CN102960852B - Light-fragrance electronic cigarette atomized smoke solution and preparation method thereof - Google Patents
Light-fragrance electronic cigarette atomized smoke solution and preparation method thereof Download PDFInfo
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- CN102960852B CN102960852B CN201210457376.6A CN201210457376A CN102960852B CN 102960852 B CN102960852 B CN 102960852B CN 201210457376 A CN201210457376 A CN 201210457376A CN 102960852 B CN102960852 B CN 102960852B
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- 239000003571 electronic cigarette Substances 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title claims abstract description 22
- 239000000779 smoke Substances 0.000 title abstract description 10
- 239000003205 fragrance Substances 0.000 title abstract description 5
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 67
- 239000003814 drug Substances 0.000 claims abstract description 45
- 239000007788 liquid Substances 0.000 claims abstract description 37
- 239000000284 extract Substances 0.000 claims abstract description 35
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 33
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 32
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 25
- 239000000203 mixture Substances 0.000 claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000008367 deionised water Substances 0.000 claims abstract description 15
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 15
- 240000005250 Chrysanthemum indicum Species 0.000 claims abstract description 13
- 235000018959 Chrysanthemum indicum Nutrition 0.000 claims abstract description 13
- 244000269722 Thea sinensis Species 0.000 claims abstract description 13
- 235000009569 green tea Nutrition 0.000 claims abstract description 13
- 238000000605 extraction Methods 0.000 claims abstract description 9
- 238000004821 distillation Methods 0.000 claims abstract description 7
- 241000208125 Nicotiana Species 0.000 claims description 65
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 27
- 238000003756 stirring Methods 0.000 claims description 20
- 239000003390 Chinese drug Substances 0.000 claims description 18
- 244000242564 Osmanthus fragrans Species 0.000 claims description 11
- 235000019083 Osmanthus fragrans Nutrition 0.000 claims description 11
- 235000011187 glycerol Nutrition 0.000 claims description 11
- 239000001771 mentha piperita Substances 0.000 claims description 11
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 11
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 10
- 239000007864 aqueous solution Substances 0.000 claims description 10
- 235000010413 sodium alginate Nutrition 0.000 claims description 10
- 239000000661 sodium alginate Substances 0.000 claims description 10
- 229940005550 sodium alginate Drugs 0.000 claims description 10
- 239000002904 solvent Substances 0.000 claims description 10
- 229920001285 xanthan gum Polymers 0.000 claims description 10
- 238000002481 ethanol extraction Methods 0.000 claims description 6
- 239000000243 solution Substances 0.000 claims description 5
- 238000005374 membrane filtration Methods 0.000 claims description 4
- 239000002994 raw material Substances 0.000 claims description 2
- 230000000391 smoking effect Effects 0.000 abstract description 7
- 206010011224 Cough Diseases 0.000 abstract description 6
- 210000004072 lung Anatomy 0.000 abstract description 5
- 206010062717 Increased upper airway secretion Diseases 0.000 abstract description 3
- 208000026435 phlegm Diseases 0.000 abstract description 3
- 230000001105 regulatory effect Effects 0.000 abstract description 2
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 abstract 3
- 244000061176 Nicotiana tabacum Species 0.000 abstract 2
- 244000061508 Eriobotrya japonica Species 0.000 abstract 1
- 235000009008 Eriobotrya japonica Nutrition 0.000 abstract 1
- 241000935235 Fritillaria meleagris Species 0.000 abstract 1
- 235000006679 Mentha X verticillata Nutrition 0.000 abstract 1
- 235000002899 Mentha suaveolens Nutrition 0.000 abstract 1
- 235000001636 Mentha x rotundifolia Nutrition 0.000 abstract 1
- 241000333181 Osmanthus Species 0.000 abstract 1
- 235000019082 Osmanthus Nutrition 0.000 abstract 1
- 210000000621 bronchi Anatomy 0.000 abstract 1
- 239000000796 flavoring agent Substances 0.000 abstract 1
- 235000019634 flavors Nutrition 0.000 abstract 1
- 230000007794 irritation Effects 0.000 abstract 1
- 210000003800 pharynx Anatomy 0.000 abstract 1
- 210000003437 trachea Anatomy 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 14
- 238000001816 cooling Methods 0.000 description 9
- 235000019504 cigarettes Nutrition 0.000 description 6
- 238000010992 reflux Methods 0.000 description 6
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 4
- 239000003546 flue gas Substances 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 238000013019 agitation Methods 0.000 description 3
- 238000002386 leaching Methods 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 229920001817 Agar Polymers 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- 239000008272 agar Substances 0.000 description 2
