CN104489913A - E-cigarette nicotine liquid with functions of heat clearing and fire removing - Google Patents
E-cigarette nicotine liquid with functions of heat clearing and fire removing Download PDFInfo
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- CN104489913A CN104489913A CN201410788639.0A CN201410788639A CN104489913A CN 104489913 A CN104489913 A CN 104489913A CN 201410788639 A CN201410788639 A CN 201410788639A CN 104489913 A CN104489913 A CN 104489913A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
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Abstract
The invention discloses E-cigarette nicotine liquid with functions of heat clearing and removing fire. The E-cigarette nicotine liquid comprises, by weight, 50 to 80 parts of propylene glycol, 5 to 30 parts of glycerol, 2 to 5 parts of edible alcohol , 1 to 30 parts of tobacco extract, 0.5 to 15 parts of tobacco flavor, and 0.5 to 10 parts of herbal extract. The herbal extract with the functions of heat clearing and fire removing is prepared and mixed with the tobacco extract, mixture is modified with the proper amount of the tobacco flavor, and the E-cigarette nicotine liquid which has rich fragrance, good taste and high satisfying ability and has the health functions of heat clearing and fire removing is prepared.
Description
Technical field
The present invention relates to electronic cigarette technical field, particularly a kind of tobacco juice for electronic smoke with heat-clearing and fire-reducing function.
Background technology
Traditional cigarette is generally provide nicotine and relevant aroma components by the mode of cigarette of burning to consumer.Because the reasons such as Pintsch process and flue gas migration cause containing a large amount of harmful components in main flume in sucking process, fraction is wherein had to have carcinogenic danger as condensed-nuclei aromatics is proved.Also produce a large amount of flue gas smog in the process of smoking property of cigarette, not only cause environmental pollution, also bring the harm of second-hand-cigarette simultaneously to non-smoker.Along with the progressively enforcement of the international Framework Convention on Tobacco Control and the enhancing gradually of health of people consciousness, traditional cigarette selling market is subject to powerful impact.Electronic cigarette takes atomizing type to generate smog sensation, does not produce tar and CO, produces second-hand-cigarette harm hardly simultaneously, is regarded as non-harmful smoking cessation product or substitute of tobacco, receives showing great attention to and extensively studying of domestic and international each large tobacco enterprise.The selling market of current electronic cigarette is mainly in the U.S., and Europe, Asia then possess good growth trends, and particularly the market of China Electronics's cigarette is also in the cultivation and exploitation stage.The electronic cigarette product taste developed at present is partial to blended type cigarette, compares the taste custom meeting foreign consumers, and Chinese Consumer's preference flue-cured tobacco, taste is comparatively strong, and the mouthfeel of electronic cigarette is difficult to reach requirement.It is the key opening Chinese market that improvement electronic cigarette formula of liquid makes it to meet Chinese Consumer's custom.
Electronic cigarette, as a kind of form in novel tobacco goods, presents great market prospect, and reason is mainly to provide the consumption habit similar with traditional cigarette and satisfaction on the one hand, and the hazard index of electronic cigarette reduces greatly than traditional cigarette on the other hand.Electronic cigarette formula of liquid is the key highlighting electronic cigarette advantage.In order to simulate the fragrance of traditional cigarette, fragrance and mouthfeel to the full extent, solution the most general at present adds tobacco extract in tobacco juice.Tobacco juice for electronic smoke is mixed to get according to a certain ratio by the essential oil of tobaccos and Alevaire, flavouring essence for tobacco that extract acquisition.The less harmful of electronic cigarette is that what to make to suck human body by incombustible mode is atomized liquid and non-burning pyrolysis product.But still there is the uncomfortable shortcoming without health-care efficacy of mouthfeel in tobacco juice for electronic smoke of the prior art.
Summary of the invention
The shortcoming of prior art in view of the above, the object of the present invention is to provide a kind of tobacco juice for electronic smoke with heat-clearing and fire-reducing function, improving, tobacco juice for electronic smoke mouthfeel in prior art is not good, on the fragrant not enough basis of tobacco, gives the health care of tobacco juice for electronic smoke heat-clearing and fire-reducing.
To achieve these goals or other objects, the present invention is achieved by the following technical solutions.
