CN102960852A - Light-fragrance electronic cigarette atomized smoke solution and preparation method thereof - Google Patents
Light-fragrance electronic cigarette atomized smoke solution and preparation method thereof Download PDFInfo
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- CN102960852A CN102960852A CN2012104573766A CN201210457376A CN102960852A CN 102960852 A CN102960852 A CN 102960852A CN 2012104573766 A CN2012104573766 A CN 2012104573766A CN 201210457376 A CN201210457376 A CN 201210457376A CN 102960852 A CN102960852 A CN 102960852A
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- 239000003571 electronic cigarette Substances 0.000 title claims abstract description 35
- 238000002360 preparation method Methods 0.000 title claims abstract description 20
- 239000000779 smoke Substances 0.000 title claims abstract description 11
- 239000003205 fragrance Substances 0.000 title abstract description 6
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 79
- 239000007788 liquid Substances 0.000 claims abstract description 51
- 239000003814 drug Substances 0.000 claims abstract description 49
- 239000000284 extract Substances 0.000 claims abstract description 39
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 38
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 35
- 239000000203 mixture Substances 0.000 claims abstract description 30
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 29
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 26
- 240000005250 Chrysanthemum indicum Species 0.000 claims abstract description 17
- 235000018959 Chrysanthemum indicum Nutrition 0.000 claims abstract description 17
- 244000269722 Thea sinensis Species 0.000 claims abstract description 17
- 239000008367 deionised water Substances 0.000 claims abstract description 17
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 17
- 235000009569 green tea Nutrition 0.000 claims abstract description 17
- 238000004821 distillation Methods 0.000 claims abstract description 9
- 238000000605 extraction Methods 0.000 claims abstract description 6
- 241000208125 Nicotiana Species 0.000 claims description 77
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 35
- 239000003390 Chinese drug Substances 0.000 claims description 24
- 244000242564 Osmanthus fragrans Species 0.000 claims description 15
- 235000019083 Osmanthus fragrans Nutrition 0.000 claims description 15
- 239000001771 mentha piperita Substances 0.000 claims description 15
- 238000003756 stirring Methods 0.000 claims description 15
- 235000011187 glycerol Nutrition 0.000 claims description 13
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 13
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 10
- 239000007864 aqueous solution Substances 0.000 claims description 10
- 235000010413 sodium alginate Nutrition 0.000 claims description 10
- 239000000661 sodium alginate Substances 0.000 claims description 10
- 229940005550 sodium alginate Drugs 0.000 claims description 10
- 239000002904 solvent Substances 0.000 claims description 10
- 229920001285 xanthan gum Polymers 0.000 claims description 10
- 238000002481 ethanol extraction Methods 0.000 claims description 8
- 239000000243 solution Substances 0.000 claims description 5
- 229920001817 Agar Polymers 0.000 claims description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 4
- 239000008272 agar Substances 0.000 claims description 4
- 239000005018 casein Substances 0.000 claims description 4
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 claims description 4
- 235000021240 caseins Nutrition 0.000 claims description 4
- 238000005374 membrane filtration Methods 0.000 claims description 4
- 229910052708 sodium Inorganic materials 0.000 claims description 4
- 239000011734 sodium Substances 0.000 claims description 4
- 239000002994 raw material Substances 0.000 claims description 2
- 230000000391 smoking effect Effects 0.000 abstract description 7
- 206010011224 Cough Diseases 0.000 abstract description 6
- 210000004072 lung Anatomy 0.000 abstract description 5
- 210000003800 pharynx Anatomy 0.000 abstract description 5
- 206010062717 Increased upper airway secretion Diseases 0.000 abstract description 3
- 208000026435 phlegm Diseases 0.000 abstract description 3
- 210000000621 bronchi Anatomy 0.000 abstract description 2
- 230000001105 regulatory effect Effects 0.000 abstract description 2
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 abstract 3
- 244000061176 Nicotiana tabacum Species 0.000 abstract 2
- 244000061508 Eriobotrya japonica Species 0.000 abstract 1
- 235000009008 Eriobotrya japonica Nutrition 0.000 abstract 1
- 241000935235 Fritillaria meleagris Species 0.000 abstract 1
- 235000006679 Mentha X verticillata Nutrition 0.000 abstract 1
