CN106214579A - A kind of noni ferment Whitening sunscreen cream and preparation method thereof - Google Patents

A kind of noni ferment Whitening sunscreen cream and preparation method thereof Download PDF

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CN106214579A
CN106214579A CN201610777641.7A CN201610777641A CN106214579A CN 106214579 A CN106214579 A CN 106214579A CN 201610777641 A CN201610777641 A CN 201610777641A CN 106214579 A CN106214579 A CN 106214579A
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noni
phase
noni ferment
sunscreen cream
ferment
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CN106214579B (en
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郑超
杨平顺
纪明慧
周学明
钟婉淇
秦伟
陈光英
宋小平
郑彩娟
那日松
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Shenzhen Rongda Biotechnology Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/342Alcohols having more than seven atoms in an unbroken chain
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • A61K8/375Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4946Imidazoles or their condensed derivatives, e.g. benzimidazoles
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/63Steroids; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/891Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/04Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/74Biological properties of particular ingredients
    • A61K2800/78Enzyme modulators, e.g. Enzyme agonists
    • A61K2800/782Enzyme inhibitors; Enzyme antagonists
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/85Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine

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Abstract

The present invention proposes a kind of noni ferment Whitening sunscreen cream and preparation method thereof, count by weight percentage, its formula composition includes: tristerin, 16/18 natural fatty alcohols, caprylic/capric triglyceride, isononyl isononanoate, Jojoba oil, polydimethylsiloxane, sterol ester, vitamin E, methyl hydroxybenzoate, propylparaben, glycerol, amino acid humectant, allantoin, lauryl alcohol, noni ferment and deionized water.The noni ferment Whitening sunscreen cream that the present invention proposes has significant radical scavenging activity, effectively the growth of suppression melanin, and effective to ultra-violet absorption, it is achieved the effect of whitening sun protection skin protection, its preparation method is simple to operation, and production cost is relatively low.

