KR920004333A - 히드록시 아미드 화합물 제조공정 - Google Patents

히드록시 아미드 화합물 제조공정 Download PDF

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Publication number
KR920004333A
KR920004333A KR1019910014861A KR910014861A KR920004333A KR 920004333 A KR920004333 A KR 920004333A KR 1019910014861 A KR1019910014861 A KR 1019910014861A KR 910014861 A KR910014861 A KR 910014861A KR 920004333 A KR920004333 A KR 920004333A
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South Korea
Prior art keywords
compound
slurry
lower alkyl
integer
hydrogen
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KR1019910014861A
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KR100190511B1 (ko
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윌리암 쉬래퍼 프랜시스
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원본미기재
롬 앤드 하스 캄파니
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/22—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Investigating Or Analyzing Materials By The Use Of Ultrasonic Waves (AREA)
  • Measuring Pulse, Heart Rate, Blood Pressure Or Blood Flow (AREA)
  • Diaphragms For Electromechanical Transducers (AREA)

Abstract

내용 없음

Description

히드록시 아미드 화합물 제조공정
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (7)

  1. 하기 식 Ⅰ의 히드록시아미드 화합물을 제조하는 공정에 있어서, 하기식 Ⅱ의 화합물을 임의로 촉매 존재하에 주위온도에서 200℃까지의 온도범위에서 하기 식 Ⅲ의 화합물로 처리하고, 상기 식 Ⅰ산물이 결정화하여 슬러리를 형성하도록 온도를 조절하고, 약 0.25~12시간 동안 온도조절 및 교반으로 상기 슬러리를 유지한 후, 상기 히드록시아미드 화합물을 분리시킴을 특징으로하는 공정.
    단, 상기 식에서 A는 결합, 다가 유리래디컬이거나, n'가 0일때 A는 수소이거나 혹은 일가유기래디컬이며 ; R'은 수소, 저급알킬 혹은 히드록시저급알킬이며 ; n은 1~10의 정수이고 ; n'는 0~2의 정수이다.
    단, 상기 식에서 A, n 및 n'는 앞에서 정의한 바와 같다.
    단, 상기 식에서 R1,R2,n 및 n'는 앞에서 정의한 바와 같다.
  2. 1항에 있어서, A는 결합, 수소이거나, 혹은 포화되었거나 불포화된 알킬, 아릴, 카복시 저급알케닐 혹은 저급 알콕시카보닐 저급 알케닐에서 선택된 일가 혹은 다가 유기래디컬이며; R1은 수소, 저급알킬, 혹은 히드록시 저급 알킬이며; n'은 1 혹은 2의 정수이며, n'는 특정 반응 온도에서 0~2의 정수임을 특징으로 하는 공정.
  3. 2항에 있어서, 상기 슬러리의 온도 조절은 약 25℃~200℃로 유지됨을 특징으로 하는 공정.
  4. 2항에 있어서, 상기 슬러리의 온도 조절은 약 80°~115℃로 유지됨을 특징으로 하는 공정.
  5. 2항에 있어서, 상기 슬러리는 약 1~3시간 유지됨을 특징으로 하는 공정.
  6. 2항에 있어서, 상기 히드록시아미드 화합물은 편상화(fiaking), 프릴링(prilling), 분사건조(spray drying) 혹은 케스팅(casting)에 의해 고화(固化)됨을 특징으로 하는 공정.
  7. 2항에 있어서, 상기 A는 (C2-C8) 알키렌이며; R1은 히드록시 저급알킬이며, n및 n'는 1임을 특징으로 하는 공정.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019910014861A 1990-08-27 1991-08-27 히드록시 아미드 화합물 제조공정 KR100190511B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US573,524 1990-08-27
US07/573,524 US5101073A (en) 1990-08-27 1990-08-27 Production of β-hydroxyalkylamides

Publications (2)

Publication Number Publication Date
KR920004333A true KR920004333A (ko) 1992-03-27
KR100190511B1 KR100190511B1 (ko) 1999-06-01

