NL7602794A - PROCESS FOR PREPARING N.N-DIMETHYLHYDRAZINE. - Google Patents
PROCESS FOR PREPARING N.N-DIMETHYLHYDRAZINE.Info
- Publication number
- NL7602794A NL7602794A NL7602794A NL7602794A NL7602794A NL 7602794 A NL7602794 A NL 7602794A NL 7602794 A NL7602794 A NL 7602794A NL 7602794 A NL7602794 A NL 7602794A NL 7602794 A NL7602794 A NL 7602794A
- Authority
- NL
- Netherlands
- Prior art keywords
- dimethylhydrazine
- march
- preparing
- acylhydrazine
- hydrazinolysis
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C243/00—Compounds containing chains of nitrogen atoms singly-bound to each other, e.g. hydrazines, triazanes
- C07C243/10—Hydrazines
- C07C243/12—Hydrazines having nitrogen atoms of hydrazine groups bound to acyclic carbon atoms
- C07C243/14—Hydrazines having nitrogen atoms of hydrazine groups bound to acyclic carbon atoms of a saturated carbon skeleton
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C241/00—Preparation of compounds containing chains of nitrogen atoms singly-bound to each other, e.g. hydrazines, triazanes
- C07C241/02—Preparation of hydrazines
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C241/00—Preparation of compounds containing chains of nitrogen atoms singly-bound to each other, e.g. hydrazines, triazanes
- C07C241/04—Preparation of hydrazides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
1488637 N,N - Dimethylhydrazine ASHLAND OIL Inc 17 March 1976 ]19 March 1975] 10750/76 Heading C2C N;N - Dimethylhydrazine is made by (a) reductively alkylating an acid hydrazide of formula in which R represents a C 1-3 alkyl group with formaldehyde at a pH of less than 7À5 to provide the corresponding N,N-dimethyl-2- acylhydrazine and (b) cleaning the above product by the base hydrolysis or the hydrazinolysis thereof to the desired N,N-dimethylhydrazine. In step (a) the reduction is preferably effected by hydrogen in the presence of Pd, Pt, Rh, Ni, Co or Ir as catalyst.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US55975575A | 1975-03-19 | 1975-03-19 |
Publications (1)
Publication Number | Publication Date |
---|---|
NL7602794A true NL7602794A (en) | 1976-09-21 |
Family
ID=24234890
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
NL7602794A NL7602794A (en) | 1975-03-19 | 1976-03-17 | PROCESS FOR PREPARING N.N-DIMETHYLHYDRAZINE. |
Country Status (9)
Country | Link |
---|---|
JP (1) | JPS51115407A (en) |
BE (1) | BE839664A (en) |
CA (1) | CA1051928A (en) |
DE (1) | DE2611724C3 (en) |
FR (1) | FR2304599A1 (en) |
GB (1) | GB1488637A (en) |
IT (1) | IT1062084B (en) |
MX (1) | MX3256E (en) |
NL (1) | NL7602794A (en) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
USRE43252E1 (en) | 1992-10-27 | 2012-03-20 | Vast Power Portfolio, Llc | High efficiency low pollution hybrid Brayton cycle combustor |
-
1976
- 1976-02-20 CA CA246,275A patent/CA1051928A/en not_active Expired
- 1976-02-26 MX MX2576U patent/MX3256E/en unknown
- 1976-03-09 IT IT2100676A patent/IT1062084B/en active
- 1976-03-17 GB GB1075076A patent/GB1488637A/en not_active Expired
- 1976-03-17 NL NL7602794A patent/NL7602794A/en unknown
- 1976-03-17 BE BE165252A patent/BE839664A/en not_active IP Right Cessation
- 1976-03-18 FR FR7607882A patent/FR2304599A1/en active Granted
- 1976-03-19 JP JP2938976A patent/JPS51115407A/en active Granted
- 1976-03-19 DE DE19762611724 patent/DE2611724C3/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
BE839664A (en) | 1976-07-16 |
DE2611724A1 (en) | 1977-02-10 |
FR2304599B1 (en) | 1978-11-17 |
MX3256E (en) | 1980-08-12 |
DE2611724B2 (en) | 1978-09-28 |
JPS51115407A (en) | 1976-10-12 |
DE2611724C3 (en) | 1979-05-23 |
FR2304599A1 (en) | 1976-10-15 |
CA1051928A (en) | 1979-04-03 |
JPS5716978B2 (en) | 1982-04-08 |
IT1062084B (en) | 1983-06-25 |
GB1488637A (en) | 1977-10-12 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
ES452063A1 (en) | New benzhydrysulphinyl derivatives | |
GB1440767A (en) | Oxidation process for the manufacture of 4-aminodiphenylamine and related higher amines | |
GB1317499A (en) | Process for the manufacture of n,n-dihaloalkyl-2,6-dinitro-4- substituted anilines | |
NL7602794A (en) | PROCESS FOR PREPARING N.N-DIMETHYLHYDRAZINE. | |
GB864198A (en) | A process for the manufacture of ferrocene derivatives | |
KR830008971A (en) | Method for preparing phenylalkanoic acid | |
ES424803A1 (en) | Process for producing a quinoxaline-di-n-oxide derivative | |
GB1476818A (en) | Process for the semihydrogenation of citral and its homo logues to citronellal and its homologues | |
GB1431078A (en) | Mannich bases, a process for their preparation and their use in the preparation of polyurethanes | |
ES465346A1 (en) | 2h-imidazole-2-thione derivatives | |
ES430457A1 (en) | Preparation of 2-alkoxy-5-sulphamoylbenzoic acids | |
GB1398314A (en) | Process for the manufacture of hexahydroindane-4-carboxylic acid derivatives | |
GB1290923A (en) | ||
GB1286795A (en) | New azomethines and their production | |
JPS5212119A (en) | Method of manufacturing n**n*** disubstituted acid hydrazide | |
ES329218A1 (en) | A procedure for the preparation of tetrahydro-isoquinoline derivatives. (Machine-translation by Google Translate, not legally binding) | |
GB1220946A (en) | Process for the manufacture of piperidine derivatives | |
GB921322A (en) | Substituted hydrazide compounds | |
ES414765A1 (en) | Procedure for obtaining a new adamantamine derivative. (Machine-translation by Google Translate, not legally binding) | |
FR2228757A2 (en) | Oxidn. of halo-indanes to halo-anthraquinones - in the presence of vanadic catalysts, at 200-500 (350-470) deg C | |
GB1012492A (en) | Improvements in or relating to 6-alkylmorphinan derivatives and their preparation | |
GB1448961A (en) | Preparation of n-tertiaryaminoalkyl-acrylamides | |
GB1491134A (en) | Hydroformylation of olefins | |
ES443459A1 (en) | A procedure for the preparation of new derivatives of 3-cyanopyridines. (Machine-translation by Google Translate, not legally binding) | |
ES437040A1 (en) | A procedure for preparing a derivative of ftalazone. (Machine-translation by Google Translate, not legally binding) |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
BN | A decision not to publish the application has become irrevocable |