A kind of tobacco juice for electronic smoke, described tobacco juice for electronic smoke comprises following raw material components and weight portion:
Preferably, described tobacco juice for electronic smoke, its raw material according to the mass fraction, comprises following component:
Most preferred, described tobacco juice for electronic smoke, its raw material according to the mass fraction, comprises following component:
Described Chinese herbal medicine be selected from honeysuckle, the capsule of weeping forsythia, the root of large-flowered skullcap, golden cypress, the coptis, giant knotweed, cape jasmine, Paris polyphylla, radix bupleuri, isatis root, dandelion, the root bark of Chinese wolf-berry, the wind-weed, radix rehmanniae recen, radix scrophulariae, the sterculia seed, sargentodoxa cuneata, the radix paeoniae rubrathe, the Chinese bulbul, moutan bark one or more.
Preferably, Chinese herbal medicine described in the present invention comprises honeysuckle 100g, root of large-flowered skullcap 50g, cape jasmine 50g, radix bupleuri 75g, isatis root 50g, dandelion 50g, sterculia seed 100g; Or described Chinese herbal medicine comprises honeysuckle 50g, cape jasmine 50g, isatis root 50g, sterculia seed 100g, Chinese bulbul 50g, radix scrophulariae 50g, moutan bark 50g; Or described Chinese herbal medicine comprises sterculia seed 100g, cape jasmine 50g, radix bupleuri 75g, isatis root 50g, radix scrophulariae 50g, moutan bark 50g, capsule of weeping forsythia 50g.
Chinese herbal medicine extract described in the present invention can adopt method conventional in prior art to obtain.
Preferably, Chinese herbal medicine extract adopts following preparation method to obtain: Chinese herbal medicine is ground into 40 ~ 100 object powder, adds solvent and seal immersion; Afterwards soaking solution is added hot reflux and obtain extract, gained extract is got supernatant and is used filtering with microporous membrane after centrifugation; Namely last gained filtrate obtain Chinese herbal medicine extract by reduced pressure concentration.
Preferably, Chinese herbal medicine is ground into 40 ~ 60 object powder.
Preferably, described solvent is the mixed solvent of ethanol and water, and with the entire volume of mixed solvent, the volumn concentration of ethanol is 40 ~ 80%.
Preferably, the mass ratio of described Chinese herbal medicine and described solvent is 1:2 ~ 5.More preferably, the mass ratio of described Chinese herbal medicine and described solvent is 1:2.5 ~ 3.5.
Preferably, described heating reflux temperature is 80 ~ 120 DEG C, and heating return time is 1 ~ 5h.More preferably, described heating reflux temperature is 100 DEG C, and heating return time is 2.5 ~ 3.5h.
Preferably, in the preparation method of the Chinese herbal medicine extract in the present invention, above-mentioned extract is obtained supernatant after centrifugal 10 ~ 30 minutes under 2500 ~ 4000r/min; More preferably centrifugal 20min under 4000r/min.
Preferably, described miillpore filter is the miillpore filter that aperture is not more than 0.5 μm.More preferably, described miillpore filter is the miillpore filter in 0.45 μm, aperture.
Preferably, in the preparation method of the Chinese herbal medicine extract in the present invention, above-mentioned filtrate reduced pressure concentration at 50 ~ 90 DEG C is obtained concentrate.More preferably, reduced pressure concentration temperature is 60-80 DEG C.
Offal described in the present invention is by one or more combinations in flue-cured tobacco, air-curing of tobacco leaves and suncured tabacco; Described air-curing of tobacco leaves comprises burley tobaccos, Maryland; Described suncured tabacco comprises Turkish tobaccos, Dark sun-cured, Sun cured tobacco and Nicotiniana rustica.
Preferably, described offal is the composition of flue-cured tobacco and burley tobaccos, and the mass percent of described flue-cured tobacco and white rib is 1:0.9 ~ 1.1.
Tobacco extract described in the present invention can adopt method conventional in prior art to obtain.
Preferably, described tobacco extract is for obtain by following preparation method: added by offal in solvent, through sedimentation, filtration and reduced pressure concentration and get final product after ultrasonic extraction.
Preferably, described offal is 40 ~ 100 orders; More preferably, described offal is 40 ~ 60 orders.
Preferably, described solvent is water or ethanol, and the mass ratio of described offal and described solvent is 1:2 ~ 5.