- 238000000889 atomisation Methods 0.000 description 2
- 239000005018 casein Substances 0.000 description 2
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 description 2
- 235000021240 caseins Nutrition 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- 208000020401 Depressive disease Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 244000246386 Mentha pulegium Species 0.000 description 1
- 235000016257 Mentha pulegium Nutrition 0.000 description 1
- 235000004357 Mentha x piperita Nutrition 0.000 description 1
- 239000008896 Opium Substances 0.000 description 1
- 208000004224 Opium Dependence Diseases 0.000 description 1
- 201000007100 Pharyngitis Diseases 0.000 description 1
- 206010036790 Productive cough Diseases 0.000 description 1
- 206010043521 Throat irritation Diseases 0.000 description 1
- 206010044302 Tracheitis Diseases 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 208000006673 asthma Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 206010006451 bronchitis Diseases 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 210000002919 epithelial cell Anatomy 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 235000001050 hortel pimenta Nutrition 0.000 description 1
- 210000000867 larynx Anatomy 0.000 description 1
- 201000003102 mental depression Diseases 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 238000002670 nicotine replacement therapy Methods 0.000 description 1
- 229960001027 opium Drugs 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 230000002685 pulmonary effect Effects 0.000 description 1
- 210000002345 respiratory system Anatomy 0.000 description 1
- 208000023504 respiratory system disease Diseases 0.000 description 1
- 238000004088 simulation Methods 0.000 description 1
- 208000024794 sputum Diseases 0.000 description 1
- 210000003802 sputum Anatomy 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
- A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
Abstract
The invention discloses light-fragrance electronic cigarette atomized smoke solution and a preparation method thereof. The atomized smoke solution comprises the following components in percentage by weight: 30-45 percent of propylene glycol, 20-35 percent of glycerol, 5-15 percent of deionized water, 5-15 percent of alcohol, 15-45 percent of traditional Chinese medicine liquid, 2-5 percent of tobacco flavor, 2-6 percent of tobacco extract and 0.1-2 percent of forming agent, wherein the traditional Chinese medicine liquid is extraction liquid which is obtained by extracting traditional Chinese medicine mixture through water distillation or alcohol extraction, and the traditional Chinese medicine mixture consists of tendrilleaf fritillary bulb, mint leaf, loquat leaf, dendranthema indicum, violet, sweet-scented osmanthus and green tea. The light-fragrance electronic cigarette atomized smoke solution not only can meet the smoking demands of smokers, but also can effectively reduce irritation of smoke to tracheas, bronchi, throats and lungs of bodies, and has the efficacies of clearing heat, moistening lungs, arresting coughs, expelling phlegm, refreshing and restoring consciousness, regulating qi-flowing, resolving stagnation and the like.
Description
Technical field
The present invention relates to a kind of tobacco juice for electronic smoke and preparation method thereof, refer to a kind of simple and elegant odor type electronic cigarette atomizing tobacco juice and preparation method thereof particularly.
Background technology
Reducing tar and reducing harm is the emphasis problem of tobacco business always, in recent years, along with various circles of society are to the pay attention to day by day of smoking and healthy relation, Tobacco Control action is in a lot of local rise, banning on opium-smoking and the opium trade the appearance of regulation in public arena comprehensively, is proposed new requirement to the impact in the market of cigarette with to the raising of cigarette quality.
The consumption pattern of the cigarette flue gas that mainly cigarette combustion produces carries out, and flue gas easily causes smoker to suffer from various respiratory disease, the symptoms such as such as tracheitis, bronchitis, pharyngitis, coughing with a lot of sputum.In order to reduce harm of smoking, electronic cigarette is in 2005 at Chinese invention, and its Nicotine replacement therapy, obtains the accreditation of numerous smokers.Electronic cigarette is that the solution mist containing nicotine and essence is changed into particulate, and by pulmonary absorption, spue simulation smoke simultaneously, and not containing the tar in cigarette and other harmful components, also can not produce second-hand-cigarette also can not fill the air or curl up in confined space; And conventional cigarette is with tobacco leaf or tobacco ignition, compromise the health of smoker and non-smoker simultaneously.
Although but electronic cigarette can reduce harm of smoking, the discomfort of smoker's throat and lung cannot be improved.