- 235000002899 Mentha suaveolens Nutrition 0.000 abstract 1
- 235000001636 Mentha x rotundifolia Nutrition 0.000 abstract 1
- 241000333181 Osmanthus Species 0.000 abstract 1
- 235000019082 Osmanthus Nutrition 0.000 abstract 1
- 239000000796 flavoring agent Substances 0.000 abstract 1
- 235000019634 flavors Nutrition 0.000 abstract 1
- 230000007794 irritation Effects 0.000 abstract 1
- 210000003437 trachea Anatomy 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 14
- 238000001816 cooling Methods 0.000 description 9
- 238000005303 weighing Methods 0.000 description 9
- 235000019504 cigarettes Nutrition 0.000 description 6
- 238000002156 mixing Methods 0.000 description 6
- 238000010992 reflux Methods 0.000 description 6
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 4
- 239000003546 flue gas Substances 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 238000013019 agitation Methods 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 238000002386 leaching Methods 0.000 description 3
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- 208000020401 Depressive disease Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 244000246386 Mentha pulegium Species 0.000 description 1
- 235000016257 Mentha pulegium Nutrition 0.000 description 1
- 235000004357 Mentha x piperita Nutrition 0.000 description 1
- 239000008896 Opium Substances 0.000 description 1
- 208000004224 Opium Dependence Diseases 0.000 description 1
- 201000007100 Pharyngitis Diseases 0.000 description 1
- 206010036790 Productive cough Diseases 0.000 description 1
- 206010043521 Throat irritation Diseases 0.000 description 1
- 206010044302 Tracheitis Diseases 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 208000006673 asthma Diseases 0.000 description 1
- 238000000889 atomisation Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 206010006451 bronchitis Diseases 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 235000001050 hortel pimenta Nutrition 0.000 description 1
- 210000000867 larynx Anatomy 0.000 description 1
- 201000003102 mental depression Diseases 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 238000002670 nicotine replacement therapy Methods 0.000 description 1
- 229960001027 opium Drugs 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 230000002685 pulmonary effect Effects 0.000 description 1
- 210000002345 respiratory system Anatomy 0.000 description 1
- 208000023504 respiratory system disease Diseases 0.000 description 1
- 238000004088 simulation Methods 0.000 description 1
- 208000024794 sputum Diseases 0.000 description 1
- 210000003802 sputum Anatomy 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
- A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Cosmetics (AREA)
- Manufacture Of Tobacco Products (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses light-fragrance electronic cigarette atomized smoke solution and a preparation method thereof. The atomized smoke solution comprises the following components in percentage by weight: 30-45 percent of propylene glycol, 20-35 percent of glycerol, 5-15 percent of deionized water, 5-15 percent of alcohol, 15-45 percent of traditional Chinese medicine liquid, 2-5 percent of tobacco flavor, 2-6 percent of tobacco extract and 0.1-2 percent of forming agent, wherein the traditional Chinese medicine liquid is extraction liquid which is obtained by extracting traditional Chinese medicine mixture through water distillation or alcohol extraction, and the traditional Chinese medicine mixture consists of tendrilleaf fritillary bulb, mint leaf, loquat leaf, dendranthema indicum, violet, sweet-scented osmanthus and green tea. The light-fragrance electronic cigarette atomized smoke solution not only can meet the smoking demands of smokers, but also can effectively reduce irritation of smoke to tracheas, bronchi, throats and lungs of bodies, and has the efficacies of clearing heat, moistening lungs, arresting coughs, expelling phlegm, refreshing and restoring consciousness, regulating qi-flowing, resolving stagnation and the like.
Description
Technical field
The present invention relates to a kind of tobacco juice for electronic smoke and preparation method thereof, refer to particularly a kind of simple and elegant odor type electronic cigarette atomizing tobacco juice and preparation method thereof.
Background technology
Reducing tar and reducing harm is the emphasis problem of tobacco business always, in recent years, along with the pay attention to day by day of various circles of society to smoking and healthy relation, the Tobacco Control action is a lot of local rises, comprehensively the ban on opium-smoking and the opium trade appearance of rules of public arena, give cigarette market impact and the raising of cigarette quality all proposed Secretary.
