CN104585858A - Electronic cigarette tobacco juice with bowel relaxing function - Google Patents
Electronic cigarette tobacco juice with bowel relaxing function Download PDFInfo
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- CN104585858A CN104585858A CN201410849780.7A CN201410849780A CN104585858A CN 104585858 A CN104585858 A CN 104585858A CN 201410849780 A CN201410849780 A CN 201410849780A CN 104585858 A CN104585858 A CN 104585858A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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Abstract
The invention provides an electronic cigarette tobacco juice. Raw materials of the electronic cigarette tobacco juice comprise the following components in parts by mass: 1-30 parts of tobacco extract, 0.5-15 parts of tobacco flavor, 0.5-10 parts of Chinese herb extract with the bowel relaxing efficacy, 5-30 parts of glycerinum, 2-5 parts of edible ethyl alcohol, and 50-80 parts of propylene glycol. The Chinese herb extract with the bowel relaxing efficacy is mixed with the tobacco extract, the fragrance of the electronic cigarette tobacco juice is richer and more harmonious, the satisfaction degree is good, the defect that the fragrance and the taste of the electronic cigarette tobacco juice are insufficient is solved to a certain degree, and the electronic cigarette tobacco juice is endowed with a certain bowel relaxing health care function.
Description
Technical field
The present invention relates to electronic cigarette technical field, be specifically related to a kind of tobacco juice for electronic smoke with function of relaxing bowel.
Background technology
Traditional cigarette is generally provide nicotine and relevant aroma components by the mode of cigarette of burning to consumer.Because the reasons such as Pintsch process and flue gas migration cause containing a large amount of harmful components in main flume in sucking process, fraction is wherein had to have carcinogenic danger as condensed-nuclei aromatics is proved.Also produce a large amount of flue gas smog in the process of smoking property of cigarette, not only cause environmental pollution, also bring the harm of second-hand-cigarette simultaneously to non-smoker.Along with the progressively enforcement of the international Framework Convention on Tobacco Control and the enhancing gradually of health of people consciousness, traditional cigarette selling market is subject to powerful impact.Electronic cigarette takes atomizing type to generate smog sensation, does not produce tar and CO, produces second-hand-cigarette harm hardly simultaneously, is regarded as non-harmful smoking cessation product or substitute of tobacco, receives showing great attention to and extensively studying of domestic and international each large tobacco enterprise.The selling market of current electronic cigarette is mainly in the U.S., and Europe, Asia then possess good growth trends, and particularly the market of China Electronics's cigarette is also in the cultivation and exploitation stage.The electronic cigarette product taste developed at present is partial to blended type cigarette, compares the taste custom meeting foreign consumers, and Chinese Consumer's preference flue-cured tobacco, taste is comparatively strong, and the mouthfeel of electronic cigarette is difficult to reach requirement.It is the key opening Chinese market that improvement electronic cigarette formula of liquid makes it to meet Chinese Consumer's custom.
Electronic cigarette, as a kind of form in novel tobacco goods, presents great market prospect, and reason is mainly to provide the consumption habit similar with traditional cigarette and satisfaction on the one hand, and the hazard index of electronic cigarette reduces greatly than traditional cigarette on the other hand.Electronic cigarette formula of liquid is the key highlighting electronic cigarette advantage.In order to simulate the fragrance of traditional cigarette, fragrance and mouthfeel to the full extent, solution the most general at present adds tobacco extract in tobacco juice.Tobacco juice for electronic smoke is mixed to get according to a certain ratio by the essential oil of tobaccos and Alevaire, flavouring essence for tobacco that extract acquisition.The less harmful of electronic cigarette is that what to make to suck human body by incombustible mode is atomized liquid and non-burning pyrolysis product.Many Chinese herbal medicine compositions not only have certain characteristic flavor compounds, also have certain health-care effect simultaneously, have even and alleviate some disease effect.Tobacco extract is combined with Chinese herbal medicine extract, not only compensate for the shortcoming of tobacco juice for electronic smoke flavor component deficiency to a certain extent, be different from external tobacco juice for electronic smoke simultaneously, the tobacco juice for electronic smoke of Chinese style characteristic can be built, meet consumer's custom, certain health-care effect is provided simultaneously.
The present invention has the Chinese herbal medicine extract of effect of relaxing bowel by preparation, afterwards it is mixed with tobacco extract, be aided with and use suitable essence spice for cigarette to modify, can prepare that fragrance enriches, comfortable taste, satisfaction are got well and there is the tobacco juice for electronic smoke of the health care that necessarily relaxes bowel.
