CN106820270A - A kind of electronic cigarette tobacco tar and preparation method thereof - Google Patents
A kind of electronic cigarette tobacco tar and preparation method thereof Download PDFInfo
- Publication number
- CN106820270A CN106820270A CN201710052064.XA CN201710052064A CN106820270A CN 106820270 A CN106820270 A CN 106820270A CN 201710052064 A CN201710052064 A CN 201710052064A CN 106820270 A CN106820270 A CN 106820270A
- Authority
- CN
- China
- Prior art keywords
- fruit
- dairy products
- electronic cigarette
- tobacco tar
- cigarette tobacco
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A24F47/008—
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Confectionery (AREA)
Abstract
The invention provides a kind of electronic cigarette tobacco tar, including following mass percent component：The mixed extract of 95% 99% atomized liquid and 1% 5% fruit and dairy products；Fruit is 1 according to mass ratio by fruit and dairy products with the mixed extract of dairy products:1‑10:Extracted after 1 mixing and formed, fruit includes at least one in apple, pears, grape and strawberry, dairy products include at least one in milk, cheese and cream.Mixed extract containing a certain amount of fruit and dairy products in the electronic cigarette tobacco tar that the present invention is provided, can prepare that fragrance is abundant, comfortable taste, satisfaction are good and with the electronic cigarette tobacco tar of certain expelling cold, eliminating effect.Present invention also offers a kind of preparation method of electronic cigarette tobacco tar, including：Mass percent is respectively 95% 99% atomized liquid and 1% 5% fruit mixes with the mixed extract of dairy products, be stirred at room temperature uniform, the electronic cigarette tobacco tar is obtained；Fruit is 1 according to mass ratio by fruit and dairy products with the mixed extract of dairy products:1‑10:Extracted after 1 mixing and formed.
Description
Technical field
The present invention relates to electronic cigarette field, and in particular to a kind of electronic cigarette tobacco tar and preparation method thereof.
Background technology
Electronic cigarette is presented huge market prospects as a kind of form in novel tobacco product, and reason essentially consists in one
It provides the consumption habit and satisfaction similar with traditional cigarette to aspect, and the hazard index of another aspect electronic cigarette compares traditional cigarette
Substantially reduce.The public place management rule that no smoking is put into effect in Chinese increasing city, it is believed that electronic cigarette exists soon
Chinese market can occupy a tiny space.
Electronics smoke product taste in the market is partial to blended type cigarette, and the taste for being more conform with foreign consumers is practised
Used, and Chinese Consumer's preference flue-cured tobacco, taste is more strong, and the mouthfeel of electronic cigarette is extremely difficult to require.Therefore, electronic cigarette is improved
It is to open the important means of Chinese market that tobacco tar formula is allowed to meet Chinese Consumer's custom.
In order to be able to simulate fragrance, fragrance and the mouthfeel of traditional cigarette to the full extent, current electronic cigarette tobacco tar is most common
Be addition tobacco extract, by extracting the tobacco extract and propane diols, glycerine, the flavouring essence for tobacco that obtain according to a certain ratio
Mix, although in the market has various tastes electronic cigarette tobacco tar, also not for modern with expelling cold, eliminating
Effect has the electronic cigarette tobacco tar of abundant fruit and cream mix of flavors true to nature simultaneously.
The content of the invention
To solve the above problems, the invention provides a kind of electronic cigarette tobacco tar, in the electronic cigarette tobacco tar containing fruit with
The mixed extract of dairy products, fruit is mixed by dairy products with the mixed extract of dairy products with the fruit with expelling cold, eliminating effect
Extracted after conjunction and formed.The electronic cigarette tobacco tar it is good in taste, while there is abundant fruit and cream mix of flavors true to nature and have
The health-care efficacy of expelling cold, eliminating effect.Present invention also offers the preparation method of the electronic cigarette tobacco tar.
First aspect present invention provide a kind of electronic cigarette tobacco tar, including following mass percent component：
The atomized liquid of 95%-99%, the fruit of 1%-5% and the mixed extract of dairy products；
The fruit is 1 according to mass ratio by fruit and dairy products with the mixed extract of dairy products:1-10:After 1 mixing
Extraction is formed, the fruit include apple, pears, grape and strawberry at least one, the dairy products include milk, cheese and
At least one in cream.
Wherein, in the electronic cigarette tobacco tar, the fruit is 2%- with the mass percent of the mixed extract of dairy products
4%.
Wherein, the fruit also includes at least one in banana, blueberry, pineapple, lemon, hawthorn, red tangerine and lichee.
Wherein, after the fruit is mixed with the mixed extract of dairy products by the component of following mass percent extract and
Into：Apple 5%-50%, strawberry 5%-50%, dairy products 10%-50%, pears 2%-10%, banana 1%-10%, blueberry 1%-
10%th, pineapple 2%-10%, grape 1%-10%, lemon 1%-10%, hawthorn 1%-10%, red tangerine 1%-10%, lichee
2%-10%.
Wherein, after the fruit is mixed with the mixed extract of dairy products by the component of following mass percent extract and
Into：Apple 5%-30%, strawberry 5%-35%, dairy products 10%-50%, pears 2%-6%, banana 1%-8%, blueberry 1%-
10%th, pineapple 2%-8%, grape 1%-10%, lemon 1%-6%, hawthorn 1%-10%, red tangerine 1%-8%, lichee 2%-
10%.
Wherein, the atomized liquid includes food flavor, tobacco extract and organic solvent, and the food flavor includes ethyl
In vanillic aldehyde, citronellol, ethyl acetate, geraniol, linalool, rhodinol, dorinone, Megastigmatrienone, dihydro-actinidia
At least one in ester, alpha, beta-lonone and phenmethylol, the organic solvent includes at least one in propane diols and glycerine.
