IT1062084B - PROCEDURE FOR THE PREPARATION OF N, N-DIMETHYL-HYDRAZINE - Google Patents

PROCEDURE FOR THE PREPARATION OF N, N-DIMETHYL-HYDRAZINE

Info

Publication number
IT1062084B
IT1062084B IT2100676A IT2100676A IT1062084B IT 1062084 B IT1062084 B IT 1062084B IT 2100676 A IT2100676 A IT 2100676A IT 2100676 A IT2100676 A IT 2100676A IT 1062084 B IT1062084 B IT 1062084B
Authority
IT
Italy
Prior art keywords
dimethyl
dimethylhydrazine
hydrazine
procedure
preparation
Prior art date
Application number
IT2100676A
Other languages
Italian (it)
Original Assignee
Ashland Oil Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ashland Oil Inc filed Critical Ashland Oil Inc
Application granted granted Critical
Publication of IT1062084B publication Critical patent/IT1062084B/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C243/00—Compounds containing chains of nitrogen atoms singly-bound to each other, e.g. hydrazines, triazanes
    • C07C243/10—Hydrazines
    • C07C243/12—Hydrazines having nitrogen atoms of hydrazine groups bound to acyclic carbon atoms
    • C07C243/14—Hydrazines having nitrogen atoms of hydrazine groups bound to acyclic carbon atoms of a saturated carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C241/00—Preparation of compounds containing chains of nitrogen atoms singly-bound to each other, e.g. hydrazines, triazanes
    • C07C241/02—Preparation of hydrazines
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C241/00—Preparation of compounds containing chains of nitrogen atoms singly-bound to each other, e.g. hydrazines, triazanes
    • C07C241/04—Preparation of hydrazides

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

1488637 N,N - Dimethylhydrazine ASHLAND OIL Inc 17 March 1976 ]19 March 1975] 10750/76 Heading C2C N;N - Dimethylhydrazine is made by (a) reductively alkylating an acid hydrazide of formula in which R represents a C 1-3 alkyl group with formaldehyde at a pH of less than 7À5 to provide the corresponding N,N-dimethyl-2- acylhydrazine and (b) cleaning the above product by the base hydrolysis or the hydrazinolysis thereof to the desired N,N-dimethylhydrazine. In step (a) the reduction is preferably effected by hydrogen in the presence of Pd, Pt, Rh, Ni, Co or Ir as catalyst.
IT2100676A 1975-03-19 1976-03-09 PROCEDURE FOR THE PREPARATION OF N, N-DIMETHYL-HYDRAZINE IT1062084B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US55975575A 1975-03-19 1975-03-19

Publications (1)

Publication Number Publication Date
IT1062084B true IT1062084B (en) 1983-06-25

Family

ID=24234890

Family Applications (1)

Application Number Title Priority Date Filing Date
IT2100676A IT1062084B (en) 1975-03-19 1976-03-09 PROCEDURE FOR THE PREPARATION OF N, N-DIMETHYL-HYDRAZINE

Country Status (9)

Country Link
JP (1) JPS51115407A (en)
BE (1) BE839664A (en)
CA (1) CA1051928A (en)
DE (1) DE2611724C3 (en)
FR (1) FR2304599A1 (en)
GB (1) GB1488637A (en)
IT (1) IT1062084B (en)
MX (1) MX3256E (en)
NL (1) NL7602794A (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
USRE43252E1 (en) 1992-10-27 2012-03-20 Vast Power Portfolio, Llc High efficiency low pollution hybrid Brayton cycle combustor

Also Published As

Publication number Publication date
JPS5716978B2 (en) 1982-04-08
FR2304599A1 (en) 1976-10-15
CA1051928A (en) 1979-04-03
DE2611724C3 (en) 1979-05-23
FR2304599B1 (en) 1978-11-17
DE2611724A1 (en) 1977-02-10
GB1488637A (en) 1977-10-12
JPS51115407A (en) 1976-10-12
DE2611724B2 (en) 1978-09-28
BE839664A (en) 1976-07-16
NL7602794A (en) 1976-09-21
MX3256E (en) 1980-08-12

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