More preferably, the mass ratio of described offal and described solvent is 1:2.5 ~ 3.5.
Preferably, ultrasonic time is 2 ~ 5h.More preferably, ultrasonic time is 3.5 ~ 4.5h.
Preferably, ultrasonic under 30 ~ 60 DEG C of conditions.More preferably, time ultrasonic, temperature is 40 ~ 60 DEG C.
Preferably, carry out under being concentrated in 50 ~ 90 DEG C of conditions.More preferably, thickening temperature controls at 60 ~ 80 DEG C.
The present invention does not have special restriction to the kind of described tobacco essence and source, adopts flavouring essence for tobacco well known to those skilled in the art.
Preferably; described flavouring essence for tobacco is selected from Ethyl vanillin, benzyl acetate, furfural, dorinone, β-damascone, Megastigmatrienone, dihydroactinidiolide, dimethyl succinate, 2; 6; 6-trimethyl-2-cyclohexene-1; 4-diketone, 2-hydroxyl-3; 5; 5-trimethyl-2-cyclonene, geranyl acetone, alpha, beta-lonone, phenmethylol, palmitic acid, isovaleric acid, 2 methyl valeric acid, indoles, pyridine, 3-acetylpyridine, 2; one or more combinations in 3,5-trimethylpyrazine.
More preferably, described flavouring essence for tobacco is the mixture comprising 8wt% dorinone, 5wt% β-damascone, 13wt% Megastigmatrienone, 24wt% alpha, beta-lonone, 9wt% Ethyl vanillin, 7wt% benzyl acetate, 5wt% furfural, 5wt% phenmethylol, 4wt% palmitic acid, 12wt% dihydroactinidiolide, 8wt% dimethyl succinate.
The invention also discloses a kind of preparation method of tobacco juice for electronic smoke as described above, for according to each raw material components weight portion by propane diols, glycerine, edible alcohol, tobacco extract, flavouring essence for tobacco, and Chinese herbal medicine extract mixes.
Many Chinese herbal medicine compositions not only have certain characteristic flavor compounds, also have certain health-care effect simultaneously, have even and alleviate some disease effect.Tobacco extract is combined with Chinese herbal medicine extract, not only compensate for the shortcoming of tobacco juice for electronic smoke flavor component deficiency to a certain extent, be different from external tobacco juice for electronic smoke simultaneously, the tobacco juice for electronic smoke of Chinese style characteristic can be built, meet consumer's custom, certain health-care effect is provided simultaneously.
The present invention has the Chinese herbal medicine extract of heat-clearing and fire-reducing function by preparation, afterwards it is mixed with tobacco extract, be aided with and use suitable essence spice for cigarette to modify, can prepare that fragrance enriches, comfortable taste, satisfaction are got well and there is the tobacco juice for electronic smoke of certain heat-clearing and fire-reducing health care.
The Chinese herbal medicine extract with heat-clearing and fire-reducing function provided by the present invention, is mixed to get tobacco juice for electronic smoke with tobacco extract, flavouring essence for tobacco, propane diols, glycerine etc.Compared with prior art, the present invention has following beneficial effect:
(1) the present invention is by mixing the Chinese herbal medicine extract with heat-clearing and fire-reducing function with tobacco extract, make tobacco juice for electronic smoke fragrance abundanter, fragrance is coordinated more, and satisfaction is good, to some extent solves the shortcoming of tobacco juice for electronic smoke fragrance and taste deficiency.
(2) tobacco juice for electronic smoke of the present invention generates smog sensation owing to taking atomizing type, does not produce tar and CO, does not produce second-hand-cigarette harm simultaneously.
(3) the present invention is by adding containing the Chinese herbal medicine extract with heat-clearing and fire-reducing function, has the effect such as reducing fever and causing diuresis, removing pattogenic heat from the blood and toxic material from the body.
Detailed description of the invention
Below by way of specific instantiation, embodiments of the present invention are described, those skilled in the art the content disclosed by this description can understand other advantages of the present invention and effect easily.The present invention can also be implemented or be applied by detailed description of the invention different in addition, and the every details in this description also can based on different viewpoints and application, carries out various modification or change not deviating under spirit of the present invention.
Embodiment 1
There is provided a kind of tobacco juice for electronic smoke in the present embodiment, described tobacco juice for electronic smoke comprises following raw material components and weight portion:
Adopt the existing mix and blend instruments such as vortex oscillator to mix above-mentioned each component, namely obtain tobacco juice for electronic smoke.