Wherein, in the electronic cigarette tobacco tar, the mass percent of food flavor is 1%-10%, the quality of tobacco extract
Percentage is 1%-5%, and the mass percent of propane diols is 10%-80%, and the mass percent of glycerine is 10%-80%.
Wherein, the fruit is extracted and obtained in accordance with the following steps with the mixed extract of dairy products：
After the fruit is crushed, dairy products are added, form mixture, the mass ratio of fruit and dairy products is 1:1-10:
1；Supercritical carbon dioxide fluid is subsequently adding, supercritical extract is carried out to fruit and dairy products by isothermal pressure-changing method, obtained
The mixed extract of the fruit and dairy products.
Wherein, the mixture is placed in extractor, add supercritical carbon dioxide fluid, temperature be 20.0 DEG C-
50.0 DEG C, pressure has been extracted the supercritical carbon dioxide fluid of solute, by institute to be stirred under 7.0MPa-10.0MPa
State and extracted the supercritical carbon dioxide fluid of solute and entered in separator by expansion valve, reduce pressure to 6.0MPa-
6.9MPa, the solute separates out the mixed extract for obtaining the fruit and dairy products.
The electronic cigarette tobacco tar that embodiment of the present invention first aspect is provided, with fruit and cream mix of flavors, fragrance is abundant, mouth
Sense is comfortable, satisfaction is good, meanwhile, because containing various fruits and effective ingredients in plant in the mixed extract of fruit and dairy products,
Can inducing diaphoresis dissipate wind, eliminating cold to stop pain, with health-care effects such as expelling cold, eliminating effects.
Second aspect present invention provides a kind of preparation method of electronic cigarette tobacco tar, comprises the following steps：
Mass percent is respectively into the atomized liquid of 95%-99% and the fruit of 1%-5% to be extracted with the mixing of dairy products
Thing mixes, and uniform, the prepared electronic cigarette tobacco tar is stirred at room temperature；The mixed extract of the fruit and dairy products is by fruit
With dairy products according to mass ratio be 1:1-10:Extracted after 1 mixing and formed, the fruit is included in apple, pears, grape and strawberry
At least one, the dairy products include at least one in milk, cheese and cream.
The preparation method of the electronic cigarette tobacco tar that second aspect present invention is provided, by by atomized liquid and fruit and dairy products
Mixed extract is simply mixed, and it is gentle, comfortable and with the electronic cigarette tobacco tar of expelling cold, eliminating effect to be obtained mouthfeel, while this
The preparation method of invention is simple to operation, is adapted to industrialization production.
To sum up, beneficial effect of the present invention includes the following aspects：
1st, the electronic cigarette tobacco tar that the present invention is provided, with fruit milk mix of flavors, fragrance is abundant, comfortable taste, satisfaction
Feel, meanwhile, because containing various fruits and effective ingredients in plant in the mixed extract of fruit and dairy products, can inducing diaphoresis it is scattered
Wind, eliminating cold to stop pain, with health-care effects such as expelling cold, eliminating effects.
2nd, the preparation method of the electronic cigarette tobacco tar that the present invention is provided is simple to operation, is adapted to industrialization production.
Specific embodiment
As described below is the preferred embodiment of the present invention, it is noted that for those skilled in the art
For, under the premise without departing from the principles of the invention, some improvements and modifications can also be made, these improvements and modifications are also considered as
Protection scope of the present invention.
Embodiment of the present invention first aspect provide a kind of electronic cigarette tobacco tar, including following mass percent component：
The atomized liquid of 95%-99%, the fruit of 1%-5% and the mixed extract of dairy products；
The fruit is 1 according to mass ratio by fruit and dairy products with the mixed extract of dairy products:1-10:After 1 mixing
Extraction is formed, the fruit include apple pear, grape and strawberry at least one, the dairy products include milk, cheese and
At least one in cream.
In an embodiment of the present invention, atomized liquid includes food flavor, tobacco extract and organic solvent, and the food is fragrant
Spermatophore includes Ethyl vanillin, citronellol, ethyl acetate, geraniol, linalool, rhodinol, dorinone, Megastigmatrienone, two
At least one in hydrogen actinidia lactone, alpha, beta-lonone and phenmethylol.Food flavor is that each tobacco articles perfuming flavoring makes
With, make tobacco product that the additive of a tobacco articles of good flue gas effect is produced when burning and sucking, therefore in electronics tobacco tar
Proportioning to food flavor is particularly significant.Alternatively, in electronic cigarette tobacco tar, the mass percent of food flavor is 1%-10%.
Still optionally further, in electronic cigarette tobacco tar, the mass percent of food flavor is 2%-3%.
In an embodiment of the present invention, the tobacco extract is conventional tobacco extract；Such as, including non-nitrogen containing chemical combination
Thing, nitrogen-containing compound, mineral matter and tobacco flavor material etc.；Wherein, non-nitrogen containing compound includes monosaccharide and disaccharide, starch, organic
Acid, phenols, lipid, sterols, terpenoid, cellulose and pectic substance etc.；Tobacco flavor material includes organic acid, phenol
Class, lipid, sterols and terpenoid.Alternatively, in electronic cigarette tobacco tar, the mass percent of tobacco extract is 1%-
10%.Still optionally further, the mass percent of tobacco extract is 1%-5%.Specifically, tobacco extract selects Yunnan Tobacco
Careless absolute oil.