Summary of the invention
The object of the invention is to the deficiency overcoming existing electronic cigarette, a kind of smoking demand that can meet smoker is provided, cough-relieving refreshing effect can be played again simultaneously, increase simple and elegant odor type electronic cigarette atomizing tobacco juice of throat's comfort and preparation method thereof.
For achieving the above object, simple and elegant odor type electronic cigarette atomizing tobacco juice provided by the present invention, its component and weight percent content are: propane diols 30 ~ 45%, glycerine 20 ~ 35%, deionized water 5 ~ 15%, alcohol 5 ~ 15%, traditional Chinese medicine liquid 15 ~ 45%, flavouring essence for tobacco 2 ~ 5%, tobacco extract 2 ~ 6%, forming agent 0.1 ~ 2%, wherein, described traditional Chinese medicine liquid is with the extract that water distillation is extracted or ethanol extraction Traditional Chinese drug mixture obtains, in described Traditional Chinese drug mixture, the percentage by weight of each component is: Bulbus Fritillariae Cirrhosae 0.1% ~ 50%, dried peppermint leaf 0.1% ~ 50%, loguat leaf 0.1% ~ 50%, Dendranthema indicum 0.1% ~ 50%, violet 0.1% ~ 50%, sweet osmanthus 0.1% ~ 50%, green tea 0.1% ~ 50%.
Preferably, the percentage by weight of each component of described Traditional Chinese drug mixture is: Bulbus Fritillariae Cirrhosae 1% ~ 20%, dried peppermint leaf 1% ~ 20%, loguat leaf 1% ~ 20%, Dendranthema indicum 1% ~ 20%, violet 1% ~ 20%, sweet osmanthus 1% ~ 20%, green tea 1% ~ 20%.
Preferably, described forming agent is the mixture of one or more in sodium alginate, agar, xanthans and casein sodium.
In conjunction with above-mentioned preferable range, the better component of described simple and elegant odor type electronic cigarette atomizing tobacco juice and weight percent content are: propane diols 30%, glycerine 25%, deionized water 10%, alcohol 10%, traditional Chinese medicine liquid 17%, flavouring essence for tobacco 3%, tobacco extract 5%, forming agent 0.1%, wherein, described traditional Chinese medicine liquid is with the extract that water distillation is extracted or ethanol extraction Traditional Chinese drug mixture obtains, in described Traditional Chinese drug mixture, the percentage by weight of each component is: Bulbus Fritillariae Cirrhosae 13.3%, dried peppermint leaf 10%, loguat leaf 16.7%, Dendranthema indicum 13.3%, violet 13.3%, sweet osmanthus 16.7%, green tea 16.7%.
Present invention also offers a kind of preparation method of simple and elegant odor type electronic cigarette atomizing tobacco juice, the percentage by weight of its raw material consists of: propane diols 30 ~ 45%, glycerine 20 ~ 35%, deionized water 5 ~ 15%, alcohol 5 ~ 15%, traditional Chinese medicine liquid 15 ~ 45%, flavouring essence for tobacco 2 ~ 5%, tobacco extract 2 ~ 6%, forming agent 0.1 ~ 2%, wherein, described traditional Chinese medicine liquid is with the extract that water distillation is extracted or ethanol extraction Traditional Chinese drug mixture obtains, in described Traditional Chinese drug mixture, the percentage by weight of each component is: Bulbus Fritillariae Cirrhosae 0.1% ~ 50%, dried peppermint leaf 0.1% ~ 50%, loguat leaf 0.1% ~ 50%, Dendranthema indicum 0.1% ~ 50%, violet 0.1% ~ 50%, sweet osmanthus 0.1% ~ 50%, green tea 0.1% ~ 50%,
Preparation process is as follows:
1) deionized water is heated to 60 DEG C, adds forming agent, stirs and continues to be heated to 85 ~ 95 DEG C, forming agent being dissolved completely and obtains the forming agent aqueous solution;
2) get propane diols and glycerine is uniformly mixed, after then the forming agent aqueous solution being added, remain on 80 DEG C and stir and obtain forming agent solvent mixed liquor, be incubated for subsequent use;
3) by traditional Chinese medicine liquid, flavouring essence for tobacco and tobacco extract are dissolved in alcohol in the lump, stir and obtain Chinese medicine tobacco mixed liquor, for subsequent use;
4) Chinese medicine tobacco mixed liquor is poured in forming agent solvent mixed liquor, constantly stir, make its temperature be down to room temperature, obtained simple and elegant odor type health care electronic cigarette atomizing tobacco juice.
