JPH10502450A - 陽イオン交換器の廃棄処分方法及び装置 - Google Patents
陽イオン交換器の廃棄処分方法及び装置Info
- Publication number
- JPH10502450A JPH10502450A JP8503610A JP50361096A JPH10502450A JP H10502450 A JPH10502450 A JP H10502450A JP 8503610 A JP8503610 A JP 8503610A JP 50361096 A JP50361096 A JP 50361096A JP H10502450 A JPH10502450 A JP H10502450A
- Authority
- JP
- Japan
- Prior art keywords
- cation exchanger
- cation
- cations
- complex
- converted
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 150000001768 cations Chemical class 0.000 title claims abstract description 114
- 238000000034 method Methods 0.000 title claims abstract description 27
- 230000002285 radioactive effect Effects 0.000 claims abstract description 19
- 150000001450 anions Chemical class 0.000 claims abstract description 16
- 239000008139 complexing agent Substances 0.000 claims abstract description 13
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims description 40
- 235000006408 oxalic acid Nutrition 0.000 claims description 13
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 12
- 229910052742 iron Inorganic materials 0.000 claims description 11
- -1 iron cations Chemical class 0.000 claims description 10
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 8
- 239000007800 oxidant agent Substances 0.000 claims description 7
- 150000002500 ions Chemical class 0.000 claims description 5
- 230000003647 oxidation Effects 0.000 claims description 4
- 238000007254 oxidation reaction Methods 0.000 claims description 4
- 230000001590 oxidative effect Effects 0.000 claims description 4
- 125000000129 anionic group Chemical group 0.000 claims description 3
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 claims description 2
- 230000007935 neutral effect Effects 0.000 claims description 2
- 230000000415 inactivating effect Effects 0.000 claims 1
- 239000011347 resin Substances 0.000 description 23
- 229920005989 resin Polymers 0.000 description 23
- 238000005202 decontamination Methods 0.000 description 18
- 230000003588 decontaminative effect Effects 0.000 description 16
- 230000008929 regeneration Effects 0.000 description 8
- 238000011069 regeneration method Methods 0.000 description 8
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 6
- 238000006243 chemical reaction Methods 0.000 description 4
- 229910002092 carbon dioxide Inorganic materials 0.000 description 3
- 239000001569 carbon dioxide Substances 0.000 description 3
- 238000005341 cation exchange Methods 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 238000000746 purification Methods 0.000 description 3
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- 239000012857 radioactive material Substances 0.000 description 2
- 230000000717 retained effect Effects 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- VYZAMTAEIAYCRO-BJUDXGSMSA-N Chromium-51 Chemical compound [51Cr] VYZAMTAEIAYCRO-BJUDXGSMSA-N 0.000 description 1
- GUTLYIVDDKVIGB-OUBTZVSYSA-N Cobalt-60 Chemical compound [60Co] GUTLYIVDDKVIGB-OUBTZVSYSA-N 0.000 description 1
- 241000238631 Hexapoda Species 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- GUTLYIVDDKVIGB-BJUDXGSMSA-N cobalt-58 Chemical compound [58Co] GUTLYIVDDKVIGB-BJUDXGSMSA-N 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- VEPSWGHMGZQCIN-UHFFFAOYSA-H ferric oxalate Chemical compound [Fe+3].[Fe+3].[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O VEPSWGHMGZQCIN-UHFFFAOYSA-H 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- PWHULOQIROXLJO-BJUDXGSMSA-N manganese-54 Chemical compound [54Mn] PWHULOQIROXLJO-BJUDXGSMSA-N 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
