CN108938479A - A kind of mildy wash of the extract containing water lily and preparation method thereof - Google Patents
A kind of mildy wash of the extract containing water lily and preparation method thereof Download PDFInfo
- Publication number
- CN108938479A CN108938479A CN201710382813.5A CN201710382813A CN108938479A CN 108938479 A CN108938479 A CN 108938479A CN 201710382813 A CN201710382813 A CN 201710382813A CN 108938479 A CN108938479 A CN 108938479A
- Authority
- CN
- China
- Prior art keywords
- parts
- water lily
- mildy wash
- skin
- extract
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Dermatology (AREA)
- Emergency Medicine (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention provides mildy wash of a kind of extract containing water lily and preparation method thereof.Mildy wash formula are as follows: by weight, 5-10 parts of water lily flower extract, 3-5 parts of rose oil, 2-5 parts of grape seed oil, 2-5 parts of tea extraction, 0.6-1 parts of thickener, 13-23 parts of surfactant, 8-11 parts of moisturizer.The emphasis of of the invention component is different; but pass through the coordinated of various substances; from two aspect of face cleaning and skin care; and start with for skin care from multiple dimensions; eliminate comprehensively cause skin oxidative, raw spot, dehydration factor, promote skin self-protection and repair function, and be at good operating condition; skin condition is significantly improved, achievees the purpose that deep layer cleaning skin while playing moisturizing moisturizing effect.In addition, since water lily also plays reconciliation in formula, the mildy wash is all non-stimulated to all kinds of skin quality, and can releive skin, and use is milder, and skin sense is good.
Description
Technical field
The present invention relates to cosmetic fields, more particularly, to a kind of mildy wash and preparation method thereof of extract containing water lily.
Background technique
Water lily is known as " undine ", while having ornamental, water body purification and edible, medical value.Modern medicine is ground
Study carefully and show that the nutrition extracts such as nymphaea tetragona embryo, water lily pollen, water lily nectar have very high nutritive value, it is rich in
Microelements such as anthocyanin, vitamin B1, vitamin C, plant flavonoids, selenium (Se), zinc (Zn), manganese (Mn), potassium (K) and each
Kind amino acid.Water lily whole body is treasured, mainly contains pollen, anthocyanin, hasubanonine, lotus Hua Su and the big essence of nectar five.Water lily
Pollen in, stamen generate essence be lotus flower full nutrition library, enter water and change, health beauty treatment.Nymphaea tetragona is rich in a variety of flavones
The anthocyanin of component, anti-oxidant safer, more excellent, more strength.The hasubanonine that water lily is rich in can supplement comprehensively human body cannot
The amino acid of synthesis balances vitamin and microelement.Lotus Hua Su is to open the power source that night closes, 100000000 years biogens, salubrity daytime
Brain tonic prolongs life, and is called " delicious wine ".Nectar is the slightly existing stigmatic fluid to die of gynoecium secretion, and non-honey is precious, tool
There is the effect with all worries set aside that takes care of health, is called " good wine ".But current water lily is mostly used for water body purification and ornamental, about water lily it is edible,
Application in terms of health care, cosmetics is very few.
In view of this, the present invention is specifically proposed.
Summary of the invention
The first object of the present invention is to provide a kind of mildy wash of extract containing water lily, which, which takes full advantage of, sleeps
The essence of lotus flower and its mild characteristic, also use cooperateing between nymphaea tetragona and rose oil, grape seed oil and tea extraction
Effect has efficient replenishing water and preserving moisture effect, and mild non-stimulated, is suitble to all kinds of skin quality.
The second object of the present invention is to provide the preparation method of the mildy wash of the above-mentioned extract containing water lily, the preparation method
Process is simple, and the essential ingredient in energy effective protection water lily is not damaged.
In order to solve the above technical problems, the present invention provides following technical schemes:
A kind of mildy wash of the extract containing water lily, is mainly mixed by following component: by weight,
5-10 parts of water lily flower extract,
3-5 parts of rose oil,
2-5 parts of grape seed oil,
2-5 parts of tea extraction,
0.6-1 parts of thickener,
13-23 parts of surfactant,
8-11 parts of moisturizer.
