CN103724134B - A kind of Humic acid type organic-inorganic medicine fertilizer composition comprising subtilis and/or bacillus megaterium utilizing sugar refinery, grain distillery's waste - Google Patents
A kind of Humic acid type organic-inorganic medicine fertilizer composition comprising subtilis and/or bacillus megaterium utilizing sugar refinery, grain distillery's waste Download PDFInfo
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- CN103724134B CN103724134B CN201410006021.4A CN201410006021A CN103724134B CN 103724134 B CN103724134 B CN 103724134B CN 201410006021 A CN201410006021 A CN 201410006021A CN 103724134 B CN103724134 B CN 103724134B
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- humic acid
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- 239000003337 fertilizer Substances 0.000 title claims abstract description 128
- QJZYHAIUNVAGQP-UHFFFAOYSA-N 3-nitrobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid Chemical compound C1C2C=CC1C(C(=O)O)C2(C(O)=O)[N+]([O-])=O QJZYHAIUNVAGQP-UHFFFAOYSA-N 0.000 title claims abstract description 87
- 239000000203 mixture Substances 0.000 title claims abstract description 60
- 241000194107 Bacillus megaterium Species 0.000 title claims abstract description 48
- 239000004021 humic acid Substances 0.000 title claims abstract description 45
- 239000003814 drug Substances 0.000 title claims abstract description 44
- 239000002699 waste material Substances 0.000 title claims abstract description 42
- 230000000813 microbial effect Effects 0.000 claims abstract description 26
- 230000000844 anti-bacterial effect Effects 0.000 claims abstract description 23
- 239000003899 bactericide agent Substances 0.000 claims abstract description 23
- 239000011573 trace mineral Substances 0.000 claims abstract description 21
- 235000013619 trace mineral Nutrition 0.000 claims abstract description 20
- 239000007788 liquid Substances 0.000 claims description 82
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical group [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 claims description 42
- 239000006228 supernatant Substances 0.000 claims description 34
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 31
- 240000008042 Zea mays Species 0.000 claims description 29
- 235000002017 Zea mays subsp mays Nutrition 0.000 claims description 29
- 238000001704 evaporation Methods 0.000 claims description 24
- 230000008020 evaporation Effects 0.000 claims description 24
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 23
- 235000010333 potassium nitrate Nutrition 0.000 claims description 21
- 239000004323 potassium nitrate Substances 0.000 claims description 21
- 239000000575 pesticide Substances 0.000 claims description 19
- 238000002360 preparation method Methods 0.000 claims description 19
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical group [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims description 17
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 17
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 17
- 235000013339 cereals Nutrition 0.000 claims description 17
- 238000005352 clarification Methods 0.000 claims description 17
- 229910052748 manganese Inorganic materials 0.000 claims description 17
- 239000011572 manganese Substances 0.000 claims description 17
- 239000011701 zinc Substances 0.000 claims description 17
- 229910052725 zinc Inorganic materials 0.000 claims description 17
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 16
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 16
- 230000004913 activation Effects 0.000 claims description 16
- 229910017604 nitric acid Inorganic materials 0.000 claims description 16
- 238000012216 screening Methods 0.000 claims description 15
- 235000016383 Zea mays subsp huehuetenangensis Nutrition 0.000 claims description 12
- 238000001035 drying Methods 0.000 claims description 12
- 235000009973 maize Nutrition 0.000 claims description 12
- 238000010298 pulverizing process Methods 0.000 claims description 7
- 230000001105 regulatory effect Effects 0.000 claims description 7
- 241001122767 Theaceae Species 0.000 abstract description 20
- 239000001397 quillaja saponaria molina bark Substances 0.000 abstract description 20
- 229930182490 saponin Natural products 0.000 abstract description 20
- 150000007949 saponins Chemical class 0.000 abstract description 20
- 239000000047 product Substances 0.000 description 47
- 238000003756 stirring Methods 0.000 description 23
- 230000000052 comparative effect Effects 0.000 description 18
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 17
- 235000005822 corn Nutrition 0.000 description 17
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 16
- 238000000034 method Methods 0.000 description 16
- 239000000843 powder Substances 0.000 description 16
- 244000063299 Bacillus subtilis Species 0.000 description 15
- 235000014469 Bacillus subtilis Nutrition 0.000 description 15
- 239000007858 starting material Substances 0.000 description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 12
- 230000008569 process Effects 0.000 description 10
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 9
- 239000004563 wettable powder Substances 0.000 description 9
- 229910052742 iron Inorganic materials 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 8
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 7
- 229930006000 Sucrose Natural products 0.000 description 7
- 230000000694 effects Effects 0.000 description 7
- 229960004793 sucrose Drugs 0.000 description 7
- CZMRCDWAGMRECN-UHFFFAOYSA-N Rohrzucker Natural products OCC1OC(CO)(OC2OC(CO)C(O)C(O)C2O)C(O)C1O CZMRCDWAGMRECN-UHFFFAOYSA-N 0.000 description 6
- 230000001737 promoting effect Effects 0.000 description 6
- 238000005469 granulation Methods 0.000 description 5
- 230000003179 granulation Effects 0.000 description 5
- 239000002245 particle Substances 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 229910000389 calcium phosphate Inorganic materials 0.000 description 4
- 239000001506 calcium phosphate Substances 0.000 description 4
- 235000011010 calcium phosphates Nutrition 0.000 description 4
- 230000012010 growth Effects 0.000 description 4
- 244000005700 microbiome Species 0.000 description 4
- 239000002689 soil Substances 0.000 description 4
- 239000007921 spray Substances 0.000 description 4
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 4
- 230000009286 beneficial effect Effects 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- MKYBYDHXWVHEJW-UHFFFAOYSA-N N-[1-oxo-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propan-2-yl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(C(C)NC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 MKYBYDHXWVHEJW-UHFFFAOYSA-N 0.000 description 2
- 240000007594 Oryza sativa Species 0.000 description 2
- 235000007164 Oryza sativa Nutrition 0.000 description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 238000005056 compaction Methods 0.000 description 2
- 238000009472 formulation Methods 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 229910052698 phosphorus Inorganic materials 0.000 description 2
- 239000011574 phosphorus Substances 0.000 description 2
- 239000011591 potassium Substances 0.000 description 2
- 229910052700 potassium Inorganic materials 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 235000009566 rice Nutrition 0.000 description 2
- 238000005070 sampling Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
- 229910021536 Zeolite Inorganic materials 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 239000003905 agrochemical Substances 0.000 description 1
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000013270 controlled release Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical group O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 210000003608 fece Anatomy 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 238000003973 irrigation Methods 0.000 description 1
- 230000002262 irrigation Effects 0.000 description 1
- 239000012669 liquid formulation Substances 0.000 description 1
- 239000010871 livestock manure Substances 0.000 description 1
- 239000002609 medium Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 235000013379 molasses Nutrition 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 230000008635 plant growth Effects 0.000 description 1
- 239000003223 protective agent Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000002786 root growth Effects 0.000 description 1
- 238000009938 salting Methods 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000009923 sugaring Methods 0.000 description 1
- 239000000375 suspending agent Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 230000007306 turnover Effects 0.000 description 1
- 239000010457 zeolite Substances 0.000 description 1
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- Fertilizers (AREA)
Abstract
The present invention relates to a kind of Humic acid type organic-inorganic medicine fertilizer composition comprising subtilis and/or bacillus megaterium utilizing sugar refinery, grain distillery's waste, described fertilizer comprises activated humic acid, inorganic fertilizer, trace element fertilizer, tea saponin and microbial bactericide subtilis and/or bacillus megaterium etc., and described product obviously can promote that crop takes root, volume increase.