Preferably, the percentage by weight of each component of described Traditional Chinese drug mixture is: Bulbus Fritillariae Cirrhosae 1% ~ 20%, dried peppermint leaf 1% ~ 20%, loguat leaf 1% ~ 20%, Dendranthema indicum 1% ~ 20%, violet 1% ~ 20%, sweet osmanthus 1% ~ 20%, green tea 1% ~ 20%.
Preferably, described forming agent is the mixture of one or more in sodium alginate, agar, xanthans and casein sodium.
Preferably, the preparation method of described traditional Chinese medicine liquid is: utilize 50% ~ 95% alcohol extract Traditional Chinese drug mixture, and extraction time is 2 ~ 6 hours, extracts the membrane filtration of gained solution 0.2 ~ 0.8 micron, then reduced pressure concentration, obtained traditional Chinese medicine liquid.
More preferably, the preparation method of described traditional Chinese medicine liquid is: utilize 70% ~ 95% alcohol extract Traditional Chinese drug mixture, and extraction time is 3 ~ 4 hours, extracts the membrane filtration of gained solution 0.2 ~ 0.8 micron, then reduced pressure concentration, obtained traditional Chinese medicine liquid.
In conjunction with above-mentioned preferable range, the better component of described simple and elegant odor type electronic cigarette atomizing tobacco juice and weight percent content are: propane diols 30%, glycerine 25%, deionized water 10%, alcohol 10%, traditional Chinese medicine liquid 17%, flavouring essence for tobacco 3%, tobacco extract 5%, forming agent 0.1%, wherein, described traditional Chinese medicine liquid is with the extract that water distillation is extracted or ethanol extraction Traditional Chinese drug mixture obtains, in described Traditional Chinese drug mixture, the percentage by weight of each component is: Bulbus Fritillariae Cirrhosae 13.3%, dried peppermint leaf 10%, loguat leaf 16.7%, Dendranthema indicum 13.3%, violet 13.3%, sweet osmanthus 16.7%, green tea 16.7%.
The main of forming agent in above-mentioned atomization tobacco juice can be more the viscosity improving tobacco juice for electronic smoke, prevents tobacco juice in practical process, and what meeting was too much flow in the middle of electronic smoke atomizer, causes the existence of the problems such as atomizing effect is low.Meanwhile, the viscosity improving tobacco juice for electronic smoke also can conveniently be transported and preserve.
Beneficial effect of the present invention: the simple and elegant odor type health care electronic cigarette atomizing tobacco juice provided, the smoking demand of smoker can not only be met, also can effectively reduce the stimulation of flue gas to health trachea-bronchial epithelial cell, larynx, lung, there is clearing heat and moistening lung, cough-relieving apophlegmatic, produce refreshing effect to the mind, the effect such as regulating qi to alleviate mental depression.Wherein peppermint add the effect can played and produce refreshing effect to the mind.Green tea and Dendranthema indicum not only have obvious cough-relieving, anti-inflammatory, the effect of eliminating the phlegm, relievining asthma, and add in tobacco juice, make flue gas exquisiteness soft, significantly can reduce side effect after suction, alleviate throat's discomfort reaction.Can play a protective role to the throat of smoker, respiratory tract, can significantly reduce the ill symptomses such as the cough caused by smoking, many phlegm, and the elegant gracefulness of fragrance, this perfume of tobacco and simple and elegant natural plants fragrance one integrated mass.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in further detail.
Embodiment 1
(1) preparation of traditional Chinese medicine liquid:
First Bulbus Fritillariae Cirrhosae 20g, dried peppermint leaf 15g, loguat leaf 25g, Dendranthema indicum 20g, violet 20g, sweet osmanthus 25g, green tea 25g is taken, ethanol 300ml with 75% heats extraction, cooling for reflux is carried out in leaching process, after backflow 3h, extract is taken out in cooling, then 75% ethanol adding equivalent carries out second time and extracts, and adds hot reflux 3h.Take out second time extract after cooling, mixed by extracted twice liquid, filter, reduced pressure concentration, obtains the traditional Chinese medicine liquid 1 that relative density is the 50ml of 1.05, for subsequent use.
(2) simple and elegant odor type electronic cigarette atomizing tobacco juice preparation:
1. get 10g deionized water, deionized water is heated to 60 DEG C, add 0.05g sodium alginate and 0.05g xanthans, continue to add thermal agitation, be heated to 90 DEG C, until sodium alginate and xanthans dissolve completely, obtain the forming agent aqueous solution 1.