Water lily flower extract contains the multiple beneficials ingredient such as a variety of saponin(es, flavones, phenol, amino acid, alkali, protein, wherein
Contained flavones, phenol have antioxidation, and 17 kinds of contained amino acid have replenishing water and preserving moisture and promote collagen synthesis
Effect, contained saponin(e have antibacterial action, the metabolic processes of alkali and each albuminoid energy balance skin.
Citronellol contained by rose oil, geraniol, nerol, benzyl carbinol, linalool, fanesol, eugenol, cloves
The endocrine system of the ingredients such as phenol methyl ether, rose oxide, nerol oxide, rosefuran not only adjustable human body, but also human body can be increased
Immunity, while promoting the decomposition of pigment, it activates, promote blood circulation.
Grape seed oil contains linoleic acid and other a variety of unsaturated fatty acids, vitamin F, minerals, protein, flaxseed
Oleic acid, chlorophyll etc..Linoleic acid is fatty acid that is needed by human and cannot synthesizing for human body.Flaxseed in grape seed oil
Oleic acid can resist free radical, anti-aging, help absorbs vitamin C and E, strengthen the elasticity of the circulatory system, reduce ultraviolet light
The collagen in skin is protected in injury, improves venous engorgement and oedema, prevents melanin deposition.The original that grape seed oil contains
Cyanine is known as protection blood vessel elasticity, protects skin afflicting with great suffering torment from ultraviolet light, prevents the destruction of collagenous fibres and elastomer, makes
Skin keeps due elasticity and tension, and skin sagging and wrinkle is avoided to generate.
Tea extraction mainly includes tea polyphenols, caffeine, aromatic oil, moisture, minerals, pigment, carbohydrate, albumen
Matter, amino acid, vitamin etc. have the effects that anti-oxidant, removing free radical.
Thickener makes product in emulsus for being formed.The main functionality of surfactant performance face cleaning.Moisturizer was both kept
The stability of product, and there is moisture-keeping function to skin.
In the present invention, skin care ingredient is wanted based on water lily flower extract, main rise moisturizes the skin and coordinate to rush between each ingredient
Prominent effect makes mildy wash milder；Rose oil, grape seed oil are cooperateed with water lily flower extract for adjusting the new old of skin
Metabolic process, and cutaneous immunisation power is improved, also unfavorable stimulation of the inhibition external environment to skin, while also cooperating with tea extraction
Its antioxidation, on the one hand prevents mildy wash itself to be oxidized, and on the other hand skin is inhibited to be oxidized.It can be seen that this hair
In the mildy wash of bright offer, the emphasis of each component is different, but by the coordinated of various substances, from face cleaning and skin care
Two aspect set out, and for skin care from promote collagen synthesis, decompose melanin, resist exogenous microbial, enhance skin
Skin immunity, eliminate superoxide radical, multiple dimensions such as water lock are started with, eliminate comprehensively cause skin oxidative, raw spot, dehydration because
Element promotes skin self-protection and repairs function, and is at good operating condition, significantly improves skin condition,
Reach deep layer cleaning skin while playing the effect of moisturizing moisturizing.In addition, since water lily also plays reconciliation in formula, because
This, the mildy wash is all non-stimulated to all kinds of skin quality, and can releive skin, and use is milder, and skin sense is good.
The above formula can also advanced optimize, to obtain the effect of better replenishing water and preserving moisture and skin of releiving, such as with
Side are as follows: by weight,
5-8 parts of water lily flower extract,
3-4 parts of rose oil,
2-4 parts of grape seed oil,
2-4 parts of tea extraction,
0.6-1 parts of thickener,
13-20 parts of surfactant,
10-11 parts of moisturizer.
The skin effect of the pairs of mildy wash of group of water lily flower extract has a major impact in all formulas described above, is
Improve the extract of skin effect preferably following quality:
The preferably extract of Nymphaea caerulea flower variety.
It is highly preferred that including general flavone mg/g, total phenol 50-55mg/g, gallic acid 2.5- in the water lily flower extract
2.7mg/g, Nicotifiorin 3-3.2mg/g and anthocyanin 35-40mg/g.
The water lily flower extract of the quality can be through ultramicro grinding, CO2Supercritical extract is prepared, the supercritical extract
The temperature that method uses is 25-35 DEG C, pressure 20-40MPa.
