CN103896661B - A kind ofly utilize sugar refinery, grain distillery, the humic acid type fluid of yeast factory waste or SOLID ORGANIC-inorganic composite mixed fertilizer composition - Google Patents
A kind ofly utilize sugar refinery, grain distillery, the humic acid type fluid of yeast factory waste or SOLID ORGANIC-inorganic composite mixed fertilizer composition Download PDFInfo
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- CN103896661B CN103896661B CN201410031038.5A CN201410031038A CN103896661B CN 103896661 B CN103896661 B CN 103896661B CN 201410031038 A CN201410031038 A CN 201410031038A CN 103896661 B CN103896661 B CN 103896661B
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- 239000003337 fertilizer Substances 0.000 title claims abstract description 154
- 239000012530 fluid Substances 0.000 title claims abstract description 40
- QJZYHAIUNVAGQP-UHFFFAOYSA-N 3-nitrobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid Chemical compound C1C2C=CC1C(C(=O)O)C2(C(O)=O)[N+]([O-])=O QJZYHAIUNVAGQP-UHFFFAOYSA-N 0.000 title claims abstract description 32
- 239000007787 solid Substances 0.000 title claims abstract description 31
- 239000002131 composite material Substances 0.000 title claims abstract description 14
- 239000004021 humic acid Substances 0.000 title claims abstract description 11
- 240000004808 Saccharomyces cerevisiae Species 0.000 title abstract description 9
- 239000002699 waste material Substances 0.000 title abstract description 5
- 239000000203 mixture Substances 0.000 title description 32
- 238000000855 fermentation Methods 0.000 claims abstract description 73
- 230000004151 fermentation Effects 0.000 claims abstract description 73
- 239000000126 substance Substances 0.000 claims abstract description 54
- 240000008067 Cucumis sativus Species 0.000 claims abstract description 32
- 239000011573 trace mineral Substances 0.000 claims abstract description 31
- 235000013619 trace mineral Nutrition 0.000 claims abstract description 31
- 239000005776 Fenhexamid Substances 0.000 claims abstract description 30
- VDLGAVXLJYLFDH-UHFFFAOYSA-N fenhexamid Chemical compound C=1C=C(O)C(Cl)=C(Cl)C=1NC(=O)C1(C)CCCCC1 VDLGAVXLJYLFDH-UHFFFAOYSA-N 0.000 claims abstract description 30
- 235000010799 Cucumis sativus var sativus Nutrition 0.000 claims abstract description 24
- ATNHDLDRLWWWCB-AENOIHSZSA-M chlorophyll a Chemical compound C1([C@@H](C(=O)OC)C(=O)C2=C3C)=C2N2C3=CC(C(CC)=C3C)=[N+]4C3=CC3=C(C=C)C(C)=C5N3[Mg-2]42[N+]2=C1[C@@H](CCC(=O)OC\C=C(/C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)[C@H](C)C2=C5 ATNHDLDRLWWWCB-AENOIHSZSA-M 0.000 claims abstract description 24
- 229930002875 chlorophyll Natural products 0.000 claims abstract description 22
- 235000019804 chlorophyll Nutrition 0.000 claims abstract description 22
- 239000007788 liquid Substances 0.000 claims description 58
- 238000000034 method Methods 0.000 claims description 44
- 239000003795 chemical substances by application Substances 0.000 claims description 38
- 238000003756 stirring Methods 0.000 claims description 35
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 29
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 claims description 28
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical group [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 claims description 28
- 239000007921 spray Substances 0.000 claims description 21
- 229930006000 Sucrose Natural products 0.000 claims description 20
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 20
- 229960004793 sucrose Drugs 0.000 claims description 20
- 238000010792 warming Methods 0.000 claims description 16
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 15
- YYRMJZQKEFZXMX-UHFFFAOYSA-L calcium bis(dihydrogenphosphate) Chemical compound [Ca+2].OP(O)([O-])=O.OP(O)([O-])=O YYRMJZQKEFZXMX-UHFFFAOYSA-L 0.000 claims description 15
- 229910000389 calcium phosphate Inorganic materials 0.000 claims description 15
- 235000019691 monocalcium phosphate Nutrition 0.000 claims description 15
- 229910052943 magnesium sulfate Inorganic materials 0.000 claims description 14
- 235000019341 magnesium sulphate Nutrition 0.000 claims description 14
- SQQMAOCOWKFBNP-UHFFFAOYSA-L manganese(II) sulfate Chemical compound [Mn+2].[O-]S([O-])(=O)=O SQQMAOCOWKFBNP-UHFFFAOYSA-L 0.000 claims description 14
- 241000193755 Bacillus cereus Species 0.000 claims description 13
- 239000004202 carbamide Substances 0.000 claims description 13
- 229910010272 inorganic material Inorganic materials 0.000 claims description 13
- 239000002689 soil Substances 0.000 claims description 13
- XSQUKJJJFZCRTK-UHFFFAOYSA-N urea group Chemical group NC(=O)N XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 13
- 239000003415 peat Substances 0.000 claims description 12
- TVXXNOYZHKPKGW-UHFFFAOYSA-N sodium molybdate (anhydrous) Chemical compound [Na+].[Na+].[O-][Mo]([O-])(=O)=O TVXXNOYZHKPKGW-UHFFFAOYSA-N 0.000 claims description 12
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical group [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 claims description 12
- 229910000368 zinc sulfate Inorganic materials 0.000 claims description 12
- 229960001763 zinc sulfate Drugs 0.000 claims description 12
- 230000000149 penetrating effect Effects 0.000 claims description 11
- 238000009736 wetting Methods 0.000 claims description 11
- 238000010899 nucleation Methods 0.000 claims description 9
- 238000013019 agitation Methods 0.000 claims description 8
- 230000000737 periodic effect Effects 0.000 claims description 8
- -1 oleoyl methyl Sodium taurine salt Chemical class 0.000 claims description 7
- 241000219112 Cucumis Species 0.000 claims description 5
- 235000015510 Cucumis melo subsp melo Nutrition 0.000 claims description 5
- FJJCIZWZNKZHII-UHFFFAOYSA-N [4,6-bis(cyanoamino)-1,3,5-triazin-2-yl]cyanamide Chemical compound N#CNC1=NC(NC#N)=NC(NC#N)=N1 FJJCIZWZNKZHII-UHFFFAOYSA-N 0.000 claims description 5
- 239000000843 powder Substances 0.000 abstract description 30
- 239000000243 solution Substances 0.000 description 29
- 241000894006 Bacteria Species 0.000 description 16
- 239000000047 product Substances 0.000 description 15
- 230000008569 process Effects 0.000 description 14
- CZMRCDWAGMRECN-UHFFFAOYSA-N Rohrzucker Natural products OCC1OC(CO)(OC2OC(CO)C(O)C(O)C2O)C(O)C1O CZMRCDWAGMRECN-UHFFFAOYSA-N 0.000 description 9
- 230000000052 comparative effect Effects 0.000 description 9
- 210000003608 fece Anatomy 0.000 description 9
- 239000010871 livestock manure Substances 0.000 description 9
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 description 8
- 238000004140 cleaning Methods 0.000 description 8
- 238000001035 drying Methods 0.000 description 7
- 229910052700 potassium Inorganic materials 0.000 description 6
- 238000012360 testing method Methods 0.000 description 6
- PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 description 5
- 241000228245 Aspergillus niger Species 0.000 description 5
- 241000194107 Bacillus megaterium Species 0.000 description 5
- 229910019142 PO4 Inorganic materials 0.000 description 5
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 5
- 239000010452 phosphate Substances 0.000 description 5
- 239000011591 potassium Substances 0.000 description 5
- 238000012216 screening Methods 0.000 description 5
- 239000004563 wettable powder Substances 0.000 description 5
- 241000196324 Embryophyta Species 0.000 description 4
- APUPEJJSWDHEBO-UHFFFAOYSA-P ammonium molybdate Chemical compound [NH4+].[NH4+].[O-][Mo]([O-])(=O)=O APUPEJJSWDHEBO-UHFFFAOYSA-P 0.000 description 4
- 239000011609 ammonium molybdate Substances 0.000 description 4
- 235000018660 ammonium molybdate Nutrition 0.000 description 4
- 229940010552 ammonium molybdate Drugs 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 230000012010 growth Effects 0.000 description 4
- 229910001629 magnesium chloride Inorganic materials 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 description 4
- 240000006439 Aspergillus oryzae Species 0.000 description 3
- 235000002247 Aspergillus oryzae Nutrition 0.000 description 3
- 241000589941 Azospirillum Species 0.000 description 3
- 240000000111 Saccharum officinarum Species 0.000 description 3
- 235000007201 Saccharum officinarum Nutrition 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 3