Description
Technical field
The present invention relates to fertilizer field, be specifically related to a kind of Humic acid type organic-inorganic medicine fertilizer composition utilizing sugar refinery, grain distillery's waste.
Background technology
Alcohol waste liquid for sugar refinery is a kind of with remaining the acid waste liquid be left after molasses prepare alcohol from the sugaring such as cane sugar factory, beet-sugar factory factory, containing a large amount of organic matters and beneficial element in such waste liquid.China discharges this waste liquid ton up to a million at present every year, has caused serious problem of environmental pollution.The main Land use systems of current this waste liquid remains direct irrigation, and on the one hand, the method for application of this extensive style is unfavorable for effective utilization of nutrition; On the other hand, due to the restriction of the aspects such as transport, this method of application is only limitted to factory's periphery; Moreover the waste liquid of directly discharge is in acid, and life-time service can cause soil compaction.
Life-time service inorganic fertilizer can cause soil compaction, and utilization rate of fertilizer reduces, polluted underground water etc.
Document CN1480430A discloses liquid fertilizer and the preparation method of the manufacture of a kind of molasses alcohol waste liquid.
CN101524089 discloses a kind of complex microorganism preparations promoting paddy growth and preparation method thereof.The complex microorganism preparations of described promotion paddy growth, it is made up of microbial strain culture 20-40 weight part and microbe carrier 60-80 weight part; Wherein, described microbial strain culture comprises subtilis, bacillus megaterium, S. cervisiae and root nodule bacterium; Described microbe carrier is zeolite, wilkinite or their mixture, described mixture promotes beneficial microorganism growth and breeding, promote rice root to the absorption of nitrogen, phosphorus, potassium and other organic matters simultaneously, promote the normal development of root system, thus promote that chemical fertilizer is used in paddy growth minimizing.
CN103288560A discloses a kind of complex microorganism rhzomorph saltings seedling protecting agent, comprise biological rhzomorph and the fertile alkaline land modifying agent of middle element, described microbiobacterial agent specifically comprises subtilis (Bacillus subtilis) and bacillus megaterium (Bacillus megaterium), the potential of hydrogen of the adjustable soil of described modifying agent, reduce saline and alkaline toxic action, regulate rice root microbial environment, accelerate the conversion of nitrogen, phosphorus, potassium and medium trace element, accelerate root growth, extraneous root, send out seedling and strong seedling.
At present, about being equipped with after carrying out special processing to alcohol waste liquid for sugar refinery, other inorganic fertilizers, trace element fertilizer, tea saponin and microbial bactericide etc. promote the volume increase of crop, especially corn, taking root has no report.The present inventor finds alcohol waste liquid for sugar refinery to carry out the obtained activated humic acid of special processing and is equipped with described component and significantly can increases crop yield, but also can promote that crop takes root, and increases crop tuber ratio.Just based on above-mentioned discovery, contriver completes the present invention.
Summary of the invention
An object of the present invention is to provide a kind of Humic acid type organic-inorganic medicine fertilizer composition comprising subtilis (Bacillus subtilis) and/or bacillus megaterium (Bacillus megaterium) utilizing sugar refinery, grain distillery's waste.In order to achieve the above object, the present invention adopts following technical scheme.
One object of the present invention relates to a kind of Humic acid type organic-inorganic medicine fertilizer composition comprising subtilis and/or bacillus megaterium utilizing sugar refinery, grain distillery's waste, and described composition comprises activated humic acid, inorganic fertilizer, trace element fertilizer, tea saponin and microbial bactericide; Wherein, described microbial bactericide is one or both in subtilis, bacillus megaterium.
The described Humic acid type organic-inorganic medicine fertilizer composition comprising subtilis and/or bacillus megaterium utilizing sugar refinery, grain distillery's waste, it is characterized in that, described medicine fertilizer composition is solid-state form or liquid form.
In one aspect of the invention, described utilizes sugar refinery, the Humic acid type organic-inorganic medicine fertilizer composition comprising subtilis and/or bacillus megaterium of grain distillery's waste is solid-state form, and the weight part of described component is:
Preferably, the weight part of described component is:
The preparation method of wherein said activated humic acid is: alcohol waste liquid for sugar refinery is left standstill clarification, obtain supernatant liquor, then described supernatant liquor is heated to 60 ~ 90 DEG C, preferably 70 ~ 80 DEG C are carried out evaporation concentration, be concentrated into 1/4 ~ 1/6 of initial weight, obtain concentrated solution, nitric acid or sulfuric acid is added in concentrated solution, the pH regulating concentrated solution is 1 ~ 4, preferably 2 ~ 3, normal temperature leaves standstill activation 12 ~ 24 hours, preferably 16 ~ 20 hours, then adding ammoniacal liquor regulates pH to be 6 ~ 8, obtain activated humic acid liquid, activated humic acid liquid is dry, pulverize, screening, obtain activated humic acid,
Described inorganic fertilizer be selected from saltpetre, Repone K, calcium phosphate one or both;
Described trace element be selected from manganese fertilizer, iron fertilizer, zinc fertilizer one or both;
Described microbial bactericide is one or both in subtilis, bacillus megaterium, and in described microbial bactericide, living spores number is 3 × 10
8~ 5 × 10
11living spores/gram, preferably 3 × 10
9~ 5 × 10
10living spores/gram.