The consumption pattern of cigarette mainly is that the flue gas that cigarette combustion produces carries out, and flue gas causes that easily the smoker suffers from various respiratory diseases, symptoms such as tracheitis, bronchitis, pharyngitis, coughing with a lot of sputum.In order to reduce harm of smoking, electronic cigarette was invented in China in 2005, and its Nicotine replacement therapy obtains numerous smokers' approval.Electronic cigarette is that the solution mist that will contain nicotine and essence changes into particulate, by pulmonary absorption, and the simulation smoke that spues simultaneously, and do not contain tar in the cigarette and other harmful components, also can not produce second-hand-cigarette also can not fill the air or curl up in confined space; And conventional cigarette is with tobacco leaf or tobacco ignition, has endangered simultaneously smoker and non-smoker's health.
Although but electronic cigarette can reduce harm of smoking, can't improve the discomfort of smoker's throat and lung.
Summary of the invention
The object of the invention is to overcome the deficiency of existing electronic cigarette, a kind of smoking demand that can satisfy the smoker is provided, can play the cough-relieving refreshing effect again simultaneously, increase simple and elegant odor type electronic cigarette atomizing tobacco juice of throat's comfort and preparation method thereof.
For achieving the above object, simple and elegant odor type electronic cigarette atomizing tobacco juice provided by the present invention, its component and weight percent content are: propane diols 30 ~ 45%, glycerine 20 ~ 35%, deionized water 5 ~ 15%, alcohol 5 ~ 15%, traditional Chinese medicine liquid 15 ~ 45%, flavouring essence for tobacco 2 ~ 5%, tobacco extract 2 ~ 6%, forming agent 0.1 ~ 2%, wherein, described traditional Chinese medicine liquid is the extract that the water distillation is extracted or the ethanol extraction Traditional Chinese drug mixture obtains, and the percentage by weight of each component is in the described Traditional Chinese drug mixture: Bulbus Fritillariae Cirrhosae 0.1% ~ 50%, dried peppermint leaf 0.1% ~ 50%, loguat leaf 0.1% ~ 50%, Dendranthema indicum 0.1% ~ 50%, violet 0.1% ~ 50%, sweet osmanthus 0.1% ~ 50%, green tea 0.1% ~ 50%.
Preferably, the percentage by weight of described each component of Traditional Chinese drug mixture is: Bulbus Fritillariae Cirrhosae 1% ~ 20%, dried peppermint leaf 1% ~ 20%, loguat leaf 1% ~ 20%, Dendranthema indicum 1% ~ 20%, violet 1% ~ 20%, sweet osmanthus 1% ~ 20%, green tea 1% ~ 20%.
Preferably, described forming agent is one or more the mixture in sodium alginate, agar, xanthans and the casein sodium.
In conjunction with above-mentioned preferable range, the described simple and elegant better component of odor type electronic cigarette atomizing tobacco juice and weight percent content are: propane diols 30%, glycerine 25%, deionized water 10%, alcohol 10%, traditional Chinese medicine liquid 17%, flavouring essence for tobacco 3%, tobacco extract 5%, forming agent 0.1%, wherein, described traditional Chinese medicine liquid is the extract that the water distillation is extracted or the ethanol extraction Traditional Chinese drug mixture obtains, and the percentage by weight of each component is in the described Traditional Chinese drug mixture: Bulbus Fritillariae Cirrhosae 13.3%, dried peppermint leaf 10%, loguat leaf 16.7%, Dendranthema indicum 13.3%, violet 13.3%, sweet osmanthus 16.7%, green tea 16.7%.
The present invention also provides a kind of preparation method of simple and elegant odor type electronic cigarette atomizing tobacco juice, the percentage by weight of its raw material consists of: propane diols 30 ~ 45%, glycerine 20 ~ 35%, deionized water 5 ~ 15%, alcohol 5 ~ 15%, traditional Chinese medicine liquid 15 ~ 45%, flavouring essence for tobacco 2 ~ 5%, tobacco extract 2 ~ 6%, forming agent 0.1 ~ 2%, wherein, described traditional Chinese medicine liquid is the extract that the water distillation is extracted or the ethanol extraction Traditional Chinese drug mixture obtains, and the percentage by weight of each component is in the described Traditional Chinese drug mixture: Bulbus Fritillariae Cirrhosae 0.1% ~ 50%, dried peppermint leaf 0.1% ~ 50%, loguat leaf 0.1% ~ 50%, Dendranthema indicum 0.1% ~ 50%, violet 0.1% ~ 50%, sweet osmanthus 0.1% ~ 50%, green tea 0.1% ~ 50%;
Preparation process is as follows:
1) deionized water is heated to 60 ℃, adds forming agent, stirs and continues to be heated to 85 ~ 95 ℃, forming agent is dissolved fully obtain the forming agent aqueous solution;
2) get propane diols and glycerine mixes, after then the forming agent aqueous solution being added, remain on 80 ℃ and stir and obtain forming agent solvent liquid, be incubated for subsequent use;
3) with traditional Chinese medicine liquid, flavouring essence for tobacco and tobacco extract are dissolved in the alcohol in the lump, stir to obtain Chinese medicine tobacco mixed liquor, and be for subsequent use;
4) Chinese medicine tobacco mixed liquor is poured in the forming agent solvent liquid, constantly stirred, make its temperature be down to room temperature, make simple and elegant odor type health care electronic cigarette atomizing tobacco juice.