In the present invention, dry nymphaea tetragona is after pulverizing, and the partial size of powder is less than 100 μm, and powder diameter is uniform, carefully
Cell wall is broken, and surface area and porosity increase, and passes through CO later2Supercritical extract, CO2The temperature that supercritical extraction uses
For room temperature, grape pip is in CO2Atmosphere in, under this condition can guarantee nymphaea tetragona in active constituent it is especially temperature sensitive
Active material and oxidizable active material do not degraded by high-temperature oxygen, and the recovery rate of active constituent is high, obtains
Extract quality it is good.
Preferably, the surfactant is oat amino acids and/or anionic surfactant, preferably oat amino
Acids and anionic surfactant, and the weight ratio of the two is preferably 10-15:3-8.
Oat amino acids foaming power is strong, resistance to hard water, can form white matter foam, and feel is extremely mild, comfortable.Oat amino
Acids is also easy to thicken, and can have significant nutrition moist and moisture-keeping efficacy, especially as the important medium for lockking moisture of skin
People suitable for dry skin.
Anionic surfactant has a characteristics such as preferable decontamination, foaming, dispersion, emulsification, wetting, and with oat ammonia
Cleaning capacity and water holding capacity are stronger after the collocation of base acids, tests determined, and the preferred weight ratio of the two is 10-15:3-8.
In order to improve cleaning capacity and water holding capacity, it is preferable that the oat amino acids are selected from glutamic acid, phenylpropyl alcohol ammonia
It is one or more in acid, leucine and isoleucine.
Preferably, the anionic surfactant be lauroyl glutamate disodium and/or sodium lauroyl sarcosine, preferably
Lauroyl glutamate disodium and sodium lauroyl sarcosine, and the weight ratio of the two is preferably 2-5:1-3.
For the moisturizer in mildy wash of the present invention, it is preferred to use a kind of in glycerol, butanediol, sorbierite and hyaluronic acid
Or it is a variety of, these types of compound is small to the irritation of skin, and is suitble to all kinds of skin quality, wherein preferably glycerine.
For the thickener in mildy wash of the present invention, it is preferred to use in polyacrylic, cellulose family and natural gum class
One or more, the collaborative effect of this few class thickeners and above-mentioned surfactant is preferable, there is certain effect of releiving to skin,
And by safe and harmless, wherein it is preferred that polyacrylic.
Preferably, polyacrylic is cetyl polyethoxymethacrylate copolymer.
Preferably, the tea extraction is green-tea extract.The ratio of tea polyphenols and amino acid, vitamin in green-tea extract
Example with the collaborative effect of water lily more preferably.
The production method of mildy wash described above mainly has emulsification and mixes two committed steps, basic process flow
Are as follows:
Thickener is dissolved in water, surfactant and moisturizer is then added, heating mixes, and is cooled to 45 DEG C later
Hereinafter, be added remaining raw material to get.
The purpose that various extracts and oil are added when temperature is 45 DEG C or less is to prevent effective component by high temperature.
To sum up, compared with prior art, invention achieves following technical effects:
(1) water lily flower extract is used for mildy wash for the first time, and it is assisted with rose oil, grape seed oil, tea extraction
Make, increase the replenishing water and preserving moisture of mildy wash and soothes the skin function；
(2) type and ratio of the face cleanings ingredient such as surfactant, thickener and moisturizer in mildy wash are improved, and its with
The proportion of plant skin care ingredient improves face cleaning effect and replenishing water and preserving moisture effect；
(3) the preparation method mild condition of mildy wash, process is simple, is suitable for existing workshop, it is easier to promote
Product.
Specific embodiment
Technical solution of the present invention is clearly and completely described below in conjunction with specific embodiment, but ability
Field technique personnel will be understood that following described embodiments are some of the embodiments of the present invention, instead of all the embodiments,
It is merely to illustrate the present invention, and is not construed as limiting the scope of the invention.Based on the embodiments of the present invention, the common skill in this field
Art personnel every other embodiment obtained without making creative work belongs to the model that the present invention protects
It encloses.The person that is not specified actual conditions in embodiment, carries out according to conventional conditions or manufacturer's recommended conditions.Agents useful for same or instrument
Production firm person is not specified, is the conventional products that can be obtained by commercially available purchase.