Summary of the invention
The object of the present invention is to provide a kind of tobacco juice for electronic smoke, not good to improve existing tobacco juice for electronic smoke mouthfeel, the shortcomings such as fragrance is not enough, give electronic cigarette certain health care that relaxes bowel simultaneously.
For achieving the above object and other relevant objects, the present invention is by the following technical solutions:
A kind of tobacco juice for electronic smoke, its raw material according to the mass fraction, comprises following component:
Preferably, described tobacco juice for electronic smoke, its raw material according to the mass fraction, comprises following component:
Most preferred, described tobacco juice for electronic smoke, its raw material according to the mass fraction, comprises following component:
Preferably, described tobacco extract is that tobacco tobacco leaf is through extracting obtained concentrate.
Further, described tobacco leaf is selected from one or more the combination in flue-cured tobacco, air-curing of tobacco leaves or suncured tabacco; Described air-curing of tobacco leaves is selected from one or more the combination in burley tobaccos or Maryland; Described suncured tabacco is selected from one or more the combination in Turkish tobaccos, Dark sun-cured, Sun cured tobacco or Nicotiniana rustica.
Preferred, described tobacco leaf is the combination of flue-cured tobacco and burley tobaccos, and the mass ratio of the two is 1:0.9 ~ 1.1.
Tobacco extract described in the present invention can adopt method conventional in prior art to obtain.
Preferably, the extracting method of described tobacco extract, specifically comprises the steps:
(1) get drying tobacco, be cooled to room temperature, pulverize, obtain offal;
(2) get gained offal, add Extraction solvent and soak, extract under uniform temperature, through sedimentation, filtration, concentrate and obtain tobacco extract.
Preferably, in step (1), the temperature of described drying is 30 ~ 80 DEG C, and the dry time is 1 ~ 9h.Preferred, described drying is specifically at 40 DEG C of dry 3h.
Preferably, in step (1), the Average Particle Diameters of described offal is 40 ~ 100 orders; Be more preferably 40 ~ 60 orders.
Preferably, in step (2), described Extraction solvent is deionized water or ethanol.
Preferably, in step (2), the feed liquid mass ratio of offal and Extraction solvent is 1:2 ~ 5, is more preferably 1:2.5 ~ 3.5; Most preferably be 1:3.
Preferably, in step (2), described in be extracted as ultrasonic extraction; The temperature of described ultrasonic extraction is 30 ~ 60 DEG C; The time of ultrasonic extraction is 2 ~ 5h.Preferred, the temperature of described ultrasonic extraction is 45 ~ 55 DEG C; The time of ultrasonic extraction is 3.5 ~ 4.5h.
Preferably, in step (2), the time of described sedimentation is >=4h.
Preferably, in step (2), described simmer down to reduced pressure concentration.
Further, the temperature of described reduced pressure concentration is 50 ~ 90 DEG C; Be more preferably 60 ~ 80 DEG C.
Preferably; described flavouring essence for tobacco is selected from Ethyl vanillin, benzyl acetate, furfural, dorinone, β-damascone, Megastigmatrienone, dihydroactinidiolide, dimethyl succinate, 2; 6; 6-trimethyl-2-cyclohexene-1; 4-diketone, 2-hydroxyl-3; 5; 5-trimethyl-2-cyclonene, geranyl acetone, alpha, beta-lonone, phenmethylol, palmitic acid, isovaleric acid, 2 methyl valeric acid, indoles, pyridine, 3-acetylpyridine, 2; combination multiple arbitrarily in 3,5-trimethylpyrazine.
Further, the total content of described flavouring essence for tobacco with percentage by weight shared by flavouring essence for tobacco in described tobacco juice for electronic smoke for benchmark.
Further, described flavouring essence for tobacco is selected from 1-10% Ethyl vanillin, 1-10% benzyl acetate, 1-8% furfural, 4-20% dorinone, 2-15% β-damascone, 10-30% Megastigmatrienone, 2-15% dihydroactinidiolide, 1-8% dimethyl succinate, 1-5%2, 6, 6-trimethyl-2-cyclohexene-1, 4-diketone, 1-5%2-hydroxyl-3, 5, 5-trimethyl-2-cyclonene, 3-15% geranyl acetone, 5-30% alpha, beta-lonone, 3-15% phenmethylol, 2-7% palmitic acid, 1-4% isovaleric acid, 1-4%2-methylvaleric acid, 1-3% indoles, 1-3% pyridine, 1-3%3-acetylpyridine, 1-5%2, 3, any multiple combination in 5-trimethylpyrazine.Above-mentioned tobacco flavor components content with 100% weight percent meter.