Preferred, the weight part of described component is:
Wherein, in described activated humic acid preparation process, evaporation concentration temperature preferably 75 DEG C; Preferably alcohol waste liquid for sugar refinery is concentrated into 1/5 of initial weight; The pH of concentrated solution is preferably adjusted to 3; Normal temperature leaves standstill soak time preferably 18 hours; Preferably adding ammoniacal liquor regulates pH to be 7;
Described inorganic fertilizer is saltpetre and Repone K, and the weight ratio of the two is 1: 1;
Described trace element is manganese fertilizer and zinc fertilizer, and the weight ratio of the two is 2: 1;
Described microbial bactericide is subtilis and bacillus megaterium, and the weight ratio of the two is 3: 1, and in described subtilis, living spores number is 7 × 10
9living spores/gram, in described bacillus megaterium, living spores number is 3 × 10
10living spores/gram;
Described Humic acid type organic-inorganic medicine fertilizer composition can promote maize rooting, volume increase, such as can make corn yield increasing about more than 5%, preferably more than 10%, and make corn rhizome ratio (measuring during about 4 leaf phase) increase by more than 5% simultaneously, preferably increase by more than 10%.
In the preferred embodiment of the present invention, above-mentioned Humic acid type organic-inorganic medicine fertilizer composition comprises biotic pesticide further, and described biotic pesticide are pleocidin or ethyl pleocidin, and now, the weight part of described component is:
Preferably, the weight part of described component is:
The preparation method of wherein said activated humic acid is: alcohol waste liquid for sugar refinery is left standstill clarification, obtain supernatant liquor, then described supernatant liquor is heated to 60 ~ 90 DEG C, preferably 70 ~ 80 DEG C are carried out evaporation concentration, be concentrated into 1/4 ~ 1/6 of initial weight, obtain concentrated solution, nitric acid or sulfuric acid is added in concentrated solution, the pH regulating concentrated solution is 1 ~ 4, preferably 2 ~ 3, normal temperature leaves standstill activation 12 ~ 24 hours, preferably 16 ~ 20 hours, then adding ammoniacal liquor regulates pH to be 6 ~ 8, obtain activated humic acid liquid, activated humic acid liquid is dry, pulverize, screening, obtain activated humic acid,
Described inorganic fertilizer be selected from saltpetre, Repone K, calcium phosphate one or both;
Described trace element be selected from manganese fertilizer, iron fertilizer, zinc fertilizer one or both;
Described microbial bactericide is one or both in subtilis, bacillus megaterium, and in described microbial bactericide, living spores number is 3 × 10
8~ 5 × 10
11living spores/gram, preferably 3 × 10
9~ 5 × 10
10living spores/gram.
Biotic pesticide are pleocidin or ethyl pleocidin.
Preferred further, in described Humic acid type organic-inorganic medicine fertilizer composition, each component and weight part are:
Wherein, in described activated humic acid preparation process, evaporation concentration temperature preferably 75 DEG C; Preferably alcohol waste liquid for sugar refinery is concentrated into 1/5 of initial weight; The pH of concentrated solution is preferably adjusted to 3; Normal temperature leaves standstill soak time preferably 18 hours; Preferably adding ammoniacal liquor regulates pH to be 7;
Described inorganic fertilizer is saltpetre and Repone K, and the weight ratio of the two is 1: 1;
Described trace element is manganese fertilizer and zinc fertilizer, and the weight ratio of the two is 2: 1;
Described microbial bactericide is subtilis and bacillus megaterium, and the weight ratio of the two is 3: 1, and in described subtilis, living spores number is 7 × 10
9living spores/gram, in described bacillus megaterium, living spores number is 3 × 10
10living spores/gram;
Described biotic pesticide are pleocidin.
Described Humic acid type organic-inorganic medicine fertilizer composition can significantly promote maize rooting, volume increase, such as can make corn yield increasing about more than 10%, preferably more than 20%, and make corn rhizome ratio (measuring during about 4 leaf phase) increase by more than 10% simultaneously, preferably increase by more than 20%.That is, when add in described organic-inorganic medicine fertilizer composition biotic pesticide as pleocidin or and pleocidin time, the taking root of crop can be promoted further, increase production.
In another aspect of the present invention, described utilizes sugar refinery, the Humic acid type organic-inorganic medicine fertilizer composition comprising subtilis and/or bacillus megaterium of grain distillery's waste is liquid form, and the weight part of described component is:
Preferably, the weight part of described component is:
The preparation method of wherein said activated humic acid is: alcohol waste liquid for sugar refinery is left standstill clarification, obtain supernatant liquor, then described supernatant liquor is heated to 60 ~ 90 DEG C, preferably 70 ~ 80 DEG C carry out evaporation concentration, be concentrated into 1/4 ~ 1/6 of initial weight, obtain concentrated solution, nitric acid or sulfuric acid is added in concentrated solution, the pH regulating concentrated solution is 1 ~ 4, preferably 2 ~ 3, normal temperature leaves standstill activation 12 ~ 24 hours, preferably 16 ~ 20 hours, then adding ammoniacal liquor regulates pH to be 6 ~ 8, obtains liquid reactive humic acids;
Described inorganic fertilizer be selected from saltpetre, Repone K, calcium phosphate one or both;
Described trace element be selected from manganese fertilizer, iron fertilizer, zinc fertilizer one or both;
Described microbial bactericide is one or both in subtilis, bacillus megaterium, and in described microbial bactericide, living spores number is 3 × 10
8~ 5 × 10
11living spores/gram, preferably 3 × 10
9~ 5 × 10
10living spores/gram.