Description

A kind of noni ferment Whitening sunscreen cream and preparation method thereof
Technical field
The present invention relates to cosmetic technical field, particularly to a kind of noni ferment Whitening sunscreen cream and preparation method thereof.
Background technology
Cosmetics on Cosmetic Market all contain essence, preservative, antibacterial at present.Consumer is similar at life-time service After product, skin, it is possible that anaphylaxis, even induces other diseases.Accordingly, it would be desirable to a kind of cosmetics, not only have good Good using effect, and not there is side effect, healthy without compromising on consumer.Affect human skin healthy because of In element, two maximum killers are melanin and aging, and wherein whitening cosmetics market is the most active, sales volume Quickly increase.
Noni (Noni), has another name called Morinda Citifolia, Morinda citrifolia Linn., Solanum pseudo-capsicumvar diflorum (Vell.)Bitter etc., genus rubia section Morinda plant.This plant master The South Sea Islands to be distributed in small island, such as Philippine, Australia etc..Existing China is mainly distributed on the heat such as Hainan, the Xisha Islands Band area, has been carried out planting on a large scale.Noni has stronger functional character, and root, stem, leaf, flower and fruit all can be used as medicine. Root can obtain the dyestuff of yellow or redness for contaminating clothes, and edible fruit use, as food stage health product.Noni is as a kind of generation Boundary medicinal plants new lover, has caused food, the extensive concern of medicine researcher, therefrom the most about 200 compounds of isolation identification, main The composition of the compositions such as anthraquinone to be comprised, flavone, coumarin, glucosides, triterpenes, its Middle East scopola booth, rutin, maloic acid, tannin Card is considered as the effective active composition in noni.In addition noni is rich in unsaturated fatty acid, vitamin, mineral, antioxidation Agent, rare element and celo are the most former, the peaceful invertase of celo etc..At present the bioactivity research to noni focus primarily upon antibacterial, Prophylaxis of tumours, removing free radical and antioxidation and other functional characteristics.Due to the functional characteristic that noni is unique, be the whole world One of health-oriented products salable, the demand of noni is increased by existing market with the speed of annual 50%, and government is also strengthening promise Beautiful exploitation and development.Flavone compound and phenolic compound all have inhibitory action to tryrosinase according to the literature, can press down Melanin processed increases.In we study, find Noni fruit fermentation liquid exists many phenolic compounds.
Summary of the invention
Mirror, with this, it is an object of the invention to propose a kind of noni ferment Whitening sunscreen cream and preparation method thereof, it is intended to solve Certainly there is certain side effect in existing Whitening sunscreen cream, stimulates skin to cause allergy, the problem of whitening sun protection poor effect.
The technical scheme is that and be achieved in that:
A kind of noni ferment Whitening sunscreen cream, count by weight percentage, its formula composition includes: tristerin 1 ~1.5%, 16/18 natural fatty alcohol 0.5~1%, caprylic/capric triglyceride 2~3%, isononyl isononanoate 3~ 5%, Jojoba oil 1~1.2%, polydimethylsiloxane 0.5~1%, sterol ester 0.8~1%, vitamin E 0.5~1%, Methyl hydroxybenzoate 0.1~0.2%, propylparaben 0.1~0.2%, glycerol 3~5%, amino acid humectant 2~3%, allantois Element 0.1~0.3%, lauryl alcohol 0.8~1% and noni ferment 0.2~0.3%, surplus is deionized water.
Further, count by weight percentage, its formula composition includes: tristerin 3%, 16/18 days So fatty alcohol 2.5%, caprylic/capric triglyceride 6%, isononyl isononanoate 8%, Jojoba oil 1.8%, polydimethylsiloxanes Alkane 2.5%, sterol ester 1.6%, vitamin E 2.5%, methyl hydroxybenzoate 0.5%, propylparaben 0.5%, glycerol 10%, ammonia Base acid wetting agent 4.5%, allantoin 0.1%, lauryl alcohol 1.6% and noni ferment 0.6%, surplus is deionized water.
Further, described noni ferment is prepared by following steps:
Take the chopping of fresh Noni fruit, add distilled water and sucrose, mixing, through high-pressure sterilizing pot sterilizing, after cooling, add ferment Female bacterium, standing for fermentation, it is filtrated to get fermentation liquid and is noni ferment.
Further, in the preparation process of described noni ferment, the adding proportion of Noni fruit, distilled water and sucrose is: every 100g Noni fruit adds 100mL distilled water and 4g sucrose.
Further, in the preparation process of described noni ferment, fermentation time is 30~40 days.
The preparation method of a kind of noni ferment Whitening sunscreen cream, comprises the steps:
S1, taking A phase and B phase respectively, heated and stirred to 80~90 DEG C is in homogeneously;