Embodiment 1
1, it pre-processes: dry Egyptian blue nymphaea tetragona being cleaned, dust and other impurity are screened out.
2、CO2Supercritical extract: it is extracted under conditions of temperature is 25 DEG C, pressure is 40MPa or so.
The ingredient of detection gained water lily flower extract, the general flavone contained are 150mg/g, total phenol 55mg/g, galla turcica
Sour 2.5mg/g, Nicotifiorin 3.2mg/g and anthocyanin 40mg/g.
Embodiment 2
1, it pre-processes: dry Egyptian blue nymphaea tetragona being cleaned, dust and other impurity are screened out.
2、CO2Supercritical extract: it is extracted under conditions of temperature is 35 DEG C, pressure is 20MPa or so.
The ingredient of detection gained water lily flower extract, the general flavone contained are 160mg/g, total phenol 50mg/g, galla turcica
Sour 2.7mg/g, Nicotifiorin 3mg/g and anthocyanin 35mg/g.
Embodiment 3
Prepare mildy wash:
1, feeding: water lily flower extract (embodiment 1 is made) 8g, rose oil 5g, grape seed oil 4g, green-tea extract
4g, cetyl polyethoxymethacrylate copolymer 0.6g, oat amino acids (weight such as glutamic acid and phenylalanine)
15g, lauroyl glutamate disodium 2g, sodium lauroyl sarcosine 3g, glycerol 8g.
2, Jiang Shui, acrylic copolymer are added in vacuum emulsification pot, and homogeneous 3-5 minutes, stirring was warming up to 85 DEG C, by swallow
Wheat amino acids, glycerol, lauroyl glutamate disodium, sodium lauroyl sarcosine are added, and after stirring, keep the temperature 30 points
Clock, after begin to cool water cooling；45 DEG C are cooled to sleep hereinafter, rose oil, grape seed oil, green-tea extract, Egyptian blue is added
Flos Nelumbinis extract is discharged after stirring, is stood.
Embodiment 4
Difference with embodiment 3 is to introduce pH adjusting agent, anti-sensitizer and chelating agent in mildy wash, specific as follows:
1, feeding: water lily flower extract (embodiment 1 is made) 8g, rose oil 5g, grape seed oil 4g, green-tea extract
4g, cetyl polyethoxymethacrylate copolymer 0.6g, oat amino acids (weight such as glutamic acid and phenylalanine)
15g, lauroyl glutamate disodium 2g, sodium lauroyl sarcosine 3g, glycerol 8g, appropriate triethanolamine, appropriate EDETATE SODIUM, allantois
Plain 0.3g.
2, Jiang Shui, acrylic copolymer are added in vacuum emulsification pot, and homogeneous 3-5 minutes, stirring was warming up to 85 DEG C, by swallow
Wheat amino acids, glycerol, lauroyl glutamate disodium, sodium lauroyl sarcosine, EDETATE SODIUM are added, after stirring,
Heat preservation 30 minutes, after begin to cool water cooling；Be cooled to 45 DEG C hereinafter, be added rose oil, grape seed oil, green-tea extract,
Egyptian blue water lily flower extract, triethanolamine (making lotion pH 7 or so), allantoin are discharged after stirring, are stood.
Embodiment 5
It is that the proportion of each ingredient is different from the difference of embodiment 3, are as follows: water lily flower extract (embodiment 1 is made) 10g,
Rose oil 3g, grape seed oil 5g, green-tea extract 2g, cetyl polyethoxymethacrylate copolymer 1 g, oat ammonia
Base acids 10g, lauroyl glutamate disodium 2g, sodium lauroyl sarcosine 1g, glycerol 11g, remaining step is the same as embodiment 3.
Embodiment 6
It is that the proportion of each ingredient is different from the difference of embodiment 3, are as follows: water lily flower extract (embodiment 1 is made) 5g, rose
Rare caul-fat 5g, grape seed oil 2g, green-tea extract 5g, cetyl polyethoxymethacrylate copolymer 0.6g, oat ammonia
Base acids 15g, lauroyl glutamate disodium 5g, sodium lauroyl sarcosine 3g, glycerol 8g, remaining step is the same as embodiment 3.