Preferred, described flavouring essence for tobacco is following several formula (percentage by weight):
Formula one: 8% dorinone, 5% β-damascone, 13% Megastigmatrienone, 24% alpha, beta-lonone, 9% Ethyl vanillin, 7% benzyl acetate, 5% furfural, 5% phenmethylol, 4% palmitic acid, 12% dihydroactinidiolide, 8% dimethyl succinate.Said components is mixed in vortex oscillator.Above-mentioned tobacco flavor components content with 100% weight percent meter.
Formula two: 15% dorinones, 3% indoles, 15% Megastigmatrienone, 5%2,3,5-trimethylpyrazine, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 9% alpha, beta-lonone, 15% phenmethylol; Said components is mixed in vortex oscillator.Above-mentioned tobacco flavor components content with 100% weight percent meter.
Preferably, the Chinese herbal medicine extract described in effect of relaxing bowel is selected from one or more combination in cassia seed, Radix Angelicae Sinensis, folium sennae, saline cistanche, radish seed, fructus cannabis, the fleece-flower root, lily, radix polygonati officinalis, Fructus Aurantii, rattletop, rheum officinale, mulberries, brush-cherry seed, perilla seed, mulberry leaf, Snakegourd Seed, cynomorium songaricum, chingma abutilon seed, sheep hoof, Momordica grosvenori, lotus leaf, the compound of glauber-salt and liquorice, the bighead atractylodes rhizome through extracting obtained concentrate.
Preferred, described in there is effect of relaxing bowel Chinese herbal medicine be following several formula (parts by weight):
Formula one: saline cistanche 60 parts; Radish seed 45 parts; Cassia seed 45 parts; The bighead atractylodes rhizome 60 parts.
Formula two: cassia seed 50 parts; The fleece-flower root 25 parts; Fructus Aurantii 15 parts; Rattletop 10 parts.
Formula three: cassia seed 45 parts; Lily 30 parts; Radix polygonati officinalis 20 parts; 20 parts, mulberry leaf; 15 parts, mulberry fruit; Momordica grosvenori 8 parts; 30 parts, lotus leaf.
The Chinese herbal medicine extract described in the present invention with effect of relaxing bowel can adopt method conventional in prior art to obtain.
Preferably, described in there is the extracting method of the Chinese herbal medicine extract of effect of relaxing bowel, comprise the steps:
(1) take Chinese herbal medicine powder, add ethanol water, shake up, sealing, soaked overnight;
(2) heating and refluxing extraction 1 ~ 5h under 80 ~ 120 DEG C of conditions, cooling, isolated by filtration liquid and the dregs of a decoction, by centrifugal for gained liquid, get supernatant and filter, obtain filtrate;
(3) filtrate reduced in volume is obtained Chinese herbal medicine extract.
Preferably, in step (1), described Chinese herbal medicine powder is 40 ~ 60 orders.
Preferably, in step (1), the concentration of described ethanol water is 40 ~ 80% (v/v).
Preferably, in step (1), the feed liquid mass ratio of described Chinese herbal medicine powder and ethanol water is 1:2 ~ 5; Be more preferably 1:2.5 ~ 3.5.
Preferably, in step (2), the time of described heating and refluxing extraction is 2.5 ~ 3.5h.
Preferably, in step (2), described centrifugal speed is 2500 ~ 4000r/min, and centrifugation time is 10 ~ 30min; Preferred, described centrifugal speed is 4000r/min, and centrifugation time is 20min.
Preferably, in step (2), get supernatant and adopt 0.45 μm of membrane filtration.
Preferably, in step (3), described simmer down to reduced pressure concentration, the temperature of reduced pressure concentration is 50 ~ 90 DEG C; Be more preferably 60 ~ 80 DEG C.
Preferably, described edible ethanol, glycerine, propane diols are market and buy.
Second aspect present invention discloses the preparation method of above-mentioned tobacco juice for electronic smoke, for described each component is mixed by setting number mix and blend and be get final product.
The invention also discloses aforementioned electronic cigarette tobacco juice and prepare the application in electronic cigarette.
Compared with prior art, the present invention has following beneficial effect:
(1) the present invention is by mixing the Chinese herbal medicine extract with effect of relaxing bowel with tobacco extract, make tobacco juice for electronic smoke fragrance abundanter, fragrance is coordinated more, and satisfaction is good, improves the shortcoming of tobacco juice for electronic smoke fragrance and taste deficiency to a certain extent.
(2) tobacco juice for electronic smoke of the present invention generates smog sensation owing to taking atomizing type, does not produce tar and CO, does not produce second-hand-cigarette harm simultaneously.
(3) the present invention is by adding containing the Chinese herbal medicine extract with effect of relaxing bowel, is conducive to improving intestinal environment, has the effect well relaxed bowel.