In the present embodiment, the preparation method of tobacco extract is: get cured tobacco leaf sample dry 3h in 40 DEG C of baking ovens, after being cooled to room temperature, is crushed to 40 ~ 100 object offals.Take the conical flask that 100g offal is placed in 1L, add 300mL deionized water, ultrasonic extraction 4h under 50 ± 5 DEG C of conditions, standing sedimentation 4h afterwards, sand core funnel filters to get filtrate, and vacuum rotary steam is concentrated into 3mL, obtains tobacco extract.
Flavouring essence for tobacco in the present embodiment is composed as follows: the mixture of 8wt% dorinone, 5wt% β-damascone, 13wt% Megastigmatrienone, 24wt% alpha, beta-lonone, 9wt% Ethyl vanillin, 7wt% benzyl acetate, 5wt% furfural, 5wt% phenmethylol, 4wt% palmitic acid, 12wt% dihydroactinidiolide, 8wt% dimethyl succinate.Said mixture can adopt instrument such as vortex oscillator etc. conventional in prior art to mix.
In the present embodiment, the extracting method of Chinese herbal medicine extract is: take honeysuckle 100g, root of large-flowered skullcap 50g, cape jasmine 50g, radix bupleuri 75g, isatis root 50g, dandelion 50g, sterculia seed 100g, grind as mixing after 40-100 order powder through pulverizer, with the aqueous solution of the ethanol containing 80% volume fraction for solvent, controlling feed liquid mass ratio is 1:3, shake up, sealing, soaked overnight.By soaked vlil 3h, be separated liquid and the dregs of a decoction after extraction, extract obtains supernatant in the centrifugal 20min of 4000r/min, supernatant 0.45 μm of membrane filtration, control temperature is 70 ± 10 DEG C, and vacuum rotary steam is concentrated into 14mL, and gained liquid is Chinese herbal medicine extract.
Wherein, glycerine and propane diols are food grade product.
The tobacco juice for electronic smoke obtained is smoked panel test by the present invention, and result is as shown in table 2, and table 2 is the smoking result of the tobacco juice for electronic smoke that the embodiment of the present invention and comparative example obtain.
Embodiment 2
There is provided a kind of tobacco juice for electronic smoke in the present embodiment, described tobacco juice for electronic smoke comprises following raw material components and weight portion:
Adopt the existing mix and blend instruments such as vortex oscillator to mix above-mentioned each component, namely obtain tobacco juice for electronic smoke.
In the present embodiment, the preparation method of tobacco extract is: get burley tobaccos tobacco sample dry 3h in 40 DEG C of baking ovens, after being cooled to room temperature, is crushed to 40 ~ 100 object offals.Take the conical flask that 100g offal is placed in 1L, add 300mL deionized water, ultrasonic extraction 4h under 50 ± 5 DEG C of conditions, standing sedimentation 4h afterwards, sand core funnel filters to get filtrate, and vacuum rotary steam is concentrated into 3mL, obtains tobacco extract.
Flavouring essence for tobacco in the present embodiment is composed as follows: the mixture of 8wt% dorinone, 5wt% β-damascone, 13wt% Megastigmatrienone, 24wt% alpha, beta-lonone, 9wt% Ethyl vanillin, 7wt% benzyl acetate, 5wt% furfural, 5wt% phenmethylol, 4wt% palmitic acid, 12wt% dihydroactinidiolide, 8wt% dimethyl succinate.Said mixture can adopt instrument such as vortex oscillator etc. conventional in prior art to mix.
In the present embodiment, the extracting method of Chinese herbal medicine extract is: take honeysuckle 50g, cape jasmine 50g, isatis root 50g, sterculia seed 100g, Chinese bulbul 50g, radix scrophulariae 50g, moutan bark 50g, through pulverizer grind be 40 ~ 100 order powder after mix, with the aqueous solution of the ethanol containing 80% volume fraction for solvent, Mass Control is than being 1:3, shake up, sealing, soaked overnight.By soaked vlil 3h, be separated liquid and the dregs of a decoction after extraction, extract obtains supernatant in the centrifugal 20min of 4000r/min, supernatant 0.45 μm of membrane filtration, control temperature is 70 ± 10 DEG C, and vacuum rotary steam is concentrated into 12mL, and gained liquid is Chinese herbal medicine extract.