Embodiment 7
Difference with embodiment 3 is that selected raw material type has difference, are as follows: water lily flower extract (embodiment 1 is made)
8g, rose oil 5g, grape seed oil 4g, black tea extract 4g, polyacrylic acid 0.6g, oat amino acids (leucine and different bright
The weight such as propylhomoserin) 15g, lauroyl glutamate disodium 2g, sodium lauroyl sarcosine 3g, butanediol 8g.Remaining step is the same as embodiment 3.
Comparative example 1
The difference of comparative example 1 and embodiment 4 is in mildy wash without water lily flower extract, remaining raw material type, between
Proportion it is same as Example 4, preparation method is the same as embodiment 4.
Comparative example 2
The difference of comparative example 2 and embodiment 4 is in mildy wash without grape seed oil, remaining raw material type, between match
Than same as Example 4, preparation method is the same as embodiment 4.
One, replenishing water and preserving moisture effect is tested
Test philosophy
According to cosmetic composition moisture absorption, the difference of performance of keeping humidity, different moisturizing agent molecules to the active force of hydrone not
Together, it is different with the ability of moisture is kept to absorb moisture.Oil content has sealing process to moisture, can prevent scattering and disappearing for moisture.Moisture absorption is made
It is firmly big, it is strong to water molecules power, it absorbs and keeps the amount of moisture also bigger, closure is good, moisture loss
It is few.The biomaterial that cuticula, epidermis etc. are imitated using adhesive tape is coated with cosmetics on adhesive tape, simulates answering for practical cosmetics
Use situation.Under conditions of constant temperature and humidity after a certain period of time, it weighs sample and places the of poor quality of front and back, find out the damage of sample size
It loses, the effect of moisturizing ingredient moisturizing can be calculated.
Experimental method and testing procedure
Weigh 6 pieces of glass plate weight (M for posting 3M adhesive plaster0), it records respectively, 3 pieces are blank control, and 3 pieces are tried for sample
It tests.It takes 200 μ L samples to be added dropwise on the glass plate for posting 3M adhesive plaster with liquid-transfering gun, weighs weight M with assay balance1It is (accurate
To 0.000lg), sample is smoothened, glass plate is put into the drier of the constant humidity of requirement, is repeated 3 times.By remaining 3 pieces of sky
White control glass plate is put into togerther in the drier of constant humidity.After placing 4h, 8h, glass plate is taken out, the glass plate is weighed
Weight (M2), its moisturizing rate and relative humidity rate are tested, is immediately placed into the drier of constant humidity after weighing.
Moisturizing rate calculation formula:
Moisturizing rate=(M2–M0)/(M1-M0) X 100%
In formula:
M0: hollow plate quality/g；
M1: sample-adding rear glass plate quality/g；
M2: quality/g after several hours is placed in drier；
Test its relative humidity be 60% when 4h and 8h in moisturizing rate.
Experimental result such as table 1.
Moisturizing rate (%) of 1 face cream of table in RH60%
Two, safety detection
As a result, it has been found that the content of microorganisms in the product of embodiment 3 to 7 meets national standard, as a result such as the following table 2.
Table 2
| Inspection project | Inspection result | Limit value |
| Total plate count (CFU/g) | <10 | ≤1000 |
| Yeast and mold (CFU/g) | <10 | ≤100 |
| Excrement colibacillus group (/g) | It is not detected | It must not detect |
| Staphylococcus aureus (/g) | It is not detected | It must not detect |
| Pseudomonas aeruginosa (/g) | It is not detected | It must not detect |
In addition, the present invention has also randomly selected 100 subjects, scratch test is carried out, does not find allergic problem.
Finally, it should be noted that the above embodiments are only used to illustrate the technical solution of the present invention., rather than its limitations；To the greatest extent
Pipe present invention has been described in detail with reference to the aforementioned embodiments, those skilled in the art should understand that: its according to
So be possible to modify the technical solutions described in the foregoing embodiments, or to some or all of the technical features into
Row equivalent replacement；And these are modified or replaceed, various embodiments of the present invention technology that it does not separate the essence of the corresponding technical solution
The range of scheme.