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Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019910014861A KR100190511B1 (ko) 1990-08-27 1991-08-27 히드록시 아미드 화합물 제조공정

Country Status (24)

Country Link
US (1) US5101073A (ko)
EP (1) EP0473380B1 (ko)
JP (1) JP2939369B2 (ko)
KR (1) KR100190511B1 (ko)
AT (1) ATE112258T1 (ko)
AU (1) AU652170B2 (ko)
BR (1) BR9103632A (ko)
CA (1) CA2049563C (ko)
CZ (1) CZ289065B6 (ko)
DE (1) DE69104312T2 (ko)
DK (1) DK0473380T3 (ko)
ES (1) ES2062692T3 (ko)
FI (1) FI113761B (ko)
HK (1) HK15895A (ko)
HU (1) HUT66673A (ko)
IE (1) IE74386B1 (ko)
IL (1) IL99299A (ko)
MX (1) MX174501B (ko)
MY (1) MY107195A (ko)
NO (1) NO300207B1 (ko)
NZ (1) NZ239524A (ko)
PT (1) PT98772B (ko)
TR (1) TR27054A (ko)
ZA (1) ZA916639B (ko)

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JP3490441B2 (ja) * 1992-09-25 2004-01-26 ベーリンガー インゲルハイム （カナダ） リミテッド レニン阻害剤としてのｎ−（ヒドロキシエチル）ブタンジアミド誘導体
ATE164831T1 (de) * 1992-10-07 1998-04-15 Quest Int Hydroxy-alkyl-amide von dicarbonsäure und deren verwendung in kosmetischen präparaten
US5646318A (en) * 1995-04-26 1997-07-08 Akzo Nobel Nv Process for the preparation of hydroxyalkylamides
DE19821883B4 (de) * 1998-05-15 2005-11-10 Degussa Ag Verfahren zur kontinuierlichen Herstellung von Hydroxyalkylamiden
DE19823925C2 (de) 1998-05-28 2001-01-11 Inventa Ag Verfahren zur Herstellung von beta-Hydroxyalkylamiden
IT1308624B1 (it) * 1999-02-22 2002-01-09 Sir Ind Spa Processo per la produzione industriale di beta-idrossialchil ammidi.
IT1311895B1 (it) * 1999-03-12 2002-03-20 Sir Ind Spa Miscele di b-idrossialchilammidi e loro impiego come agentireticolanti per la preparazione di vernici in polvere.
US20050043560A1 (en) * 2000-06-19 2005-02-24 Pergo (Europe) Ab Novel beta-hydroxyamides
DE10053194A1 (de) * 2000-10-26 2002-05-16 Ems Chemie Ag ß-Hydroxyalkylamide, Verfahren zu ihrer Herstellung und deren Verwendung
JP4873208B2 (ja) * 2001-03-28 2012-02-08 ナガセケムテックス株式会社 新規化合物ならびにそれを用いた吸水性樹脂用架橋剤および吸水性樹脂
DE10204938A1 (de) * 2002-02-07 2003-08-21 Stockhausen Chem Fab Gmbh Verfahren zur Nachvernetzung im Bereich der Oberfläche von wasserabsorbierenden Polymeren mit beta-Hydroxyalkylamiden
BR0311481A (pt) * 2002-05-31 2005-03-15 Grace Gmbh & Co Kg Agente para fosqueamento de revestimento em pó comprendendo produto de condensação de éster amida
US20050288450A1 (en) * 2003-05-23 2005-12-29 Tim Fletcher Coating matting agent comprising amide condensation product
EP1726621A1 (en) 2005-05-26 2006-11-29 Cytec Surface Specialties, S.A. Thermosetting powder compositions
JP5148911B2 (ja) * 2007-04-03 2013-02-20 関西ペイント株式会社 硬化剤組成物およびその製造方法。
EP1980582A1 (en) 2007-04-13 2008-10-15 Cytec Italy, S.R.L. Branched polyester for powder coatings
EP2085440A1 (en) 2008-01-31 2009-08-05 Cytec Italy, S.R.L. Powder Compositions
EP2085441A1 (en) 2008-01-31 2009-08-05 Cytec Surface Specialties, S.A. Powder Composition
CN101704762B (zh) * 2009-11-13 2013-01-09 六安市捷通达化工有限责任公司 一种β-羟烷基酰胺的生产工艺
CN101928225A (zh) * 2009-12-17 2010-12-29 太仓市运通化工厂 一种n,n,n’,n’-四(2-羟乙基)己二酰胺的制备方法
CN103119018A (zh) 2010-03-11 2013-05-22 赢创德固赛有限公司 β-羟烷基酰胺、它们的制造方法及其用途
EP2937332A1 (en) * 2014-04-22 2015-10-28 Cromogenia Units, S.A. Process for preparing a solid hydroxyalkylamide
US10676637B2 (en) 2014-07-25 2020-06-09 Dsm Ip Assets B.V. Matt powder coatings
CN105384654B (zh) * 2015-12-11 2017-08-25 六安市捷通达化工有限责任公司 一种羟烷基酰胺的结晶纯化方法
CN105646268A (zh) * 2016-03-02 2016-06-08 沈阳化工大学 一种以负载固体碱催化剂合成N,N,N’,N’-四（β-羟丙基）己二酰胺方法
ES2906771T3 (es) 2018-03-08 2022-04-20 Covestro Netherlands Bv Composiciones para revestimiento en polvo termoendurecibles de un componente (1k) para revestimientos en polvo mate resistentes a impacto y de bajo brillo consistentes
CN110776437A (zh) * 2019-11-07 2020-02-11 六安捷通达新材料有限公司 一种挤出机制备羟烷基酰胺的方法
WO2021144061A1 (en) 2020-01-13 2021-07-22 Dsm Ip Assets B.V. Non-porous microparticles
US20240084167A1 (en) 2021-04-27 2024-03-14 Allnex Austria Gmbh Aqueous coating composition for corrosion protection
CN114276270A (zh) * 2021-12-10 2022-04-05 湖北文理学院 一种具有酰胺键的化合物的合成方法