Classifications
-
- G—PHYSICS
- G21—NUCLEAR PHYSICS; NUCLEAR ENGINEERING
- G21F—PROTECTION AGAINST X-RADIATION, GAMMA RADIATION, CORPUSCULAR RADIATION OR PARTICLE BOMBARDMENT; TREATING RADIOACTIVELY CONTAMINATED MATERIAL; DECONTAMINATION ARRANGEMENTS THEREFOR
- G21F9/00—Treating radioactively contaminated material; Decontamination arrangements therefor
- G21F9/28—Treating solids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
- B01J49/50—Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents
- B01J49/53—Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents for cationic exchangers
-
- G—PHYSICS
- G21—NUCLEAR PHYSICS; NUCLEAR ENGINEERING
- G21F—PROTECTION AGAINST X-RADIATION, GAMMA RADIATION, CORPUSCULAR RADIATION OR PARTICLE BOMBARDMENT; TREATING RADIOACTIVELY CONTAMINATED MATERIAL; DECONTAMINATION ARRANGEMENTS THEREFOR
- G21F9/00—Treating radioactively contaminated material; Decontamination arrangements therefor
- G21F9/04—Treating liquids
- G21F9/06—Processing
- G21F9/12—Processing by absorption; by adsorption; by ion-exchange
Landscapes
- Physics & Mathematics (AREA)
- Engineering & Computer Science (AREA)
- General Engineering & Computer Science (AREA)
- High Energy & Nuclear Physics (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Processing Of Solid Wastes (AREA)
- Treatment Of Water By Ion Exchange (AREA)
Abstract
Description
Claims (1)
- 【特許請求の範囲】 1.放射性陽イオン及び不活性陽イオンで汚染されている陽イオン交換器(3) において、2価でない不活性陽イオンが陰イオン錯体に変換され、この錯体が陽 イオン交換器(3)から洗い流されることを特徴とする陽イオン交換器の廃棄処 分方法。 2.2価の鉄陽イオンが3価の鉄陽イオンに酸化され、3価の鉄陽イオンが陰イ オン錯体に変換されることを特徴とする請求項1記載の方法。 3.酸化剤が2価の鉄陽イオンを酸化させるために使用されることを特徴とする 請求項2記載の方法。 4.酸化剤として少量の過酸化水素が使用されることを特徴とする請求項3記載 の方法。 5.不活性陽イオンが20℃以上の温度で陰イオン錯体に変換されることを特徴 とする請求項1乃至4の1つに記載の方法。 6.不活性陽イオンが60℃乃至80℃の温度で陰イオン錯体に変換されること を特徴とする請求項5記載の方法。 7.錯体生成剤が汚染された陽イオン交換器(3)に投入され、これにより不活 性陽イオンが陰イオン錯体に変換されることを特徴とする請求項1乃至6の1つ にに記載の方法。 8.酸化剤としてシュウ酸が汚染された陽イオン交換器(3)に供給されること を特徴とする請求項7記載の方法。 9.錯体生成剤として0.1モル以上のシュウ酸を含む溶液が供給されることを 特徴とする請求項8記載の方法。 10.錯体生成剤として1モルのシュウ酸溶液が供給されることを特徴とする請 求項9記載の方法。 11.陽イオン交換器(3)から洗い流された陰イオン錯体が酸化によって破壊 されることを特徴とする請求項1乃至10の1つに記載の方法。 12.陰イオン錯体に過酸化水素及び/又はオゾンが添加され、これにより陰イ オン錯体が酸化により破壊されることを特徴とする請求項11記載の方法。 13.陽イオン交換器(3)が錯体形成剤のための供給管(4)及び排出管(6 )に接続されていることを特徴とする陽イオン交換器の廃棄処分装置。 14.排出管(6)が精選装置(7)に接続され、この装置に酸化剤のための配 管(8)が接続されていることを特徴とする請求項13記載の装置。 15.陽イオン交換器(3)が最終貯蔵可能な容器(12)内に配置されている ことを特徴とする請求項13又は14記載の装置。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE4423398.1 | 1994-07-04 | ||
DE4423398A DE4423398A1 (de) | 1994-07-04 | 1994-07-04 | Verfahren und Einrichtung zum Entsorgen eines Kationenaustauschers |
PCT/DE1995/000802 WO1996001478A1 (de) | 1994-07-04 | 1995-06-21 | Verfahren und einrichtung zum entsorgen eines kationenaustauschers |
Publications (2)
Publication Number | Publication Date |
---|---|
JPH10502450A true JPH10502450A (ja) | 1998-03-03 |
JP3124555B2 JP3124555B2 (ja) | 2001-01-15 |
Family
ID=6522212
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP08503610A Expired - Fee Related JP3124555B2 (ja) | 1994-07-04 | 1995-06-21 | 陽イオン交換器の廃棄処分方法及び装置 |
Country Status (10)
Country | Link |
---|---|
US (1) | US5835865A (ja) |
EP (1) | EP0769191B1 (ja) |
JP (1) | JP3124555B2 (ja) |
CA (1) | CA2194293C (ja) |
DE (2) | DE4423398A1 (ja) |
ES (1) | ES2123256T3 (ja) |
FI (1) | FI114250B (ja) |
HU (1) | HU220400B (ja) |
SK (1) | SK281355B6 (ja) |
WO (1) | WO1996001478A1 (ja) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2013044588A (ja) * | 2011-08-23 | 2013-03-04 | Hitachi-Ge Nuclear Energy Ltd | 原子力発電所の廃樹脂処理方法及び処理システム |