S2, when A phase and B phase temperature difference are not more than 5 DEG C, continuously stirred while, slowly by A phase oil solution add B Phase aqueous solution is thoroughly mixed to biphase, starts homogenizer, it is thus achieved that stable and glossiness emulsion;
S3, when emulsion temperature is down to 60~70 DEG C, add C phase, again start homogenizer until emulsion mix homogeneously, treat Temperature is down to when 40~45 DEG C add D phase, and continuously stirred emulsion is down to room temperature, closes agitator, stands 5~12h, to obtain final product;
Wherein, A phase includes tristerin, 16/18 natural fatty alcohols, caprylic/capric triglyceride, different n-nonanoic acid Different nonyl ester, Jojoba oil, polydimethylsiloxane, sterol ester, vitamin E, methyl hydroxybenzoate and propylparaben;B phase includes Glycerol, amino acid humectant, allantoin and deionized water;C phase includes lauryl alcohol;D phase includes noni ferment.
Compared with prior art, the invention have the benefit that
The noni ferment Whitening sunscreen cream that the present invention proposes has significant radical scavenging activity, effectively suppresses tyrosine The activity of enzyme, suppression melanin growth, effective to ultra-violet absorption, it is achieved the effect of whitening sun protection skin protection, its preparation method Simple to operation, production cost is relatively low.It addition, the noni ferment Whitening sunscreen cream that the present invention proposes may be directly applied to skin protection U.S. In vain, it is also possible to be applied to prepare other skin-lightening cosmetics or skin care item product.
Detailed description of the invention
For the technical scheme in the present invention is clearly and completely described, it is clear that inventor says in conjunction with the embodiments Bright, but the only a part of embodiment of the present invention rather than the whole embodiments described by following example.Based on the present invention In embodiment, the every other enforcement that those of ordinary skill in the art are obtained under not making creative work premise Example, broadly falls into the scope of protection of the invention.
Embodiment 1
A kind of noni ferment Whitening sunscreen cream, its formula composition is as shown in table 1:
Table 1
Embodiment 2
A kind of noni ferment Whitening sunscreen cream, its formula composition is as shown in table 2:
Table 2
Embodiment 3
A kind of noni ferment Whitening sunscreen cream, its formula composition is as shown in table 3:
Table 3
Embodiment 4
A kind of noni ferment Whitening sunscreen cream, its formula composition is as shown in table 4:
Table 4
Embodiment 5
A kind of noni ferment Whitening sunscreen cream, its formula composition is as shown in table 5:
Table 5
Embodiment 6
A kind of noni ferment Whitening sunscreen cream, its formula composition is as shown in table 6:
Table 6
Embodiment 7
A kind of noni ferment Whitening sunscreen cream, its formula composition is as shown in table 7:
Table 7
Embodiment 8
A kind of noni ferment Whitening sunscreen cream, its formula composition is as shown in table 8:
Table 8
Noni ferment in above-mentioned Whitening sunscreen cream is prepared by following steps:
The fresh Noni fruit chopping taking 500g is positioned over clean 2L wide mouthed bottle, adds 500mL distilled water and 20g sucrose, Mixing, through high-pressure sterilizing pot sterilizing, adds yeast, room temperature standing for fermentation 30~40 days, is filtrated to get fermentation liquid i.e. after cooling For noni ferment.Wherein, the adding proportion of Noni fruit, distilled water and sucrose is, every 100g Noni fruit add 100mL distilled water and 4g sucrose, sucrose, as the nutrient of yeast, provides the energy for sweat, and under the conditions of this adding proportion, ferment effect is preferable.
The preparation method of the noni ferment Whitening sunscreen cream that the present invention proposes, comprises the steps:
S1, take the 150mL beaker after two sterilizing-dryings, be separately added into A phase and B phase, heated and stirred to 80~90 DEG C in Homogeneously.
S2, aqueous solution (i.e. B phase) temperature more slightly higher than oil solution (i.e. A phase), when biphase temperature difference is not more than 5 DEG C Time, continuously stirred while, slowly A phase oil solution is added in B phase aqueous solution and is thoroughly mixed to the most biphase, start homogenizer, obtain Must stablize and glossiness emulsion.
S3, when emulsion temperature is down to 60~70 DEG C, add C phase, again start homogenizer until after emulsion mix homogeneously, Adding D when its temperature is down to 40~45 DEG C, continuously stirred emulsion is down to room temperature, closes agitator, stands 5~12h, after bottling Sunscreen cream.
The active testing of suppression tryrosinase
Containing tryrosinase in Rhizoma Solani tuber osi extracting solution, tryrosinase is a kind of oxidoreductase, and tryrosinase oxidation can promote Enter TYR generate melanin, tyrosine formed melanic during, tryrosinase can promote TYR produce L- DOPA further effect make L-3,4 dihydroxyphenylalanine form bar quinone, and DOPA quinone ultimately generates melanin.