Wherein, glycerine and propane diols are food grade product.
The tobacco juice for electronic smoke obtained is smoked panel test by the present invention, and result is as shown in table 2, and table 2 is the smoking result of the tobacco juice for electronic smoke that the embodiment of the present invention and comparative example obtain.
Embodiment 3
There is provided a kind of tobacco juice for electronic smoke in the present embodiment, described tobacco juice for electronic smoke comprises following raw material components and weight portion:
Adopt the existing mix and blend instruments such as vortex oscillator to mix above-mentioned each component, namely obtain tobacco juice for electronic smoke.
In the present embodiment, the preparation method of tobacco extract is: get Sun cured tobacco tobacco sample dry 3h in 40 DEG C of baking ovens, after being cooled to room temperature, is crushed to 40 ~ 100 object offals.Take the conical flask that 100g offal is placed in 1L, add 300mL deionized water, ultrasonic extraction 4h under 50 ± 5 DEG C of conditions, standing sedimentation 4h afterwards, sand core funnel filters to get filtrate, and vacuum rotary steam is concentrated into 3mL, obtains tobacco extract.
Flavouring essence for tobacco in the present embodiment is composed as follows: the mixture of 8wt% dorinone, 5wt% β-damascone, 13wt% Megastigmatrienone, 24wt% alpha, beta-lonone, 9wt% Ethyl vanillin, 7wt% benzyl acetate, 5wt% furfural, 5wt% phenmethylol, 4wt% palmitic acid, 12wt% dihydroactinidiolide, 8wt% dimethyl succinate.Said mixture can adopt instrument such as vortex oscillator etc. conventional in prior art to mix.
In the present embodiment, the extracting method of Chinese herbal medicine extract is: take sterculia seed 100g, cape jasmine 50g, radix bupleuri 75g, isatis root 50g, radix scrophulariae 50g, moutan bark 50g, the capsule of weeping forsythia through 50g, through pulverizer grind be 40 ~ 100 order powder after mix, with the aqueous solution of the ethanol containing 80% volume fraction for solvent, controlling material quality is 1:3, shake up, sealing, soaked overnight.By soaked vlil 3h, be separated liquid and the dregs of a decoction after extraction, extract obtains supernatant in the centrifugal 20min of 4000r/min, supernatant 0.45 μm of membrane filtration, control temperature is 70 ± 10 DEG C, and vacuum rotary steam is concentrated into 13mL, and gained liquid is Chinese herbal medicine extract.
Wherein, glycerine and propane diols are food grade product.
The tobacco juice for electronic smoke obtained is smoked panel test by the present invention, and result is as shown in table 2, and table 2 is the smoking result of the tobacco juice for electronic smoke that the embodiment of the present invention and comparative example obtain.
Embodiment 4
There is provided a kind of tobacco juice for electronic smoke in the present embodiment, described tobacco juice for electronic smoke comprises following raw material components and weight portion:
Adopt the existing mix and blend instruments such as vortex oscillator to mix above-mentioned each component, namely obtain tobacco juice for electronic smoke.
In the present embodiment, the preparation method of tobacco extract is: the flue-cured tobacco and the burley tobaccos tobacco sample dry 3h in 40 DEG C of baking ovens that get 1:1, after being cooled to room temperature, be crushed to 40 ~ 100 object offals.Take the conical flask that 100g offal is placed in 1L, add 300mL deionized water, ultrasonic extraction 4h under 50 ± 5 DEG C of conditions, standing sedimentation 4h afterwards, sand core funnel filters to get filtrate, and vacuum rotary steam is concentrated into 3mL, obtains tobacco extract.
Flavouring essence for tobacco in the present embodiment is composed as follows: the mixture of 8wt% dorinone, 5wt% β-damascone, 13wt% Megastigmatrienone, 24wt% alpha, beta-lonone, 9wt% Ethyl vanillin, 7wt% benzyl acetate, 5wt% furfural, 5wt% phenmethylol, 4wt% palmitic acid, 12wt% dihydroactinidiolide, 8wt% dimethyl succinate.Said mixture can adopt instrument such as vortex oscillator etc. conventional in prior art to mix.