(4) solvent in electronic cigarette liquid provided by the invention and flavouring essence for tobacco are food-grade, harmless to smoker.
Detailed description of the invention
Below by way of specific instantiation, embodiments of the present invention are described, those skilled in the art the content disclosed by this description can understand other advantages of the present invention and effect easily.The present invention can also be implemented or be applied by detailed description of the invention different in addition, and the every details in this description also can based on different viewpoints and application, carries out various modification or change not deviating under spirit of the present invention.
The leaf tobacco extract used in the present invention, if flue-cured tobacco, burley tobaccos, Maryland, Turkish tobaccos, Dark sun-cured, Sun cured tobacco or Nicotiniana rustica are manufacturer's self-control; Tobacco flavor components also can adopt commercial goods; Having the Chinese herbal medicine of effect of relaxing bowel, edible ethanol, glycerine, propane diols also can be commercially.Deionized water is that manufacturer adopts water purification machine self-control.The equipment used in the present invention and reagent needed for other are all commercially available.
In addition should be understood that the one or more method steps mentioned in the present invention do not repel and can also to there is additive method step or can also insert additive method step before and after described combination step between these steps clearly mentioned, except as otherwise noted.
Embodiment 1
The preparation of tobacco extract in the present embodiment: get cured tobacco leaf sample dry 3h in 40 DEG C of baking ovens, after being cooled to room temperature, be crushed to 40 ~ 100 orders.Take the conical flask that 100g offal is placed in 1L, add 300mL deionized water, ultrasonic extraction 4h under 50 ± 5 DEG C of conditions, afterwards standing sedimentation 4h, sand core funnel filters to get filtrate, and 70 ± 10 DEG C of vacuum rotary steams are concentrated into 3mL, obtain tobacco extract.
In the present embodiment, the extracting method with the Chinese herbal medicine extract of effect of relaxing bowel is: take saline cistanche 60g, radish seed 45g, cassia seed 45g and bighead atractylodes rhizome 60g, through pulverizer grind be 40 ~ 100 order powder after mix, add 80% ethanol/water mixed solvent, controlling feed liquid mass ratio is 1:3, shake up, sealing, soaked overnight.By soaked vlil 3h, be separated liquid and the dregs of a decoction after extraction, extract is in the centrifugal 20min of 4000r/min, and supernatant 0.45 μm of membrane filtration, control temperature is 70 ± 10 DEG C, and vacuum rotary steam is concentrated into 7mL, obtains Chinese herbal medicine extract.
Suitable component is selected to be made into flavouring essence for tobacco again.Described flavouring essence for tobacco mainly comprises: 8% dorinone, 5% β-damascone, 13% Megastigmatrienone, 24% alpha, beta-lonone, 9% Ethyl vanillin, 7% benzyl acetate, 5% furfural, 5% phenmethylol, 4% palmitic acid, 12% dihydroactinidiolide, 8% dimethyl succinate.Above-mentioned tobacco flavor components content with 100% weight percent meter.Said components is mixed in vortex oscillator.
Composition and each composition weight number in the present embodiment with the tobacco juice for electronic smoke of function of relaxing bowel are: tobacco extract 15 parts, and flavouring essence for tobacco 3 parts has the Chinese herbal medicine extract 3 parts of effect of relaxing bowel, glycerine 20 parts, edible ethanol 3 parts, propane diols 70 parts.Mix and obtain tobacco juice for electronic smoke 1# by each component vortex oscillator.
The tobacco juice for electronic smoke 1# obtained smokes panel test by the present invention, and result is as shown in table 2.
Embodiment 2
The preparation of tobacco extract in the present embodiment: get burley tobaccos tobacco sample dry 3h in 40 DEG C of baking ovens, after being cooled to room temperature, be crushed to 40 ~ 100 orders.Take the conical flask that 100g offal is placed in 1L, add 300mL deionized water, ultrasonic extraction 4h, standing sedimentation 4h afterwards under 50 ± 5 DEG C of conditions, sand core funnel filters to get filtrate, and 70 ± 10 DEG C of vacuum rotary steams are concentrated into 3mL, obtain tobacco extract.
In the present embodiment, the Chinese herbal medicine extract extracting method with effect of relaxing bowel is: take cassia seed 50g, fleece-flower root 25g, Fructus Aurantii 15g and rattletop 10g, grind as mixing after 40-100 order powder through pulverizer, add 60% ethanol/water mixed solvent, controlling feed liquid mass ratio is 1:3, shake up, sealing, soaked overnight.By soaked vlil 3h, be separated liquid and the dregs of a decoction after extraction, extract is in the centrifugal 30min of 2500r/min, and supernatant 0.45 μm of membrane filtration, control temperature is 70 ± 10 DEG C, and vacuum rotary steam is concentrated into 5mL, obtains Chinese herbal medicine extract.