JP2015064334A (ja) * | 2013-06-21 | 2015-04-09 | 日立Geニュークリア・エナジー株式会社 | 放射性有機廃棄物の処理方法及び処理システム |
Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19818772C2 (de) * | 1998-04-27 | 2000-05-31 | Siemens Ag | Verfahren zum Abbau der Radioaktivität eines Metallteiles |
JP2002529751A (ja) * | 1998-11-10 | 2002-09-10 | シーメンス アクチエンゲゼルシヤフト | 金属陽イオンの除去方法 |
US6711620B1 (en) * | 1999-04-14 | 2004-03-23 | Matsushita Electric Industrial Co. | Event control device and digital broadcasting system |
JP2003098294A (ja) * | 2001-09-27 | 2003-04-03 | Hitachi Ltd | オゾンを用いた除染方法及びその装置 |
CA2698694A1 (en) | 2007-10-12 | 2009-04-16 | Dsm Ip Assets B.V. | A helmet containing polyethylene fibers |
US8916090B2 (en) | 2011-07-07 | 2014-12-23 | Karl Storz Imaging, Inc. | Endoscopic camera component manufacturing method |
JP6439242B2 (ja) * | 2013-10-24 | 2018-12-19 | 栗田工業株式会社 | 放射性廃イオン交換樹脂の除染方法および除染装置 |
US10083769B2 (en) | 2013-10-24 | 2018-09-25 | Kurita Water Industries Ltd. | Treatment method and treatment apparatus of iron-group metal ion-containing liquid, method and apparatus for electrodepositing Co and Fe, and decontamination method and decontamination apparatus of radioactive waste ion exchange resin |
WO2016078704A1 (en) | 2014-11-19 | 2016-05-26 | Areva Gmbh | Method and apparatus for the recovery of radioactive nuclides from spent resin materials |
CN109727697B (zh) * | 2017-10-31 | 2024-04-09 | 中核核电运行管理有限公司 | 一种高放射性废物接收装置 |
Family Cites Families (24)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2694681A (en) * | 1952-03-07 | 1954-11-16 | Univ Idaho Res Foundation Inc | Recycling the complexing agent in the separation of ions by ion exchange |
US3262883A (en) * | 1962-11-13 | 1966-07-26 | Rohm & Haas | Defouling ion exchange resins by the removal of iron oxides therefrom |
DE1257692B (de) * | 1964-02-25 | 1967-12-28 | Joh A Benckiss G M B H Chem Fa | Regenerieren von Gemischen stark und schwach saurer Ionenaustauscher |
US3340200A (en) * | 1964-09-15 | 1967-09-05 | Stone & Webster Eng Corp | Removal and disposal of radioactive contaminants in mixed ion exchange resins with alkali metal halide |
US3454503A (en) * | 1967-07-19 | 1969-07-08 | Shell Oil Co | Process for regenerating cation exchange resins |
US3732191A (en) * | 1972-02-07 | 1973-05-08 | Goodrich Co B F | Polythiol vulcanization of epihalohydrin elastomers |
US3887498A (en) * | 1973-03-12 | 1975-06-03 | Morton Norwich Products Inc | Method for regeneration of cation exchange resins and for removal of iron deposits therefrom |
DE2358688C3 (de) * | 1973-11-24 | 1979-02-22 | Kernforschungszentrum Karlsruhe Gmbh, 7500 Karlsruhe | Verfahren zur Erhöhung der Lebensdauer von organischen Extraktionsmitteln |
DE2607292C2 (de) * | 1976-02-23 | 1985-08-29 | Kraftwerk Union AG, 4330 Mülheim | Verfahren zur Befreiung von im Kernreaktorbetrieb verbrauchten Ionenaustauscherharzen von radioaktiven Korrosionsprodukten |
FR2361724A1 (fr) * | 1976-08-12 | 1978-03-10 | Commissariat Energie Atomique | Procede de stockage de resines echangeuses d'ions contaminees |
US4235713A (en) * | 1978-06-06 | 1980-11-25 | Redondo Abad Angel Luis | Process for the elimination of accumulated iron in organic phases of fluid-fluid extraction that contain di-2-ethyl-hexyl phosphoric acid |
US4156646A (en) * | 1978-06-16 | 1979-05-29 | The United States Of America As Represented By The United States Department Of Energy | Removal of plutonium and americium from alkaline waste solutions |