- 230000008635 plant growth Effects 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 241000222122 Candida albicans Species 0.000 description 2
- 206010007134 Candida infections Diseases 0.000 description 2
- 238000009825 accumulation Methods 0.000 description 2
- 239000011230 binding agent Substances 0.000 description 2
- 201000003984 candidiasis Diseases 0.000 description 2
- 229930002868 chlorophyll a Natural products 0.000 description 2
- 229910000365 copper sulfate Inorganic materials 0.000 description 2
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- YIXJRHPUWRPCBB-UHFFFAOYSA-N magnesium nitrate Chemical compound [Mg+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O YIXJRHPUWRPCBB-UHFFFAOYSA-N 0.000 description 2
- 229910052698 phosphorus Inorganic materials 0.000 description 2
- 230000037039 plant physiology Effects 0.000 description 2
- 235000010333 potassium nitrate Nutrition 0.000 description 2
- 239000004323 potassium nitrate Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000005070 sampling Methods 0.000 description 2
- 239000011592 zinc chloride Substances 0.000 description 2
- 235000005074 zinc chloride Nutrition 0.000 description 2
- OVSKIKFHRZPJSS-UHFFFAOYSA-N 2,4-D Chemical compound OC(=O)COC1=CC=C(Cl)C=C1Cl OVSKIKFHRZPJSS-UHFFFAOYSA-N 0.000 description 1
- FRXSZNDVFUDTIR-UHFFFAOYSA-N 6-methoxy-1,2,3,4-tetrahydroquinoline Chemical compound N1CCCC2=CC(OC)=CC=C21 FRXSZNDVFUDTIR-UHFFFAOYSA-N 0.000 description 1
- 235000017060 Arachis glabrata Nutrition 0.000 description 1
- 244000105624 Arachis hypogaea Species 0.000 description 1
- 235000010777 Arachis hypogaea Nutrition 0.000 description 1
- 235000018262 Arachis monticola Nutrition 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 235000019750 Crude protein Nutrition 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 208000002720 Malnutrition Diseases 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 230000003698 anagen phase Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- ZFXVRMSLJDYJCH-UHFFFAOYSA-N calcium magnesium Chemical compound [Mg].[Ca] ZFXVRMSLJDYJCH-UHFFFAOYSA-N 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 229930002869 chlorophyll b Natural products 0.000 description 1
- NSMUHPMZFPKNMZ-VBYMZDBQSA-M chlorophyll b Chemical compound C1([C@@H](C(=O)OC)C(=O)C2=C3C)=C2N2C3=CC(C(CC)=C3C=O)=[N+]4C3=CC3=C(C=C)C(C)=C5N3[Mg-2]42[N+]2=C1[C@@H](CCC(=O)OC\C=C(/C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)[C@H](C)C2=C5 NSMUHPMZFPKNMZ-VBYMZDBQSA-M 0.000 description 1
- 238000005352 clarification Methods 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 239000002361 compost Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 235000019784 crude fat Nutrition 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000012262 fermentative production Methods 0.000 description 1
- 230000035558 fertility Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 230000034659 glycolysis Effects 0.000 description 1
- 229930182470 glycoside Natural products 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 239000003864 humus Substances 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- 239000002068 microbial inoculum Substances 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 235000018343 nutrient deficiency Nutrition 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 239000011368 organic material Substances 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 235000020232 peanut Nutrition 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 230000007480 spreading Effects 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
- 239000010902 straw Substances 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- 238000009923 sugaring Methods 0.000 description 1
- 239000006228 supernatant Substances 0.000 description 1
- 239000000375 suspending agent Substances 0.000 description 1
- 230000007306 turnover Effects 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
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- Fertilizers (AREA)
Abstract
The present invention relates to a kind of sugar refinery, grain distillery, the humic acid type fluid comprising filter mud and medium trace element of yeast factory waste or SOLID ORGANIC-inorganic composite mixed fertilizer, it comprises fertilizer and inorganic fertilizer.Wherein said fertilizer comprises filter mud fermentation thing, and described filter mud is from sugar refinery, grain distillery, Gourmet Powder Factory or yeast factory; Described inorganic fertilizer comprises weight element fertilizer and trace element fertilizer.Preferably, also suitable sterilant such as fenhexamid is contained in described Chemical Mixed Fertilizer.Described Chemical Mixed Fertilizer can effectively increase cucumber leaves chlorophyll content, but also can increase cucumber yield.
Description
Technical field
The present invention relates to fertilizer field, be specifically related to a kind ofly utilize sugar refinery, grain distillery, the humic acid type fluid of yeast factory waste or SOLID ORGANIC-inorganic composite mixed fertilizer composition.
Background technology
Filter mud is in cane sugar manufacture process, and sugarcane juice is by clarification, by the residue after pressure filter or vacuum suction filter filtration.In industry sugaring process, (sulfurous method or carbonatation process etc.) there will be a large amount of mud waste things, comprise sucrose, crude fat in these filter muds, slightly tie up the abundant organic matter such as fibre, crude protein and a large amount of beneficial element such as nitrogen, phosphorus, potassium, calcium, sulphur, magnesium, zinc, sodium, manganese, be applicable to very much being developed as fertilizer.
The way of current routine filter mud accumulation is allowed its spontaneous fermentation, or carry out solid fermentation after being mixed with organism of fermentation by filter mud.Such as, CN102746038A discloses a kind of with the humus organic material material of cane sugar filter mud fermentation, comprises following raw materials according component: filter mud, sugarcane marrow, peanut press pulp, system chaff, Mai Pi and bacterium powder, standby and obtain through fermentation.CN102924133A discloses a kind of method utilizing filter mud of sugar refinery fermentative production microbiobacterial agent, get the fresh filter mud of sugar refinery milling shop, humic acids weathered coal, dry straw ash mix, make its water content control about 50%, in above-mentioned 1 ton of mixture, add soil fertility prosperous EM third generation microbiobacterial agent (living bacteria count >=10,000,000,000/milliliter) stir, ferment.CN101618982 disclose a kind of utilize microorganism to make cane sugar filter mud fermentation and add appropriate N P and K produce the method for efficient composite biological fertilizer, when preparing composite biological fertilizer, the thalline of composite biological fertilizer is inserted in the organism based on cane sugar filter mud and carry out piling rotten glycolysis.CN1055351 mono-kind makes the method for fertilizer with filtrated sludge of cane sugar refinery, wherein in the wet filter mud of undried process, directly add one or more amendments that can change wet filter mud physical behavior, and control PH, through being uniformly mixed reaction, through stacking process or without stacking process, namely making in powdery or granular organic-inorganic mixed fertilizer.CN103288522 discloses a kind of sugarcane organic-inorganic compound fertilizer special utilizing filter mud of sugar refinery to produce, and it comprises urea, calcium superphosphate or fused(calcium magnesium)phosphate, Repone K, dry filter mud; Wherein filter mud adopts accumulation natural fermentating method to become thoroughly decomposed.
But, because fresh filter mud water content is comparatively large, usually reach 60-70%, or naturally need dry and just can carry out pulverizing, fermenting through super-dry, wherein consume energy in drying process comparatively greatly, naturally dry, need larger place, and consuming time; Most important, solid fermentation is not easy filter mud to mix with organism of fermentation, once mix uneven, can cause incomplete phenomenon of fermenting, and then affect fertilizer efficiency.