Claims (10)
1. a kind of mildy wash of extract containing water lily, which is characterized in that mainly mixed by following component: by weight,
5-10 parts of water lily flower extract,
3-5 parts of rose oil,
2-5 parts of grape seed oil,
2-5 parts of tea extraction,
0.6-1 parts of thickener,
13-23 parts of surfactant,
8-11 parts of moisturizer.
2. the mildy wash of the extract according to claim 1 containing water lily, which is characterized in that by weight,
5-8 parts of water lily flower extract,
3-4 parts of rose oil,
2-4 parts of grape seed oil,
2-4 parts of tea extraction,
0.6-1 parts of thickener,
13-20 parts of surfactant,
10-11 parts of moisturizer.
3. the mildy wash of the extract according to claim 1 containing water lily, which is characterized in that the water lily flower extract is angstrom
And Nymphaea caerulea flower extract；
It preferably, include general flavone 150-160mg/g, total phenol 50-55mg/g, gallic acid 2.5- in the water lily flower extract
2.7mg/g, Nicotifiorin 3-3.2mg/g and anthocyanin 35-40mg/g.
4. the mildy wash of the extract according to claim 3 containing water lily, which is characterized in that the system of the water lily flower extract
Preparation Method are as follows:
Nymphaea tetragona is through ultramicro grinding, CO2Supercritical extract is prepared, the temperature that the supercritical extract uses for 25-35 DEG C,
Pressure is 20-40MPa.
5. the mildy wash of the extract according to claim 1 containing water lily, which is characterized in that the surfactant is oat
Amino acids and/or anionic surfactant, preferably oat amino acids and anionic surfactant, and the weight of the two
Than being preferably 10-15:3-8；
Preferably, the oat amino acids are one or more in glutamic acid, phenylalanine, leucine and isoleucine；
Preferably, the anionic surfactant is lauroyl glutamate disodium and/or sodium lauroyl sarcosine, preferably laurel
Acyl disodium glutamate and sodium lauroyl sarcosine, and the weight ratio of the two is preferably 2-5:1-3.
6. the mildy wash of the extract according to claim 1 containing water lily, which is characterized in that the moisturizer be selected from glycerol,
One or more, preferably glycerine in butanediol, sorbierite and hyaluronic acid.
7. the mildy wash of the extract according to claim 1 containing water lily, which is characterized in that the thickener is selected from polypropylene
One of acids, cellulose family and natural gum class are a variety of, preferably polyacrylic；
Preferably, polyacrylic is cetyl polyethoxymethacrylate copolymer.
8. the mildy wash of the extract according to claim 1 containing water lily, which is characterized in that the tea extraction mentions for green tea
Take object.
9. the mildy wash of the extract according to claim 1-8 containing water lily, which is characterized in that further include that pH is adjusted
One of agent, anti-sensitizer and chelating agent are a variety of；
Preferably, the pH adjusting agent is triethanolamine；
Preferably, the anti-sensitizer is allantoin；
Preferably, the chelating agent is EDETATE SODIUM.
10. the preparation method of the mildy wash of the described in any item extracts containing water lily of claim 1-9, which is characterized in that including
Following steps:
Thickener is dissolved in water, surfactant and moisturizer is then added, heating mixes, be cooled to later 45 DEG C with
Under, be added remaining raw material to get.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710382813.5A CN108938479A (en) | 2017-05-26 | 2017-05-26 | A kind of mildy wash of the extract containing water lily and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710382813.5A CN108938479A (en) | 2017-05-26 | 2017-05-26 | A kind of mildy wash of the extract containing water lily and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108938479A true CN108938479A (en) | 2018-12-07 |
Family
ID=64494626
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710382813.5A Pending CN108938479A (en) | 2017-05-26 | 2017-05-26 | A kind of mildy wash of the extract containing water lily and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108938479A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109846784A (en) * | 2019-03-13 | 2019-06-07 | 广州莱倩化妆品有限公司 | A kind of formula and preparation method thereof of elasticity muffin |