Preferred further, in described Humic acid type organic-inorganic medicine fertilizer composition, each component and weight part are:
Wherein, in described activated humic acid preparation process, evaporation concentration temperature preferably 75 DEG C; Preferably alcohol waste liquid for sugar refinery is concentrated into 1/5 of initial weight; The pH of concentrated solution is preferably adjusted to 3; Normal temperature leaves standstill soak time preferably 18 hours; Preferably adding ammoniacal liquor regulates pH to be 7;
Described inorganic fertilizer is saltpetre and Repone K, and the weight ratio of the two is 1: 1;
Described trace element is manganese fertilizer and zinc fertilizer, and the weight ratio of the two is 2: 1;
Described microbial bactericide is subtilis and bacillus megaterium, and the weight ratio of the two is 3: 1, and in described subtilis, living spores number is 7 × 10
9living spores/gram, in described bacillus megaterium, living spores number is 3 × 10
10living spores/gram;
Described Humic acid type organic-inorganic medicine fertilizer composition can promote maize rooting, volume increase, such as can make corn yield increasing about more than 5%, preferably more than 10%, and make corn rhizome ratio (measuring during about 4 leaf phase) increase by more than 5% simultaneously, preferably increase by more than 10%.
In the preferred embodiment of the present invention, described medicine fertilizer composition comprises biotic pesticide further, and described biotic pesticide are pleocidin or ethyl pleocidin, and the weight part of described component is:
Preferably, the weight part of described component is:
The preparation method of wherein said activated humic acid is: alcohol waste liquid for sugar refinery is left standstill clarification, obtain supernatant liquor, then described supernatant liquor is heated to 60 ~ 90 DEG C, preferably 70 ~ 80 DEG C carry out evaporation concentration, be concentrated into 1/4 ~ 1/6 of initial weight, obtain concentrated solution, nitric acid or sulfuric acid is added in concentrated solution, the pH regulating concentrated solution is 1 ~ 4, preferably 2 ~ 3, normal temperature leaves standstill activation 12 ~ 24 hours, preferably 16 ~ 20 hours, then adding ammoniacal liquor regulates pH to be 6 ~ 8, obtains liquid reactive humic acids;
Described inorganic fertilizer be selected from saltpetre, Repone K, calcium phosphate one or both;
Described trace element be selected from manganese fertilizer, iron fertilizer, zinc fertilizer one or both;
Described microbial bactericide is one or both in subtilis, bacillus megaterium, and in described microbial bactericide, living spores number is 3 × 10
8~ 5 × 10
11living spores/gram, preferably 3 × 10
9~ 5 × 10
10living spores/gram.
Described biotic pesticide are pleocidin or ethyl pleocidin.
Further preferred, of the present invention utilize sugar refinery, grain distillery's waste comprise in the Humic acid type organic-inorganic medicine fertilizer composition of subtilis and/or bacillus megaterium, each component and weight part are:
Wherein, in described activated humic acid preparation process, evaporation concentration temperature preferably 75 DEG C; Preferably alcohol waste liquid for sugar refinery is concentrated into 1/5 of initial weight; The pH of concentrated solution is preferably adjusted to 3; Normal temperature leaves standstill soak time preferably 18 hours; Preferably adding ammoniacal liquor regulates pH to be 7;
Described inorganic fertilizer is saltpetre and Repone K, and the weight ratio of the two is 1: 1;
Described trace element is manganese fertilizer and zinc fertilizer, and the weight ratio of the two is 2: 1;
Described microbial bactericide is subtilis and bacillus megaterium, and the weight ratio of the two is 3: 1, and in described subtilis, living spores number is 7 × 10
9living spores/gram, in described bacillus megaterium, living spores number is 3 × 10
10living spores/gram;
Described biotic pesticide are pleocidin.
Described Humic acid type organic-inorganic medicine fertilizer composition can significantly promote maize rooting, volume increase, such as can make corn yield increasing about more than 10%, preferably more than 20%, and make corn rhizome ratio (measuring during about 4 leaf phase) increase by more than 10% simultaneously, preferably increase by more than 20%.That is, when add in described organic-inorganic medicine fertilizer composition biotic pesticide as pleocidin or and pleocidin time, the taking root of crop can be promoted further, increase production.
Another object of the present invention relates to the described preparation method comprising the Humic acid type organic-inorganic medicine fertilizer composition of subtilis and/or bacillus megaterium utilizing sugar refinery, grain distillery's waste, and wherein concrete preparation method is:
(1) when the Humic acid type organic-inorganic medicine fertilizer composition described in is solid-state form:
Step 1: alcohol waste liquid for sugar refinery is left standstill clarification, obtain supernatant liquor, then described supernatant liquor is heated to 60 ~ 90 DEG C, preferably 70 ~ 80 DEG C, more preferably 75 DEG C are carried out evaporation concentration, be concentrated into 1/4 ~ 1/6 of initial weight, obtain concentrated solution, nitric acid or sulfuric acid is added in concentrated solution, the pH regulating concentrated solution is 1 ~ 4, preferably 2 ~ 3, more preferably 3, normal temperature leaves standstill activation 12 ~ 24 hours, preferably 16 ~ 20 hours, more preferably 18 hours, then adding ammoniacal liquor regulates pH to be 6 ~ 8, preferably 7, obtain activated humic acid liquid, activated humic acid liquid is dry, pulverize, screening, obtain activated humic acid,
Step 2: take described activated humic acid, inorganic fertilizer, trace element fertilizer, tea saponin, microbial bactericide and optional biotic pesticide respectively by formula rate, and mix, obtain mixture;
Step 3: add in said mixture by the adhesive solution accounting for said mixture gross weight 1-10%, carries out granulation;
Step 4: the particle obtained is carried out drying, screening, obtains described Humic acid type organic-inorganic medicine fertilizer composition;
(2) when the Humic acid type organic-inorganic medicine fertilizer composition described in is liquid form:
Step 1: alcohol waste liquid for sugar refinery is left standstill clarification, obtain supernatant liquor, then described supernatant liquor is heated to 60 ~ 90 DEG C, preferably 70 ~ 80 DEG C, more preferably 75 DEG C carry out evaporation concentration, be concentrated into 1/4 ~ 1/6 of initial weight, obtain concentrated solution, nitric acid or sulfuric acid is added in concentrated solution, regulate the pH of concentrated solution to be 1 ~ 4, preferably 2 ~ 3, more preferably 3, normal temperature leaves standstill activation 12 ~ 24 hours, preferably 16 ~ 20 hours, more preferably 18 hours, then adding ammoniacal liquor regulates pH to be 6 ~ 8, preferably 7, obtains liquid reactive humic acids;
Step 2: take described activated humic acid, inorganic fertilizer, trace element fertilizer, tea saponin, microbial bactericide, water and optional biotic pesticide respectively by formula rate, wherein: 1) inorganic fertilizer, trace element fertilizer are added in liquid reactive humic acids, and stir, obtain A liquid; 2) first tea saponin is added to the water, and stirring and dissolving, add microbial bactericide and optional biotic pesticide afterwards successively, and stir, obtain B liquid;
Step 3: add A liquid while stirring in B liquid, adds rear continuation and stirs, until form uniform liquid, obtain described Humic acid type organic-inorganic medicine fertilizer composition.