The present inventor, through groping for a long time, testing, attempts carrying out liquid state fermentation to filter mud, is used in agriculture production by fermented product.Discovery surprised in experimentation, filter mud liquid state fermentation thing is equipped with other nutritive elements, such as macroelement, moderate-element and trace element etc., significantly can increase the chlorophyll content of crop leaf and increase crop tuber ratio, to time can also make crop yield.And when above-mentioned fermented product is mixed with suitable sterilant, above-mentioned effect is more obvious.Just based on above-mentioned discovery, contriver completes the present invention.
Summary of the invention
An object of the present invention is to provide a kind of the humic acid type fluid or the SOLID ORGANIC-inorganic composite mixed fertilizer that comprise filter mud and medium trace element.The present invention adopts following technical scheme.
The present invention relates to a kind of the humic acid type fluid or the SOLID ORGANIC-inorganic composite mixed fertilizer that comprise filter mud and medium trace element, it comprises following component and weight part thereof:
Fertilizer: 5-500 part
Inorganic fertilizer: 5-500 part
Wherein said fertilizer comprises filter mud fermentation thing, and described filter mud is from sugar refinery, grain distillery, Gourmet Powder Factory or yeast factory;
Described inorganic fertilizer comprises moderate-element fertilizer and trace element fertilizer.
In one embodiment of the invention, Chemical Mixed Fertilizer of the present invention is fluid Chemical Mixed Fertilizer, and described fluid Chemical Mixed Fertilizer comprises following component and weight part thereof:
Filter mud fermentation liquid: 30-80 part
Macroelement is fertile: 8-20 part
Moderate-element fertilizer: 2-6 part
Trace element fertilizer: 1-5 part
Activated humic acid: 5-10 part
Wetting and penetrating agent: 1-5 part.
Preferably, described Chemical Mixed Fertilizer comprises fenhexamid further, wherein each component and weight part as follows:
Filter mud fermentation liquid: 40-60 part
Macroelement is fertile: 10-15 part
Moderate-element fertilizer: 3-5 part
Trace element fertilizer: 2-4 part
Activated humic acid: 6-9 part
Wetting and penetrating agent: 2-3 part
Fenhexamid: 0.05-0.3 part.
Preferred, in fluid Chemical Mixed Fertilizer of the present invention, each component and weight part as follows:
Filter mud fermentation liquid: 50 parts
Macroelement is fertile: 12 parts
Moderate-element fertilizer: 4 parts
Trace element fertilizer: 3 parts
Activated humic acid: 8 parts
Wetting and penetrating agent: 3 parts
Fenhexamid: 0.06 part.
In described formula, described filter mud from sugar refinery, grain distillery, Gourmet Powder Factory or yeast factory, preferred sugar refinery, more preferably cane sugar factory or beet-sugar factory, and described filter mud fermentation liquid obtains by the following method:
1) in fermentor tank, add water, then fermentor tank is warming up to 50-80 DEG C;
2) then, in fermentor tank, add fresh filter mud and fermenting agent successively, and stir; Wherein the weight ratio of filter mud, water and fermenting agent controls to be 100 ~ 200: 200 ~ 600: 0.5 ~ 5;
3) broth temperature is maintained 50-80 DEG C, fermentation 5-10 days, period periodic agitation fermented liquid;
4) after, fermented liquid normal temperature is left standstill 5-10 hour, collect fermented liq, abandon bottom settlings thing;
5) by concentrated at 60-80 DEG C for the fermented liq obtained, be concentrated into and collect 1/6 to 1/15 of fermented liq initial weight, stop concentrated, concentrated solution is down to normal temperature, and regulates described concentrated solution pH value to 6-8, obtain filter mud fermentation liquid;
Wherein, described fermenting agent be selected from aspergillus oryzae, aspergillus niger, bacillus cereus, bacillus megaterium, thermally candiyeast, nitrogen-fixing rhizobia, azospirillum one or more;
Preferably, described filter mud is from cane sugar factory or beet-sugar factory, and described filter mud fermentation liquid obtains by the following method:
1) in fermentor tank, add water, then fermentor tank is warming up to 60-75 DEG C;
2) then, in fermentor tank, add fresh filter mud and fermenting agent successively, and stir; Wherein the weight ratio of filter mud, water and fermenting agent controls to be 120 ~ 160: 300 ~ 500: 1 ~ 3;
3) broth temperature is maintained 60-80 DEG C, fermentation 6-9 days, period periodic agitation fermented liquid;
4) after, fermented liquid normal temperature is left standstill 6-8 hour, collect fermented liq, abandon bottom settlings thing;
5) by concentrated at 60-80 DEG C for the fermented liq obtained, be concentrated into and collect 1/8 to 1/12 of fermented liq initial weight, stop concentrated, concentrated solution is down to normal temperature, and regulates described concentrated solution pH value to 7, obtain filter mud fermentation liquid;
Wherein, described fermenting agent is bacillus cereus, thermally candiyeast and nitrogen-fixing rhizobia, and its weight ratio is 1: 1 ~ 3: 1 ~ 3
Preferred, described filter mud is from cane sugar factory, and described filter mud fermentation liquid obtains by the following method:
1) in fermentor tank, add water, then fermentor tank is warming up to 70 DEG C;
2) then, in fermentor tank, add fresh filter mud and fermenting agent successively, and stir; Wherein the weight ratio of filter mud, water and fermenting agent controls to be 140: 400: 2;
3) broth temperature is maintained 70 DEG C, ferments 8 days, period periodic agitation fermented liquid;
4) after, fermented liquid normal temperature is left standstill 8 hours, collect fermented liq, abandon bottom settlings thing;
5) by concentrated at 75 DEG C for the fermented liq obtained, be concentrated into and collect 1/10 of fermented liq initial weight, stop concentrated, concentrated solution is down to normal temperature, and regulates described concentrated solution pH value to 7, obtain filter mud fermentation liquid;
Wherein, described fermenting agent is bacillus cereus, thermally candiyeast and nitrogen-fixing rhizobia, and its weight ratio is 1: 2: 1;
In described formula, described macroelement fertilizer be selected from urea, ammonium nitrate, potassium primary phosphate, calcium superphosphate, Repone K, saltpetre one or more; Preferably, described macroelement fertilizer is urea, calcium superphosphate, Repone K, and its weight ratio is 1: 1 ~ 2: 1 ~ 2, preferably 1: 1: 2;
In described formula, described moderate-element fertilizer be selected from calcium sulfate, magnesium sulfate, magnesium chloride one or more; Preferably, described moderate-element fertilizer is calcium sulfate and magnesium sulfate, and its weight ratio is 1: 1 ~ 3, preferably 1: 3;
In described formula, described trace element fertilizer be selected from zinc sulfate, manganous sulfate, zinc chloride, copper sulfate, ammonium molybdate, Sodium orthomolybdate one or more; Preferably, described trace element fertilizer is zinc sulfate, manganous sulfate and Sodium orthomolybdate, and its weight ratio is 1: 1 ~ 3: 1 ~ 3, preferably 1: 1: 1;
In described formula, described wetting and penetrating agent be selected from penetrant t, alkyl glycoside, trisiloxanes Soxylat A 25-7, oleoyl methyl Sodium taurine salt one or more; Preferably, described wetting and penetrating agent is penetrant t, trisiloxanes Soxylat A 25-7 and oleoyl methyl Sodium taurine salt, and its weight ratio is 1: 1 ~ 2: 1 ~ 2, preferably 1: 1: 1.
In another embodiment of the invention, Chemical Mixed Fertilizer of the present invention is solid Chemical Mixed Fertilizer, and described solid Chemical Mixed Fertilizer comprises following component and weight part thereof:
Filter mud fermentation thing: 5-20 part
Macroelement is fertile: 8-20 part
Moderate-element fertilizer: 2-6 part
Trace element fertilizer: 1-5 part
Activated humic acid: 5-10 part
Peat soil: 1-5 part.
