CN104559942A - 混合熔盐储热传热材料及其制备方法 - Google Patents
混合熔盐储热传热材料及其制备方法 Download PDFInfo
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- CN104559942A CN104559942A CN201510056451.1A CN201510056451A CN104559942A CN 104559942 A CN104559942 A CN 104559942A CN 201510056451 A CN201510056451 A CN 201510056451A CN 104559942 A CN104559942 A CN 104559942A
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- 150000003839 salts Chemical class 0.000 title claims abstract description 101
- 238000012546 transfer Methods 0.000 title claims abstract description 67
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 239000000463 material Substances 0.000 title claims abstract description 11
- 238000005338 heat storage Methods 0.000 title abstract description 7
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 36
- 239000011780 sodium chloride Substances 0.000 claims abstract description 18
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims abstract description 11
- KWGKDLIKAYFUFQ-UHFFFAOYSA-M lithium chloride Chemical compound [Li+].[Cl-] KWGKDLIKAYFUFQ-UHFFFAOYSA-M 0.000 claims abstract description 10
- 238000009825 accumulation Methods 0.000 claims description 61
- 229910013553 LiNO Inorganic materials 0.000 claims description 38
- 238000000034 method Methods 0.000 claims description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- 229910052791 calcium Inorganic materials 0.000 claims description 8
- 238000001035 drying Methods 0.000 claims description 8
- 238000010907 mechanical stirring Methods 0.000 claims description 7
- 239000010419 fine particle Substances 0.000 claims description 6
- 230000008569 process Effects 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 5
- 239000013078 crystal Substances 0.000 claims description 4
- 229910052744 lithium Inorganic materials 0.000 claims description 4
- 239000000843 powder Substances 0.000 claims description 3
- 238000002844 melting Methods 0.000 abstract description 8
- 230000008018 melting Effects 0.000 abstract description 8
- 238000004146 energy storage Methods 0.000 abstract description 5
- ZCCIPPOKBCJFDN-UHFFFAOYSA-N calcium nitrate Chemical compound [Ca+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ZCCIPPOKBCJFDN-UHFFFAOYSA-N 0.000 abstract 2
- IIPYXGDZVMZOAP-UHFFFAOYSA-N lithium nitrate Chemical compound [Li+].[O-][N+]([O-])=O IIPYXGDZVMZOAP-UHFFFAOYSA-N 0.000 abstract 2
- INHCSSUBVCNVSK-UHFFFAOYSA-L lithium sulfate Chemical compound [Li+].[Li+].[O-]S([O-])(=O)=O INHCSSUBVCNVSK-UHFFFAOYSA-L 0.000 abstract 2
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 abstract 2
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 abstract 2
- LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 abstract 2
- 239000007832 Na2SO4 Substances 0.000 abstract 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 abstract 1
- IWOUKMZUPDVPGQ-UHFFFAOYSA-N barium nitrate Inorganic materials [Ba+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O IWOUKMZUPDVPGQ-UHFFFAOYSA-N 0.000 abstract 1
- 235000010333 potassium nitrate Nutrition 0.000 abstract 1
- 235000010289 potassium nitrite Nutrition 0.000 abstract 1
- 229910052939 potassium sulfate Inorganic materials 0.000 abstract 1
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 abstract 1
- 235000010344 sodium nitrate Nutrition 0.000 abstract 1
- 235000010288 sodium nitrite Nutrition 0.000 abstract 1
- 229910052938 sodium sulfate Inorganic materials 0.000 abstract 1
- 235000011152 sodium sulphate Nutrition 0.000 abstract 1