Suitable component is selected to be made into flavouring essence for tobacco again.Described flavouring essence for tobacco mainly comprises: 15% dorinone, 3% indoles, 15% Megastigmatrienone, 5%2,3,5-trimethylpyrazine, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 9% alpha, beta-lonone, 15% phenmethylol.Above-mentioned tobacco flavor components content with 100% weight percent meter.Said components is mixed in vortex oscillator.
Composition and each weight percentages of components in the present embodiment with the tobacco juice for electronic smoke of function of relaxing bowel are: tobacco extract 25 parts, flavouring essence for tobacco 5 parts, has the Chinese herbal medicine extract 4 parts of effect of relaxing bowel, glycerine 30 parts, edible ethanol 4 parts, propane diols 80 parts.Mix and obtain tobacco juice for electronic smoke 2# by each component vortex oscillator.
The tobacco juice for electronic smoke 2# obtained smokes panel test by the present invention, and result is as shown in table 2.
Embodiment 3
Tobacco extract preparation in the present embodiment: get Sun cured tobacco tobacco sample dry 3h in 40 DEG C of baking ovens, after being cooled to room temperature, be crushed to 40 ~ 100 object offals.Take the conical flask that 100g offal is placed in 1L, add 300mL deionized water, ultrasonic extraction 4h under 50 ± 5 DEG C of conditions, standing sedimentation 4h afterwards, sand core funnel filters to get filtrate, and vacuum rotary steam is concentrated into 3mL, obtains tobacco extract.
In the present embodiment, the Chinese herbal medicine extract extracting method with effect of relaxing bowel is: take cassia seed 45g, lily 30g, radix polygonati officinalis 20g, mulberry leaf 20g, mulberry fruit 15g, Momordica grosvenori 8g and lotus leaf 30g, grind as mixing after 40-100 order powder through pulverizer, add 80% ethanol/water mixed solvent, controlling feed liquid mass ratio is 1:3, shake up, sealing, soaked overnight.By soaked vlil 3h, be separated liquid and the dregs of a decoction after extraction, extract is in the centrifugal 20min of 4000r/min, and supernatant 0.45 μm of membrane filtration, control temperature is 70 ± 10 DEG C, and vacuum rotary steam is concentrated into 7mL, obtains Chinese herbal medicine extract.
Suitable component is selected to be made into flavouring essence for tobacco again.Described flavouring essence for tobacco mainly comprises: 8% dorinone, 5% β-damascone, 13% Megastigmatrienone, 24% alpha, beta-lonone, 9% Ethyl vanillin, 7% benzyl acetate, 5% furfural, 5% phenmethylol, 4% palmitic acid, 12% dihydroactinidiolide, 8% dimethyl succinate.Above-mentioned tobacco flavor components content with 100% weight percent meter.Said components is mixed in vortex oscillator.
Composition and each weight percentages of components in the present embodiment with the tobacco juice for electronic smoke of function of relaxing bowel are: tobacco extract 10 parts, flavouring essence for tobacco 2 parts, has the Chinese herbal medicine extract 3 parts of effect of relaxing bowel, glycerine 20 parts, edible ethanol 3 parts, propane diols 65 parts.Mix and obtain tobacco juice for electronic smoke 3# by each component vortex oscillator.
The tobacco juice for electronic smoke 3# obtained smokes panel test by the present invention, and result is as shown in table 2.
Embodiment 4
Tobacco extract preparation in the present embodiment: the flue-cured tobacco and the burley tobaccos tobacco sample dry 3h in 40 DEG C of baking ovens that get 1:1, after being cooled to room temperature, be crushed to 40 ~ 100 object offals.Take the conical flask that 100g offal is placed in 1L, add 300mL deionized water, ultrasonic extraction 4h under 50 ± 5 DEG C of conditions, standing sedimentation 4h afterwards, sand core funnel filters to get filtrate, and vacuum rotary steam is concentrated into 3mL, obtains tobacco extract.
In the present embodiment, the Chinese herbal medicine extract extracting method with effect of relaxing bowel is: take saline cistanche 60g, radish seed 45g, cassia seed 45g and bighead atractylodes rhizome 60g, grind as mixing after 40-100 order powder through pulverizer, add 80% ethanol/water mixed solvent, controlling feed liquid mass ratio is 1:3, shake up, sealing, soaked overnight.By soaked vlil 3h, be separated liquid and the dregs of a decoction after extraction, extract is in the centrifugal 20min of 4000r/min, and supernatant 0.45 μm of membrane filtration, control temperature is 70 ± 10 DEG C, and vacuum rotary steam is concentrated into 7mL, obtains Chinese herbal medicine extract.