Preferably, described Chemical Mixed Fertilizer comprises fenhexamid further, wherein each component and weight part as follows:
Filter mud fermentation thing: 6-15 part
Macroelement is fertile: 10-15 part
Moderate-element fertilizer: 3-5 part
Trace element fertilizer: 2-4 part
Activated humic acid: 6-9 part
Peat soil: 2-3 part
Fenhexamid: 0.05-0.3 part.
Preferred, in solid Chemical Mixed Fertilizer of the present invention, each component and weight part as follows:
Filter mud fermentation thing: 10 parts
Macroelement is fertile: 12 parts
Moderate-element fertilizer: 4 parts
Trace element fertilizer: 3 parts
Activated humic acid: 8 parts
Peat soil: 3 parts
Fenhexamid: 0.06 part.
In described formula, described filter mud from sugar refinery, grain distillery, Gourmet Powder Factory or yeast factory, preferred sugar refinery, more preferably cane sugar factory or beet-sugar factory, and described filter mud fermentation thing obtains by the following method:
1) in fermentor tank, add water, then fermentor tank is warming up to 50-80 DEG C;
2) then, in fermentor tank, add fresh filter mud and fermenting agent successively, and stir; Wherein the weight ratio of filter mud, water and fermenting agent controls to be 100 ~ 200: 200 ~ 500: 0.5 ~ 5;
3) broth temperature is maintained 50-80 DEG C, fermentation 5-10 days, period periodic agitation fermented liquid;
4) after, fermented liquid normal temperature is left standstill 5-10 hour, collect fermented liq, abandon bottom settlings thing;
5) by concentrated until dope at 60-80 DEG C for the fermented liq obtained, concentrated dope is down to normal temperature, and regulates described dope pH value to 6-8, obtain filter mud fermentation thing;
Wherein, described fermenting agent be selected from aspergillus oryzae, aspergillus niger, bacillus cereus, bacillus megaterium, thermally candiyeast, nitrogen-fixing rhizobia, azospirillum one or more;
Preferably, described filter mud is from cane sugar factory or beet-sugar factory, and described filter mud fermentation thing obtains by the following method:
1) in fermentor tank, add water, then fermentor tank is warming up to 60-75 DEG C;
2) then, in fermentor tank, add fresh filter mud and fermenting agent successively, and stir; Wherein the weight ratio of filter mud, water and fermenting agent controls to be 120 ~ 160: 250 ~ 400: 1 ~ 3;
3) broth temperature is maintained 60-80 DEG C, fermentation 6-9 days, period periodic agitation fermented liquid;
4) after, fermented liquid normal temperature is left standstill 6-8 hour, collect fermented liq, abandon bottom settlings thing;
5) by concentrated until dope at 60-80 DEG C for the fermented liq obtained, concentrated dope is down to normal temperature, and regulates described dope pH value to 6-8, obtain filter mud fermentation thing;
Wherein, described fermenting agent is bacillus cereus, thermally candiyeast and nitrogen-fixing rhizobia, and its weight ratio is 1: 1 ~ 3: 1 ~ 3;
Preferred, described filter mud is from cane sugar factory, and described filter mud fermentation thing obtains by the following method:
1) in fermentor tank, add water, then fermentor tank is warming up to 70 DEG C;
2) then, in fermentor tank, add fresh filter mud and fermenting agent successively, and stir; Wherein the weight ratio of filter mud, water and fermenting agent controls to be 150: 300: 2;
3) broth temperature is maintained 70 DEG C, ferments 8 days, period periodic agitation fermented liquid;
4) after, fermented liquid normal temperature is left standstill 8 hours, collect fermented liq, abandon bottom settlings thing;
5) by concentrated until dope at 75 DEG C for the fermented liq obtained, concentrated dope is down to normal temperature, and regulates described dope pH value to 6-8, obtain filter mud fermentation thing;
Wherein, described fermenting agent is bacillus cereus, thermally candiyeast and nitrogen-fixing rhizobia, and its weight ratio is 1: 2: 1;
In described formula, described macroelement fertilizer be selected from urea, ammonium nitrate, potassium primary phosphate, calcium superphosphate, Repone K, saltpetre one or more; Preferably, described macroelement fertilizer is urea, calcium superphosphate, Repone K, and its weight ratio is 1: 1 ~ 2: 1 ~ 2, preferably 1: 1: 2;
In described formula, described moderate-element fertilizer be selected from calcium sulfate, magnesium sulfate, magnesium chloride one or more; Preferably, described moderate-element fertilizer is calcium sulfate and magnesium sulfate, and its weight ratio is 1: 1 ~ 3, preferably 1: 3;
In described formula, described trace element fertilizer be selected from zinc sulfate, manganous sulfate, zinc chloride, copper sulfate, ammonium molybdate, Sodium orthomolybdate one or more; Preferably, described trace element fertilizer is zinc sulfate, manganous sulfate and Sodium orthomolybdate, and its weight ratio is 1: 1 ~ 3: 1 ~ 3, preferably 1: 1: 1.
The present invention relates to the preparation method of described fluid Chemical Mixed Fertilizer on the other hand, and wherein concrete method steps is:
Step 1: prepare filter mud fermentation liquid according to the method described above;
Step 2: successively the macroelement of formula ratio fertilizer, moderate-element fertilizer, trace element fertilizer, activated humic acid, wetting and penetrating agent and optional fenhexamid are added in the filter mud fermentation liquid of formula ratio;
Step 3: the filter mud fermentation liquid of step 2 is stirred 30min under 100-1000rpm, mixes, obtains fluid Chemical Mixed Fertilizer of the present invention.
The present invention relates to the preparation method of described solid Chemical Mixed Fertilizer on the other hand, and wherein concrete method steps is:
Step 1: prepare thickness filter mud fermentation thing according to the method described above;
Step 2: take the macroelement fertilizer of formula ratio, moderate-element fertilizer, trace element fertilizer, activated humic acid and peat soil respectively, then mixes said components and porphyrize, obtains powder mixture;
Step 3: the optional powder mixture fenhexamid of formula ratio being added step 2 and obtain, and mix
Step 4: the thickness filter mud fermentation thing of formula ratio is evenly mixed in the mixture that step 3 (if being step 2 when not adding fenhexamid) obtains, obtain wet feed, containing a large amount of organic matters and tunning in wherein said thickness filter mud fermentation thing, there is certain binding property, itself has adhesive effect concurrently again as while fertilizer components, in granulation process, play the effect of binding agent simultaneously, therefore, extra binder constituents can be added; Then, described wet feed is carried out extruder grain, and carry out drying, screening etc., obtain solid-state Chemical Mixed Fertilizer of the present invention.
Another aspect of the present invention relates to a kind of method increasing crop leaf chlorophyll content and/or increase crop tuber ratio and/or increase crop yield, is specially and uses fluid of the present invention and/or solid Chemical Mixed Fertilizer to crop or its growing environment.In a preferred method of the invention, preferably use solid Chemical Mixed Fertilizer of the present invention at seeding time, mu consumption is 40-60kg; Spray fluid Chemical Mixed Fertilizer of the present invention in vegetative period, mu consumption is 3-6kg, and extension rate 15-30 doubly.
Preferably, described crop is cucumber, and described fluid Chemical Mixed Fertilizer respectively sprays 1 time with the knot melon phase of containing in 10 days after cucumber initial bloom stage respectively, and spray 2 times altogether, mu consumption is 5kg, and extension rate is 20 times.