DE2934863A1 (de) * | 1979-08-29 | 1981-04-09 | Tetra Werke Dr.Rer.Nat. Ulrich Baensch Gmbh, 4520 Melle | Verfahren zur regenerierung von ionenaustauschern |
SE420249B (sv) * | 1980-01-31 | 1981-09-21 | Asea Atom Ab | Sett for behandling av en i en reningskrets i en kernreaktoranleggning anvend organisk jonbytarmassa |
DE3007716A1 (de) * | 1980-02-29 | 1981-09-10 | Rheinisch-Westfälisches Elektrizitätswerk AG, 4300 Essen | Verfahren zum aufbereiten von radionuklide enthaltenden abfallfluessigkeiten aus kernkraftwerken o.dgl. |
CA1199043A (en) * | 1982-11-05 | 1986-01-07 | Majesty (Her) In Right Of Canada As Represented By Atomic Energy Of Canada Limited/L'energie Atomique Du Canada Limitee | Radioactive waste immobilization using ion-exchange materials which form glass-ceramics |
JPS59162493A (ja) * | 1983-03-07 | 1984-09-13 | 株式会社日立製作所 | イオン交換樹脂に付着する鉄酸化物除去法 |
JPS59231493A (ja) * | 1983-06-15 | 1984-12-26 | 住友金属鉱山株式会社 | 低レベル放射性廃液の処理方法 |
CS245861B1 (en) * | 1984-06-01 | 1986-10-16 | Zdenek Matejka | Method of heavy metals separation from aminocarboxyl complexing substances |
DE3427258A1 (de) * | 1984-07-24 | 1986-01-30 | Kraftwerk Union AG, 4330 Mülheim | Einrichtung zur abtrennung und zum konditionieren von kontaminierten feststoffen |
JPS6238247A (ja) * | 1985-08-12 | 1987-02-19 | Hitachi Ltd | イオン交換樹脂の再生方法 |
GB2229312B (en) * | 1989-03-14 | 1993-01-06 | British Nuclear Fuels Plc | Actinide dissolution |
US5139734A (en) * | 1990-11-26 | 1992-08-18 | Westinghouse Electric Corp. | Resin processing system |
DE4137947C2 (de) * | 1991-11-18 | 1996-01-11 | Siemens Ag | Verfahren zur Behandlung von radioaktivem Abfall |
-
1994
- 1994-07-04 DE DE4423398A patent/DE4423398A1/de not_active Withdrawn
-
1995
- 1995-06-21 ES ES95921717T patent/ES2123256T3/es not_active Expired - Lifetime
- 1995-06-21 JP JP08503610A patent/JP3124555B2/ja not_active Expired - Fee Related
- 1995-06-21 DE DE59503719T patent/DE59503719D1/de not_active Expired - Lifetime
- 1995-06-21 SK SK7-97A patent/SK281355B6/sk unknown
- 1995-06-21 CA CA002194293A patent/CA2194293C/en not_active Expired - Fee Related
- 1995-06-21 EP EP95921717A patent/EP0769191B1/de not_active Expired - Lifetime
- 1995-06-21 WO PCT/DE1995/000802 patent/WO1996001478A1/de active IP Right Grant
- 1995-06-21 HU HU9700015A patent/HU220400B/hu not_active IP Right Cessation
-
1997
- 1997-01-03 FI FI970040A patent/FI114250B/fi not_active IP Right Cessation
- 1997-01-06 US US08/779,368 patent/US5835865A/en not_active Expired - Lifetime
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2013044588A (ja) * | 2011-08-23 | 2013-03-04 | Hitachi-Ge Nuclear Energy Ltd | 原子力発電所の廃樹脂処理方法及び処理システム |
JP2015064334A (ja) * | 2013-06-21 | 2015-04-09 | 日立Geニュークリア・エナジー株式会社 | 放射性有機廃棄物の処理方法及び処理システム |
Also Published As
Publication number | Publication date |
---|---|
DE4423398A1 (de) | 1996-01-11 |
SK797A3 (en) | 1997-08-06 |
WO1996001478A1 (de) | 1996-01-18 |
CA2194293A1 (en) | 1996-01-18 |
ES2123256T3 (es) | 1999-01-01 |
FI970040A (fi) | 1997-01-03 |
DE59503719D1 (de) | 1998-10-29 |
EP0769191B1 (de) | 1998-09-23 |
JP3124555B2 (ja) | 2001-01-15 |
FI970040A0 (fi) | 1997-01-03 |
US5835865A (en) | 1998-11-10 |
HU9700015D0 (en) | 1997-02-28 |
HUT77579A (hu) | 1998-06-29 |
CA2194293C (en) | 2002-01-29 |
FI114250B (fi) | 2004-09-15 |
HU220400B (hu) | 2002-01-28 |
EP0769191A1 (de) | 1997-04-23 |
SK281355B6 (sk) | 2001-02-12 |
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Free format text: JAPANESE INTERMEDIATE CODE: R250 |
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LAPS | Cancellation because of no payment of annual fees |