- DHEQXMRUPNDRPG-UHFFFAOYSA-N strontium nitrate Inorganic materials [Sr+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O DHEQXMRUPNDRPG-UHFFFAOYSA-N 0.000 abstract 1
- 238000005979 thermal decomposition reaction Methods 0.000 abstract 1
- 238000000354 decomposition reaction Methods 0.000 description 21
- 239000011575 calcium Substances 0.000 description 13
- 239000000523 sample Substances 0.000 description 13
- 238000010248 power generation Methods 0.000 description 11
- 238000005516 engineering process Methods 0.000 description 10
- 239000000203 mixture Substances 0.000 description 8
- 238000012360 testing method Methods 0.000 description 7
- 239000007789 gas Substances 0.000 description 6
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- ZWWCURLKEXEFQT-UHFFFAOYSA-N dinitrogen pentoxide Inorganic materials [O-][N+](=O)O[N+]([O-])=O ZWWCURLKEXEFQT-UHFFFAOYSA-N 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 238000010998 test method Methods 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 2
- WLQXPAUZYVXSNE-UHFFFAOYSA-N [Ca].O[N+]([O-])=O Chemical compound [Ca].O[N+]([O-])=O WLQXPAUZYVXSNE-UHFFFAOYSA-N 0.000 description 2
- QDWNJWYHGDYFOG-UHFFFAOYSA-N [N+](=O)(O)[O-].[Li] Chemical compound [N+](=O)(O)[O-].[Li] QDWNJWYHGDYFOG-UHFFFAOYSA-N 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 238000001938 differential scanning calorimetry curve Methods 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 230000005611 electricity Effects 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000013529 heat transfer fluid Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000012423 maintenance Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- 229910002651 NO3 Inorganic materials 0.000 description 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 238000004364 calculation method Methods 0.000 description 1
- 238000007707 calorimetry Methods 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000004590 computer program Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 239000010432 diamond Substances 0.000 description 1
- 229940000406 drug candidate Drugs 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 230000005496 eutectics Effects 0.000 description 1
- 239000003777 experimental drug Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000009533 lab test Methods 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 229910002059 quaternary alloy Inorganic materials 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 238000012795 verification Methods 0.000 description 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K5/00—Heat-transfer, heat-exchange or heat-storage materials, e.g. refrigerants; Materials for the production of heat or cold by chemical reactions other than by combustion
- C09K5/08—Materials not undergoing a change of physical state when used
- C09K5/10—Liquid materials
- C09K5/12—Molten materials, i.e. materials solid at room temperature, e.g. metals or salts
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Combustion & Propulsion (AREA)
- Thermal Sciences (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Thermotherapy And Cooling Therapy Devices (AREA)
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Cited By (22)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105419732A (zh) * | 2015-12-09 | 2016-03-23 | 西安工程大学 | 一种三元硝酸熔融盐相变储热材料的制备方法 |
CN105838337A (zh) * | 2016-04-25 | 2016-08-10 | 碧城(上海)新能源科技有限公司 | 一种高比热纳米混合熔盐传热蓄热介质及其制备方法 |
CN105907379A (zh) * | 2016-04-25 | 2016-08-31 | 碧城(上海)新能源科技有限公司 | 一种低熔点纳米混合熔盐传热蓄热介质及其制备方法 |