Wherein, relative to not using crop as cucumber, use of the present invention when comprising humic acid type fluid or the solid Chemical Mixed Fertilizer of filter mud and medium trace element, obviously can increase the chlorophyll content of cucumber leaves and/or increase crop tuber ratio and/or increase crop yield.Such as, chlorophyll content can be made to increase by 3%, preferably increase by 5%, can volume increase 5%, preferably 10%, can be that crop tuber is than increase by 3%, preferably 8%.In addition, it should be noted that, when planting seeds solid Chemical Mixed Fertilizer of the present invention is used as base manure, and when crop growth period sprays fluid Chemical Mixed Fertilizer of the present invention, above-mentioned chlorophyll content, output and rhizome ratio etc. increases more obvious, therefore, use the solid Chemical Mixed Fertilizer of the present invention as base manure at seeding time, and to spray fluid Chemical Mixed Fertilizer of the present invention at crop growth period be the preferred embodiment of the present invention.
Another aspect of the present invention relates to Chemical Mixed Fertilizer of the present invention for increasing crop leaf chlorophyll content and/or the purposes increasing crop tuber ratio and/or increase crop yield, wherein uses fluid of the present invention and/or solid Chemical Mixed Fertilizer to crop or its growing environment.In a preferred method of the invention, preferably use solid Chemical Mixed Fertilizer of the present invention at seeding time, mu consumption is 40-60kg; Spray fluid Chemical Mixed Fertilizer of the present invention in vegetative period, mu consumption is 3-6kg, and extension rate 15-30 doubly.
Preferably, described crop is cucumber, and described fluid Chemical Mixed Fertilizer respectively sprays 1 time with the knot melon phase of containing in 10 days after cucumber initial bloom stage respectively, and spray 2 times altogether, mu consumption is 5kg, and extension rate is 20 times.
Wherein, relative to not using crop as cucumber, use of the present invention when comprising humic acid type fluid or the solid Chemical Mixed Fertilizer of filter mud and medium trace element, obviously can increase the chlorophyll content of cucumber leaves and/or increase crop tuber ratio and/or increase crop yield.Such as, chlorophyll content can be made to increase by 3%, preferably increase by 5%, can volume increase 5%, preferably 10%, can be that crop tuber is than increase by 3%, preferably 8%.In addition, it should be noted that, when planting seeds solid Chemical Mixed Fertilizer of the present invention is used as base manure, and when crop growth period sprays fluid Chemical Mixed Fertilizer of the present invention, above-mentioned chlorophyll content, output and rhizome ratio etc. increases more obvious, therefore, use the solid Chemical Mixed Fertilizer of the present invention as base manure at seeding time, and to spray fluid Chemical Mixed Fertilizer of the present invention at crop growth period be the preferred embodiment of the present invention.
In the present invention, the method described in " plant physiology experiment instructs (second edition) " that chlorophyll content is edited according to Chen Jianxun, press of South China Science & Engineering University publishes measures, and the wavelength of mensuration is respectively 663nm (chlorophyll a) and 645nm (chlorophyll b).
The present invention's various materials used are commercially available or hold facile.Such as, the present invention's filter mud used from sugar refinery, grain distillery, Gourmet Powder Factory or yeast factory, such as cane sugar factory or beet-sugar factory; The present invention's macroelement used is fertile, moderate-element fertilizer and trace element fertilizer, peat etc. are commercially available; Activated humic acid used is water miscible, for commercially available.The present invention's fermenting agent such as aspergillus oryzae, aspergillus niger, bacillus cereus, bacillus megaterium, thermally candiyeast, nitrogen-fixing rhizobia, azospirillum used is all that market is easy to, such as purchased from Cangzhou City fortune western beneficial micro-yield increasing fungus biotechnological formulation factory, Jiangsu Lv Ke Bioisystech Co., Ltd, red autumnal leaves bio tech ltd of hazard prevention etc., described microbial inoculum can be bacterium powder or bacterium liquid, viable bacteria content such as 50-150 hundred million/g in bacterium powder, viable bacteria content such as 50-150 hundred million/ml in bacterium liquid; Described wetting and penetrating agent is commercially available, such as can purchased from BASF, Rhodia, Mai Tu new high-tech material company limited etc.; Described fenhexamid is the former medicine of fenhexamid or its preparation, and as 50% fenhexamid wettable powder pulvis, 50% fenhexamid suspension agent etc., described preparation is commercially available.
Beneficial effect of the present invention is:
1, filter mud is carried out liquid fermenting at specified conditions, make fermentation more complete, benefit materials utilizes more abundant, and described fermented liquid can increase chlorophyll content of plant, and makes crop yield, increase crop tuber ratio etc.;
2, find to add suitable sterilant such as fenhexamid in above-mentioned fluid Chemical Mixed Fertilizer, chlorophyll content of plant can be increased further, improve crop yield simultaneously further, increase rhizome ratio;
3, the multiple nutrients material that compound of the present invention plant-growth is necessary, ensures the sufficient nutrition needed for plant-growth, avoids plant-growth nutritional deficiency.
Embodiment
For a better understanding of the present invention, explain explanation further by way of example below, but the present invention is not restricted to this.
Embodiment 1
Take the fresh filter mud of 140kg cane sugar factory, 2kg zymophyte powder (wherein bacillus cereus 0.5kg, thermally candiyeast 1kg, nitrogen-fixing rhizobia 0.5kg, and viable bacteria content is greater than 10,000,000,000/g) is for subsequent use.
Cleaning fermentor tank, and 400kg water is added in fermentor tank, then fermentor tank is warming up to 70 DEG C; Afterwards, in fermentor tank, add load weighted fresh filter mud and zymophyte powder successively, and stir; Then ferment to filter mud, wherein broth temperature maintains 70 DEG C, continuing fermentation 8 days, within every 0.5 day, stirs once.
After having fermented, fermented liquid normal temperature is left standstill 8 hours, collect fermented liq, abandon bottom settlings thing; And by concentrated at 75 DEG C for the fermented liq obtained, be concentrated into about 45kg, now stop concentrated, concentrated solution is down to normal temperature, and regulates described concentrated solution pH value to 7, obtain filter mud fermentation liquid, about 45kg.
Take above-mentioned filter mud fermentation liquid 25kg, then add urea 1.5kg, calcium superphosphate 1.5kg, Repone K 3kg, calcium sulfate 0.5kg, magnesium sulfate 1.5kg, zinc sulfate 0.5kg, manganous sulfate 0.5kg, Sodium orthomolybdate 0.5kg, activated humic acid 4kg, penetrant t 0.5kg, trisiloxanes Soxylat A 25-7 0.5kg, oleoyl methyl Sodium taurine salt 0.5kg while stirring wherein.Then described fermented liquid is continued under 150rpm to stir 30min, make it mix, obtain fluid Chemical Mixed Fertilizer of the present invention.
Embodiment 2.
Take the fresh filter mud of 140kg cane sugar factory, 2kg zymophyte powder (wherein bacillus cereus 0.5kg, thermally candiyeast 1kg, nitrogen-fixing rhizobia 0.5kg, and viable bacteria content is greater than 10,000,000,000/g) is for subsequent use.
Cleaning fermentor tank, and 400kg water is added in fermentor tank, then fermentor tank is warming up to 70 DEG C; Afterwards, in fermentor tank, add load weighted fresh filter mud and zymophyte powder successively, and stir; Then ferment to filter mud, wherein broth temperature maintains 70 DEG C, continuing fermentation 8 days, within every 0.5 day, stirs once.
After having fermented, fermented liquid normal temperature is left standstill 8 hours, collect fermented liq, abandon bottom settlings thing; And by concentrated at 75 DEG C for the fermented liq obtained, be concentrated into about 45kg, now stop concentrated, concentrated solution is down to normal temperature, and regulates described concentrated solution pH value to 7, obtain filter mud fermentation liquid, about 45kg.
Take above-mentioned filter mud fermentation liquid 25kg, then add urea 1.5kg, calcium superphosphate 1.5kg, Repone K 3kg, calcium sulfate 0.5kg, magnesium sulfate 1.5kg, zinc sulfate 0.5kg, manganous sulfate 0.5kg, Sodium orthomolybdate 0.5kg, activated humic acid 4kg, penetrant t 0.5kg, trisiloxanes Soxylat A 25-7 0.5kg, oleoyl methyl Sodium taurine salt 0.5kg, 50% fenhexamid wettable powder 60g (amounting to activeconstituents 30g) while stirring wherein.Then described fermented liquid is continued under 150rpm to stir 30min, make it mix, obtain fluid Chemical Mixed Fertilizer of the present invention.