2. after taking 30g propane diols and the mixing of 25g glycerine, fully stir, after then the forming agent aqueous solution 1 being added, remain on 80 DEG C and stir and obtain forming agent solvent mixed liquor 1, be incubated for subsequent use.
3. take alcohol 10g, 17g traditional Chinese medicine liquid 1,3g flavouring essence for tobacco is put in alcohol together with 5g tobacco extract, stir and obtain Chinese medicine tobacco mixed liquor 1, for subsequent use.
4. Chinese medicine tobacco mixed liquor 1 is poured in forming agent solvent mixed liquor 1, constantly stirs, make its slowly temperature be down to room temperature, obtained simple and elegant odor type electronic cigarette atomizing tobacco juice 1.
Embodiment 2
(1) preparation of traditional Chinese medicine liquid:
First Bulbus Fritillariae Cirrhosae 20g, dried peppermint leaf 15g, loguat leaf 25g, Dendranthema indicum 20g, violet 20g, sweet osmanthus 25g, green tea 25g is taken, ethanol 300 ml with 75% heats extraction, cooling for reflux is carried out in leaching process, after backflow 3h, extract is taken out in cooling, then 75% ethanol adding equivalent carries out second time and extracts, and adds hot reflux 3h.Take out second time extract after cooling, mixed by extracted twice liquid, filter, reduced pressure concentration, obtains the traditional Chinese medicine liquid 2 that relative density is the 50ml of 1.10, for subsequent use.
(2) simple and elegant odor type electronic cigarette atomizing tobacco juice preparation:
1. get 10g deionized water, deionized water is heated to 60 DEG C, add 0.05g sodium alginate and 0.05g xanthans, continue to add thermal agitation, be heated to 95 DEG C, until sodium alginate and xanthans dissolve completely, obtain the forming agent aqueous solution 2.
2. after taking 30g propane diols and the mixing of 23g glycerine, fully stir, after then the forming agent aqueous solution 2 being added, remain on 80 DEG C and stir and obtain forming agent solvent mixed liquor 2, be incubated for subsequent use.
3. take alcohol 12g, 18g traditional Chinese medicine liquid 2,4g flavouring essence for tobacco is put in alcohol together with 4g tobacco extract, stir and obtain Chinese medicine tobacco mixed liquor 2, for subsequent use.
4. Chinese medicine tobacco mixed liquor 2 is poured in forming agent solvent mixed liquor 2, constantly stirs, make its slowly temperature be down to room temperature, obtained simple and elegant odor type electronic cigarette atomizing tobacco juice 2.
Embodiment 3
(1) preparation of traditional Chinese medicine liquid:
First Bulbus Fritillariae Cirrhosae 15g, dried peppermint leaf 20g, loguat leaf 20g, Dendranthema indicum 25g, violet 15g, sweet osmanthus 25g, green tea 30g is taken, ethanol 300 ml with 75% heats extraction, cooling for reflux is carried out in leaching process, after backflow 3h, extract is taken out in cooling, then 75% ethanol adding equivalent carries out second time and extracts, and adds hot reflux 3h.Take out second time extract after cooling, mixed by extracted twice liquid, filter, reduced pressure concentration, obtains the traditional Chinese medicine liquid 3 that relative density is the 50ml of 1.17, for subsequent use.
(2) simple and elegant odor type electronic cigarette atomizing tobacco juice preparation:
1. get 10g deionized water, deionized water is heated to 60 DEG C, add 0.05g sodium alginate and 0.05g xanthans, continue to add thermal agitation, be heated to 85 DEG C, until sodium alginate and xanthans dissolve completely, obtain the forming agent aqueous solution 3.
2. after taking 30g propane diols and the mixing of 25g glycerine, fully stir, after then the forming agent aqueous solution 3 being added, remain on 80 DEG C and stir and obtain forming agent solvent mixed liquor 3, be incubated for subsequent use.
3. take alcohol 10g, 17g traditional Chinese medicine liquid 3,3g flavouring essence for tobacco is put in alcohol together with 5g tobacco extract, stir and obtain Chinese medicine tobacco mixed liquor 3, for subsequent use.
4. Chinese medicine tobacco mixed liquor 3 is poured in forming agent solvent mixed liquor 3, constantly stirs, make its slowly temperature be down to room temperature, obtained simple and elegant odor type electronic cigarette atomizing tobacco juice 3.