In an embodiment of the present invention, alternatively, the organic solvent is at least one in propane diols and glycerine.Tool
Body ground, the propane diols, glycerine are food grade or pharmaceutical grade product.Alternatively, in electronic cigarette tobacco tar, the quality of propane diols
Percentage is 10%-80%, and the mass percent of glycerine is 10%-80%.Still optionally further, the quality percentage of propane diols
Than being 40%-80%, the mass percent of glycerine is 20%-50%.
In an embodiment of the present invention, electronic cigarette tobacco tar includes the component of following mass percent：The food of 1%-10%
Essence, the tobacco extract of 1%-5%, the fruit of 1%-5% and the mixed extract of dairy products, balance of organic solvent.Can
Selection of land, electronic cigarette tobacco tar includes the component of following mass percent：The propane diols of 10%-80%, the glycerine of 10%-80%,
The food flavor of 1%-10%, the tobacco extract of 1%-5%, the fruit of 1%-5% and the mixed extract of dairy products.
In an embodiment of the present invention, in the electronic cigarette tobacco tar, the matter of the mixed extract of the fruit and dairy products
Amount percentage is 2%-4%.
In an embodiment of the present invention, the fruit includes apple, 1%-20% pears, the 1%-30% grapes of 5%-50%
With 5%-50% strawberries.Alternatively, fruit is also including at least in banana, blueberry, pineapple, lemon, hawthorn, red tangerine and lichee
Kind.Alternatively, fruit is extracted after being mixed by the component of following mass percent with the mixed extract of dairy products and formed：5%-
50% apple, the pears of 2%-10%, the grape of 1%-10%, the strawberry of 5%-50%, the dairy products of 10%-50%, 1%-
70% auxiliary material, auxiliary material includes at least one in banana, blueberry, pineapple, lemon, hawthorn, red tangerine and lichee.Specifically, water
Fruit is extracted after being mixed by the component of following mass percent with the mixed extract of dairy products and forms：Apple 5%-50%, strawberry
5%-50%, dairy products 10%-50%, pears 2%-10%, banana 1%-10%, blueberry 1%-10%, pineapple 2%-10%, Portugal
Grape 1%-10%, lemon 1%-10%, hawthorn 1%-10%, red tangerine 1%-10%, lichee 2%-10%.Still optionally further,
Fruit is extracted after can also being mixed by the component of following mass percent with the mixed extract of dairy products and formed：
Apple 5%-30%, strawberry 0.5%-35%, dairy products 10%-50%, pears 2%-6%, banana 1%-8%, indigo plant
Certain kind of berries 1%-10%, pineapple 2%-8%, grape 1%-10%, lemon 1%-6%, hawthorn 1%-10%, red tangerine 1%-8%, lichee
2%-10%.
In the mixed extract component of fruit of the present invention and dairy products：
Apple has functions that inducing sweat and dispelling exogenous evils, warming middle energizer to arrest vomiting, warm lung cough-relieving.
Strawberry has the effect of nourishing Yin and falling fire, moisturize laxation, sharp stool and urine.
Dairy products such as milk has the effect of tonifying middle-Jiao and Qi, strengthening the spleen and stomach, eliminate dampness and have diuretic effect, resolving sputum, hidroschesis, antiabortive, increasing appetite.
Pears energy sweating expelling pathogenic factors from muscles and skin, warming meridians and promoting circulation of qi, helps yang transforming qi, eliminating cold to stop pain.
Get rid of illness dehumidifying, apocenosis myogenic, promoting blood circulation and stopping pain, inducing diaphoresis of banana dissipates wind, the function such as sensible.
Blueberry energy inducing sweat and dispelling exogenous evils, dampness elimination and in, inducing diuresis for removing edema.
During pineapple energy sweating cold dispelling, promoting the circulation of qi are wide, it is pleasant antiabortive.
Grape is expelled pathogenic wind from the body surface, wins wet analgesic, only convulsion.
Lemon has functions that expelling cold, eliminating, clearing the nasal passage, wind-damp dispelling, analgesic.
The effects such as hawthorn has clearing heat and detoxicating, expelling phlegm and arresting coughing, gastral cavity abdomen.
Red tangerine have functions that sweating cold dispelling, freeing lung and relieving asthma, inducing diuresis for removing edema.
Lichee has expelling cold and relieving exterior syndrome, wind-damp dispelling, effect of analgesic.
The present invention selects above-mentioned raw materials and carries out compatibility, and each raw material acts synergistically that the effect of maximum can be played.
In an embodiment of the present invention, the fruit is extracted and obtained in accordance with the following steps with the mixed extract of dairy products：
After the fruit is crushed, dairy products are added, form mixture, the mass ratio of fruit and dairy products is 1:1-10:
1；Supercritical carbon dioxide fluid is subsequently adding, supercritical extract is carried out to fruit and dairy products by isothermal pressure-changing method, obtained
The mixed extract of the fruit and dairy products；Wherein, supercritical carbon dioxide fluid is used as extractant；According to quality percentage
Than supercritical carbon dioxide fluid is 50 with extract (i.e. the mixture of fruit and dairy products):1-200:1.Specifically, by institute
State mixture to be placed in extractor, add supercritical carbon dioxide fluid, be 20.0 DEG C -50.0 DEG C in temperature, pressure is
It is stirred under 7.0MPa-10.0MPa, has been extracted the Co 2 supercritical fluid of solute, solute has been extracted by described
Co 2 supercritical fluid entered in separator by expansion valve, reduce pressure to 6.0MPa-6.9MPa, solute analysis
Go out the mixed extract for obtaining the fruit and dairy products.Specifically, temperature be 30 DEG C, pressure be 7.4MPa under stirred
Mix, extracted the Co 2 supercritical fluid of solute, the Co 2 supercritical fluid for having extracted solute is led to
Cross expansion valve to enter in separator, reduce pressure to 6.8MPa, the solute separates out the mixing for obtaining the fruit and dairy products
Extract.