Embodiment 3
Take the fresh filter mud of 200kg beet-sugar factory, 4kg zymophyte powder (wherein aspergillus niger 2kg, bacillus megaterium 2kg, and viable bacteria content is greater than 10,000,000,000/g) is for subsequent use.
Cleaning fermentor tank, and 500kg water is added in fermentor tank, then fermentor tank is warming up to 60 DEG C; Afterwards, in fermentor tank, add load weighted fresh filter mud and zymophyte powder successively, and stir; Then ferment to filter mud, wherein broth temperature maintains 60 DEG C, continuing fermentation 10 days, within every 0.5 day, stirs once.
After having fermented, fermented liquid normal temperature is left standstill 10 hours, collect fermented liq, abandon bottom settlings thing; And by concentrated at 85 DEG C for the fermented liq obtained, be concentrated into about 50kg, now stop concentrated, concentrated solution is down to normal temperature, and regulates described concentrated solution pH value to 7, obtain filter mud fermentation liquid, about 50kg.
Take above-mentioned filter mud fermentation liquid 30kg, then add ammonium nitrate 4.5kg, potassium primary phosphate 4.5kg, magnesium chloride 3kg, manganous sulfate 1kg, ammonium molybdate 1.5kg, activated humic acid 4kg, trisiloxanes Soxylat A 25-7 1kg, penetrant t 1kg while stirring wherein.Then described fermented liquid is continued under 150rpm to stir 30min, make it mix, obtain fluid Chemical Mixed Fertilizer of the present invention.
Embodiment 4
Take the fresh filter mud of 200kg beet-sugar factory, 4kg zymophyte powder (wherein aspergillus niger 2kg, bacillus megaterium 2kg, and viable bacteria content is greater than 10,000,000,000/g) is for subsequent use.
Cleaning fermentor tank, and 500kg water is added in fermentor tank, then fermentor tank is warming up to 60 DEG C; Afterwards, in fermentor tank, add load weighted fresh filter mud and zymophyte powder successively, and stir; Then ferment to filter mud, wherein broth temperature maintains 60 DEG C, continuing fermentation 10 days, within every 0.5 day, stirs once.
After having fermented, fermented liquid normal temperature is left standstill 10 hours, collect fermented liq, abandon bottom settlings thing; And by concentrated at 85 DEG C for the fermented liq obtained, be concentrated into about 50kg, now stop concentrated, concentrated solution is down to normal temperature, and regulates described concentrated solution pH value to 7, obtain filter mud fermentation liquid, about 50kg.
Take above-mentioned filter mud fermentation liquid 30kg, then add ammonium nitrate 4.5kg, potassium primary phosphate 4.5kg, magnesium chloride 3kg, manganous sulfate 1kg, ammonium molybdate 1.5kg, activated humic acid 4kg, trisiloxanes Soxylat A 25-7 1kg, penetrant t 1kg, 50% fenhexamid wettable powder 100g (amounting to activeconstituents 50g) while stirring wherein.Then described fermented liquid is continued under 150rpm to stir 30min, make it mix, obtain fluid Chemical Mixed Fertilizer of the present invention.
Embodiment 5
Take the fresh filter mud of 150kg cane sugar factory, 2kg zymophyte powder (wherein bacillus cereus 0.5kg, thermally candiyeast 1kg, nitrogen-fixing rhizobia 0.5kg, and viable bacteria content is greater than 10,000,000,000/g) is for subsequent use.
Cleaning fermentor tank, and 300kg water is added in fermentor tank, then fermentor tank is warming up to 70 DEG C; Afterwards, in fermentor tank, add load weighted fresh filter mud and zymophyte powder successively, and stir; Then ferment to filter mud, wherein broth temperature maintains 70 DEG C, continuing fermentation 8 days, within every 0.5 day, stirs once.
After having fermented, fermented liquid normal temperature is left standstill 8 hours, collect fermented liq, abandon bottom settlings thing; And the fermented liq obtained is concentrated into concentrated solution at 75 DEG C is thick, now stops concentrated, concentrated solution is down to normal temperature, and regulates described concentrated solution pH value to 7, obtain filter mud fermentation thing, about 20kg, for subsequent use.
Take urea 3kg, calcium superphosphate 3kg, Repone K 6kg, calcium sulfate 1kg, magnesium sulfate 3kg, zinc sulfate 1kg, manganous sulfate 1kg, Sodium orthomolybdate 1kg, activated humic acid 8kg, peat soil 3kg respectively, mix and porphyrize, obtain powder mixture.
Take above-mentioned filter mud fermentation thing 10kg, be evenly mixed in mixture obtained above, obtain wet feed.Then, described wet feed is carried out extruder grain, and carry out drying, screening etc., obtain solid-state Chemical Mixed Fertilizer of the present invention.
Embodiment 6
Take the fresh filter mud of 150kg cane sugar factory, 2kg zymophyte powder (wherein bacillus cereus 0.5kg, thermally candiyeast 1kg, nitrogen-fixing rhizobia 0.5kg, and viable bacteria content is greater than 10,000,000,000/g) is for subsequent use.
Cleaning fermentor tank, and 300kg water is added in fermentor tank, then fermentor tank is warming up to 70 DEG C; Afterwards, in fermentor tank, add load weighted fresh filter mud and zymophyte powder successively, and stir; Then ferment to filter mud, wherein broth temperature maintains 70 DEG C, continuing fermentation 8 days, within every 0.5 day, stirs once.
After having fermented, fermented liquid normal temperature is left standstill 8 hours, collect fermented liq, abandon bottom settlings thing; And the fermented liq obtained is concentrated into concentrated solution at 75 DEG C is thick, now stops concentrated, concentrated solution is down to normal temperature, and regulates described concentrated solution pH value to 7, obtain filter mud fermentation thing, about 20kg, for subsequent use.
Take urea 3kg, calcium superphosphate 3kg, Repone K 6kg, calcium sulfate 1kg, magnesium sulfate 3kg, zinc sulfate 1kg, manganous sulfate 1kg, Sodium orthomolybdate 1kg, activated humic acid 8kg, peat soil 3kg respectively, mix and porphyrize, obtain powder mixture; Backward described mixture in add 120g50% fenhexamid wettable powder (amounting to activeconstituents 60g), and to mix, obtain mixture.
Take above-mentioned filter mud fermentation thing 10kg, be evenly mixed in mixture obtained above, obtain wet feed.Then, described wet feed is carried out extruder grain, and carry out drying, screening etc., obtain solid-state Chemical Mixed Fertilizer of the present invention.
Embodiment 7
Thermally candidiasis powder (viable bacteria content is greater than 10,000,000,000/g) is for subsequent use to take the fresh filter mud of 100kg beet-sugar factory, 2kg.
Cleaning fermentor tank, and 200kg water is added in fermentor tank, then fermentor tank is warming up to 80 DEG C; Afterwards, in fermentor tank, add load weighted fresh filter mud and zymophyte powder successively, and stir; Then ferment to filter mud, wherein broth temperature maintains 80 DEG C, continuing fermentation 6 days, within every 0.5 day, stirs once.
After having fermented, fermented liquid normal temperature is left standstill 6 hours, collect fermented liq, abandon bottom settlings thing; And the fermented liq obtained is concentrated into concentrated solution at 75 DEG C is thick, now stops concentrated, concentrated solution is down to normal temperature, and regulates described concentrated solution pH value to 7, obtain filter mud fermentation thing, about 15kg, for subsequent use.
Take calcium superphosphate 6kg, Repone K 6kg respectively, calcium sulfate 3kg, magnesium sulfate 4kg, activated humic acid 6 parts, peat soil 3 parts mix and porphyrize, obtain powder mixture.