In the present embodiment, the extracting method of Chinese herbal medicine extract is: take sterculia seed 100g, cape jasmine 50g, radix bupleuri 75g, isatis root 50g, radix scrophulariae 50g, moutan bark 50g, the capsule of weeping forsythia through 50g, through pulverizer grind be 40 ~ 100 order powder after mix, with the aqueous solution of the ethanol containing 80% volume fraction for solvent, Mass Control is than being 1:3, shake up, sealing, soaked overnight.By soaked vlil 3h, be separated liquid and the dregs of a decoction after extraction, extract obtains supernatant in the centrifugal 20min of 4000r/min, supernatant 0.45 μm of membrane filtration, control temperature is 70 ± 10 DEG C, and vacuum rotary steam is concentrated into 13mL, and gained liquid is Chinese herbal medicine extract.
Wherein, glycerine and propane diols are food grade product.
The tobacco juice for electronic smoke obtained is smoked panel test by the present invention, and result is as shown in table 2, and table 2 is the smoking result of the tobacco juice for electronic smoke that the embodiment of the present invention and comparative example obtain.
Embodiment 5
There is provided a kind of tobacco juice for electronic smoke in the present embodiment, described tobacco juice for electronic smoke comprises following raw material components and weight portion:
Adopt the existing mix and blend instruments such as vortex oscillator to mix above-mentioned each component, namely obtain tobacco juice for electronic smoke.
In the present embodiment, the preparation method of tobacco extract is: the flue-cured tobacco and the burley tobaccos tobacco sample dry 3h in 40 DEG C of baking ovens that get 1:1, after being cooled to room temperature, be crushed to 40 ~ 100 object offals.Take the conical flask that 100g offal is placed in 1L, add 300mL deionized water, ultrasonic extraction 4h under 50 ± 5 DEG C of conditions, standing sedimentation 4h afterwards, sand core funnel filters to get filtrate, and vacuum rotary steam is concentrated into 3mL, obtains tobacco extract.
Flavouring essence for tobacco in the present embodiment is composed as follows: 8wt% dorinone, 5wt% β-damascone, 13wt% Megastigmatrienone, 24wt% alpha, beta-lonone, 9wt% Ethyl vanillin, 7wt% benzyl acetate, 5wt% furfural, 5wt% phenmethylol, 4wt% palmitic acid, 12wt% dihydroactinidiolide, 8wt% dimethyl succinate mixture.Said mixture can adopt instrument such as vortex oscillator etc. conventional in prior art to mix.
In the present embodiment, the extracting method of Chinese herbal medicine extract is: take honeysuckle 50g, cape jasmine 50g, isatis root 50g, Chinese bulbul 50g, radix scrophulariae 50g, moutan bark 50g, through pulverizer grind be 40 ~ 100 order powder after mix, with the aqueous solution of the ethanol containing 80% volume fraction for solvent, Mass Control is than being 1:3, shake up, sealing, soaked overnight.By soaked vlil 3h, be separated liquid and the dregs of a decoction after extraction, extract obtains supernatant in the centrifugal 20min of 4000r/min, supernatant 0.45 μm of membrane filtration, control temperature is 50 ± 10 DEG C, and vacuum rotary steam is concentrated into 15mL, and gained liquid is Chinese herbal medicine extract.
Wherein, glycerine and propane diols are food grade product.
The tobacco juice for electronic smoke obtained is smoked panel test by the present invention, and result is as shown in table 2, and table 2 is the smoking result of the tobacco juice for electronic smoke that the embodiment of the present invention and comparative example obtain.
Comparative example 1 (not containing Chinese herbal medicine extract)
There is provided a kind of tobacco juice for electronic smoke in the present embodiment, described tobacco juice for electronic smoke comprises following raw material components and weight portion:
Wherein tobacco extract composition and extracting mode, flavouring essence for tobacco formula are with embodiment 1;
The tobacco juice for electronic smoke obtained is smoked panel test by the present invention, and result is as shown in table 2, and table 2 is the smoking result of the tobacco juice for electronic smoke that the embodiment of the present invention and comparative example obtain.