The present invention is extracted by the method for supercritical extract to the mixture of fruit and cream, in extraction process, when
When reducing pressure to 6.0MPa-6.9MPa, carbon dioxide becomes gaseous state by supercriticality, is extracted material in overcritical dioxy
Change the solubility reduction in carbon flow body, wherein extract is segregated into separator.By gaseous carbon dioxide pressurization extremely
7.0MPa-10.0MPa becomes Supercritical Conditions and is passed through Reusability in extractor, finally, needed for being obtained in separator
Fruit is standby with the mixed extract of dairy products.The present invention extracts fruit and is carried with the mixing of dairy products by supercritical extraction technique
Thing is taken for electronic cigarette tobacco tar, the original composition of food materials is remained to greatest extent, obtaining a kind of brand-new both has expelling cold, eliminating
Effect can lift the electronic cigarette tobacco tar of mouthfeel again.
In embodiment of the present invention, electronic cigarette tobacco tar includes the mixed extract of atomized liquid and fruit and dairy products, fruit
Extracted after mixing with the mixed extract dairy products and fruit of dairy products and formed, so that the mixing of used time, fruit and dairy products
Extract gasifies with atomized liquid after the atomizer of electronic cigarette is heated, and is drawn by human body, so as to quickly be absorbed, reaches
Effect of expelling cold, eliminating effect.Meanwhile, the present invention passes through to prepare the mixed extract with fruit with dairy products, is aided with and uses conjunction
Suitable food flavor is modified, and can prepare that fragrance is abundant, comfortable taste, satisfaction are good and with certain expelling cold, eliminating
The electronic cigarette tobacco tar of effect.
The electronic cigarette tobacco tar that embodiment of the present invention first aspect is provided, the mix of flavors with fruit and cream, without second-hand
The harm of cigarette, can also use completely in public, can not only meet smoker's smoking demand, and not interfere with other people and be good for
Health.Meanwhile, because containing various fruits and effective ingredients in plant in the mixed extract of fruit and dairy products, can the scattered wind of inducing diaphoresis,
Eliminating cold to stop pain, with health-care effects such as expelling cold, eliminating effects.
Second aspect present invention provides a kind of preparation method of electronic cigarette tobacco tar, comprises the following steps：
Mass percent is respectively into the atomized liquid of 95%-99% and the fruit of 1%-5% to be extracted with the mixing of dairy products
Thing mixes, and uniform, the prepared electronic cigarette tobacco tar is stirred at room temperature；The mixed extract of the fruit and dairy products is by fruit
With dairy products according to mass ratio be 1:1-10:Extracted after 1 mixing and formed, the fruit is included in apple, pears, grape and strawberry
At least one, the dairy products include at least one in milk, cheese and cream.
In an embodiment of the present invention, the food flavor is added in the organic solvent, at room temperature stirring and dissolving
20-30min, obtains mixed solution, is subsequently adding the fruit and is stirred until homogeneous with the mixed extract of dairy products, is obtained described
Electronic cigarette tobacco tar.
The preparation method of the electronic cigarette tobacco tar that second aspect present invention is provided, by by atomized liquid and fruit and dairy products
Mixed extract is simply mixed, and it is gentle, comfortable and with the electronic cigarette tobacco tar of expelling cold, eliminating effect to be obtained mouthfeel, while this
The preparation method of invention is simple to operation, is adapted to industrialization production.
Embodiment 1：
A kind of electronic cigarette tobacco tar, including following mass percent component：
Propane diols 71%, glycerine 20%, food flavor 2%, tobacco extract 5%, fruit is extracted with the mixing of milk
Thing 2%.The flavoring essence be Ethyl vanillin, citronellol, ethyl acetate, geraniol, linalool, rhodinol, dorinone,
Megastigmatrienone, dihydroactinidiolide and phenmethylol.
The preparation method of above-mentioned electronic cigarette tobacco tar, comprises the following steps：
(1) preparation of the mixed extract of fruit and milk：Weigh apple (20g), strawberry (15g), milk (15g), pears
(20g), blueberry (5g), pineapple (5g), grape (8g), banana (3g), lemon (5g), hawthorn (4g), clean, and use pulverizer powder
It is broken, supercritical carbon dioxide extraction device is passed through, (i.e. fruit is mixed with dairy products with extract for supercritical carbon dioxide fluid
Compound) mass ratio be 50:1, temperature setting is 30 degree, pressure 7.4MPa.Mix, extraction mixed liquor be passed through expansion valve,
Pressure is reduced to 6.8MPa, carbon dioxide becomes gaseous state by supercriticality, wherein extract is segregated into separator.By gas
The carbon dioxide pressurization of state becomes Supercritical Conditions and is passed through Reusability in extractor to 7.4MPa, finally, by separator
In to obtain required fruit standby with the mixed extract of milk.
(2) preparation of electronic cigarette tobacco tar：In clean reactor, propane diols (71g) and glycerine are separately added into
Ethyl vanillin (0.7g), citronellol (0.1g), ethyl acetate (0.12g), geraniol are sequentially added under (20g), stirring
(0.12g), linalool (0.12g), rhodinol (0.12g), dorinone (0.16g), Megastigmatrienone (0.24g), dihydro Mi
Monkey peach lactone (0.28g), phenmethylol (0.04g).At room temperature stir 30 minutes, after dissolving, add (5g) tobacco extract and
Fruit is well mixed with the mixed extract (2g) of milk and obtains final product with fruit and cream mix of flavors type electronic cigarette tobacco tar.