Preferably, when preparing described liquid state and solid active humic acids, wherein in step 1, evaporation concentration temperature preferably 75 DEG C; The pH of concentrated solution is preferably adjusted to 3; Normal temperature leaves standstill soak time preferably 18 hours; Preferably adding ammoniacal liquor regulates pH to be 7.
Another object of the present invention relates to the described purposes of the Humic acid type organic-inorganic medicine fertilizer composition comprising subtilis and/or bacillus megaterium in promotion crop yield utilizing sugar refinery, grain distillery's waste, especially promoting the purposes in corn yield increasing, such as, corn yield increasing about 5%, preferably 10%, more preferably more than 20% can be made.
Another object of the present invention relates to the described purposes of the Humic acid type organic-inorganic medicine fertilizer composition comprising subtilis and/or bacillus megaterium in promoting crop to take root utilizing sugar refinery, grain distillery's waste, is especially promoting the purposes in maize rooting.It significantly can increase its rhizome ratio (measuring during about 4 leaf phase), such as, increase by 5%, preferably 10%, more preferably more than 20%.
Another object of the present invention relate to describedly utilize sugar refinery, the Humic acid type organic-inorganic medicine fertilizer composition comprising subtilis and/or bacillus megaterium of grain distillery's waste promoting crop to take root and purposes in increase production, especially promoting maize rooting and application in increasing production.Such as can make corn yield increasing about 5%, preferably 10%, more preferably more than 20%, and make corn rhizome ratio (measuring during about 4 leaf phase) increase by 5%, preferably 10%, more preferably more than 20% simultaneously.
The present invention microbial bactericide such as subtilis, bacillus megaterium used is commercially available.In described bacillus subtilis starter powder, living spores number is 3 × 10
8~ 5 × 10
11living spores/gram, preferably 3 × 10
9~ 5 × 10
10living spores/gram.In the female powder of described bacillus megaterium, living spores number is 3 × 10
8~ 5 × 10
11living spores/gram, preferably 3 × 10
9~ 5 × 10
10living spores/gram.
The form of biotic pesticide used in the present invention is not particularly limited, and can be activeconstituents itself or agriculturally acceptable solid formulation such as wettable powder etc., or liquid formulation is as suspension agent etc.Such as directly can add pleocidin and pleocidin activeconstituents, or use its conventional formulation, such as 10% pleocidin wettable powder, 20% ethyl pleocidin wettable powder etc.Described activeconstituents is commercially available, and described preparation such as wettable powder also can obtain from commercially available, or uses conventional agricultural chemicals type working method self-control.
Other various raw materials used by the application are all available on market.Such as alcohol waste liquid for sugar refinery can be cane sugar factory alcohol slops or beet-sugar factory alcohol slops, can obtain from sugar refinery or grain distillery.Described inorganic fertilizer, trace element fertilizer, tea saponin etc. are commercially available.
Beneficial effect of the present invention is:
The present invention by activated humic acid that special methods is prepared and inorganic fertilizer, trace element fertilizer, tea saponin and microbial bactericide etc. used in combination, obviously can either promote crop yield, obviously can also increase the rhizome ratio of crop simultaneously, strengthen lodging resistance;
In above-mentioned organic-inorganic medicine fertilizer, add the biotic pesticide such as pleocidin, ethyl pleocidin further, crop yield can be improved further and increase crop tuber ratio.
The present invention, by Combination application such as multiple fertilizer and trace element fertilizers, overcomes the applied defect of single fertilizer, saves labor force, and will dilute each other respectively, disperse due to each component, adds somewhat to slowly-releasing, controlled-release effect.
Embodiment
In order to understand the present invention, further illustrate the present invention with embodiment below, but do not limit the present invention.
Embodiment 1
Get cane sugar factory alcohol slops 950kg, leave standstill clarification, obtain supernatant liquor, then described supernatant liquor is heated to 75 DEG C and carries out evaporation concentration, obtain concentrated solution 190kg, in concentrated solution, add nitric acid until the pH of concentrated solution is 3, normal temperature leaves standstill activation 18 hours, then adds ammoniacal liquor and regulates pH to be 7, obtain activated humic acid liquid, by the drying of activated humic acid liquid, pulverizing, screening, obtain activated humic acid, about 80kg is for subsequent use.
Take saltpetre 12.5kg and Repone K 12.5kg respectively, manganese fertilizer 2kg and zinc fertilizer 1kg, tea saponin 200g, living spores number be 7 × 109 living spores/gram bacillus subtilis starter powder 60g and living spores number be 3 × 10
10living spores/gram bacillus megaterium 20g for subsequent use.
Above-mentioned each composition is mixed, obtains mixture; And add 4kg10% amidin wherein, carry out granulation.
The particle obtained is carried out drying, screening, obtains described Humic acid type organic-inorganic medicine fertilizer composition.
Embodiment 2
Get beet-sugar factory alcohol slops 1200kg, leave standstill clarification, obtain supernatant liquor, then described supernatant liquor is heated to 85 DEG C and carries out evaporation concentration, obtain concentrated solution 240kg, in concentrated solution, add nitric acid until the pH of concentrated solution is 2, normal temperature leaves standstill activation 15 hours, then adds ammoniacal liquor and regulates pH to be 7, obtain activated humic acid liquid, by the drying of activated humic acid liquid, pulverizing, screening, obtain activated humic acid, about 100kg is for subsequent use.
Take saltpetre 20kg respectively, iron fertilizer 5kg, tea saponin 1000g, living spores number is 5 × 10
10living spores/gram bacillus subtilis starter powder 200g for subsequent use.