Preferably, the percentage by weight of described each component of Traditional Chinese drug mixture is: Bulbus Fritillariae Cirrhosae 1% ~ 20%, dried peppermint leaf 1% ~ 20%, loguat leaf 1% ~ 20%, Dendranthema indicum 1% ~ 20%, violet 1% ~ 20%, sweet osmanthus 1% ~ 20%, green tea 1% ~ 20%.
Preferably, described forming agent is one or more the mixture in sodium alginate, agar, xanthans and the casein sodium.
Preferably, the preparation method of described traditional Chinese medicine liquid is: utilize 50% ~ 95% alcohol extract Traditional Chinese drug mixture, extraction time is 2 ~ 6 hours, extracts gained solution with the membrane filtration of 0.2 ~ 0.8 micron, and then reduced pressure concentration makes traditional Chinese medicine liquid.
More preferably, the preparation method of described traditional Chinese medicine liquid is: utilize 70% ~ 95% alcohol extract Traditional Chinese drug mixture, extraction time is 3 ~ 4 hours, extracts gained solution with the membrane filtration of 0.2 ~ 0.8 micron, and then reduced pressure concentration makes traditional Chinese medicine liquid.
In conjunction with above-mentioned preferable range, the described simple and elegant better component of odor type electronic cigarette atomizing tobacco juice and weight percent content are: propane diols 30%, glycerine 25%, deionized water 10%, alcohol 10%, traditional Chinese medicine liquid 17%, flavouring essence for tobacco 3%, tobacco extract 5%, forming agent 0.1%, wherein, described traditional Chinese medicine liquid is the extract that the water distillation is extracted or the ethanol extraction Traditional Chinese drug mixture obtains, and the percentage by weight of each component is in the described Traditional Chinese drug mixture: Bulbus Fritillariae Cirrhosae 13.3%, dried peppermint leaf 10%, loguat leaf 16.7%, Dendranthema indicum 13.3%, violet 13.3%, sweet osmanthus 16.7%, green tea 16.7%.
The main of forming agent in the above-mentioned atomizing tobacco juice more can be the viscosity that improves tobacco juice for electronic smoke, prevents tobacco juice in practical process, and too much the flowing in the middle of the electronic smoke atomizer of meeting causes the existence of the problems such as atomizing effect is low.Simultaneously, the viscosity that improves tobacco juice for electronic smoke also can conveniently be transported and preserve.
Beneficial effect of the present invention: the simple and elegant odor type health care electronic cigarette atomizing tobacco juice that provides, not only can satisfy smoker's smoking demand, also can effectively reduce flue gas to the stimulation of health tracheae, bronchus, larynx, lung, have clearing heat and moistening lung, cough-relieving apophlegmatic, produce refreshing effect to the mind, the effect such as regulating qi to alleviate mental depression.Wherein the adding of peppermint can be played the effect that produces refreshing effect to the mind.The effect that green tea and Dendranthema indicum not only have obvious cough-relieving, anti-inflammatory, eliminate the phlegm, relieving asthma is added in the tobacco juice, makes the flue gas exquisiteness soft, can significantly reduce side effect after the suction, alleviates the uncomfortable reaction of throat.Throat, respiratory tract to the smoker can play a protective role, and can significantly reduce the ill symptomses such as the caused cough of smoking, many phlegm, and the elegant gracefulness of fragrance, this perfume of tobacco and simple and elegant natural plants fragrance one integrated mass.
The specific embodiment
The present invention is described in further detail below in conjunction with specific embodiment.