Comparative example 2 (not containing Chinese herbal medicine extract)
There is provided a kind of tobacco juice for electronic smoke in the present embodiment, described tobacco juice for electronic smoke comprises following raw material components and weight portion:
Wherein tobacco extract composition and extracting mode, flavouring essence for tobacco formula are with embodiment 4;
The tobacco juice for electronic smoke obtained is smoked panel test by the present invention, and result is as shown in table 2, and table 2 is the smoking result of the tobacco juice for electronic smoke that the embodiment of the present invention and comparative example obtain.
Tobacco juice for electronic smoke in above-described embodiment and comparative example is added in electronic cigarette device and carries out sensory effects evaluation respectively.
Sensory effects evaluation method comprises the following steps:
(1) 9 evaluation indexes are provided with, comprise excitant, satisfaction, concentration, comfort level, feature style, tobacco perfume, aroma quality, perfume quantity and the amount of being fuming, and give different score value according to the Different Effects degree of every evaluation index to tobacco juice for electronic smoke aesthetic quality.
Described excitant refers to: suck the discomfort that flue gas comprises oral cavity to sense organ, throat and nasal cavity produce that tobacco juice for electronic smoke produces through atomization and be subject to.
Described satisfaction refers to: the flue gas strength that tobacco juice for electronic smoke produces through atomization, concentration and note are to the comprehensive impression that sense organ produces;
Described concentration refers to: the impression of tobacco juice for electronic smoke oral cavity filling degree when the flue gas firm suction inlet that atomization produces;
Described comfort level refers to: the impact of flue gas on oral cavity level of comfort after sucking oral cavity and exhalation that tobacco juice for electronic smoke produces through atomization; Described feature style refers to: a kind of tobacco juice for electronic smoke is different from the sense organ Main Differences performance of other homogeneous e cigarette tobacco juices in joyful sense;
Described tobacco perfume (or spice) refers to: in process of smokeing panel test, sensory feel is to the breath of this perfume (or spice) of tobacco;
Described aroma quality refers to: felt the good and bad degree of pleasant breath in process of smokeing panel test by sense of smell and the sense of taste;
Described perfume quantity refers to: in process of smokeing panel test by oral cavity and nasal cavity weigh pleasant breath amount number;
The described amount of being fuming refers to: tobacco juice for electronic smoke through atomization produce exhaust gas volumn number.
(2) member of smoking of 9 people is set, everyone a tobacco juice for electronic smoke sensory quality assessment table, adopt the marking mode secretly commented, adopt the overall method of smokeing panel test that circulates, tobacco juice for electronic smoke is aspirated, according to the implication of 9 sensory quality assessment index score values in table 1, adopt hundred-mark system point system to carry out comprehensive grading to the aesthetic quality of tobacco juice for electronic smoke, every evaluation index is by five points, ten point system or the scoring of ten the five-grade marking systems.The concrete meaning of the score value of tobacco juice for electronic smoke evaluation index sees the following form 1:
The score value implication table of table 1 tobacco juice for electronic smoke sensory quality assessment index
(3) evaluation method: according to the evaluation index in table 1 and score value, member of smoking tackles each evaluation index and carries out sensory quality assessment, and records its evaluation result, and the minimum score unit of score value is 0.5.
(4) result statistics: remove minimum point and a best result in the sensory quality assessment result of all members of smoking, calculate remaining effective single item evaluation index scoring arithmetic mean of instantaneous value, result retains two-decimal, the sensory quality assessment comprehensive grading of last electronic cigarette liquid is the arithmetic mean of instantaneous value sum calculating the scoring of each single index, obtain total score, result retains a decimal.
The evaluation result of above-described embodiment and comparative example is in table 2:
Table 2 tobacco juice for electronic smoke sensory effects evaluation result
Table 2 result shows, the amount of being fuming abundance when tobacco juice for electronic smoke is embodied in suction in above-described embodiment, and fragrance enriches strong, and tobacco and faint medicine perfume are coordinated, and strength is moderate, comfortable taste, and humectation is effective, shortens the aesthetic quality's difference with traditional cigarette.But the Chinese herbal medicine kind used, Tobacco Types, extract adding proportion, essence spice for cigarette adding proportion produce Different Effects to adopted 9 indexs; Chinese herbal medicine extract used can provide the action and efficacy such as heat-clearing and fire-reducing simultaneously.