Above-mentioned each composition is mixed, obtains mixture; And add 7kg15% amidin wherein, carry out granulation.
The particle obtained is carried out drying, screening, obtains described Humic acid type organic-inorganic medicine fertilizer composition.
Embodiment 3
Get cane sugar factory alcohol slops 950kg, leave standstill clarification, obtain supernatant liquor, then described supernatant liquor is heated to 75 DEG C and carries out evaporation concentration, obtain concentrated solution 190kg, in concentrated solution, add nitric acid until the pH of concentrated solution is 3, normal temperature leaves standstill activation 18 hours, then adds ammoniacal liquor and regulates pH to be 7, obtain activated humic acid liquid, by the drying of activated humic acid liquid, pulverizing, screening, obtain activated humic acid, about 80kg is for subsequent use.
Take saltpetre 12.5kg and Repone K 12.5kg respectively, manganese fertilizer 2kg and zinc fertilizer 1kg, tea saponin 200g, living spores number is 7 × 10
9living spores/gram bacillus subtilis starter powder 60g and living spores number be 3 × 10
10living spores/gram bacillus megaterium 20g, 10% pleocidin wettable powder 50g (amounting to pleocidin activeconstituents 5g) is for subsequent use.
Above-mentioned each composition is mixed, obtains mixture; And add 4kg10% amidin wherein, carry out granulation.
The particle obtained is carried out drying, screening, obtains described Humic acid type organic-inorganic medicine fertilizer composition.
Embodiment 4
Get beet-sugar factory alcohol slops 1200kg, leave standstill clarification, obtain supernatant liquor, then described supernatant liquor is heated to 85 DEG C and carries out evaporation concentration, obtain concentrated solution 240kg, in concentrated solution, add nitric acid until the pH of concentrated solution is 2, normal temperature leaves standstill activation 15 hours, then adds ammoniacal liquor and regulates pH to be 7, obtain activated humic acid liquid, by the drying of activated humic acid liquid, pulverizing, screening, obtain activated humic acid, about 100kg is for subsequent use.
Take saltpetre 20kg respectively, iron fertilizer 5kg, tea saponin 1000g, living spores number is 5 × 10
10living spores/gram bacillus subtilis starter powder 200g, 20% ethyl pleocidin wettable powder 100g (amounting to pleocidin activeconstituents 20g) is for subsequent use.
Above-mentioned each composition is mixed, obtains mixture; And add 7kg15% amidin wherein, carry out granulation.
The particle obtained is carried out drying, screening, obtains described Humic acid type organic-inorganic medicine fertilizer composition.
Embodiment 5
Get cane sugar factory alcohol to give up 1000kg, leave standstill clarification, obtain supernatant liquor, then described supernatant liquor is heated to 75 DEG C and carries out evaporation concentration, obtain concentrated solution 200kg, in concentrated solution, add nitric acid until the pH of concentrated solution is 3, normal temperature leaves standstill activation 18 hours, then adding ammoniacal liquor regulates pH to be 7, and it is for subsequent use that acquisition activated humic acid liquid is about 200kg.
Take saltpetre 12.5kg and Repone K 12.5kg respectively, manganese fertilizer 2kg and zinc fertilizer 1kg, tea saponin 200g, living spores number is 7 × 10
9living spores/gram bacillus subtilis starter powder 60g and living spores number be 3 × 10
10living spores/gram bacillus megaterium 20g, water 300kg is for subsequent use.
Saltpetre, Repone K, manganese fertilizer, zinc fertilizer are added in liquid reactive humic acids, and stir, obtains A liquid;
First tea saponin is added to the water, and stirring and dissolving, add bacillus subtilis starter powder and the female powder of bacillus megaterium afterwards, and stir, obtain B liquid;
In B liquid, add A liquid while stirring, add rear continuation and stir, until form uniform liquid, obtain described Humic acid type organic-inorganic medicine fertilizer composition.
Embodiment 6
Get beet-sugar factory alcohol slops 1500kg, leave standstill clarification, obtain supernatant liquor, then described supernatant liquor is heated to 85 DEG C and carries out evaporation concentration, obtain concentrated solution 300kg, in concentrated solution, add nitric acid until the pH of concentrated solution is 2, normal temperature leaves standstill activation 15 hours, then adds ammoniacal liquor and regulates pH to be 7, obtain activated humic acid liquid, by the drying of activated humic acid liquid, pulverizing, screening, obtain activated humic acid, about 300kg is for subsequent use.
Take saltpetre 20kg respectively, iron fertilizer 5kg, tea saponin 800g, living spores number is 2 × 10
10living spores/gram bacillus subtilis starter powder 500g, water 400kg is for subsequent use.
First tea saponin is added to the water, and stirring and dissolving, add bacillus subtilis starter powder afterwards, and stir, obtain B liquid;
In B liquid, add A liquid while stirring, add rear continuation and stir, until form uniform liquid, obtain described Humic acid type organic-inorganic medicine fertilizer composition.
Embodiment 7
Get cane sugar factory alcohol to give up 1000kg, leave standstill clarification, obtain supernatant liquor, then described supernatant liquor is heated to 75 DEG C and carries out evaporation concentration, obtain concentrated solution 200kg, in concentrated solution, add nitric acid until the pH of concentrated solution is 3, normal temperature leaves standstill activation 18 hours, then adding ammoniacal liquor regulates pH to be 7, and it is for subsequent use that acquisition activated humic acid liquid is about 200kg.
Take saltpetre 12.5kg and Repone K 12.5kg respectively, manganese fertilizer 2kg and zinc fertilizer 1kg, tea saponin 200g, living spores number is 7 × 10
9living spores/gram bacillus subtilis starter powder 60g and living spores number be 3 × 10
10living spores/gram bacillus megaterium 20g, 10% pleocidin wettable powder 50g (amounting to pleocidin activeconstituents 5g), water 300kg is for subsequent use.
Saltpetre, Repone K, manganese fertilizer, zinc fertilizer are added in liquid reactive humic acids, and stir, obtains A liquid;
First tea saponin is added to the water, and stirring and dissolving, add bacillus subtilis starter powder, the female powder of bacillus megaterium and pleocidin afterwards, and stir, obtain B liquid;
In B liquid, add A liquid while stirring, add rear continuation and stir, until form uniform liquid, obtain described Humic acid type organic-inorganic medicine fertilizer composition.