Embodiment 2：
A kind of electronic cigarette tobacco tar, including following mass percent component：
Propane diols 61%, glycerine 30%, food flavor 2%, tobacco extract 3%, fruit is extracted with the mixing of milk
Thing 4%.The flavouring essence for tobacco be Ethyl vanillin, citronellol, ethyl acetate, geraniol, linalool, rhodinol, dorinone,
Megastigmatrienone, dihydroactinidiolide and phenmethylol.
The preparation method of above-mentioned electronic cigarette tobacco tar, comprises the following steps：
(1) preparation of the mixed extract of fruit and milk：Weigh apple (20g), strawberry (10g), milk (20g), pears
(10g), blueberry (5g), pineapple (5g), grape (8g), banana (4g), lemon (8g), hawthorn (10g), clean, and use pulverizer powder
It is broken, supercritical carbon dioxide extraction device is passed through, (i.e. fruit is mixed with dairy products with extract for supercritical carbon dioxide fluid
Compound) mass ratio be 200:1, temperature setting is 30 degree, pressure 7.4MPa.Mix, extraction mixed liquor be passed through expansion valve,
Pressure is reduced to 6.8MPa, carbon dioxide becomes gaseous state by supercriticality, wherein extract is segregated into separator.By gas
The carbon dioxide pressurization of state becomes Supercritical Conditions and is passed through Reusability in extractor to 7.4MPa, finally, by separator
In obtain required fruit and the mixed extract of milk is standby.
(2) preparation of electronic cigarette tobacco tar：In clean reactor, propane diols (61g) and glycerine are separately added into
Ethyl vanillin (0.7g), citronellol (0.1g), ethyl acetate (0.12g), geraniol are sequentially added under (30g), stirring
(0.12g), linalool (0.12g), rhodinol (0.12g), dorinone (0.16g), Megastigmatrienone (0.24g), dihydro Mi
Monkey peach lactone (0.28g), phenmethylol (0.04g).At room temperature stir 30 minutes, after dissolving, add (3g) tobacco extract and
Fruit is well mixed with the mixed extract (4g) of milk and obtains final product with fruit and cream mix of flavors type electronic cigarette tobacco tar.
Embodiment 3：
A kind of electronic cigarette tobacco tar, including following mass percent component：
The mixed extract 2% of propane diols 44%, glycerine 50%, food flavor 2%, fruit and milk.The cigarette is used
Essence is Ethyl vanillin, citronellol, ethyl acetate, geraniol, linalool, rhodinol, dorinone, Megastigmatrienone, two
Hydrogen actinidia lactone and alpha, beta-lonone.
The preparation method of above-mentioned electronic cigarette tobacco tar, comprises the following steps：
(1) preparation of the mixed extract of fruit and milk：Weigh apple (20g), strawberry (20g), milk (15g), pears
(20g), grape (8g), banana (3g), lemon (4g), hawthorn (10g), clean, and are crushed with pulverizer, are passed through overcritical titanium dioxide
Carbon Fluid Extractor, supercritical carbon dioxide fluid is 100 with extract (i.e. the mixture of fruit and dairy products) mass ratio:1,
Temperature setting is 30 degree, pressure 7.4MPa.Mix, extraction mixed liquor is passed through expansion valve, reduce pressure to 6.8MPa, two
Carbonoxide becomes gaseous state by supercriticality, wherein extract is segregated into separator.By gaseous carbon dioxide pressurization extremely
7.4MPa becomes Supercritical Conditions and is passed through Reusability in extractor, finally, by obtaining required fruit and ox in separator
The mixed extract of milk is standby.
(2) preparation of electronic cigarette tobacco tar：In clean reactor, propane diols (44g) and glycerine are separately added into
Ethyl vanillin (0.7g), citronellol (0.1g), ethyl acetate (0.12g), geraniol are sequentially added under (50g), stirring
(0.12g), linalool (0.2g), rhodinol (0.16g), dorinone (0.16g), Megastigmatrienone (0.2g), dihydro macaque
Peach lactone (0.2g), alpha, beta-lonone (0.04g).At room temperature stir 30 minutes, after dissolving, add (2g) tobacco extract and
Fruit is well mixed with the mixed extract (2g) of milk and obtains final product with fruit and cream mix of flavors type electronic cigarette tobacco tar.
Embodiment 4：
A kind of electronic cigarette tobacco tar, including following mass percent component：
The mixed extract of propane diols 72%, glycerine 20%, food flavor 3%, the fruit of tobacco extract 3% and milk
2%.The flavouring essence for tobacco be Ethyl vanillin, geraniol, linalool, phenmethylol, rhodinol, dorinone, Megastigmatrienone,
Dihydroactinidiolide.
The preparation method of above-mentioned electronic cigarette tobacco tar, comprises the following steps：
(1) preparation of the mixed extract of fruit and milk：Weigh apple (30g), strawberry (15g), milk (15g), pears
(20g), grape (4g), banana (3g), red tangerine (4g), lichee (5g), hawthorn (4g), clean, and are crushed with pulverizer, are passed through super facing
Boundary's CO 2 fluid extractor, supercritical carbon dioxide fluid and extract (i.e. the mixture of fruit and dairy products) mass ratio
It is 100:1, temperature setting is 30 degree, pressure 7.4MPa.Mix, extraction mixed liquor is passed through expansion valve, reduce pressure extremely
6.8MPa, carbon dioxide becomes gaseous state by supercriticality, wherein extract is segregated into separator.By gaseous titanium dioxide
Carbon is forced into 7.4MPa and becomes Supercritical Conditions and is passed through Reusability in extractor, finally, needed for being obtained in separator
Fruit is standby with the mixed extract of milk.