The computing formula of suppression ratio: [1-(T2-T1)/(C2-C1)] * 100%
C1 is the absorbance of the mixed liquor of buffer solution and Rhizoma Solani tuber osi extracting solution, C2 be buffer solution, Rhizoma Solani tuber osi extracting solution and The absorbance of the mixed liquor of tyrosine, is C2-C1 with the absorbance that C1 surveys C2 for reference, represents and extracts at deduction Rhizoma Solani tuber osi The melanic absorbance generated after the absorbance of liquid.T1 is the mixed of noni ferment sample, Rhizoma Solani tuber osi extracting solution and buffer solution Closing the absorbance of liquid, T2 is the absorbance of the mixed liquor of noni ferment sample, buffer solution, Rhizoma Solani tuber osi extracting solution and tyrosine Value, same is that reference is surveyed the absorbance of T2 and obtained T2-T1 with T1, represents at deduction sample and Rhizoma Solani tuber osi extracting solution absorbance Under the influence of, the melanic absorbance after the suppression of noni ferment sample.Keep, under identical test condition, surveying respectively Determine the Whitening sunscreen cream containing the noni ferment of variable concentrations in embodiment 1 to 8 inhibitory action to tryrosinase, result such as table Shown in 9:
Table 9 Whitening sunscreen cream inhibitory action to tryrosinase
As shown in Table 9, noni ferment Whitening sunscreen cream of the present invention can effectively suppress the activity of tryrosinase, suppresses black Element growth, when the mass content of noni ferment is 0.6%, maximum to the suppression ratio of tryrosinase.
Absorption ultraviolet is tested
Weigh the Whitening sunscreen cream uniform application of 0.06g embodiment 1 to 8 acquisition respectively in the microscope slide with medical adhesive tape On, with do not smear sunscreen cream microscope slide for blank product, after timebase, scanning sample and reference substance UVA (320~ Uv absorption meansigma methods 420nm), in UVB (275~320nm), UVC (200~275nm) wave band, compare sample sunscreen cream and Comparison sunscreen cream, to ultra-violet absorption situation, the results are shown in Table 10.
Table 10 Whitening sunscreen cream ultraviolet absorption value
As can be known from Table 10, the noni ferment Whitening sunscreen cream that the present invention proposes is effective to ultra-violet absorption, possesses one Fixed sun-proof function, along with the mass content of noni ferment increases, its ultraviolet absorption ability is increasing trend.
ABTS radical scavenging activity measures
This experimental applications ABTS measures free radical scavenging activity.Compound concentration is ABTS's and 2.45mmol/L of 7mmol/L Potassium peroxydisulfate mixed solution, room temperature lucifuge stands 10~16h, dilute with water so that it is and the light absorption value under 734nm is 0.7 ± 0.02 (is designated as A0);Embodiment 1 to 8 sample 1mg, ABTS working solution 1.5mL is added in ABTS working solution test tube;Blank group is used Distilled water replaces sample solution;Matched group distilled water replaces ABTS working solution.Below respectively group room temperature lucifuge places 1h, Measuring its light absorption value (being designated as A) under 734nm, ascorbic acid does positive control.
Clearance rate (%)=(A0-A)/A0* 100%.
Clearance rate during the ABTS radical scavenging activity of the Whitening sunscreen cream that embodiment 1 to embodiment 8 obtains measures is surveyed Determine result as shown in table 11:
The free radical scavenging activity of table 11 Whitening sunscreen cream
As can be known from Table 11, the noni ferment Whitening sunscreen cream that the present invention proposes has significant radical scavenging activity, Possessing good whitening and skin-protecting effect, when the mass content of noni ferment is 0.6%, radical scavenging activity is optimal.
In sum, the present invention relates to the application in cosmetics of a kind of noni ferment, it is provided that noni ferment whitening prevent Shine frost and can be applicable to cosmetic industry whitening nursing field.Noni ferment by fresh Noni fruit and sucrose at yeast fermentation Under the conditions of extract and obtain, extract the noni ferment obtained and there is preferable whitening nursing efficacy, prepared Whitening sunscreen cream has Significantly radical scavenging activity, effectively suppresses the activity of tryrosinase, and suppression melanin growth, to ultra-violet absorption effect Good, it is achieved the effect of whitening sun protection skin protection, and there is not side effect, also find no the phenomenon stimulating skin to cause allergy.This Invention preparation method is simple to operation, and equipment requirements is low, and production cost is low, energy-conserving and environment-protective, is suitable for producing in enormous quantities.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all essences in the present invention Within god and principle, any modification, equivalent substitution and improvement etc. made, should be included within the scope of the present invention.