Above-described embodiment is carried out effect assessment respectively, and its result is as following table:
Embodiment 1 effect assessment table
Embodiment 2 effect grading table
Embodiment 3 effect assessment table
The display of above-mentioned effect assessment, simple and elegant odor type electronic cigarette atomizing tobacco juice provided by the invention, fragrant, has simple and elegant and that stereovision is abundant tobacco aroma, assorted gas is comparatively light, and delicate mouthfeel, Hui Tian are little to throat irritation, there is good atomization, good haze effect can be realized.
Claims (4)
1. a simple and elegant odor type electronic cigarette atomizing tobacco juice, its component is: propane diols 30g, glycerine 25g, deionized water 10g, alcohol 10g, traditional Chinese medicine liquid 17g, flavouring essence for tobacco 3g, tobacco extract 5g, sodium alginate 0.05g and xanthans 0.05g, wherein, described traditional Chinese medicine liquid is that in described Traditional Chinese drug mixture, each component is: Bulbus Fritillariae Cirrhosae 20g, dried peppermint leaf 15g, loguat leaf 25g, Dendranthema indicum 20g, violet 20g, sweet osmanthus 25g, green tea 25g with the extract that water distillation is extracted or ethanol extraction Traditional Chinese drug mixture obtains.
2. the preparation method of a simple and elegant odor type electronic cigarette atomizing tobacco juice, its raw material consists of: propane diols 30g, glycerine 25g, deionized water 10g, alcohol 10g, traditional Chinese medicine liquid 17g, flavouring essence for tobacco 3g, tobacco extract 5g, sodium alginate 0.05g and xanthans 0.05g, wherein, described traditional Chinese medicine liquid is that in described Traditional Chinese drug mixture, each component is: Bulbus Fritillariae Cirrhosae 20g, dried peppermint leaf 15g, loguat leaf 25g, Dendranthema indicum 20g, violet 20g, sweet osmanthus 25g, green tea 25g with the extract that water distillation is extracted or ethanol extraction Traditional Chinese drug mixture obtains;
Preparation process is as follows:
1) deionized water is heated to 60 DEG C, adds forming agent, stirs and continues to be heated to 85 ~ 95 DEG C, forming agent being dissolved completely and obtains the forming agent aqueous solution;
2) get propane diols and glycerine is uniformly mixed, after then the forming agent aqueous solution being added, remain on 80 DEG C and stir and obtain forming agent solvent mixed liquor, be incubated for subsequent use;
3) alcohol measured, by traditional Chinese medicine liquid, flavouring essence for tobacco and tobacco extract are dissolved in alcohol in the lump, stir and obtain Chinese medicine tobacco mixed liquor, for subsequent use;
4) Chinese medicine tobacco mixed liquor is poured in forming agent solvent mixed liquor, constantly stir, make its temperature be down to room temperature, obtained simple and elegant odor type electronic cigarette atomizing tobacco juice.
3. the preparation method of simple and elegant odor type electronic cigarette atomizing tobacco juice according to claim 2, it is characterized in that: the preparation method of described traditional Chinese medicine liquid is: utilize 50% ~ 95% alcohol extract Traditional Chinese drug mixture, extraction time is 2 ~ 6 hours, extract the membrane filtration of gained solution 0.2 ~ 0.8 micron, then reduced pressure concentration, obtained relative density is the traditional Chinese medicine liquid of 1.02 ~ 1.20.
4. the preparation method of simple and elegant odor type electronic cigarette atomizing tobacco juice according to claim 3, it is characterized in that: the preparation method of described traditional Chinese medicine liquid is: utilize 70% ~ 95% alcohol extract Traditional Chinese drug mixture, extraction time is 3 ~ 4 hours, extract the membrane filtration of gained solution 0.2 ~ 0.8 micron, then reduced pressure concentration, obtained traditional Chinese medicine liquid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210457376.6A CN102960852B (en) | 2012-11-14 | 2012-11-14 | Light-fragrance electronic cigarette atomized smoke solution and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210457376.6A CN102960852B (en) | 2012-11-14 | 2012-11-14 | Light-fragrance electronic cigarette atomized smoke solution and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102960852A CN102960852A (en) | 2013-03-13 |
| CN102960852B true CN102960852B (en) | 2015-04-22 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210457376.6A Active CN102960852B (en) | 2012-11-14 | 2012-11-14 | Light-fragrance electronic cigarette atomized smoke solution and preparation method thereof |
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| NL2029429B1 (en) * | 2021-10-15 | 2022-06-24 | Yancheng Teachers College | Preparation method and application of atomizing mixture for electronic atomizer |
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