020-03-12 | 2020-05-29 | 金浦新材料股份有限公司 | High-temperature oil agent for polyester industrial yarn and preparation method thereof |
| CN111576046A (en) * | 2020-04-23 | 2020-08-25 | 桐乡市恒隆化工有限公司 | Oil agent for spinning and stretching one-step method of crude oil oiling and preparation method thereof |
| CN111851073A (en) * | 2020-07-14 | 2020-10-30 | 科凯精细化工（上海）有限公司 | Antistatic spinning oil and preparation method thereof |
| CN112647284A (en) * | 2020-12-17 | 2021-04-13 | 太仓旭云特种纤维科技有限公司 | PBO fiber carding oil |
| CN115045010A (en) * | 2022-06-28 | 2022-09-13 | 义乌华鼎锦纶股份有限公司 | Environment-friendly anti-yellowing oil agent for porous fine denier polyamide DTY |
| CN115404571A (en) * | 2022-09-29 | 2022-11-29 | 安徽皖维高新材料股份有限公司 | Oil agent for preparing PVA fiber through wet boron-containing cross-linked spinning |
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| CN106065527A (en) * | 2016-07-08 | 2016-11-02 | 苏州夏尔植物油脂科技有限公司 | Polyester filament FDY spinning oil and preparation method thereof |
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109281176A (en) * | 2018-09-07 | 2019-01-29 | 浙江新胜油脂科技有限公司 | A kind of extrusion spinning finish |
| CN109763335A (en) * | 2019-01-12 | 2019-05-17 | 厦门东纶股份有限公司 | A kind of nylon spinning oil and preparation method thereof |
| CN109763335B (en) * | 2019-01-12 | 2021-03-02 | 厦门东纶股份有限公司 | Nylon spinning oil and preparation method thereof |
| CN110629546A (en) * | 2019-10-31 | 2019-12-31 | 如皋市雨润纤维科技有限公司 | Green and environment-friendly oil agent for tencel fiber weaving and preparation method thereof |
| CN111074552A (en) * | 2019-11-30 | 2020-04-28 | 江苏双江能源科技股份有限公司 | Environment-friendly antioxidant polyester DTY oil agent and preparation method thereof |
| CN111206427A (en) * | 2020-03-12 | 2020-05-29 | 金浦新材料股份有限公司 | High-temperature oil agent for polyester industrial yarn and preparation method thereof |
| CN111576046A (en) * | 2020-04-23 | 2020-08-25 | 桐乡市恒隆化工有限公司 | Oil agent for spinning and stretching one-step method of crude oil oiling and preparation method thereof |
| CN111851073A (en) * | 2020-07-14 | 2020-10-30 | 科凯精细化工（上海）有限公司 | Antistatic spinning oil and preparation method thereof |
| CN112647284A (en) * | 2020-12-17 | 2021-04-13 | 太仓旭云特种纤维科技有限公司 | PBO fiber carding oil |
| CN115045010A (en) * | 2022-06-28 | 2022-09-13 | 义乌华鼎锦纶股份有限公司 | Environment-friendly anti-yellowing oil agent for porous fine denier polyamide DTY |
| CN115404571A (en) * | 2022-09-29 | 2022-11-29 | 安徽皖维高新材料股份有限公司 | Oil agent for preparing PVA fiber through wet boron-containing cross-linked spinning |
| CN115404571B (en) * | 2022-09-29 | 2023-12-01 | 安徽皖维高新材料股份有限公司 | Oiling agent for preparing PVA fibers through wet boron-containing crosslinking spinning |
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Application publication date: 20170711 |