Embodiment 1
(1) preparation of traditional Chinese medicine liquid:
At first take by weighing Bulbus Fritillariae Cirrhosae 20g, dried peppermint leaf 15g, loguat leaf 25g, Dendranthema indicum 20g, violet 20g, sweet osmanthus 25g, green tea 25g, ethanol 300ml heating with 75% is extracted, carry out cooling for reflux in the leaching process, extract is taken out in cooling behind the backflow 3h, then 75% ethanol that adds equivalent carries out the second time and extracts, and adds hot reflux 3h.Take out for the second time extract after the cooling, with extracted twice liquid mixing, filter, reduced pressure concentration obtains relative density and be the traditional Chinese medicine liquid 1 of 1.05 50ml, and is for subsequent use.
(2) simple and elegant odor type electronic cigarette atomizing tobacco juice preparation:
1. get the 10g deionized water, deionized water is heated to 60 ℃, add 0.05g sodium alginate and 0.05g xanthans, continue to add thermal agitation, be heated to 90 ℃, until sodium alginate and xanthans dissolve fully, obtain the forming agent aqueous solution 1.
2. after taking by weighing 30g propane diols and 25g glycerine and mixing, fully stir, after then the forming agent aqueous solution 1 being added, remain on 80 ℃ and stir and obtain forming agent solvent liquid 1, be incubated for subsequent use.
3. take by weighing alcohol 10g, with 17g traditional Chinese medicine liquid 1,3g flavouring essence for tobacco and 5g tobacco extract are put in the alcohol together, and stirring obtains Chinese medicine tobacco mixed liquor 1, for subsequent use.
4. Chinese medicine tobacco mixed liquor 1 is poured in the forming agent solvent liquid 1, is constantly stirred, make its slowly temperature be down to room temperature, make simple and elegant odor type electronic cigarette atomizing tobacco juice 1.
Embodiment 2
(1) preparation of traditional Chinese medicine liquid:
At first take by weighing Bulbus Fritillariae Cirrhosae 20g, dried peppermint leaf 15g, loguat leaf 25g, Dendranthema indicum 20g, violet 20g, sweet osmanthus 25g, green tea 25g, ethanol 300 ml heating with 75% is extracted, carry out cooling for reflux in the leaching process, extract is taken out in cooling behind the backflow 3h, then 75% ethanol that adds equivalent carries out the second time and extracts, and adds hot reflux 3h.Take out for the second time extract after the cooling, with extracted twice liquid mixing, filter, reduced pressure concentration obtains relative density and be the traditional Chinese medicine liquid 2 of 1.10 50ml, and is for subsequent use.
(2) simple and elegant odor type electronic cigarette atomizing tobacco juice preparation:
1. get the 10g deionized water, deionized water is heated to 60 ℃, add 0.05g sodium alginate and 0.05g xanthans, continue to add thermal agitation, be heated to 95 ℃, until sodium alginate and xanthans dissolve fully, obtain the forming agent aqueous solution 2.
2. after taking by weighing 30g propane diols and 23g glycerine and mixing, fully stir, after then the forming agent aqueous solution 2 being added, remain on 80 ℃ and stir and obtain forming agent solvent liquid 2, be incubated for subsequent use.
3. take by weighing alcohol 12g, with 18g traditional Chinese medicine liquid 2,4g flavouring essence for tobacco and 4g tobacco extract are put in the alcohol together, and stirring obtains Chinese medicine tobacco mixed liquor 2, for subsequent use.
4. Chinese medicine tobacco mixed liquor 2 is poured in the forming agent solvent liquid 2, is constantly stirred, make its slowly temperature be down to room temperature, make simple and elegant odor type electronic cigarette atomizing tobacco juice 2.
Embodiment 3
(1) preparation of traditional Chinese medicine liquid:
At first take by weighing Bulbus Fritillariae Cirrhosae 15g, dried peppermint leaf 20g, loguat leaf 20g, Dendranthema indicum 25g, violet 15g, sweet osmanthus 25g, green tea 30g, ethanol 300 ml heating with 75% is extracted, carry out cooling for reflux in the leaching process, extract is taken out in cooling behind the backflow 3h, then 75% ethanol that adds equivalent carries out the second time and extracts, and adds hot reflux 3h.Take out for the second time extract after the cooling, with extracted twice liquid mixing, filter, reduced pressure concentration obtains relative density and be the traditional Chinese medicine liquid 3 of 1.17 50ml, and is for subsequent use.