Claims (6)

1. a noni ferment Whitening sunscreen cream, it is characterised in that count by weight percentage, its formula composition includes: stearic Acid glyceride 1~4.5%, 16/18 natural fatty alcohol 0.5~4%, caprylic/capric triglyceride 2~8%, different n-nonanoic acid are different Nonyl ester 3~11%, Jojoba oil 1~2.4%, polydimethylsiloxane 0.5~4%, sterol ester 0.8~2.5%, vitamin E 0.5~4%, methyl hydroxybenzoate 0.1~0.8%, propylparaben 0.1~0.8%, glycerol 3~16%, amino acid humectant 2 ~6%, allantoin 0.1~0.3%, lauryl alcohol 0.8~2.2% and noni ferment 0.2~1.2%, surplus is deionization Water.
2. a noni ferment Whitening sunscreen cream, it is characterised in that count by weight percentage, its formula composition includes: stearic Acid glyceride 3%, 16/18 natural fatty alcohol 2.5%, caprylic/capric triglyceride 6%, isononyl isononanoate 8%, suddenly Bar oil 1.8%, polydimethylsiloxane 2.5%, sterol ester 1.6%, vitamin E 2.5%, methyl hydroxybenzoate 0.5%, Buddhist nun suddenly Pool gold propyl ester 0.5%, glycerol 10%, amino acid humectant 4.5%, allantoin 0.1%, lauryl alcohol 1.6% and noni ferment Element 0.6%, surplus is deionized water.
Noni ferment Whitening sunscreen cream the most according to claim 1 or claim 2, it is characterised in that described noni ferment is by walking as follows Rapid prepared:
Take the chopping of fresh Noni fruit, add distilled water and sucrose, mixing, through high-pressure sterilizing pot sterilizing, after cooling, add yeast, Standing for fermentation, is filtrated to get fermentation liquid and is noni ferment.
Noni ferment Whitening sunscreen cream the most according to claim 3, it is characterised in that the preparation process of described noni ferment In, the adding proportion of Noni fruit, distilled water and sucrose is: every 100g Noni fruit adds 100mL distilled water and 4g sucrose.
Noni ferment Whitening sunscreen cream the most according to claim 3, it is characterised in that the preparation process of described noni ferment In, fermentation time is 30~40 days.
6. the preparation method of a noni ferment Whitening sunscreen cream, it is characterised in that comprise the steps:
S1, taking A phase and B phase respectively, heated and stirred to 80~90 DEG C is in homogeneously;
S2, when A phase and B phase temperature difference are not more than 5 DEG C, continuously stirred while, slowly by A phase oil solution add B phase water Solution is thoroughly mixed to biphase, starts homogenizer, it is thus achieved that stable and glossiness emulsion;
S3, when emulsion temperature is down to 60~70 DEG C, add C phase, again start homogenizer until emulsion mix homogeneously, treat temperature Being down to when 40~45 DEG C add D phase, continuously stirred emulsion is down to room temperature, closes agitator, stands 5~12h, to obtain final product;
Wherein, A phase includes tristerin, 16/18 natural fatty alcohols, caprylic/capric triglyceride, the different nonyl of different n-nonanoic acid Ester, Jojoba oil, polydimethylsiloxane, sterol ester, vitamin E, methyl hydroxybenzoate and propylparaben;B phase include glycerol, Amino acid humectant, allantoin and deionized water;C phase includes lauryl alcohol;D phase includes noni ferment.
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CN106860251A (en) * 2017-01-19 2017-06-20 长沙协浩吉生物工程有限公司 A kind of compound method of ferment anti-aging suncream
CN106860362A (en) * 2017-02-24 2017-06-20 长沙协浩吉生物工程有限公司 A kind of compound method of ferment anti-acne suncream
CN106860163A (en) * 2017-02-24 2017-06-20 长沙协浩吉生物工程有限公司 A kind of compound method of ferment anti-acne suncream
CN106860044A (en) * 2017-02-24 2017-06-20 长沙协浩吉生物工程有限公司 A kind of compound method of ferment anti-acne suncream
CN106860268A (en) * 2017-01-19 2017-06-20 长沙协浩吉生物工程有限公司 A kind of compound method of ferment anti-aging suncream
CN106860130A (en) * 2017-01-18 2017-06-20 长沙协浩吉生物工程有限公司 A kind of compound method of ferment antiallergy suncream
CN106860250A (en) * 2017-01-19 2017-06-20 长沙协浩吉生物工程有限公司 A kind of compound method of ferment anti-aging suncream
CN106860112A (en) * 2017-02-24 2017-06-20 长沙协浩吉生物工程有限公司 A kind of compound method of ferment anti-acne suncream
CN106860373A (en) * 2017-02-24 2017-06-20 长沙协浩吉生物工程有限公司 A kind of compound method of ferment anti-acne suncream
CN107412073A (en) * 2017-08-30 2017-12-01 上海应用技术大学 A kind of composition containing peach gum hydrolysate and its preparation method and application
CN109199953A (en) * 2018-10-22 2019-01-15 海南师范大学 A kind of Noni fruit ferment eye patch and preparation method thereof
CN109364007A (en) * 2018-12-04 2019-02-22 天津尚美化妆品有限公司 Plant enzyme face cleaning condensation
CN110511969A (en) * 2019-09-06 2019-11-29 上海应用技术大学 Natural peach gum fermentation prepares the method for peach gum extract and its applies in cosmetics
CN115364019A (en) * 2021-05-21 2022-11-22 海南师范大学 Millettia speciosa-dendrobium-noni composite enzyme, preparation method thereof and application of millettia speciosa-dendrobium-noni composite enzyme as sun-screening agent