Above-described embodiment is illustrative principle of the present invention and effect thereof only, but not for limiting the present invention.Any person skilled in the art scholar all without prejudice under spirit of the present invention and category, can modify above-described embodiment or changes.Therefore, such as have in art usually know the knowledgeable do not depart from complete under disclosed spirit and technological thought all equivalence modify or change, must be contained by claim of the present invention.
Claims (10)
1. a tobacco juice for electronic smoke, is characterized in that, described tobacco juice for electronic smoke comprises following raw material components and weight portion:
Described tobacco extract be offal to be added in solvent after ultrasonic extraction through sedimentation, filtration and concentrated after the concentrate that obtains; Described Chinese herbal medicine extract be dry Chinese herbal medicine pulverized, soak, backflow, centrifugal, filter and the concentrated concentrate obtained; Described Chinese herbal medicine be selected from honeysuckle, the capsule of weeping forsythia, the root of large-flowered skullcap, golden cypress, the coptis, giant knotweed, cape jasmine, Paris polyphylla, radix bupleuri, isatis root, dandelion, the root bark of Chinese wolf-berry, the wind-weed, radix rehmanniae recen, radix scrophulariae, the sterculia seed, sargentodoxa cuneata, the radix paeoniae rubrathe, the Chinese bulbul and moutan bark one or more.
2. tobacco juice for electronic smoke as claimed in claim 1; it is characterized in that; described flavouring essence for tobacco is selected from Ethyl vanillin, benzyl acetate, furfural, dorinone, β-damascone, Megastigmatrienone, dihydroactinidiolide, dimethyl succinate, 2; 6; 6-trimethyl-2-cyclohexene-1; 4-diketone, 2-hydroxyl-3; 5; 5-trimethyl-2-cyclonene, geranyl acetone, alpha, beta-lonone, phenmethylol, palmitic acid, isovaleric acid, 2 methyl valeric acid, indoles, pyridine, 3-acetylpyridine and 2; one or more combinations in 3,5-trimethylpyrazine.
3. tobacco juice for electronic smoke as claimed in claim 1, it is characterized in that, described tobacco extract is for obtain by following preparation method: drying tobacco, pulverize to obtain offal, adds solvent, ultrasonic 2 ~ 5h under 30 ~ 60 DEG C of conditions; After sedimentation, filtering, filtrate is reduced pressure concentration at 50 ~ 90 DEG C.
4. tobacco juice for electronic smoke as claimed in claim 3, it is characterized in that, described solvent is water or ethanol, and the mass ratio of described offal and described solvent is 1:2 ~ 5.
5. tobacco juice for electronic smoke as claimed in claim 1, it is characterized in that, Chinese herbal medicine extract adopts following preparation method to obtain: Chinese herbal medicine is ground into 40 ~ 100 object powder, adds solvent and seal immersion; Afterwards soaking solution is added hot reflux and obtain extract, gained extract is got supernatant and is used filtering with microporous membrane after centrifugation; Namely last gained filtrate obtain Chinese herbal medicine extract by reduced pressure concentration.
6. tobacco juice for electronic smoke as claimed in claim 5, it is characterized in that, described solvent is the mixed solvent of ethanol and water, and with the entire volume of mixed solvent, the volumn concentration of ethanol is 40 ~ 80%.
7. tobacco juice for electronic smoke as claimed in claim 5, it is characterized in that, the mass ratio of described Chinese herbal medicine and described solvent is 1:2 ~ 5.
8. tobacco juice for electronic smoke as claimed in claim 5, it is characterized in that, described miillpore filter aperture is not more than 0.5 μm.
9. tobacco juice for electronic smoke as claimed in claim 5, it is characterized in that, described heating reflux temperature is 80 ~ 120 DEG C, and heating return time is 1 ~ 5h.
10. a preparation method for tobacco juice for electronic smoke as described in claim as arbitrary in claim 1 ~ 9, for mixing propane diols, glycerine, edible alcohol, tobacco extract, flavouring essence for tobacco and Chinese herbal medicine extract according to each raw material components weight portion.
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| CN201410788639.0A CN104489913A (en) | 2014-12-17 | 2014-12-17 | E-cigarette nicotine liquid with functions of heat clearing and fire removing |
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| CN201410788639.0A CN104489913A (en) | 2014-12-17 | 2014-12-17 | E-cigarette nicotine liquid with functions of heat clearing and fire removing |
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| CN104489913A true CN104489913A (en) | 2015-04-08 |
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