Suitable component is selected to be made into flavouring essence for tobacco again.Described flavouring essence for tobacco mainly comprises: 15% dorinone, 3% indoles, 15% Megastigmatrienone, 5%2,3,5-trimethylpyrazine, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 9% alpha, beta-lonone, 15% phenmethylol.Above-mentioned tobacco flavor components content with 100% weight percent meter.Said components is mixed in vortex oscillator.
Composition and each weight percentages of components in the present embodiment with the tobacco juice for electronic smoke of function of relaxing bowel are: tobacco extract 10 parts, flavouring essence for tobacco 1 part, has the Chinese herbal medicine extract 1 part of effect of relaxing bowel, glycerine 10 parts, edible ethanol 2 parts, propane diols 60 parts.Mix and obtain tobacco juice for electronic smoke 4# by each component vortex oscillator.
The tobacco juice for electronic smoke 4# obtained smokes panel test by the present invention, and result is as shown in table 2.
Embodiment 5
Composition and each weight percentages of components in the present embodiment with the tobacco juice for electronic smoke of function of relaxing bowel are: tobacco extract 5 parts, flavouring essence for tobacco 2 parts, has the Chinese herbal medicine extract 10 parts of effect of relaxing bowel, glycerine 25 parts, edible ethanol 3 parts, propane diols 70 parts.
Wherein tobacco extract composition and extracting mode, Chinese herbal medicine extract composition and extracting mode, flavouring essence for tobacco are with embodiment 4.
Mix and obtain tobacco juice for electronic smoke 5# by each component vortex oscillator.
The tobacco juice for electronic smoke 5# obtained smokes panel test by the present invention, and result is as shown in table 2.
Comparative example 1
Select the component of the tobacco juice for electronic smoke in embodiment 1 except Chinese herbal medicine extract in this comparative example, and each weight percentages of components is: tobacco extract 15 parts, flavouring essence for tobacco 3 parts, glycerine 20 parts, edible ethanol 3 parts, propane diols 70 parts.
Wherein tobacco extract composition and extracting mode, flavouring essence for tobacco formula are with embodiment 1.
Mix and obtain tobacco juice for electronic smoke 1* by each component vortex oscillator.
The tobacco juice for electronic smoke 1* obtained smokes panel test by the present invention, and result is as shown in table 2.
Comparative example 2
Select the component of the tobacco juice for electronic smoke in embodiment 2 except Chinese herbal medicine extract in this comparative example, and each weight percentages of components is: tobacco extract 25 parts, flavouring essence for tobacco 5 parts, glycerine 30 parts, edible ethanol 4 parts, propane diols 80 parts.
Wherein tobacco extract composition and extracting mode, flavouring essence for tobacco formula are with embodiment 2.
Mix and obtain tobacco juice for electronic smoke 2* by each component vortex oscillator.
The tobacco juice for electronic smoke 2* obtained smokes panel test by the present invention, and result is as shown in table 2.
Comparative example 3
Select the component of the tobacco juice for electronic smoke in embodiment 3 except Chinese herbal medicine extract in this comparative example, and each weight percentages of components is: tobacco extract 10 parts, flavouring essence for tobacco 2 parts, glycerine 20 parts, edible ethanol 3 parts, propane diols 65 parts.
Wherein tobacco extract composition and extracting mode, flavouring essence for tobacco formula are with embodiment 3.
Mix and obtain tobacco juice for electronic smoke 3* by each component vortex oscillator.
The tobacco juice for electronic smoke 3* obtained smokes panel test by the present invention, and result is as shown in table 2.
Tobacco juice for electronic smoke in above-described embodiment 1-5 and comparative example 1-3 is added in electronic cigarette device and carries out sensory effects evaluation respectively.
Sensory effects evaluation method comprises the following steps:
(1) 9 evaluation indexes are provided with, comprise excitant, satisfaction, concentration, comfort level, feature style, tobacco perfume, aroma quality, perfume quantity and the amount of being fuming, and give different score value according to the Different Effects degree of every evaluation index to tobacco juice for electronic smoke aesthetic quality.