(2) preparation of electronic cigarette tobacco tar：In clean reactor, propane diols (72g) and glycerine are separately added into
Ethyl vanillin (1.05g), geraniol (0.18g), linalool (0.3g), phenmethylol are sequentially added under (20g), stirring
(0.06), rhodinol (0.3g), dorinone (0.24g), Megastigmatrienone (0.45g), dihydroactinidiolide (0.42g).
Stir 30 minutes at room temperature, after dissolving, add (3g) tobacco extract and fruit to mix with the mixed extract (2g) of milk
Uniformly obtain final product with fruit and cream mix of flavors type electronic cigarette tobacco tar.
Embodiment 5：
Electronic cigarette tobacco tar in above-described embodiment is added in electronic cigarette device carries out sensory effects evaluation respectively.
Sensory effects evaluation method is comprised the following steps：
There is provided 6 evaluation indexes, including excitant, satisfaction, feature style, tobacco perfume, fragrance and smoke amount, and root
According to every evaluation index different score values are assigned to the Different Effects degree of electronic cigarette tobacco tar aesthetic quality.
The excitant refers to：Suction electronic cigarette tobacco tar includes oral cavity, throat through the flue gas that atomization is produced to sense organ
The discomfort produced with nasal cavity is received；
The satisfaction refers to：Flue gas strength, concentration and the note that electronic cigarette tobacco tar is produced through atomization are on sense organ
The comprehensive impression of generation；
The feature style refers to：A kind of electronic cigarette tobacco tar is different from the sense of other homogeneous e cigarette tobacco tar in pleasant feeling
Official's Main Differences are showed；
The tobacco perfume (or spice) refers to：Sensory feel this fragrant breath to tobacco during smokeing panel test；
The fragrance refers to：The good and bad degree of pleasant breath is felt during smokeing panel test by smell and the sense of taste；
The smoke amount refers to：Electronic cigarette tobacco tar through atomization produce exhaust gas volumn number.
The member of smoking of 9 people is set, everyone a electronic cigarette tobacco tar sensory quality assessment table, using the marking mode secretly commented,
Smoked panel test method using overall circulation, electronic cigarette tobacco tar is aspirated, according to 6 sensory quality assessment index score values in table 1
Implication, comprehensive grading is carried out to the aesthetic quality of electronic cigarette tobacco tar using hundred-mark system point system, and every evaluation index presses 15 points
System and twenty point system scoring.
The electronic cigarette tobacco tar sensory quality assessment index of table 1 and score value implication table
Evaluation method：Evaluation index and score value in table 1, member of smoking should carry out aesthetic quality to each evaluation index
Evaluate, and record its evaluation result, the minimum score unit of score value is 0.5.
Result is counted：Remove one minimum point and a best result in the sensory quality assessment result of all members of smoking, count
The arithmetic mean of instantaneous value of remaining effective single item evaluation index scoring is calculated, as a result retains two-decimal, the sense of last electronic cigarette tobacco tar
Official's quality evaluation comprehensive grading is the arithmetic mean of instantaneous value sum for calculating each single index scoring, obtains total score, as a result retains one
Decimal.Total score score value is higher, then it represents that the sensory evaluation effect of this electronics tobacco tar is better, the evaluation of above-described embodiment comparative example
The results are shown in Table 2.
The evaluation result of the embodiment comparative example of table 2
| Evaluation index | Excitant | Satisfaction | Feature style | Tobacco is fragrant | Fragrance | Smoke amount | Total score |
| Embodiment 1 | 12.01 | 16.5 | 12.0 | 12.22 | 11.4 | 15.6 | 79.7 |
| Embodiment 2 | 11.0 | 16.4 | 12.1 | 12.0 | 11.4 | 15.62 | 78.5 |
| Embodiment 3 | 11.98 | 16.38 | 12.0 | 11.98 | 11.4 | 15.65 | 79.4 |
| Embodiment 4 | 11.99 | 16.42 | 12.0 | 12.0 | 11.1 | 15.6 | 79.1 |
The result of table 2 shows that smoke amount is sufficient when electronic cigarette tobacco tar is embodied in suction in above-described embodiment, and fragrance enriches
Strong, strength is moderate, comfortable taste, shortens the aesthetic quality's difference with traditional cigarette.Integrated comparative, the effect of embodiment 1 is most
It is excellent.Types of fruits and ratio, food flavor species and ratio, propane diols, glycerine, food flavor, the fruit for being used and breast
Mixed extract adding proportion of product etc. produces Different Effects to 6 indexs.
Embodiment described above only expresses several embodiments of the invention, and its description is more specific and detailed, but simultaneously
Therefore the limitation to the scope of the claims of the present invention can not be interpreted as.It should be pointed out that for one of ordinary skill in the art
For, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to guarantor of the invention
Shield scope.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.
Claims (10)
1. a kind of electronic cigarette tobacco tar, it is characterised in that the component including following mass percent：
The atomized liquid of 95%-99%, the fruit of 1%-5% and the mixed extract of dairy products；
The fruit is 1 according to mass ratio by fruit and dairy products with the mixed extract of dairy products:1-10:Extracted after 1 mixing
Form, the fruit includes at least one in apple, pears, grape and strawberry, the dairy products include milk, cheese and cream
In at least one.
2. electronic cigarette tobacco tar as claimed in claim 1, it is characterised in that in the electronic cigarette tobacco tar, the fruit is made with breast
The mass percent of the mixed extract of product is 2%-4%.
3. electronic cigarette tobacco tar as claimed in claim 1, it is characterised in that the fruit also includes banana, blueberry, pineapple, lemon
At least one in lemon, hawthorn, red tangerine and lichee.