(2) simple and elegant odor type electronic cigarette atomizing tobacco juice preparation:
1. get the 10g deionized water, deionized water is heated to 60 ℃, add 0.05g sodium alginate and 0.05g xanthans, continue to add thermal agitation, be heated to 85 ℃, until sodium alginate and xanthans dissolve fully, obtain the forming agent aqueous solution 3.
2. after taking by weighing 30g propane diols and 25g glycerine and mixing, fully stir, after then the forming agent aqueous solution 3 being added, remain on 80 ℃ and stir and obtain forming agent solvent liquid 3, be incubated for subsequent use.
3. take by weighing alcohol 10g, with 17g traditional Chinese medicine liquid 3,3g flavouring essence for tobacco and 5g tobacco extract are put in the alcohol together, and stirring obtains Chinese medicine tobacco mixed liquor 3, for subsequent use.
4. Chinese medicine tobacco mixed liquor 3 is poured in the forming agent solvent liquid 3, is constantly stirred, make its slowly temperature be down to room temperature, make simple and elegant odor type electronic cigarette atomizing tobacco juice 3.
Above-described embodiment is carried out respectively effect assessment, its result such as following table:
Embodiment 1 effect assessment table
Embodiment 2 effects grading table
Embodiment 3 effect assessment tables
Above-mentioned effect assessment shows, simple and elegant odor type electronic cigarette atomizing tobacco juice provided by the invention, has tobacco aroma simple and elegant and that stereovision is abundant at smell fragrance, assorted gas is lighter, and delicate mouthfeel, Hui Tian are little to throat irritation, have preferably atomization, can realize preferably haze effect.
Claims (10)
1. simple and elegant odor type electronic cigarette atomizing tobacco juice, its component and weight percent content are: propane diols 30 ~ 45%, glycerine 20 ~ 35%, deionized water 5 ~ 15%, alcohol 5 ~ 15%, traditional Chinese medicine liquid 15 ~ 45%, flavouring essence for tobacco 2 ~ 5%, tobacco extract 2 ~ 6%, forming agent 0.1 ~ 2%, wherein, described traditional Chinese medicine liquid is the extract that the water distillation is extracted or the ethanol extraction Traditional Chinese drug mixture obtains, and the percentage by weight of each component is in the described Traditional Chinese drug mixture: Bulbus Fritillariae Cirrhosae 0.1% ~ 50%, dried peppermint leaf 0.1% ~ 50%, loguat leaf 0.1% ~ 50%, Dendranthema indicum 0.1% ~ 50%, violet 0.1% ~ 50%, sweet osmanthus 0.1% ~ 50%, green tea 0.1% ~ 50%.
2. simple and elegant odor type electronic cigarette atomizing tobacco juice according to claim 1, it is characterized in that: the percentage by weight of described each component of Traditional Chinese drug mixture is: Bulbus Fritillariae Cirrhosae 1% ~ 20%, dried peppermint leaf 1% ~ 20%, loguat leaf 1% ~ 20%, Dendranthema indicum 1% ~ 20%, violet 1% ~ 20%, sweet osmanthus 1% ~ 20%, green tea 1% ~ 20%.
3. simple and elegant odor type electronic cigarette atomizing tobacco juice according to claim 1 is characterized in that: described forming agent is one or more the mixture in sodium alginate, agar, xanthans and the casein sodium.
4. each described simple and elegant odor type electronic cigarette atomizing tobacco juice according to claim 1 ~ 3, it is characterized in that: component and the weight percent content of described simple and elegant odor type electronic cigarette atomizing tobacco juice are: propane diols 30%, glycerine 25%, deionized water 10%, alcohol 10%, traditional Chinese medicine liquid 17%, flavouring essence for tobacco 3%, tobacco extract 5%, forming agent 0.1%, wherein, described traditional Chinese medicine liquid is the extract that the water distillation is extracted or the ethanol extraction Traditional Chinese drug mixture obtains, and the percentage by weight of each component is in the described Traditional Chinese drug mixture: Bulbus Fritillariae Cirrhosae 13.3%, dried peppermint leaf 10%, loguat leaf 16.7%, Dendranthema indicum 13.3%, violet 13.3%, sweet osmanthus 16.7%, green tea 16.7%.