Wherein, described excitant refers to: suck the discomfort that flue gas comprises oral cavity to sense organ, throat and nasal cavity produce that tobacco juice for electronic smoke produces through atomization and be subject to.Described satisfaction refers to: the flue gas strength that tobacco juice for electronic smoke produces through atomization, concentration and note are to the comprehensive impression that sense organ produces.Described concentration refers to: the impression of tobacco juice for electronic smoke oral cavity filling degree when the flue gas firm suction inlet that atomization produces.Described comfort level refers to: the impact of flue gas on oral cavity level of comfort after sucking oral cavity and exhalation that tobacco juice for electronic smoke produces through atomization.Described feature style refers to: a kind of tobacco juice for electronic smoke is different from the sense organ Main Differences performance of other homogeneous e cigarette tobacco juices in joyful sense.Described tobacco perfume (or spice) refers to: in process of smokeing panel test, sensory feel is to the breath of this perfume (or spice) of tobacco.Described aroma quality refers to: felt the good and bad degree of pleasant breath in process of smokeing panel test by sense of smell and the sense of taste.Described perfume quantity refers to: in process of smokeing panel test by oral cavity and nasal cavity weigh pleasant breath amount number.The described amount of being fuming refers to: tobacco juice for electronic smoke through atomization produce exhaust gas volumn number.
(2) member of smoking of 9 people is set, everyone a tobacco juice for electronic smoke sensory quality assessment table, adopt the marking mode secretly commented, adopt the overall method of smokeing panel test that circulates, tobacco juice for electronic smoke is aspirated, according to the implication of 9 sensory quality assessment index score values in table 1, adopt hundred-mark system point system to carry out comprehensive grading to the aesthetic quality of tobacco juice for electronic smoke, every evaluation index is by five points, ten point system or the scoring of ten the five-grade marking systems.Described hundred-mark system point system refers to: 9 sensory quality assessment indexs respectively by five points, very or ten the five-grade marking systems mark, and the score value summation of 9 sensory quality assessment indexs is a percentage.The concrete meaning of the score value of tobacco juice for electronic smoke evaluation index sees the following form 1.The minimum score unit of score value is 0.5.
The score value implication table of table 1 tobacco juice for electronic smoke sensory quality assessment index
(3) the sensory quality assessment result of member of smoking is added up.By the score value of every sensory quality assessment index of all members of smoking, remove one minimum point and a best result respectively, calculate the mean value of effective score value of every sensory quality assessment index by formula I.The mean value sum of the score value of every sensory quality assessment index is calculated by formula II.
Described formula I is:
In formula:
---the average score value of the effective sense organ quality evaluation index of certain individual event, result retains two-decimal;
---the summation of the score value of the effective sense organ quality evaluation index of certain individual event;
N---total number of persons of effectively smokeing panel test.
Described formula II is:
In formula: S---general comment score value, result retains a decimal;
---the average score value sum of every effective sense organ quality evaluation index.
The tobacco juice for electronic smoke 1*-3* prepared in the tobacco juice for electronic smoke 1#-5# containing white tea tea extract prepared in embodiment 1-5 and comparative example 1-3 is added in electronic cigarette and carries out sensory quality assessment.Concrete evaluation result is in table 2, and in table 2, the scoring of every evaluation index is that the arithmetic average that 9 members of smoking effectively mark is divided.
Table 2 tobacco juice for electronic smoke sensory effects evaluation result
Table 2 result shows, the amount of being fuming abundance when tobacco juice for electronic smoke is embodied in suction in above-described embodiment, fragrance enrich strong, tobacco and faint medicine perfume is coordinated, strength is moderate, comfortable taste, humectation are effective, shortens the aesthetic quality's difference with traditional cigarette.The Chinese herbal medicine kind used, Tobacco Types, extract adding proportion, essence spice for cigarette adding proportion produce Different Effects to adopted 9 indexs; Chinese herbal medicine extract used can provide action and efficacy such as relaxing bowel simultaneously.
The above; be only preferred embodiment of the present invention; above-described embodiment is illustrative principle of the present invention and effect thereof only; and not to any formal and substantial restriction of the present invention; it should be pointed out that for those skilled in the art, under the prerequisite not departing from the inventive method; also can make some improvement and supplement, these improve and supplement and also should be considered as protection scope of the present invention.All those skilled in the art, without departing from the spirit and scope of the present invention, a little change made when utilizing disclosed above technology contents, the equivalent variations of modifying and developing, be Equivalent embodiments of the present invention; Meanwhile, all according to substantial technological of the present invention to the change of any equivalent variations that above-described embodiment is done, modify and differentiation, all still belong in the scope of technical scheme of the present invention.
Claims (10)
1. a tobacco juice for electronic smoke, its raw material according to the mass fraction, comprises following component:
2. tobacco juice for electronic smoke according to claim 1, is characterized in that, described tobacco extract is that tobacco tobacco leaf is through extracting obtained concentrate; Described tobacco leaf is selected from one or more the combination in flue-cured tobacco, air-curing of tobacco leaves or suncured tabacco; Described air-curing of tobacco leaves is selected from one or more the combination in burley tobaccos or Maryland; Described suncured tabacco is selected from one or more the combination in Turkish tobaccos, Dark sun-cured, Sun cured tobacco or Nicotiniana rustica.