Take above-mentioned filter mud fermentation thing 8kg, be evenly mixed in mixture obtained above, obtain wet feed.Then, described wet feed is carried out extruder grain, and carry out drying, screening etc., obtain solid-state Chemical Mixed Fertilizer of the present invention.
Embodiment 8
Thermally candidiasis powder (viable bacteria content is greater than 10,000,000,000/g) is for subsequent use to take the fresh filter mud of 100kg beet-sugar factory, 2kg.
Cleaning fermentor tank, and 200kg water is added in fermentor tank, then fermentor tank is warming up to 80 DEG C; Afterwards, in fermentor tank, add load weighted fresh filter mud and zymophyte powder successively, and stir; Then ferment to filter mud, wherein broth temperature maintains 80 DEG C, continuing fermentation 6 days, and often o.5 sky stirs once.
After having fermented, fermented liquid normal temperature is left standstill 6 hours, collect fermented liq, abandon bottom settlings thing; And the fermented liq obtained is concentrated into concentrated solution at 75 DEG C is thick, now stops concentrated, concentrated solution is down to normal temperature, and regulates described concentrated solution pH value to 7, obtain filter mud fermentation thing, about 15kg, for subsequent use.
Take calcium superphosphate 6kg, Repone K 6kg respectively, calcium sulfate 3kg, magnesium sulfate 4kg, activated humic acid 6 parts, peat soil 3 parts mix and porphyrize, obtain powder mixture.Backward described mixture in add 160g50% fenhexamid wettable powder (amounting to activeconstituents 80g), and to mix, obtain mixture.
Take above-mentioned filter mud fermentation thing 8kg, be evenly mixed in mixture obtained above, obtain wet feed.Then, described wet feed is carried out extruder grain, and carry out drying, screening etc., obtain solid-state Chemical Mixed Fertilizer of the present invention.
Comparative example 1
Take 500kg water, then add the fresh filter mud 200kg of cane sugar factory wherein, stir 30min, leave standstill 8 hours afterwards, disgorging, supernatant liquor is concentrated at 80 DEG C, obtain concentrated solution and be about 110kg, concentrated solution is down to normal temperature, and regulate described concentrated solution pH value to 7.Then 20kg ammonium nitrate, 7kg magnesium nitrate is added wherein.Continue after having fed in raw material to stir 30min under 150rpm, make it mix, obtain comparative fluid fertilizer, wherein fermentative processing is not carried out to filter mud.
Comparative example 2
By fresh for 300kg filter mud natural drying, to humidity 40-60%, then with 50kg activated humic acid, 80kg peat soil Homogeneous phase mixing, carry out compost treatment afterwards, place 7 days.Obtain contrasting solid fertilizer.
Test example 1 cucumber yield compares
Choose smooth open country, be divided into 1-13 Gong13Ge community, carry out respectively watering, spreading fertilizer over the fields base manure, turn over, plant cucumber (kind: Shandong cucumber No. 8) plantation afterwards.1 is seen the following form for each community fertilising situation.Wherein, if base manure, then at seeding time ploughing soil time use, mu consumption is about 50kg; If spray, then within 10 days after initial bloom stage, respectively spray 1 time with the knot melon phase of containing, wherein the amount of spraying amounts to mu consumption is at every turn 5kg, is watered dilution 20 times.Gather in the crops rear statistics each community cucumber yield, contrasted.
Table 1 respectively process cucumber yield compares
Above-mentioned data are not difficult to find out, product of the present invention is obvious relative to comparative example product effect of increasing production, such as, when using embodiment of the present invention 1-2 product (respective cell 1-2), per mu yield is respectively 5900kg, 5920kg, and when using embodiment of the present invention 5-6 product (respective cell 5-6), per mu yield is respectively 5860kg, 5875kg.Preferably, when solid Chemical Mixed Fertilizer of the present invention is used as base manure, and when the cucumber growth phase sprays fluid Chemical Mixed Fertilizer of the present invention, effect of increasing production is more obviously good, and such as the per mu yield of community 9-10 is respectively 6240kg, 6190kg.And when using comparative example 1 product, comparative example 2 product and combinationally use comparative example 1 and 2 product time (respective cell 11-13) per mu yield be only 5440kg, 5480kg and 5520kg, be starkly lower than output of the present invention.
Test example 2 cucumber leaves chlorophyll compares
Respectively process in test example 1, after second time sprays described fluid fertilizer about 10 days, application multi-point sampling method gathers each community cucumber leaves 5 leaves respectively to each process, mainly gathers plant middle and upper part healthy leaves.Then the method described in " plant physiology experiment instruct (second edition) " published according to Chen Jianxun chief editor, press of South China Science & Engineering University measures, the content of chlorophyll a, b is measured respectively at 663nm and 645nm, and then calculating the total content of blade Determination of Chlorophyll, its result is as shown in table 2 below.
Table 2 respectively process chlorophyll content compares
Above-mentioned data are not difficult to find out, relative to comparative example product, after using product of the present invention, the chlorophyll content adding cucumber leaves all in various degree, especially the fluid Chemical Mixed Fertilizer containing fenhexamid of the present invention is sprayed, such as, or use when solid Chemical Mixed Fertilizer of the present invention sprays the fluid Chemical Mixed Fertilizer containing fenhexamid of the present invention as base manure more obvious, the chlorophyll content of cell number 2,4,9,10 is respectively 2.42mg/g, 2.35mg/g, 2.45mg/g, 2.39mg/g simultaneously.That is, product of the present invention can increase cucumber leaves chlorophyll content, especially can increase the chlorophyll content of cucumber leaves after adding fenhexamid further.
Test example 3 cucumber plant rhizome frequently comparatively
For each process in test example 1, in the knot melon middle and later periods (being greater than 10 days interval apart from last fertilising), application multi-point sampling method gathers cucumber plant 5 strain of each community respectively.Afterwards plant being placed in clear water to clean, over-ground part and underground part scissors are cut off, carrying out rhizome than measuring.
Concrete measuring method is: respectively over-ground part and underground part are placed in 60 DEG C of baking ovens and dry to constant weight, by following formulae discovery rhizome ratio:
Wherein the rhizome of each process is more as shown in table 3 than data.
Table 3 respectively process rhizome compares comparatively
Above-mentioned data are not difficult to find out, relative to comparative example product, after using product of the present invention, the rhizome ratio adding cucumber plant all in various degree, use the Chemical Mixed Fertilizer increase containing fenhexamid of the present invention more obvious, especially use when the solid Chemical Mixed Fertilizer containing fenhexamid of the present invention sprays the fluid Chemical Mixed Fertilizer containing fenhexamid of the present invention as base manure simultaneously more obvious, the cucumber plant rhizome ratio of such as cell number 9,10 is respectively 0.25,0.24; The cucumber plant rhizome ratio of cell number 6,8 is respectively 0.22,0.20.That is, product of the present invention can increase the rhizome ratio of cucumber plant, especially can increase the rhizome ratio of cucumber plant after adding fenhexamid further.
Above-mentioned example is only to further explanation of the present invention, is not limitation of the invention, by the scheme simply adjusted by such scheme and then obtain, equally within the protection domain of the application.