5. the preparation method of a simple and elegant odor type electronic cigarette atomizing tobacco juice, the percentage by weight of its raw material consists of: propane diols 30 ~ 45%, glycerine 20 ~ 35%, deionized water 5 ~ 15%, alcohol 5 ~ 15%, traditional Chinese medicine liquid 15 ~ 45%, flavouring essence for tobacco 2 ~ 5%, tobacco extract 2 ~ 6%, forming agent 0.1 ~ 2%, wherein, described traditional Chinese medicine liquid is the extract that the water distillation is extracted or the ethanol extraction Traditional Chinese drug mixture obtains, and the percentage by weight of each component is in the described Traditional Chinese drug mixture: Bulbus Fritillariae Cirrhosae 0.1% ~ 50%, dried peppermint leaf 0.1% ~ 50%, loguat leaf 0.1% ~ 50%, Dendranthema indicum 0.1% ~ 50%, violet 0.1% ~ 50%, sweet osmanthus 0.1% ~ 50%, green tea 0.1% ~ 50%;
Preparation process is as follows:
1) deionized water is heated to 60 ℃, adds forming agent, stirs and continues to be heated to 85 ~ 95 ℃, forming agent is dissolved fully obtain the forming agent aqueous solution;
2) get propane diols and glycerine mixes, after then the forming agent aqueous solution being added, remain on 80 ℃ and stir and obtain forming agent solvent liquid, be incubated for subsequent use;
The alcohol of 3) measuring, with traditional Chinese medicine liquid, flavouring essence for tobacco and tobacco extract are dissolved in the alcohol in the lump, stir to obtain Chinese medicine tobacco mixed liquor, and be for subsequent use;
4) Chinese medicine tobacco mixed liquor is poured in the forming agent solvent liquid, constantly stirred, make its temperature be down to room temperature, make simple and elegant odor type electronic cigarette atomizing tobacco juice.
6. simple and elegant odor type electronic cigarette atomizing tobacco juice according to claim 5, it is characterized in that: the percentage by weight of described each component of Traditional Chinese drug mixture is: Bulbus Fritillariae Cirrhosae 1% ~ 20%, dried peppermint leaf 1% ~ 20%, loguat leaf 1% ~ 20%, Dendranthema indicum 1% ~ 20%, violet 1% ~ 20%, sweet osmanthus 1% ~ 20%, green tea 1% ~ 20%.
7. simple and elegant odor type electronic cigarette atomizing tobacco juice according to claim 5 is characterized in that: described forming agent is one or more the mixture in sodium alginate, agar, xanthans and the casein sodium.
8. simple and elegant odor type electronic cigarette atomizing tobacco juice according to claim 5, it is characterized in that: the preparation method of described traditional Chinese medicine liquid is: utilize 50% ~ 95% alcohol extract Traditional Chinese drug mixture, extraction time is 2 ~ 6 hours, extract gained solution with the membrane filtration of 0.2 ~ 0.8 micron, then reduced pressure concentration makes relative density and is 1.02 ~ 1.20 traditional Chinese medicine liquid.
9. simple and elegant odor type health-care type electronic smoke atomizing tobacco juice according to claim 8, it is characterized in that: the preparation method of described traditional Chinese medicine liquid is: utilize 70% ~ 95% alcohol extract Traditional Chinese drug mixture, extraction time is 3 ~ 4 hours, extract gained solution with the membrane filtration of 0.2 ~ 0.8 micron, then reduced pressure concentration makes traditional Chinese medicine liquid.
10. each described simple and elegant odor type electronic cigarette atomizing tobacco juice according to claim 5 ~ 9, it is characterized in that: component and the weight percent content of described simple and elegant odor type electronic cigarette atomizing tobacco juice are: propane diols 30%, glycerine 25%, deionized water 10%, alcohol 10%, traditional Chinese medicine liquid 17%, flavouring essence for tobacco 3%, tobacco extract 5%, forming agent 0.1%, wherein, described traditional Chinese medicine liquid is the extract that the water distillation is extracted or the ethanol extraction Traditional Chinese drug mixture obtains, and the percentage by weight of each component is in the described Traditional Chinese drug mixture: Bulbus Fritillariae Cirrhosae 13.3%, dried peppermint leaf 10%, loguat leaf 16.7%, Dendranthema indicum 13.3%, violet 13.3%, sweet osmanthus 16.7%, green tea 16.7%.
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