3. a kind of tobacco juice for electronic smoke according to claim 2, is characterized in that, the extracting method of described tobacco extract, specifically comprises the steps:
1) get drying tobacco, be cooled to room temperature, pulverize, obtain offal;
2) get gained offal, add Extraction solvent and soak, extract under uniform temperature, through sedimentation, filtration, concentrate, obtain tobacco extract.
4. a kind of tobacco juice for electronic smoke according to claim 3, is characterized in that, described extracting method also to comprise any one of following condition or multinomial:
I) temperature of described drying is 30 ~ 80 DEG C, and the dry time is 1 ~ 9h;
II) Average Particle Diameters of described offal is 40 ~ 100 orders;
III) described Extraction solvent is deionized water or ethanol;
IV) the feed liquid mass ratio of offal and Extraction solvent is 1:2 ~ 5;
V) be extracted as ultrasonic extraction described in, the temperature of described ultrasonic extraction is 30 ~ 60 DEG C, and the time of ultrasonic extraction is 2 ~ 5h;
VI) time of described sedimentation is >=4h;
VII) described simmer down to reduced pressure concentration, the temperature of described reduced pressure concentration is 50 ~ 90 DEG C.
5. a kind of tobacco juice for electronic smoke according to claim 1; it is characterized in that; described flavouring essence for tobacco is selected from Ethyl vanillin, benzyl acetate, furfural, dorinone, β-damascone, Megastigmatrienone, dihydroactinidiolide, dimethyl succinate, 2; 6; 6-trimethyl-2-cyclohexene-1; 4-diketone, 2-hydroxyl-3; 5; 5-trimethyl-2-cyclonene, geranyl acetone, alpha, beta-lonone, phenmethylol, palmitic acid, isovaleric acid, 2 methyl valeric acid, indoles, pyridine, 3-acetylpyridine, 2; combination multiple arbitrarily in 3,5-trimethylpyrazine.
6. a kind of tobacco juice for electronic smoke according to claim 1, it is characterized in that, described in there is effect of relaxing bowel Chinese herbal medicine extract be selected from one or more combination in cassia seed, Radix Angelicae Sinensis, folium sennae, saline cistanche, radish seed, fructus cannabis, the fleece-flower root, lily, radix polygonati officinalis, Fructus Aurantii, rattletop, rheum officinale, mulberries, brush-cherry seed, perilla seed, mulberry leaf, Snakegourd Seed, cynomorium songaricum, chingma abutilon seed, sheep hoof, Momordica grosvenori, lotus leaf, the compound of glauber-salt and liquorice, the bighead atractylodes rhizome through extracting obtained concentrate.
7. a kind of tobacco juice for electronic smoke according to claim 6, is characterized in that, described in there is the extracting method of the Chinese herbal medicine extract of effect of relaxing bowel, comprise the steps:
A) take Chinese herbal medicine powder, add ethanol water, shake up, sealing, soaked overnight;
B) heating and refluxing extraction 1 ~ 5h under 80 ~ 120 DEG C of conditions, cooling, isolated by filtration liquid and the dregs of a decoction, by centrifugal for gained liquid, get supernatant and filter, obtain filtrate;
C) filtrate reduced in volume is obtained Chinese herbal medicine extract.
8. a kind of tobacco juice for electronic smoke according to claim 7, is characterized in that, described extracting method also to comprise any one of following condition or multinomial:
I) described Chinese herbal medicine powder is 40 ~ 60 orders;
II) concentration of described ethanol water is 40 ~ 80%;
III) the feed liquid mass ratio of described Chinese herbal medicine powder and ethanol water is 1:2 ~ 5;
IV) described centrifugal speed is 2500 ~ 4000r/min, centrifugation time is 10 ~ 30min;
V) get supernatant and adopt 0.45 μm of membrane filtration;
VI) described simmer down to reduced pressure concentration, the temperature of reduced pressure concentration is 50 ~ 90 DEG C.
9. according to the preparation method of the arbitrary described a kind of tobacco juice for electronic smoke of claim 1 ~ 8, for described each component is mixed by setting number mix and blend and get final product.
10. according to the arbitrary described application of a kind of tobacco juice for electronic smoke in electronic cigarette of claim 1 ~ 8.
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| CN201410849780.7A CN104585858A (en) | 2014-12-31 | 2014-12-31 | Electronic cigarette tobacco juice with bowel relaxing function |
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| CN201410849780.7A CN104585858A (en) | 2014-12-31 | 2014-12-31 | Electronic cigarette tobacco juice with bowel relaxing function |
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