Claims (13)
1. comprise a humic acid type fluid organic-inorganic compound mixed fertilizer for filter mud and medium trace element, it comprises following component and weight part thereof:
Filter mud fermentation liquid: 40-60 part
Macroelement is fertile: 10-15 part
Moderate-element fertilizer: 3-5 part
Trace element fertilizer: 2-4 part
Activated humic acid: 6-9 part
Wetting and penetrating agent: 2-3 part
Fenhexamid: 0.05-0.3 part
Wherein,
Described filter mud is from cane sugar factory, and described filter mud fermentation liquid obtains by the following method:
1) in fermentor tank, add water, then fermentor tank is warming up to 70 DEG C;
2) then, in fermentor tank, add fresh filter mud and fermenting agent successively, and stir; Wherein the weight ratio of filter mud, water and fermenting agent controls to be 140: 400: 2;
3) broth temperature is maintained 70 DEG C, ferments 8 days, period periodic agitation fermented liquid;
4) after, fermented liquid normal temperature is left standstill 8 hours, collect fermented liq, abandon bottom settlings thing;
5) by concentrated at 75 DEG C for the fermented liq obtained, be concentrated into and collect 1/10 of fermented liq initial weight, stop concentrated, concentrated solution is down to normal temperature, and regulates described concentrated solution pH value to 7, obtain filter mud fermentation liquid;
Described fermenting agent is bacillus cereus, thermally candiyeast and nitrogen-fixing rhizobia, and its weight ratio is 1: 2: 1;
Described macroelement fertilizer is urea, calcium superphosphate, Repone K, and its weight ratio is 1: 1 ~ 2: 1 ~ 2;
Described moderate-element fertilizer is calcium sulfate and magnesium sulfate, and its weight ratio is 1: 1 ~ 3;
Described trace element fertilizer is zinc sulfate, manganous sulfate and Sodium orthomolybdate, and its weight ratio is 1: 1 ~ 3: 1 ~ 3;
Described wetting and penetrating agent is penetrant t, trisiloxanes Soxylat A 25-7 and oleoyl methyl Sodium taurine salt, and its weight ratio is 1: 1 ~ 2: 1 ~ 2.
2. Chemical Mixed Fertilizer according to claim 1, is characterized in that, each component and weight part as follows:
Filter mud fermentation liquid: 50 parts
Macroelement is fertile: 12 parts
Moderate-element fertilizer: 4 parts
Trace element fertilizer: 3 parts
Activated humic acid: 8 parts
Wetting and penetrating agent: 3 parts
Fenhexamid: 0.06 part
Wherein,
Described macroelement fertilizer is urea, calcium superphosphate, Repone K, and its weight ratio is 1: 1: 2;
Described moderate-element fertilizer is calcium sulfate and magnesium sulfate, and its weight ratio is 1: 3;
Described trace element fertilizer is zinc sulfate, manganous sulfate and Sodium orthomolybdate, and its weight ratio is 1: 1: 1;
Described wetting and penetrating agent is penetrant t, trisiloxanes Soxylat A 25-7 and oleoyl methyl Sodium taurine salt, and its weight ratio is 1: 1: 1.
3. comprise humic acid type SOLID ORGANIC-inorganic composite mixed fertilizer of filter mud and medium trace element, it comprises following component and weight part thereof:
Filter mud fermentation thing: 6-15 part
Macroelement is fertile: 10-15 part
Moderate-element fertilizer: 3-5 part
Trace element fertilizer: 2-4 part
Activated humic acid: 6-9 part
Peat soil: 2-3 part
Fenhexamid: 0.05-0.3 part
Wherein,
Described filter mud is from cane sugar factory, and described filter mud fermentation thing obtains by the following method:
1) in fermentor tank, add water, then fermentor tank is warming up to 70 DEG C;
2) then, in fermentor tank, add fresh filter mud and fermenting agent successively, and stir; Wherein the weight ratio of filter mud, water and fermenting agent controls to be 150: 300: 2;
3) broth temperature is maintained 70 DEG C, ferments 8 days, period periodic agitation fermented liquid;
4) after, fermented liquid normal temperature is left standstill 8 hours, collect fermented liq, abandon bottom settlings thing;
5) by concentrated until dope at 75 DEG C for the fermented liq obtained, concentrated dope is down to normal temperature, and regulates described dope pH value to 6-8, obtain filter mud fermentation thing;
Described fermenting agent is bacillus cereus, thermally candiyeast and nitrogen-fixing rhizobia, and its weight ratio is 1: 2: 1;
Described macroelement fertilizer is urea, calcium superphosphate, Repone K, and its weight ratio is 1: 1 ~ 2: 1 ~ 2;
Described moderate-element fertilizer is calcium sulfate and magnesium sulfate, and its weight ratio is 1: 1 ~ 3;
Described trace element fertilizer is zinc sulfate, manganous sulfate and Sodium orthomolybdate, and its weight ratio is 1: 1 ~ 3: 1 ~ 3.
4. Chemical Mixed Fertilizer according to claim 3, is characterized in that, each component and weight part as follows:
Filter mud fermentation thing: 10 parts
Macroelement is fertile: 12 parts
Moderate-element fertilizer: 4 parts
Trace element fertilizer: 3 parts
Activated humic acid: 8 parts
Peat soil: 3 parts
Fenhexamid: 0.06 part
Wherein,
Described macroelement fertilizer is urea, calcium superphosphate, Repone K, and its weight ratio is 1: 1: 2;
Described moderate-element is calcium sulfate and magnesium sulfate, and its weight ratio is 1: 3;
Described trace element fertilizer is zinc sulfate, manganous sulfate and Sodium orthomolybdate, and its weight ratio is 1: 1: 1.
5. increase a method for crop leaf chlorophyll content, it is characterized in that, use the organic-inorganic compound mixed fertilizer described in any one of claim 1-4 to crop or its growing environment.
6. method according to claim 5, is characterized in that, uses the SOLID ORGANIC-inorganic composite mixed fertilizer described in claim 3 or 4 at seeding time, and mu consumption is 40-60kg; Spray the fluid organic-inorganic compound mixed fertilizer described in claim 1 or 2 in vegetative period, mu consumption is 3-6kg, and extension rate 15-30 doubly.
7. method according to claim 6, it is characterized in that, described crop is cucumber, and the fluid organic-inorganic compound mixed fertilizer described in claim 1 or 2 respectively sprays 1 time with the knot melon phase of containing in 10 days after cucumber initial bloom stage respectively, mu consumption is 5kg, and extension rate is 20 times.
8. increase a method for crop tuber ratio, it is characterized in that, use the organic-inorganic compound mixed fertilizer described in any one of claim 1-4 to crop or its growing environment.
9. method according to claim 8, is characterized in that, uses the SOLID ORGANIC-inorganic composite mixed fertilizer described in claim 3 or 4 at seeding time, and mu consumption is 40-60kg; Spray the fluid organic-inorganic compound mixed fertilizer described in claim 1 or 2 in vegetative period, mu consumption is 3-6kg, and extension rate 15-30 doubly.
10. the organic-inorganic compound mixed fertilizer described in any one of claim 1-4, for increasing the purposes of crop leaf chlorophyll content, is characterized in that, uses the organic-inorganic compound mixed fertilizer described in any one of claim 1-4 to crop or its growing environment.
11. purposes according to claim 10, is characterized in that, described crop is cucumber; Use the SOLID ORGANIC-inorganic composite mixed fertilizer described in claim 3 or 4 at seeding time, mu consumption is 40-60kg; Spray the fluid organic-inorganic compound mixed fertilizer described in claim 1 or 2 in vegetative period, mu consumption is 3-6kg, and extension rate 15-30 doubly.
Organic-inorganic compound mixed fertilizer described in 12. any one of claim 1-4, for increasing the purposes of crop tuber ratio, is characterized in that, uses the organic-inorganic compound mixed fertilizer described in any one of claim 1-4 to crop or its growing environment.
13. purposes according to claim 12, is characterized in that, described crop is cucumber; Use the SOLID ORGANIC-inorganic composite mixed fertilizer described in claim 3 or 4 at seeding time, mu consumption is 40-60kg; Spray the fluid organic-inorganic compound mixed fertilizer described in claim 1 or 2 in vegetative period, mu consumption is 3-6kg, and extension rate 15-30 doubly.
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CN110128213A (en) * | 2019-06-19 | 2019-08-16 | 乐斯福(明光)有限公司 | A method of liquid fertilizer is produced using beer waste yeast |
CN110172007A (en) * | 2019-07-12 | 2019-08-27 | 惠州护地农科有限公司 | A kind of water solubility refined organic fertilizer and its preparation process |
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