4. electronic cigarette tobacco tar as claimed in claim 3, it is characterised in that the mixed extract of the fruit and dairy products by with
Extracted after the component mixing of lower mass percent and formed：Apple 5%-50%, strawberry 5%-50%, dairy products 10%-50%, pears
2%-10%, banana 1%-10%, blueberry 1%-10%, pineapple 2%-10%, grape 1%-10%, lemon 1%-10%, mountain
Short, bristly hair or beard 1%-10%, red tangerine 1%-10%, lichee 2%-10%.
5. electronic cigarette tobacco tar as claimed in claim 4, it is characterised in that the mixed extract of the fruit and dairy products by with
Extracted after the component mixing of lower mass percent and formed：Apple 5%-30%, strawberry 5%-35%, dairy products 10%-50%, pears
2%-6%, banana 1%-8%, blueberry 1%-10%, pineapple 2%-8%, grape 1%-10%, lemon 1%-6%, hawthorn
1%-10%, red tangerine 1%-8%, lichee 2%-10%.
6. electronic cigarette tobacco tar as claimed in claim 1, it is characterised in that the atomized liquid includes that food flavor, tobacco are extracted
Thing and organic solvent, the food flavor include Ethyl vanillin, citronellol, ethyl acetate, geraniol, linalool, rhodinol,
At least one in dorinone, Megastigmatrienone, dihydroactinidiolide, alpha, beta-lonone and phenmethylol, it is described organic molten
Agent includes at least one in propane diols and glycerine.
7. electronic cigarette tobacco tar as claimed in claim 6, it is characterised in that in the electronic cigarette tobacco tar, the quality of food flavor
Percentage is 1%-10%, and the mass percent of tobacco extract is 1%-5%, and the mass percent of propane diols is 10%-
80%, the mass percent of glycerine is 10%-80%.
8. electronic cigarette tobacco tar as claimed in claim 1, it is characterised in that the mixed extract of the fruit and dairy products according to
Following steps are extracted and obtained：
After the fruit is crushed, dairy products are added, form mixture, the fruit is 1 with the mass ratio of the dairy products:1-
10:1；Supercritical carbon dioxide fluid is subsequently adding, supercritical extract is carried out to fruit and dairy products by isothermal pressure-changing method, obtained
To the fruit and the mixed extract of dairy products.
9. electronic cigarette tobacco tar as claimed in claim 8, it is characterised in that the mixture is placed in extractor, adds super
Critical carbon dioxide fluid, is 20.0 DEG C -50.0 DEG C in temperature, and pressure is extracted to be stirred under 7.0MPa-10.0MPa
The supercritical carbon dioxide fluid of solute is taken, the supercritical carbon dioxide fluid for having extracted solute has been entered by expansion valve
Enter in separator, reduce pressure to 6.0MPa-6.9MPa, the solute separates out the mixing extraction for obtaining the fruit and dairy products
Thing.
10. a kind of preparation method of electronic cigarette tobacco tar, it is characterised in that comprise the following steps：
Mass percent is respectively into the atomized liquid of 95%-99% and the fruit of 1%-5% to be mixed with the mixed extract of dairy products
Close, uniform, the prepared electronic cigarette tobacco tar is stirred at room temperature；The mixed extract of the fruit and dairy products is by fruit and breast
Product is 1 according to mass ratio:1-10:Extracts and forms after 1 mixing, the fruit including in apple, pears, grape and strawberry at least
One kind, the dairy products include at least one in milk, cheese and cream.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710052064.XA CN106820270A (en) | 2017-01-20 | 2017-01-20 | A kind of electronic cigarette tobacco tar and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710052064.XA CN106820270A (en) | 2017-01-20 | 2017-01-20 | A kind of electronic cigarette tobacco tar and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106820270A true CN106820270A (en) | 2017-06-13 |
Family
ID=59120721
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710052064.XA Pending CN106820270A (en) | 2017-01-20 | 2017-01-20 | A kind of electronic cigarette tobacco tar and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106820270A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107581655A (en) * | 2017-08-29 | 2018-01-16 | 深圳市真味生物科技有限公司 | A kind of compound dry electronic cigarette tobacco tar and preparation method thereof |
| CN109984374A (en) * | 2019-05-16 | 2019-07-09 | 铂德（深圳）科技有限公司 | Citrus extracts solution, citrus electronics tobacco tar and preparation method thereof |
| CN113412960A (en) * | 2021-07-29 | 2021-09-21 | 海南张文科黑骨草生物科技有限公司 | Adhatoda petiolata-based lemon-flavored extract and preparation method thereof |
| CN115813006A (en) * | 2022-09-05 | 2023-03-21 | 东莞市鸿馥生物科技有限公司 | Electronic cigarette liquid capable of improving fruit aroma and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1878480A (en) * | 2003-11-03 | 2006-12-13 | 美国无烟烟草公司 | Flavored smokeless tobacco and methods of making |
| CN102309061A (en) * | 2011-03-17 | 2012-01-11 | 广州市澳键丰泽生物科技有限公司 | Tobacco feeding essence formula |
| CN104770865A (en) * | 2015-03-03 | 2015-07-15 | 华健 | Aromatic plant electronic atomization liquid and preparation method thereof |
| CN105192877A (en) * | 2015-09-21 | 2015-12-30 | 深圳瀚星翔科技有限公司 | Electronic cigarette tobacco tar, preparation method thereof, and electronic cigarette |