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CN104207293A (en) * 2014-08-08 2014-12-17 宋如珍 Processing method of Noni enzyme
CN104586741A (en) * 2015-02-05 2015-05-06 上海昊淼生物科技有限公司 Bubble enzyme facial mask

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US20020192246A1 (en) * 2001-04-17 2002-12-19 Jensen Claude Jarkae Morinda citrifolia (Noni) enhanced cosmetic intensive repair serum
CN104207293A (en) * 2014-08-08 2014-12-17 宋如珍 Processing method of Noni enzyme
CN104207997A (en) * 2014-09-18 2014-12-17 深圳朶妃生物科技有限公司 Deep revitalizing facial mask containing morinda citrifolia stock extract liquid and preparation method thereof
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Cited By (17)

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CN106860077A (en) * 2017-01-18 2017-06-20 长沙协浩吉生物工程有限公司 A kind of compound method of ferment antiallergy suncream
CN106860130A (en) * 2017-01-18 2017-06-20 长沙协浩吉生物工程有限公司 A kind of compound method of ferment antiallergy suncream
CN106860268A (en) * 2017-01-19 2017-06-20 长沙协浩吉生物工程有限公司 A kind of compound method of ferment anti-aging suncream
CN106860251A (en) * 2017-01-19 2017-06-20 长沙协浩吉生物工程有限公司 A kind of compound method of ferment anti-aging suncream
CN106860250A (en) * 2017-01-19 2017-06-20 长沙协浩吉生物工程有限公司 A kind of compound method of ferment anti-aging suncream
CN106860112A (en) * 2017-02-24 2017-06-20 长沙协浩吉生物工程有限公司 A kind of compound method of ferment anti-acne suncream
CN106860044A (en) * 2017-02-24 2017-06-20 长沙协浩吉生物工程有限公司 A kind of compound method of ferment anti-acne suncream
CN106860163A (en) * 2017-02-24 2017-06-20 长沙协浩吉生物工程有限公司 A kind of compound method of ferment anti-acne suncream
CN106860362A (en) * 2017-02-24 2017-06-20 长沙协浩吉生物工程有限公司 A kind of compound method of ferment anti-acne suncream
CN106860373A (en) * 2017-02-24 2017-06-20 长沙协浩吉生物工程有限公司 A kind of compound method of ferment anti-acne suncream
CN107412073A (en) * 2017-08-30 2017-12-01 上海应用技术大学 A kind of composition containing peach gum hydrolysate and its preparation method and application
CN109199953A (en) * 2018-10-22 2019-01-15 海南师范大学 A kind of Noni fruit ferment eye patch and preparation method thereof
CN109199953B (en) * 2018-10-22 2021-11-16 海南师范大学 Noni enzyme eye mask and preparation method thereof
CN109364007A (en) * 2018-12-04 2019-02-22 天津尚美化妆品有限公司 Plant enzyme face cleaning condensation
CN110511969A (en) * 2019-09-06 2019-11-29 上海应用技术大学 Natural peach gum fermentation prepares the method for peach gum extract and its applies in cosmetics
CN115364019A (en) * 2021-05-21 2022-11-22 海南师范大学 Millettia speciosa-dendrobium-noni composite enzyme, preparation method thereof and application of millettia speciosa-dendrobium-noni composite enzyme as sun-screening agent
CN115364019B (en) * 2021-05-21 2023-07-04 海南师范大学 Millettia speciosa-dendrobe-noni composite enzyme, preparation method thereof and application thereof as sun-screening agent

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