Embodiment 8
Get beet-sugar factory alcohol slops 1500kg, leave standstill clarification, obtain supernatant liquor, then described supernatant liquor is heated to 85 DEG C and carries out evaporation concentration, obtain concentrated solution 300kg, in concentrated solution, add nitric acid until the pH of concentrated solution is 2, normal temperature leaves standstill activation 15 hours, then adds ammoniacal liquor and regulates pH to be 7, obtain activated humic acid liquid, by the drying of activated humic acid liquid, pulverizing, screening, obtain activated humic acid, about 300kg is for subsequent use.
Take saltpetre 20kg respectively, iron fertilizer 5kg, tea saponin 800g, living spores number is 2 × 10
10living spores/gram bacillus subtilis starter powder 500g, 20% ethyl pleocidin wettable powder 250g (amounting to pleocidin activeconstituents 50g) is for subsequent use, and water 400kg is for subsequent use.
First tea saponin is added to the water, and stirring and dissolving, add bacillus subtilis starter powder and ethyl pleocidin afterwards, and stir, obtain B liquid;
In B liquid, add A liquid while stirring, add rear continuation and stir, until form uniform liquid, obtain described Humic acid type organic-inorganic medicine fertilizer composition.
Comparative example 1
Get cane sugar factory alcohol slops 1000kg, leave standstill clarification, obtain supernatant liquor, then described supernatant liquor is heated to 80 DEG C and carries out evaporation concentration, obtain concentrated solution 300kg.
Comparative example 2
Take saltpetre 25kg respectively, Repone K 25kg, manganese fertilizer 3kg, zinc fertilizer 3kg, Homogeneous phase mixing obtains inorganic-trace element fertilizer composite fertilizer.
Comparative example 3
Living spores number is 7 × 10
9living spores/gram subtilis and living spores number be 3 × 10
10living spores/gram the product that is mixed to get with weight ratio 3: 1 of bacillus megaterium.
Comparative example 4
10% pleocidin wettable powder.
Effect example 1 Effects of Increasing Yield
Respectively the invention described above embodiment 1-8 product and comparative example 1-4 product are applied to as base manure the field plots having divided region, concrete application process is:
Embodiment of the present invention 1-4 product directly spreads fertilizer over the fields to field, and mu consumption is about 40kg/ mu;
Embodiment of the present invention 5-8 product sprays or drenches to be executed to field, and mu consumption is about 150kg/ mu;
Comparative example 1 product sprays or drenches and imposes on field, and its consumption is 200kg/ mu;
Comparative example 2 product directly spreads fertilizer over the fields to field, and mu consumption is about 40kg/ mu;
Comparative example 3 product is watered and sprays to field, extension rate about 500 times, and activeconstituents mu consumption is about 50g/ mu;
Comparative example 4 product is watered and sprays to field, extension rate about 500 times, and activeconstituents mu consumption is about 50kg/ mu;
Turn over to soil afterwards, maize planting (kind: Nongda108), control lines, apart from about 40-50cm, spacing in the rows 30-40cm, is regularly watered during plant growth, is not topdressed.Wherein identical process is carried out to each process.After results, measure the per mu yield of each process.
Wherein the per mu yield data of each process are as follows:
| Process | Fertilizer mu consumption (kg) | Corn per mu yield (jin) |
| The embodiment of the present invention 1 product | 40 | 1290 |
| The embodiment of the present invention 2 product | 40 | 1275 |
| The embodiment of the present invention 3 product | 40 | 1315 |
| The embodiment of the present invention 4 product | 40 | 1302 |
| The embodiment of the present invention 5 product | 150 | 1280 |
| The embodiment of the present invention 6 product | 150 | 1270 |
| The embodiment of the present invention 7 product | 150 | 1305 |
| The embodiment of the present invention 8 product | 150 | 1300 |
| Comparative example 1 product | 200 | 1140 |
| Comparative example 2 product | 40 | 1180 |
| Comparative example 3 product | 50(g) | 1125 |
| Comparative example 4 product | 50(g) | 1110 |
| Blank (not applying fertilizer) | - | 1100 |
Above-mentioned data are not difficult to find out, under the same conditions, the effect of increasing production relative to contrast product of product of the present invention is obvious, and such as embodiment of the present invention 1-2,5-6 product increase production obviously relative to comparative example 1-4 product and blank, increase production about 150 jin, even more; Further, in the present invention, when adding biotic pesticide, crop yield improves further, and such as embodiment 3-4 product is relative to embodiment 1-2 product volume increase 25-40 jin; Embodiment 7-8 product is relative to embodiment 5-6 product volume increase 20-40 jin.
Effect example 2 rhizome compares effect test
For each process in effect example 1, wherein when corn seedling grew to about 4 leaf phases, each process is sampled (five point sampling methods, every point sampling 3) respectively, gather the corn seedling of the 4 leaf phases that were in.Afterwards seedling being placed in clear water to clean, over-ground part and underground part scissors are cut off, carrying out rhizome than measuring.
Concrete measuring method is: respectively over-ground part and underground part are placed in 60 DEG C of baking ovens and dry to constant weight, by following formulae discovery rhizome ratio:
Wherein the rhizome of each process is as follows than data:
| Process | Rhizome ratio |
| The embodiment of the present invention 1 product | 0.68 |
| The embodiment of the present invention 2 product | 0.66 |
| The embodiment of the present invention 3 product | 0.78 |
| The embodiment of the present invention 4 product | 0.74 |
| The embodiment of the present invention 5 product | 0.66 |
| The embodiment of the present invention 6 product | 0.65 |
| The embodiment of the present invention 7 product | 0.75 |
| The embodiment of the present invention 8 product | 0.73 |
| Comparative example 1 product | 0.54 |
| Comparative example 2 product | 0.52 |
| Comparative example 3 product | 0.57 |
| Comparative example 4 product | 0.56 |
| Blank (not applying fertilizer) | 0.51 |
Be not difficult to find out by above-mentioned data, on the one hand, the rhizome ratio significantly increasing Maize Seedling relative to contrast product and blank of product of the present invention.Further, in the present invention, when adding biotic pesticide, increase crop tuber ratio further, such as embodiment 3-4 product relative to embodiment 1-2 product and embodiment 7-8 product relative to embodiment 5-6 product, the rhizome ratio adding corn in various degree all further.
