FR2304599A1 - PROCESS FOR PREPARING N, N-DIMETHYLHYDRAZINE - Google Patents

PROCESS FOR PREPARING N, N-DIMETHYLHYDRAZINE

Info

Publication number
FR2304599A1
FR2304599A1 FR7607882A FR7607882A FR2304599A1 FR 2304599 A1 FR2304599 A1 FR 2304599A1 FR 7607882 A FR7607882 A FR 7607882A FR 7607882 A FR7607882 A FR 7607882A FR 2304599 A1 FR2304599 A1 FR 2304599A1
Authority
FR
France
Prior art keywords
dimethylhydrazine
march
preparing
acylhydrazine
hydrazinolysis
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7607882A
Other languages
French (fr)
Other versions
FR2304599B1 (en
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ashland LLC
Original Assignee
Ashland Oil Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ashland Oil Inc filed Critical Ashland Oil Inc
Publication of FR2304599A1 publication Critical patent/FR2304599A1/en
Application granted granted Critical
Publication of FR2304599B1 publication Critical patent/FR2304599B1/fr
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C243/00—Compounds containing chains of nitrogen atoms singly-bound to each other, e.g. hydrazines, triazanes
    • C07C243/10—Hydrazines
    • C07C243/12—Hydrazines having nitrogen atoms of hydrazine groups bound to acyclic carbon atoms
    • C07C243/14—Hydrazines having nitrogen atoms of hydrazine groups bound to acyclic carbon atoms of a saturated carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C241/00—Preparation of compounds containing chains of nitrogen atoms singly-bound to each other, e.g. hydrazines, triazanes
    • C07C241/02—Preparation of hydrazines
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C241/00—Preparation of compounds containing chains of nitrogen atoms singly-bound to each other, e.g. hydrazines, triazanes
    • C07C241/04—Preparation of hydrazides

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

1488637 N,N - Dimethylhydrazine ASHLAND OIL Inc 17 March 1976 ]19 March 1975] 10750/76 Heading C2C N;N - Dimethylhydrazine is made by (a) reductively alkylating an acid hydrazide of formula in which R represents a C 1-3 alkyl group with formaldehyde at a pH of less than 7À5 to provide the corresponding N,N-dimethyl-2- acylhydrazine and (b) cleaning the above product by the base hydrolysis or the hydrazinolysis thereof to the desired N,N-dimethylhydrazine. In step (a) the reduction is preferably effected by hydrogen in the presence of Pd, Pt, Rh, Ni, Co or Ir as catalyst.
FR7607882A 1975-03-19 1976-03-18 PROCESS FOR PREPARING N, N-DIMETHYLHYDRAZINE Granted FR2304599A1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US55975575A 1975-03-19 1975-03-19

Publications (2)

Publication Number Publication Date
FR2304599A1 true FR2304599A1 (en) 1976-10-15
FR2304599B1 FR2304599B1 (en) 1978-11-17

Family

ID=24234890

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7607882A Granted FR2304599A1 (en) 1975-03-19 1976-03-18 PROCESS FOR PREPARING N, N-DIMETHYLHYDRAZINE

Country Status (9)

Country Link
JP (1) JPS51115407A (en)
BE (1) BE839664A (en)
CA (1) CA1051928A (en)
DE (1) DE2611724C3 (en)
FR (1) FR2304599A1 (en)
GB (1) GB1488637A (en)
IT (1) IT1062084B (en)
MX (1) MX3256E (en)
NL (1) NL7602794A (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
USRE43252E1 (en) 1992-10-27 2012-03-20 Vast Power Portfolio, Llc High efficiency low pollution hybrid Brayton cycle combustor

Also Published As

Publication number Publication date
JPS5716978B2 (en) 1982-04-08
CA1051928A (en) 1979-04-03
DE2611724C3 (en) 1979-05-23
FR2304599B1 (en) 1978-11-17
DE2611724A1 (en) 1977-02-10
IT1062084B (en) 1983-06-25
GB1488637A (en) 1977-10-12
JPS51115407A (en) 1976-10-12
DE2611724B2 (en) 1978-09-28
BE839664A (en) 1976-07-16
NL7602794A (en) 1976-09-21
MX3256E (en) 1980-08-12

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Legal Events

Date Code Title Description
ST Notification of lapse