| CN111700845A (en) * | 2020-07-20 | 2020-09-25 | 湖南山润油茶科技发展有限公司 | Camellia seed moisturizing conditioning mask and preparation method thereof |
| CN112156048A (en) * | 2020-10-27 | 2021-01-01 | 浙江她创美容科技有限公司 | Natural whitening face cleaning powder and preparation method thereof |
| CN117860640A (en) * | 2024-01-15 | 2024-04-12 | 佛山市思怡诺生物科技有限公司 | A skin external composition and its preparation method |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106176360A (en) * | 2016-07-26 | 2016-12-07 | 广州众上投资控股集团有限公司 | A kind of nectar frost containing oral shui solution extract, Herba Saussureae Involueratae extract and Echinacea Angustifolia extracts and preparation method thereof |
-
2017
- 2017-05-26 CN CN201710382813.5A patent/CN108938479A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106176360A (en) * | 2016-07-26 | 2016-12-07 | 广州众上投资控股集团有限公司 | A kind of nectar frost containing oral shui solution extract, Herba Saussureae Involueratae extract and Echinacea Angustifolia extracts and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 国产非特殊用途化妆品备案信息服务平台: "原态美生态睡莲净颜活肤洁面乳", 《HTTP://FTBA.NMPA.GOV.CN:8181/FTBAN/ITOWNET/HZP_BA/FW/PZ.JSP?PROCESSID=2016070412293928FC9&NID=2016070412293928FC9》 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109846784A (en) * | 2019-03-13 | 2019-06-07 | 广州莱倩化妆品有限公司 | A kind of formula and preparation method thereof of elasticity muffin |
| CN111700845A (en) * | 2020-07-20 | 2020-09-25 | 湖南山润油茶科技发展有限公司 | Camellia seed moisturizing conditioning mask and preparation method thereof |
| CN112156048A (en) * | 2020-10-27 | 2021-01-01 | 浙江她创美容科技有限公司 | Natural whitening face cleaning powder and preparation method thereof |
| CN117860640A (en) * | 2024-01-15 | 2024-04-12 | 佛山市思怡诺生物科技有限公司 | A skin external composition and its preparation method |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| KR101723526B1 (en) | Cosmetic composition containing the extract of Camellia japonica flower, Prunus serrulata flower, Jasminum officinale flower, Chamomilla recutita flower and Nelumbo nucifera flower | |
| US20230390182A1 (en) | Process for obtaining an aqueous extract of lavender, compositions comprising such an extract, and their cosmetic uses | |
| CN105505635B (en) | A kind of skin cleansing composition and preparation method thereof containing lotus active constituent | |
| CN108938479A (en) | A kind of mildy wash of the extract containing water lily and preparation method thereof | |
| JP4425163B2 (en) | Anti-aging cosmetics | |
| CN107213069A (en) | A kind of U.S. face film and preparation method thereof | |
| JPH11228339A (en) | Melanin generation suppresser and preparation for external use for skin | |
| CN105769601B (en) | Mud mask and preparation method thereof is nourished in a kind of walnut ferment whitening | |
| CN105726439B (en) | Golden cicada spends skin whitening, moisturizing medicine cosmetic and preparation method thereof | |
| JP2000247897A (en) | Cosmetic composition | |
| JPH0892057A (en) | Cosmetic blended with extract of seed of coffee tree | |
| JP2002068953A (en) | Cosmetic composition | |
| CN112137919B (en) | Application of dictyophora indusiata egg extract in preparation of external beauty and skin care products and external beauty and skin care products based on same | |
| KR101930348B1 (en) | A composition for water tissue containing lava seawater | |
| JP2000143524A (en) | Antiinflammatory agent containing extract of amaranthus | |
| JP2002316937A (en) | Plant extract-containing anti-allergic agent | |
| CN110613663A (en) | Skin repairing composition, skin care product and preparation method thereof | |
| JP2000256171A (en) | Cosmetic composition | |
| JP2002363027A (en) | Active oxygen scavenger or cosmetic composition | |
| KR101757457B1 (en) | Cosmetic composition containing natural complex extract for anti-thermal skin aging and skin soothing | |
| JP2004026743A (en) | Polylysine preparation and cosmetic composition containing the same | |
| JP2011168543A (en) | Singlet oxygen scavenger, and skin care external preparation and cosmetic each using the singlet oxygen scavenger | |
| JP2001139489A (en) | Cosmetic composition | |
| CN108158960A (en) | With the lip care lipstick for alleviating pigmentation | |
| CN106963701A (en) | A kind of facial masks for whitening faces and removing spots |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20181207 |
|
| RJ01 | Rejection of invention patent application after publication |