Above-mentioned example is only to further explanation of the present invention, is not limitation of the invention, by the scheme simply adjusted by such scheme and then obtain, equally within the protection domain of the application.
Claims (4)
1. one kind utilizes the purposes of the Humic acid type organic-inorganic medicine fertilizer composition comprising subtilis and/or bacillus megaterium in promotion maize rooting of sugar refinery, grain distillery's waste, described medicine fertilizer composition is solid-state form, comprises following component and weight part thereof
The preparation method of wherein said activated humic acid is: alcohol waste liquid for sugar refinery is left standstill clarification, obtain supernatant liquor, then described supernatant liquor is heated to 70 ~ 80 DEG C and carries out evaporation concentration, be concentrated into 1/4 ~ 1/6 of initial weight, obtain concentrated solution, nitric acid or sulfuric acid is added in concentrated solution, the pH regulating concentrated solution is 2 ~ 3, normal temperature leaves standstill activation 16 ~ 20 hours, then adding ammoniacal liquor regulates pH to be 6 ~ 8, obtain activated humic acid liquid, by the drying of activated humic acid liquid, pulverizing, screening, obtain activated humic acid;
Described inorganic fertilizer is saltpetre and Repone K, and the weight ratio of the two is 1: 1;
Described trace element is manganese fertilizer and zinc fertilizer, and the weight ratio of the two is 2: 1;
Described microbial bactericide is subtilis and bacillus megaterium, and the weight ratio of the two is 3: 1, and in described subtilis, living spores number is 7 × 10
9living spores/gram, in described bacillus megaterium, living spores number is 3 × 10
10living spores/gram;
Described biotic pesticide are pleocidin.
2. a kind of purposes of the Humic acid type organic-inorganic medicine fertilizer composition comprising subtilis and/or bacillus megaterium in promotion maize rooting utilizing sugar refinery, grain distillery's waste according to claim 1, it is characterized in that, in described activated humic acid preparation process, evaporation concentration temperature preferably 75 DEG C; Preferably alcohol waste liquid for sugar refinery is concentrated into 1/5 of initial weight; The pH of concentrated solution is preferably adjusted to 3; Normal temperature leaves standstill soak time preferably 18 hours; Preferably adding ammoniacal liquor regulates pH to be 7.
3. one kind utilizes the purposes of the Humic acid type organic-inorganic medicine fertilizer composition comprising subtilis and/or bacillus megaterium in promotion maize rooting of sugar refinery, grain distillery's waste, described medicine fertilizer composition is liquid form, comprises following component and weight part thereof
The preparation method of wherein said activated humic acid is: alcohol waste liquid for sugar refinery is left standstill clarification, obtain supernatant liquor, then described supernatant liquor is heated to 70 ~ 80 DEG C and carries out evaporation concentration, be concentrated into 1/4 ~ 1/6 of initial weight, obtain concentrated solution, in concentrated solution, add nitric acid or sulfuric acid, the pH regulating concentrated solution is 2 ~ 3, normal temperature leaves standstill activation 16 ~ 20 hours, then adds ammoniacal liquor and regulates pH to be 6 ~ 8, obtain liquid reactive humic acids;
Described inorganic fertilizer is saltpetre and Repone K, and the weight ratio of the two is 1: 1;
Described trace element is manganese fertilizer and zinc fertilizer, and the weight ratio of the two is 2: 1;
Described microbial bactericide is subtilis and bacillus megaterium, and the weight ratio of the two is 3: 1, and in described subtilis, living spores number is 7 × 10
9living spores/gram, in described bacillus megaterium, living spores number is 3 × 10
10living spores/gram;
Described biotic pesticide are pleocidin.
4. a kind of purposes of the Humic acid type organic-inorganic medicine fertilizer composition comprising subtilis and/or bacillus megaterium in promotion maize rooting utilizing sugar refinery, grain distillery's waste according to claim 3, it is characterized in that, in described activated humic acid preparation process, evaporation concentration temperature preferably 75 DEG C; Preferably alcohol waste liquid for sugar refinery is concentrated into 1/5 of initial weight; The pH of concentrated solution is preferably adjusted to 3; Normal temperature leaves standstill soak time preferably 18 hours; Preferably adding ammoniacal liquor regulates pH to be 7.
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| CN104876719A (en) * | 2015-05-19 | 2015-09-02 | 潍坊友容实业有限公司 | Bactericidal microcapsule suspension fertilizer for saline-alkali soil and application thereof in Caryopteris clandonensis planting |
| CN104892123A (en) * | 2015-05-19 | 2015-09-09 | 潍坊友容实业有限公司 | A microcapsule suspension fertilizer having sterilizing effects for saline-alkali land and applications thereof in plantation of Chinese scholar tree |
| CN105085100A (en) * | 2015-09-22 | 2015-11-25 | 谢绪叶 | Fertilizing method for sugarcane |
| CN106946609A (en) * | 2017-03-27 | 2017-07-14 | 王连祥 | Prevent and treat biological organic water-soluble fertilizer material of crop banded sclerotial blight and preparation method thereof |
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| CN102001870A (en) * | 2010-11-11 | 2011-04-06 | 唐清池 | Inorganic-organic microbial compound fertilizer and preparation method thereof |
| CN102408275A (en) * | 2011-07-22 | 2012-04-11 | 河北九派生物科技有限公司 | Biological water flush fertilizer and application method thereof |
| CN102599151A (en) * | 2012-03-05 | 2012-07-25 | 叶长东 | Surfactant containing tea saponin, alkyl polyglucoside, and fulvic acid |
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Denomination of invention: The utility model relates to a humic acid type organic-inorganic medicine fertilizer composition containing Bacillus subtilis and / or Bacillus megaterium utilizing the wastes of sugar and alcohol factories Effective date of registration: 20200923 Granted publication date: 20150812 Pledgee: Bank of Communications Ltd. the Guangxi Zhuang Autonomous Region branch Pledgor: Ye Changdong Registration number: Y2020450000039 |
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Granted publication date: 20150812 Pledgee: Bank of Communications Ltd. the Guangxi Zhuang Autonomous Region branch Pledgor: Ye Changdong Registration number: Y2020450000039 |