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Also Published As

Publication number Publication date
DE69104312T2 (de) 1995-02-16
PT98772B (pt) 1999-01-29
ATE112258T1 (de) 1994-10-15
NO300207B1 (no) 1997-04-28
HUT66673A (en) 1994-12-28
EP0473380A1 (en) 1992-03-04
AU8268991A (en) 1992-03-05
DE69104312D1 (de) 1994-11-03
CA2049563A1 (en) 1992-02-28
ES2062692T3 (es) 1994-12-16
MX174501B (es) 1994-05-18
CZ289065B6 (cs) 2001-10-17
FI113761B (fi) 2004-06-15
NO913279L (no) 1992-02-28
NO913279D0 (no) 1991-08-22
HU912797D0 (en) 1992-01-28
FI914017A (fi) 1992-02-28
MY107195A (en) 1995-09-30
KR100190511B1 (ko) 1999-06-01
IE913008A1 (en) 1992-03-11
NZ239524A (en) 1994-05-26
TR27054A (tr) 1994-10-11
ZA916639B (en) 1992-05-27
IE74386B1 (en) 1998-05-06
IL99299A (en) 1996-11-14
CA2049563C (en) 2003-01-07
PT98772A (pt) 1992-07-31
CS263591A3 (en) 1992-03-18
IL99299A0 (en) 1992-07-15
FI914017A0 (fi) 1991-08-26
US5101073A (en) 1992-03-31
JPH04247058A (ja) 1992-09-03
EP0473380B1 (en) 1994-09-28
DK0473380T3 (da) 1994-11-07
AU652170B2 (en) 1994-08-18
BR9103632A (pt) 1992-05-19
HK15895A (en) 1995-02-10
JP2939369B2 (ja) 1999-08-25

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