| CN105670790A (en) * | 2016-01-18 | 2016-06-15 | 广西中烟工业有限责任公司 | Tobacco flavor with natural sweet fruity aroma characteristics and preparation method thereof |
-
2017
- 2017-01-20 CN CN201710052064.XA patent/CN106820270A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1878480A (en) * | 2003-11-03 | 2006-12-13 | 美国无烟烟草公司 | Flavored smokeless tobacco and methods of making |
| CN102309061A (en) * | 2011-03-17 | 2012-01-11 | 广州市澳键丰泽生物科技有限公司 | Tobacco feeding essence formula |
| CN104770865A (en) * | 2015-03-03 | 2015-07-15 | 华健 | Aromatic plant electronic atomization liquid and preparation method thereof |
| CN105192877A (en) * | 2015-09-21 | 2015-12-30 | 深圳瀚星翔科技有限公司 | Electronic cigarette tobacco tar, preparation method thereof, and electronic cigarette |
| CN105670790A (en) * | 2016-01-18 | 2016-06-15 | 广西中烟工业有限责任公司 | Tobacco flavor with natural sweet fruity aroma characteristics and preparation method thereof |
Non-Patent Citations (6)
| Title |
|---|
| 建康: "聚会大餐之后吃什么可排毒", 《健康生活》 * |
| 张利，郭晔堃等: "抗痛风药物的临床研究进展", 《药物临床》 * |
| 成喜玲: "我国浓缩苹果汁加工业发展的优势分析", 《农业经济》 * |
| 熊国玺，朱巍等: "超临界CO2萃取与分子蒸馏联用技术在烟草香味成分提取中的应用", 《湖北农业科学》 * |
| 董洋，范志红: "乳类食物与痛风防控", 《中国乳品工业》 * |
| 陈光远，张瑞明等: "五味沙棘含片治疗急性咽炎的随机对照临床研究", 《华西医学》 * |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107581655A (en) * | 2017-08-29 | 2018-01-16 | 深圳市真味生物科技有限公司 | A kind of compound dry electronic cigarette tobacco tar and preparation method thereof |
| CN107581655B (en) * | 2017-08-29 | 2020-10-02 | 深圳市真味生物科技有限公司 | Compound sweet-taste-free electronic cigarette tobacco tar and preparation method thereof |
| CN109984374A (en) * | 2019-05-16 | 2019-07-09 | 铂德（深圳）科技有限公司 | Citrus extracts solution, citrus electronics tobacco tar and preparation method thereof |
| CN113412960A (en) * | 2021-07-29 | 2021-09-21 | 海南张文科黑骨草生物科技有限公司 | Adhatoda petiolata-based lemon-flavored extract and preparation method thereof |
| CN115813006A (en) * | 2022-09-05 | 2023-03-21 | 东莞市鸿馥生物科技有限公司 | Electronic cigarette liquid capable of improving fruit aroma and preparation method thereof |
| CN115813006B (en) * | 2022-09-05 | 2023-08-18 | 东莞市鸿馥生物科技有限公司 | Electronic cigarette liquid capable of improving fruit fragrance and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106617266B (en) | Tobacco juice for electronic smoke | |
| CN103989244B (en) | A kind of Chinese style tobacco juice for electronic smoke and preparation method thereof | |
| CN103989245B (en) | The Chinese style flue-cured tobacco odor type tobacco juice for electronic smoke of the sweet soapy feeling in a kind of effective reduction oral cavity | |
| CN104983066B (en) | A kind of substitute of tobacco and preparation method thereof | |
| CN101444331B (en) | Ultrahigh-pressure extraction method of honeysuckle flower, wild chrysanthemum and mulberry leaf and application of extract liquid thereof | |
| CN106333384B (en) | A kind of mixed type tobacco molecular distillation light component electronic cigarette liquid and preparation method thereof | |
| CN106912982A (en) | A kind of electronic cigarette tobacco tar and preparation method thereof | |
| CN106962971A (en) | Electronic cigarette tobacco tar and preparation method thereof | |
| CN106820270A (en) | A kind of electronic cigarette tobacco tar and preparation method thereof | |
| CN101666062A (en) | Tipping paper added with Chinese herbal medicinal additive and preparation method thereof | |
| CN106136303B (en) | A kind of preparation method and applications of cape jasmine cigarette extract | |
| CN106723301A (en) | Tobacco juice for electronic smoke | |
| CN104544543A (en) | Electronic cigarette smoke solution prepared through black tea leaf extract | |
| CN107549868A (en) | Electronic cigarette tobacco tar and preparation method thereof | |
| CN108703408A (en) | Tobacco juice for electronic smoke | |
| CN109123764A (en) | A kind of preparation method of Bin phenol cigarette | |
| CN106858705A (en) | A kind of tobacco juice for electronic smoke for containing 3 oxo-alpha violet alcohol radical β D glucopyranosides | |
| CN104544544A (en) | Electronic cigarette smoke solution prepared through white tea leaf extract | |
| CN109718330A (en) | One kind is refreshed oneself type aiding smoking cessation Neulized inhalation beverage and preparation method thereof | |
| CN108949347A (en) | Increase the essence and its preparation method and application for heating the new cigarette flue gas moist feeling that do not burn | |
| CN105105315B (en) | A kind of clear throat type tobacco powder spray and preparation method thereof | |
| CN107057856A (en) | A kind of mouth rod increases profit essence preparation method with radix glycyrrhizae is sweetened | |
| WO2023116222A1 (en) | Atomization base solution, cigarette liquid and electronic atomization apparatus | |
| CN110358630A (en) | A kind of clear spicy tobacco aromaticss, preparation method and the application in cigarette | |
| CN112617548A (en) | Kyara extract for preparing latex pillow for improving sleep, preparation method and latex pillow prepared from Kyara extract |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170613 |
|
| RJ01 | Rejection of invention patent application after publication |