CN106590546A (zh) * | 2016-12-13 | 2017-04-26 | 上海铂拓能源科技有限公司 | 一种三元混合熔盐储热材料及其制备方法 |
CN106854457A (zh) * | 2016-12-22 | 2017-06-16 | 华东理工大学 | 一种多元高性能传蓄热储能混合熔盐及其制备方法 |
CN106867470A (zh) * | 2016-12-13 | 2017-06-20 | 上海铂拓能源科技有限公司 | 一种四元混合熔盐储热材料及其制备工艺 |
CN107057655A (zh) * | 2016-02-18 | 2017-08-18 | 百吉瑞(天津)新能源有限公司 | 一种混合熔盐传热蓄热工质、制备方法及其应用 |
CN107573901A (zh) * | 2016-07-05 | 2018-01-12 | 青海爱能森新材料科技有限公司 | 一种低熔点传热蓄热熔盐、制备方法及其应用 |
CN108003845A (zh) * | 2017-12-08 | 2018-05-08 | 中国科学院青海盐湖研究所 | 一种三元硝酸熔盐及其制备方法 |
CN109233751A (zh) * | 2018-11-09 | 2019-01-18 | 中国建筑材料科学研究总院有限公司 | 一种碳基复合相变储能材料及其制备方法 |
CN109821485A (zh) * | 2019-04-11 | 2019-05-31 | 湖北科技学院 | 用于动力锂电池热调控的相变储热胶囊的制备方法 |
CN109913182A (zh) * | 2019-04-11 | 2019-06-21 | 湖北科技学院 | 用于动力锂电池热调控的相变储热胶囊 |
CN110724498A (zh) * | 2019-09-27 | 2020-01-24 | 天津科技大学 | 一种高性能中高温钠基相变储能材料及其制备方法 |
CN111041525A (zh) * | 2019-12-31 | 2020-04-21 | 谷波技术(常州)有限公司 | 一种低温熔盐电镀Ni-WC复合层增强微波通讯器件表面的方法 |
CN111040739A (zh) * | 2019-12-03 | 2020-04-21 | 浙江浙能技术研究院有限公司 | 一种低熔点熔盐储热材料、制备方法和应用 |
CN111087978A (zh) * | 2020-01-15 | 2020-05-01 | 湖北科技学院 | 无机有机双功能相变微胶囊储热材料及其制法 |
CN111187597A (zh) * | 2020-01-15 | 2020-05-22 | 湖北科技学院 | 熔盐高分子复合相变微胶囊储热材料及其制法与锂电池 |
CN111995990A (zh) * | 2020-07-31 | 2020-11-27 | 华北电力大学 | 一种熔点接近室温的多元熔盐及制备方法 |
CN112143464A (zh) * | 2020-09-24 | 2020-12-29 | 中盐金坛盐化有限责任公司 | 硝酸盐系熔融盐传热蓄热介质及其制备方法 |
CN112143463A (zh) * | 2020-09-24 | 2020-12-29 | 中盐金坛盐化有限责任公司 | 硝酸纳米熔盐传热蓄热介质及其制备方法 |
CN114539987A (zh) * | 2022-02-24 | 2022-05-27 | 中煤科工集团重庆研究院有限公司 | 适用于瓦斯蓄热氧化供热工艺的熔盐配方 |
CN115558472A (zh) * | 2022-11-05 | 2023-01-03 | 北京民利储能技术有限公司 | 一种传热储能熔盐材料及其制备方法 |
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Cited By (29)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105419732B (zh) * | 2015-12-09 | 2019-03-08 | 西安工程大学 | 一种三元硝酸熔融盐相变储热材料的制备方法 |
CN105419732A (zh) * | 2015-12-09 | 2016-03-23 | 西安工程大学 | 一种三元硝酸熔融盐相变储热材料的制备方法 |
CN107057655A (zh) * | 2016-02-18 | 2017-08-18 | 百吉瑞(天津)新能源有限公司 | 一种混合熔盐传热蓄热工质、制备方法及其应用 |
CN105838337A (zh) * | 2016-04-25 | 2016-08-10 | 碧城(上海)新能源科技有限公司 | 一种高比热纳米混合熔盐传热蓄热介质及其制备方法 |
CN105907379A (zh) * | 2016-04-25 | 2016-08-31 | 碧城(上海)新能源科技有限公司 | 一种低熔点纳米混合熔盐传热蓄热介质及其制备方法 |
CN107573901A (zh) * | 2016-07-05 | 2018-01-12 | 青海爱能森新材料科技有限公司 | 一种低熔点传热蓄热熔盐、制备方法及其应用 |
CN106590546A (zh) * | 2016-12-13 | 2017-04-26 | 上海铂拓能源科技有限公司 | 一种三元混合熔盐储热材料及其制备方法 |
CN106867470A (zh) * | 2016-12-13 | 2017-06-20 | 上海铂拓能源科技有限公司 | 一种四元混合熔盐储热材料及其制备工艺 |
CN106854457A (zh) * | 2016-12-22 | 2017-06-16 | 华东理工大学 | 一种多元高性能传蓄热储能混合熔盐及其制备方法 |
CN108003845A (zh) * | 2017-12-08 | 2018-05-08 | 中国科学院青海盐湖研究所 | 一种三元硝酸熔盐及其制备方法 |
CN108003845B (zh) * | 2017-12-08 | 2020-12-04 | 中国科学院青海盐湖研究所 | 一种三元硝酸熔盐及其制备方法 |
CN109233751A (zh) * | 2018-11-09 | 2019-01-18 | 中国建筑材料科学研究总院有限公司 | 一种碳基复合相变储能材料及其制备方法 |
CN109821485A (zh) * | 2019-04-11 | 2019-05-31 | 湖北科技学院 | 用于动力锂电池热调控的相变储热胶囊的制备方法 |
CN109913182A (zh) * | 2019-04-11 | 2019-06-21 | 湖北科技学院 | 用于动力锂电池热调控的相变储热胶囊 |
CN109821485B (zh) * | 2019-04-11 | 2021-12-10 | 湖北科技学院 | 用于动力锂电池热调控的相变储热胶囊的制备方法 |
CN110724498A (zh) * | 2019-09-27 | 2020-01-24 | 天津科技大学 | 一种高性能中高温钠基相变储能材料及其制备方法 |
CN111040739A (zh) * | 2019-12-03 | 2020-04-21 | 浙江浙能技术研究院有限公司 | 一种低熔点熔盐储热材料、制备方法和应用 |
CN111040739B (zh) * | 2019-12-03 | 2021-04-27 | 浙江浙能技术研究院有限公司 | 一种低熔点熔盐储热材料、制备方法和应用 |
CN111041525A (zh) * | 2019-12-31 | 2020-04-21 | 谷波技术(常州)有限公司 | 一种低温熔盐电镀Ni-WC复合层增强微波通讯器件表面的方法 |
CN111041525B (zh) * | 2019-12-31 | 2022-02-08 | 谷波技术(常州)有限公司 | 一种低温熔盐电镀Ni-WC复合层增强微波通讯器件表面的方法 |
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